data_4334_ _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'As3 Cu0.91 Fe0.43 Mg2.51 Na0.88 O12' _chemical_formula_weight 579.85 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'As' 'As' 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Mg' 'Mg' 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Na' 'Na' 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_H-M_alt 'C 2/c' _space_group_name_Hall '-C 2yc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 11.8615(4) _cell_length_b 12.7511(4) _cell_length_c 6.69583(19) _cell_angle_alpha 90 _cell_angle_beta 113.0253(14) _cell_angle_gamma 90 _cell_volume 932.04(5) _cell_formula_units_Z 4 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 4.132 _exptl_crystal_F_000 1089 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_absorpt_coefficient_mu 13.639 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 17665 _diffrn_reflns_av_unetI/netI 0.0277 _diffrn_reflns_av_R_equivalents 0.0283 _diffrn_reflns_limit_h_min -23 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_theta_min 3.195 _diffrn_reflns_theta_max 44.494 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.954 _diffrn_measured_fraction_theta_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.954 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.954 _diffrn_reflns_point_group_measured_fraction_full 0.994 _reflns_number_total 3579 _reflns_number_gt 3063 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+5.8207P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick 2014' _refine_ls_extinction_coef 0.00011(6) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_number_reflns 3579 _refine_ls_number_parameters 105 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0383 _refine_ls_R_factor_gt 0.0286 _refine_ls_wR_factor_ref 0.0607 _refine_ls_wR_factor_gt 0.0592 _refine_ls_goodness_of_fit_ref 1.261 _refine_ls_restrained_S_all 1.261 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group A2' Na 0.0000 -0.0068(2) 0.2500 0.0245(7) Uani 0.753(8) 2 d S T P . . A1' Cu 0.0000 0.50250(3) 0.2500 0.00709(10) Uani 0.848(2) 2 d S T P . . A1 Na 0.5000 0.0000 0.0000 0.015(3) Uani 0.131(7) 2 d S . P . . M1 Mg 0.0000 0.26008(8) 0.2500 0.0078(2) Uani 1.104(6) 2 d S T P . . M2 Mg 0.28665(5) 0.65532(4) 0.37646(9) 0.00522(14) Uani 1.239(4) 1 d . . P . . T1 As 0.0000 0.71312(2) 0.2500 0.00540(5) Uani 1 2 d S T P . . T2 As 0.23130(2) 0.88634(2) 0.12459(3) 0.00528(4) Uani 1 1 d . . . . . O1 O 0.46347(13) 0.71561(12) 0.5236(2) 0.0085(2) Uani 1 1 d . . . . . O2 O 0.10697(13) 0.62071(12) 0.2629(3) 0.0097(2) Uani 1 1 d . . . . . O3 O 0.33966(14) 0.67058(12) 0.1197(2) 0.0087(2) Uani 1 1 d . . . . . O4 O 0.11613(13) 0.39170(12) 0.3145(3) 0.0103(2) Uani 1 1 d . . . . . O5 O 0.21563(14) 0.81251(12) 0.3207(2) 0.0087(2) Uani 1 1 d . . . . . O6 O 0.33313(16) 0.50362(12) 0.3890(3) 0.0120(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 A2' 0.0142(10) 0.0340(14) 0.0216(11) 0.000 0.0031(8) 0.000 A1' 0.00521(17) 0.00319(16) 0.01273(18) 0.000 0.00335(13) 0.000 A1 0.010(5) 0.009(5) 0.013(5) 0.002(3) -0.009(3) -0.002(3) M1 0.0070(4) 0.0096(4) 0.0081(4) 0.000 0.0044(3) 0.000 M2 0.0052(2) 0.0058(2) 0.0054(2) -0.00072(16) 0.00281(17) -0.00055(16) T1 0.00594(10) 0.00522(10) 0.00464(9) 0.000 0.00163(8) 0.000 T2 0.00592(7) 0.00496(7) 0.00494(7) -0.00019(5) 0.00208(5) -0.00034(6) O1 0.0082(5) 0.0109(6) 0.0062(5) -0.0023(4) 0.0024(4) -0.0013(4) O2 0.0075(5) 0.0065(5) 0.0153(6) -0.0010(5) 0.0046(5) 0.0003(4) O3 0.0103(6) 0.0102(6) 0.0051(5) -0.0016(4) 0.0025(4) -0.0032(4) O4 0.0061(5) 0.0072(5) 0.0177(6) 0.0009(5) 0.0048(5) 0.0007(4) O5 0.0105(6) 0.0093(6) 0.0068(5) 0.0013(4) 0.0039(4) -0.0008(4) O6 0.0132(7) 0.0057(5) 0.0174(7) 0.0012(5) 0.0064(5) -0.0019(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag A2' O6 2.4535(18) 8_455 ? A2' O6 2.4535(18) 7_556 ? A2' O6 2.4985(17) 4_545 ? A2' O6 2.4985(17) 3_445 ? A2' O3 2.863(3) 4_545 ? A2' O3 2.863(3) 3_445 ? A2' O1 3.011(3) 8_455 ? A2' O1 3.011(3) 7_556 ? A2' T2 3.2853(12) 6_566 ? A2' T2 3.2853(12) 5_565 ? A2' A2' 3.3524(3) 5_556 ? A2' A2' 3.3524(3) 5 ? A1' A1 1.67426(5) 4 ? A1' A1 1.67426(5) 3_455 ? A1' O4 1.9012(15) . ? A1' O4 1.9012(15) 2 ? A1' O2 1.9503(15) 2 ? A1' O2 1.9503(15) . ? A1' T1 2.6856(5) . ? A1' M1 3.0910(10) . ? A1 A1' 1.67426(5) 7 ? A1 A1' 1.67426(5) 3_545 ? A1 O2 2.3087(15) 7 ? A1 O2 2.3087(15) 3_545 ? A1 O4 2.4433(16) 7 ? A1 O4 2.4433(16) 3_545 ? A1 O4 2.5858(15) 8 ? A1 O4 2.5858(15) 4_545 ? A1 O2 2.8417(15) 8 ? A1 O2 2.8417(15) 4_545 ? A1 T1 3.1917(2) 3_545 ? A1 T1 3.1917(2) 7 ? M1 O3 2.0935(15) 3_445 ? M1 O3 2.0935(15) 4_545 ? M1 O4 2.1059(17) 2 ? M1 O4 2.1059(17) . ? M1 O1 2.1179(14) 4_545 ? M1 O1 2.1179(14) 3_445 ? M1 M2 3.2530(7) 3_445 ? M1 M2 3.2530(7) 4_545 ? M1 A1 3.4872(9) 4 ? M1 A1 3.4872(9) 3_455 ? M2 O6 2.0041(16) . ? M2 O2 2.0118(16) . ? M2 O3 2.0580(15) . ? M2 O5 2.0797(15) 7_566 ? M2 O1 2.0842(16) . ? M2 O5 2.1495(16) . ? M2 M2 3.2323(11) 7_566 ? M2 T1 3.2439(6) 7_566 ? M2 T1 3.2509(6) . ? M2 M1 3.2530(7) 3 ? M2 A2' 3.3610(16) 7_556 ? M2 A2' 3.6152(16) 3 ? T1 O1 1.6729(14) 7_566 ? T1 O1 1.6729(14) 8_465 ? T1 O2 1.7089(15) 2 ? T1 O2 1.7089(15) . ? T1 A1 3.1917(2) 3_455 ? T1 A1 3.1917(2) 4 ? T1 M2 3.2439(6) 7_566 ? T1 M2 3.2439(6) 8_465 ? T1 M2 3.2509(6) 2 ? T2 O6 1.6656(15) 4 ? T2 O3 1.6832(14) 7_565 ? T2 O5 1.6838(14) . ? T2 O4 1.6937(14) 4 ? T2 A2' 3.2853(12) 5_565 ? T2 A2' 3.4485(10) 1_565 ? T2 A1 3.5085(2) 2_665 ? O1 T1 1.6729(14) 7_566 ? O1 M1 2.1179(14) 3 ? O1 A2' 3.011(3) 7_556 ? O2 A1 2.3087(15) 3_455 ? O2 A1 2.8417(15) 4 ? O3 T2 1.6832(14) 7_565 ? O3 M1 2.0936(15) 3 ? O3 A2' 2.863(3) 3 ? O4 T2 1.6937(14) 4_545 ? O4 A1 2.4432(16) 3_455 ? O4 A1 2.5858(15) 4 ? O5 M2 2.0797(15) 7_566 ? O6 T2 1.6656(15) 4_545 ? O6 A2' 2.4535(18) 7_556 ? O6 A2' 2.4986(17) 3 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O6 A2' O6 178.12(14) 8_455 7_556 ? O6 A2' O6 94.79(5) 8_455 4_545 ? O6 A2' O6 85.11(5) 7_556 4_545 ? O6 A2' O6 85.11(5) 8_455 3_445 ? O6 A2' O6 94.79(5) 7_556 3_445 ? O6 A2' O6 173.92(14) 4_545 3_445 ? O6 A2' O3 118.11(9) 8_455 4_545 ? O6 A2' O3 60.19(5) 7_556 4_545 ? O6 A2' O3 62.81(6) 4_545 4_545 ? O6 A2' O3 111.91(8) 3_445 4_545 ? O6 A2' O3 60.19(5) 8_455 3_445 ? O6 A2' O3 118.11(9) 7_556 3_445 ? O6 A2' O3 111.91(8) 4_545 3_445 ? O6 A2' O3 62.81(6) 3_445 3_445 ? O3 A2' O3 75.63(9) 4_545 3_445 ? O6 A2' O1 67.46(6) 8_455 8_455 ? O6 A2' O1 114.36(9) 7_556 8_455 ? O6 A2' O1 80.69(6) 4_545 8_455 ? O6 A2' O1 104.81(8) 3_445 8_455 ? O3 A2' O1 143.12(4) 4_545 8_455 ? O3 A2' O1 126.70(4) 3_445 8_455 ? O6 A2' O1 114.36(9) 8_455 7_556 ? O6 A2' O1 67.46(6) 7_556 7_556 ? O6 A2' O1 104.81(8) 4_545 7_556 ? O6 A2' O1 80.69(6) 3_445 7_556 ? O3 A2' O1 126.70(4) 4_545 7_556 ? O3 A2' O1 143.12(4) 3_445 7_556 ? O1 A2' O1 55.62(7) 8_455 7_556 ? O6 A2' T2 148.81(10) 8_455 6_566 ? O6 A2' T2 29.44(4) 7_556 6_566 ? O6 A2' T2 73.32(5) 4_545 6_566 ? O6 A2' T2 103.74(5) 3_445 6_566 ? O3 A2' T2 30.81(3) 4_545 6_566 ? O3 A2' T2 96.91(7) 3_445 6_566 ? O1 A2' T2 135.29(5) 8_455 6_566 ? O1 A2' T2 96.68(3) 7_556 6_566 ? O6 A2' T2 29.44(4) 8_455 5_565 ? O6 A2' T2 148.81(10) 7_556 5_565 ? O6 A2' T2 103.74(5) 4_545 5_565 ? O6 A2' T2 73.32(5) 3_445 5_565 ? O3 A2' T2 96.91(7) 4_545 5_565 ? O3 A2' T2 30.81(3) 3_445 5_565 ? O1 A2' T2 96.68(3) 8_455 5_565 ? O1 A2' T2 135.29(5) 7_556 5_565 ? T2 A2' T2 124.26(8) 6_566 5_565 ? O6 A2' A2' 131.91(4) 8_455 5_556 ? O6 A2' A2' 47.96(4) 7_556 5_556 ? O6 A2' A2' 132.74(4) 4_545 5_556 ? O6 A2' A2' 46.83(4) 3_445 5_556 ? O3 A2' A2' 85.09(7) 4_545 5_556 ? O3 A2' A2' 90.24(8) 3_445 5_556 ? O1 A2' A2' 119.49(11) 8_455 5_556 ? O1 A2' A2' 66.35(7) 7_556 5_556 ? T2 A2' A2' 62.59(4) 6_566 5_556 ? T2 A2' A2' 114.34(6) 5_565 5_556 ? O6 A2' A2' 47.96(4) 8_455 5 ? O6 A2' A2' 131.91(4) 7_556 5 ? O6 A2' A2' 46.83(4) 4_545 5 ? O6 A2' A2' 132.74(4) 3_445 5 ? O3 A2' A2' 90.24(8) 4_545 5 ? O3 A2' A2' 85.09(7) 3_445 5 ? O1 A2' A2' 66.35(7) 8_455 5 ? O1 A2' A2' 119.49(11) 7_556 5 ? T2 A2' A2' 114.34(6) 6_566 5 ? T2 A2' A2' 62.59(4) 5_565 5 ? A2' A2' A2' 174.09(17) 5_556 5 ? A1 A1' A1 177.82(3) 4 3_455 ? A1 A1' O4 92.42(5) 4 . ? A1 A1' O4 85.96(5) 3_455 . ? A1 A1' O4 85.96(5) 4 2 ? A1 A1' O4 92.42(5) 3_455 2 ? O4 A1' O4 84.00(9) . 2 ? A1 A1' O2 78.73(5) 4 2 ? A1 A1' O2 102.99(5) 3_455 2 ? O4 A1' O2 170.20(7) . 2 ? O4 A1' O2 99.40(6) 2 2 ? A1 A1' O2 103.00(5) 4 . ? A1 A1' O2 78.73(5) 3_455 . ? O4 A1' O2 99.39(6) . . ? O4 A1' O2 170.20(7) 2 . ? O2 A1' O2 78.78(9) 2 . ? A1 A1' T1 91.090(13) 4 . ? A1 A1' T1 91.090(13) 3_455 . ? O4 A1' T1 138.00(5) . . ? O4 A1' T1 138.00(5) 2 . ? O2 A1' T1 39.39(4) 2 . ? O2 A1' T1 39.39(4) . . ? A1 A1' M1 88.910(13) 4 . ? A1 A1' M1 88.910(13) 3_455 . ? O4 A1' M1 42.00(5) . . ? O4 A1' M1 42.00(5) 2 . ? O2 A1' M1 140.61(4) 2 . ? O2 A1' M1 140.61(4) . . ? T1 A1' M1 180.0 . . ? A1' A1 A1' 180.00(3) 7 3_545 ? A1' A1 O2 55.94(4) 7 7 ? A1' A1 O2 124.06(4) 3_545 7 ? A1' A1 O2 124.06(4) 7 3_545 ? A1' A1 O2 55.94(4) 3_545 3_545 ? O2 A1 O2 180.00(9) 7 3_545 ? A1' A1 O4 50.92(4) 7 7 ? A1' A1 O4 129.08(4) 3_545 7 ? O2 A1 O4 76.31(5) 7 7 ? O2 A1 O4 103.69(5) 3_545 7 ? A1' A1 O4 129.08(4) 7 3_545 ? A1' A1 O4 50.92(4) 3_545 3_545 ? O2 A1 O4 103.69(5) 7 3_545 ? O2 A1 O4 76.31(5) 3_545 3_545 ? O4 A1 O4 180.00(9) 7 3_545 ? A1' A1 O4 47.27(4) 7 8 ? A1' A1 O4 132.73(4) 3_545 8 ? O2 A1 O4 103.12(5) 7 8 ? O2 A1 O4 76.88(5) 3_545 8 ? O4 A1 O4 60.71(6) 7 8 ? O4 A1 O4 119.29(6) 3_545 8 ? A1' A1 O4 132.73(4) 7 4_545 ? A1' A1 O4 47.27(4) 3_545 4_545 ? O2 A1 O4 76.88(5) 7 4_545 ? O2 A1 O4 103.12(5) 3_545 4_545 ? O4 A1 O4 119.29(6) 7 4_545 ? O4 A1 O4 60.71(6) 3_545 4_545 ? O4 A1 O4 180.00(6) 8 4_545 ? A1' A1 O2 41.97(3) 7 8 ? A1' A1 O2 138.03(3) 3_545 8 ? O2 A1 O2 56.31(6) 7 8 ? O2 A1 O2 123.69(6) 3_545 8 ? O4 A1 O2 92.81(5) 7 8 ? O4 A1 O2 87.19(5) 3_545 8 ? O4 A1 O2 65.34(5) 8 8 ? O4 A1 O2 114.66(5) 4_545 8 ? A1' A1 O2 138.03(3) 7 4_545 ? A1' A1 O2 41.97(3) 3_545 4_545 ? O2 A1 O2 123.69(6) 7 4_545 ? O2 A1 O2 56.31(6) 3_545 4_545 ? O4 A1 O2 87.19(5) 7 4_545 ? O4 A1 O2 92.81(5) 3_545 4_545 ? O4 A1 O2 114.66(5) 8 4_545 ? O4 A1 O2 65.34(4) 4_545 4_545 ? O2 A1 O2 180.00(5) 8 4_545 ? A1' A1 T1 122.722(13) 7 3_545 ? A1' A1 T1 57.278(13) 3_545 3_545 ? O2 A1 T1 148.73(4) 7 3_545 ? O2 A1 T1 31.27(4) 3_545 3_545 ? O4 A1 T1 81.67(4) 7 3_545 ? O4 A1 T1 98.33(4) 3_545 3_545 ? O4 A1 T1 84.64(3) 8 3_545 ? O4 A1 T1 95.36(3) 4_545 3_545 ? O2 A1 T1 147.75(3) 8 3_545 ? O2 A1 T1 32.25(3) 4_545 3_545 ? A1' A1 T1 57.278(13) 7 7 ? A1' A1 T1 122.722(13) 3_545 7 ? O2 A1 T1 31.27(4) 7 7 ? O2 A1 T1 148.73(4) 3_545 7 ? O4 A1 T1 98.33(4) 7 7 ? O4 A1 T1 81.67(4) 3_545 7 ? O4 A1 T1 95.36(3) 8 7 ? O4 A1 T1 84.64(3) 4_545 7 ? O2 A1 T1 32.25(3) 8 7 ? O2 A1 T1 147.75(3) 4_545 7 ? T1 A1 T1 180.0 3_545 7 ? O3 M1 O3 113.93(10) 3_445 4_545 ? O3 M1 O4 86.23(6) 3_445 2 ? O3 M1 O4 159.16(7) 4_545 2 ? O3 M1 O4 159.16(7) 3_445 . ? O3 M1 O4 86.23(6) 4_545 . ? O4 M1 O4 74.33(9) 2 . ? O3 M1 O1 87.33(6) 3_445 4_545 ? O3 M1 O1 75.80(6) 4_545 4_545 ? O4 M1 O1 112.01(6) 2 4_545 ? O4 M1 O1 92.98(6) . 4_545 ? O3 M1 O1 75.80(6) 3_445 3_445 ? O3 M1 O1 87.33(6) 4_545 3_445 ? O4 M1 O1 92.98(6) 2 3_445 ? O4 M1 O1 112.01(6) . 3_445 ? O1 M1 O1 148.94(10) 4_545 3_445 ? O3 M1 A1' 123.04(5) 3_445 . ? O3 M1 A1' 123.04(5) 4_545 . ? O4 M1 A1' 37.17(4) 2 . ? O4 M1 A1' 37.17(4) . . ? O1 M1 A1' 105.53(5) 4_545 . ? O1 M1 A1' 105.53(5) 3_445 . ? O3 M1 M2 38.02(4) 3_445 3_445 ? O3 M1 M2 109.88(5) 4_545 3_445 ? O4 M1 M2 82.39(4) 2 3_445 ? O4 M1 M2 141.90(5) . 3_445 ? O1 M1 M2 123.94(5) 4_545 3_445 ? O1 M1 M2 38.90(4) 3_445 3_445 ? A1' M1 M2 114.246(18) . 3_445 ? O3 M1 M2 109.88(5) 3_445 4_545 ? O3 M1 M2 38.02(4) 4_545 4_545 ? O4 M1 M2 141.90(5) 2 4_545 ? O4 M1 M2 82.39(4) . 4_545 ? O1 M1 M2 38.90(4) 4_545 4_545 ? O1 M1 M2 123.94(5) 3_445 4_545 ? A1' M1 M2 114.246(18) . 4_545 ? M2 M1 M2 131.51(4) 3_445 4_545 ? O3 M1 A2' 56.96(5) 3_445 . ? O3 M1 A2' 56.96(5) 4_545 . ? O4 M1 A2' 142.83(4) 2 . ? O4 M1 A2' 142.83(4) . . ? O1 M1 A2' 74.47(5) 4_545 . ? O1 M1 A2' 74.47(5) 3_445 . ? A1' M1 A2' 180.0 . . ? M2 M1 A2' 65.754(18) 3_445 . ? M2 M1 A2' 65.754(18) 4_545 . ? O3 M1 A1 120.52(4) 3_445 4 ? O3 M1 A1 116.66(4) 4_545 4 ? O4 M1 A1 43.66(5) 2 4 ? O4 M1 A1 47.57(4) . 4 ? O1 M1 A1 133.51(5) 4_545 4 ? O1 M1 A1 77.37(4) 3_445 4 ? A1' M1 A1 28.687(8) . 4 ? M2 M1 A1 95.120(13) 3_445 4 ? M2 M1 A1 129.143(19) 4_545 4 ? A2' M1 A1 151.313(8) . 4 ? O3 M1 A1 116.66(4) 3_445 3_455 ? O3 M1 A1 120.52(4) 4_545 3_455 ? O4 M1 A1 47.57(4) 2 3_455 ? O4 M1 A1 43.66(5) . 3_455 ? O1 M1 A1 77.37(4) 4_545 3_455 ? O1 M1 A1 133.51(5) 3_445 3_455 ? A1' M1 A1 28.687(8) . 3_455 ? M2 M1 A1 129.143(19) 3_445 3_455 ? M2 M1 A1 95.120(13) 4_545 3_455 ? A2' M1 A1 151.313(8) . 3_455 ? A1 M1 A1 57.374(16) 4 3_455 ? O6 M2 O2 92.15(7) . . ? O6 M2 O3 87.55(7) . . ? O2 M2 O3 109.25(7) . . ? O6 M2 O5 104.94(7) . 7_566 ? O2 M2 O5 89.77(6) . 7_566 ? O3 M2 O5 157.06(6) . 7_566 ? O6 M2 O1 97.28(7) . . ? O2 M2 O1 168.81(6) . . ? O3 M2 O1 77.30(6) . . ? O5 M2 O1 82.01(6) 7_566 . ? O6 M2 O5 171.88(7) . . ? O2 M2 O5 81.59(6) . . ? O3 M2 O5 89.64(6) . . ? O5 M2 O5 80.32(6) 7_566 . ? O1 M2 O5 89.52(6) . . ? O6 M2 M2 145.51(6) . 7_566 ? O2 M2 M2 84.27(5) . 7_566 ? O3 M2 M2 126.03(5) . 7_566 ? O5 M2 M2 40.96(4) 7_566 7_566 ? O1 M2 M2 84.55(5) . 7_566 ? O5 M2 M2 39.36(4) . 7_566 ? O6 M2 T1 110.36(5) . 7_566 ? O2 M2 T1 142.80(5) . 7_566 ? O3 M2 T1 101.19(4) . 7_566 ? O5 M2 T1 56.63(4) 7_566 7_566 ? O1 M2 T1 26.81(4) . 7_566 ? O5 M2 T1 77.66(4) . 7_566 ? M2 M2 T1 60.261(17) 7_566 7_566 ? O6 M2 T1 118.18(5) . . ? O2 M2 T1 26.60(4) . . ? O3 M2 T1 113.03(5) . . ? O5 M2 T1 78.35(4) 7_566 . ? O1 M2 T1 142.76(5) . . ? O5 M2 T1 56.26(4) . . ? M2 M2 T1 60.047(17) 7_566 . ? T1 M2 T1 120.307(17) 7_566 . ? O6 M2 M1 100.25(5) . 3 ? O2 M2 M1 143.97(5) . 3 ? O3 M2 M1 38.80(4) . 3 ? O5 M2 M1 118.75(5) 7_566 3 ? O1 M2 M1 39.65(4) . 3 ? O5 M2 M1 82.17(4) . 3 ? M2 M2 M1 102.64(3) 7_566 3 ? T1 M2 M1 62.394(12) 7_566 3 ? T1 M2 M1 132.84(2) . 3 ? O6 M2 A2' 46.38(6) . 7_556 ? O2 M2 A2' 122.39(6) . 7_556 ? O3 M2 A2' 106.73(5) . 7_556 ? O5 M2 A2' 71.26(5) 7_566 7_556 ? O1 M2 A2' 62.00(5) . 7_556 ? O5 M2 A2' 141.69(6) . 7_556 ? M2 M2 A2' 108.36(4) 7_566 7_556 ? T1 M2 A2' 65.44(4) 7_566 7_556 ? T1 M2 A2' 136.72(2) . 7_556 ? M1 M2 A2' 89.38(2) 3 7_556 ? O6 M2 A2' 41.56(6) . 3 ? O2 M2 A2' 121.41(5) . 3 ? O3 M2 A2' 52.25(5) . 3 ? O5 M2 A2' 128.20(5) 7_566 3 ? O1 M2 A2' 69.78(5) . 3 ? O5 M2 A2' 139.03(5) . 3 ? M2 M2 A2' 154.16(4) 7_566 3 ? T1 M2 A2' 94.00(2) 7_566 3 ? T1 M2 A2' 145.61(2) . 3 ? M1 M2 A2' 59.12(4) 3 3 ? A2' M2 A2' 57.302(9) 7_556 3 ? O1 T1 O1 114.19(11) 7_566 8_465 ? O1 T1 O2 110.14(7) 7_566 2 ? O1 T1 O2 113.88(7) 8_465 2 ? O1 T1 O2 113.88(7) 7_566 . ? O1 T1 O2 110.14(7) 8_465 . ? O2 T1 O2 92.81(10) 2 . ? O1 T1 A1' 122.90(5) 7_566 . ? O1 T1 A1' 122.90(5) 8_465 . ? O2 T1 A1' 46.41(5) 2 . ? O2 T1 A1' 46.41(5) . . ? O1 T1 A1 152.22(5) 7_566 3_455 ? O1 T1 A1 92.31(5) 8_465 3_455 ? O2 T1 A1 62.53(5) 2 3_455 ? O2 T1 A1 44.53(5) . 3_455 ? A1' T1 A1 31.633(3) . 3_455 ? O1 T1 A1 92.31(5) 7_566 4 ? O1 T1 A1 152.22(5) 8_465 4 ? O2 T1 A1 44.53(5) 2 4 ? O2 T1 A1 62.53(5) . 4 ? A1' T1 A1 31.633(3) . 4 ? A1 T1 A1 63.266(6) 3_455 4 ? O1 T1 M2 34.19(5) 7_566 7_566 ? O1 T1 M2 105.38(5) 8_465 7_566 ? O2 T1 M2 137.35(5) 2 7_566 ? O2 T1 M2 88.72(5) . 7_566 ? A1' T1 M2 121.141(11) . 7_566 ? A1 T1 M2 133.209(10) 3_455 7_566 ? A1 T1 M2 101.301(10) 4 7_566 ? O1 T1 M2 105.38(5) 7_566 8_465 ? O1 T1 M2 34.19(5) 8_465 8_465 ? O2 T1 M2 88.72(5) 2 8_465 ? O2 T1 M2 137.35(5) . 8_465 ? A1' T1 M2 121.141(11) . 8_465 ? A1 T1 M2 101.301(10) 3_455 8_465 ? A1 T1 M2 133.209(11) 4 8_465 ? M2 T1 M2 117.72(2) 7_566 8_465 ? O1 T1 M2 103.47(5) 7_566 2 ? O1 T1 M2 90.76(5) 8_465 2 ? O2 T1 M2 31.82(5) 2 2 ? O2 T1 M2 122.49(5) . 2 ? A1' T1 M2 76.897(11) . 2 ? A1 T1 M2 83.392(11) 3_455 2 ? A1 T1 M2 74.278(11) 4 2 ? M2 T1 M2 137.655(16) 7_566 2 ? M2 T1 M2 59.694(17) 8_465 2 ? O1 T1 M2 90.76(5) 7_566 . ? O1 T1 M2 103.47(5) 8_465 . ? O2 T1 M2 122.49(5) 2 . ? O2 T1 M2 31.82(5) . . ? A1' T1 M2 76.898(11) . . ? A1 T1 M2 74.279(10) 3_455 . ? A1 T1 M2 83.393(11) 4 . ? M2 T1 M2 59.693(17) 7_566 . ? M2 T1 M2 137.655(16) 8_465 . ? M2 T1 M2 153.79(2) 2 . ? O6 T2 O3 106.84(8) 4 7_565 ? O6 T2 O5 110.88(8) 4 . ? O3 T2 O5 110.53(7) 7_565 . ? O6 T2 O4 113.65(8) 4 4 ? O3 T2 O4 109.43(7) 7_565 4 ? O5 T2 O4 105.55(8) . 4 ? O6 T2 A2' 46.39(7) 4 5_565 ? O3 T2 A2' 60.58(6) 7_565 5_565 ? O5 T2 A2' 122.87(5) . 5_565 ? O4 T2 A2' 131.27(6) 4 5_565 ? O6 T2 A2' 42.84(7) 4 1_565 ? O3 T2 A2' 105.30(5) 7_565 1_565 ? O5 T2 A2' 71.95(6) . 1_565 ? O4 T2 A2' 143.35(6) 4 1_565 ? A2' T2 A2' 59.656(6) 5_565 1_565 ? O6 T2 A1 86.39(6) 4 2_665 ? O3 T2 A1 147.47(5) 7_565 2_665 ? O5 T2 A1 91.07(5) . 2_665 ? O4 T2 A1 39.21(5) 4 2_665 ? A2' T2 A1 127.39(4) 5_565 2_665 ? A2' T2 A1 104.39(2) 1_565 2_665 ? T1 O1 M2 119.00(8) 7_566 . ? T1 O1 M1 124.77(8) 7_566 3 ? M2 O1 M1 101.45(6) . 3 ? T1 O1 A2' 95.09(6) 7_566 7_556 ? M2 O1 A2' 80.31(5) . 7_556 ? M1 O1 A2' 129.39(7) 3 7_556 ? T1 O2 A1' 94.20(7) . . ? T1 O2 M2 121.58(8) . . ? A1' O2 M2 139.55(8) . . ? T1 O2 A1 104.20(7) . 3_455 ? A1' O2 A1 45.33(3) . 3_455 ? M2 O2 A1 128.28(7) . 3_455 ? T1 O2 A1 85.22(6) . 4 ? A1' O2 A1 35.04(3) . 4 ? M2 O2 A1 123.10(7) . 4 ? A1 O2 A1 80.36(4) 3_455 4 ? T2 O3 M2 124.82(8) 7_565 . ? T2 O3 M1 131.88(8) 7_565 3 ? M2 O3 M1 103.17(6) . 3 ? T2 O3 A2' 88.61(6) 7_565 3 ? M2 O3 A2' 93.11(5) . 3 ? M1 O3 A2' 85.22(6) 3 3 ? T2 O4 A1' 134.08(9) 4_545 . ? T2 O4 M1 124.67(8) 4_545 . ? A1' O4 M1 100.83(7) . . ? T2 O4 A1 114.80(7) 4_545 3_455 ? A1' O4 A1 43.12(3) . 3_455 ? M1 O4 A1 99.83(6) . 3_455 ? T2 O4 A1 128.73(8) 4_545 4 ? A1' O4 A1 40.31(3) . 4 ? M1 O4 A1 95.48(5) . 4 ? A1 O4 A1 83.42(4) 3_455 4 ? T2 O5 M2 134.23(9) . 7_566 ? T2 O5 M2 120.11(8) . . ? M2 O5 M2 99.68(6) 7_566 . ? T2 O6 M2 138.72(10) 4_545 . ? T2 O6 A2' 104.16(9) 4_545 7_556 ? M2 O6 A2' 97.36(9) . 7_556 ? T2 O6 A2' 110.21(10) 4_545 3 ? M2 O6 A2' 106.30(9) . 3 ? A2' O6 A2' 85.21(5) 7_556 3 ? _refine_diff_density_max 0.907 _refine_diff_density_min -0.993 _refine_diff_density_rms 0.200 _shelx_res_file ; 4334_.res created by SHELXL-2014/7 TITL Johellerite 4334 CELL 0.7107300 11.86146 12.75107 6.69583 90.0000 113.0253 90.0000 ZERR 4.00 0.00035 0.00038 0.00019 0.0000 0.0014 0.0000 LATT 7 SYMM -X, Y, 0.5-Z SFAC O As Mg Fe Cu Na UNIT 48 12 10.04 1.72 3.64 3.52 L.S. 14 BOND FMAP 2 PLAN 20 acta omit 0 2 2 omit -2 6 2 omit -4 2 2 omit -4 0 4 WGHT 0.000000 5.820700 EXTI 0.000114 FVAR 0.18017 0.75296 0.84821 0.13124 1.10435 1.23941 A2' 6 0.000000 -0.006777 0.250000 20.50000 0.01424 0.03403 = 0.02156 0.00000 0.00306 0.00000 A1' 5 0.000000 0.502497 0.250000 30.50000 0.00521 0.00319 = 0.01273 0.00000 0.00335 0.00000 A1 6 0.500000 0.000000 0.000000 40.50000 0.00976 0.00864 = 0.01279 0.00229 -0.00899 -0.00187 M1 3 0.000000 0.260085 0.250000 50.50000 0.00697 0.00964 = 0.00811 0.00000 0.00438 0.00000 M2 3 0.286645 0.655321 0.376459 61.00000 0.00523 0.00576 = 0.00536 -0.00072 0.00281 -0.00055 T1 2 0.000000 0.713116 0.250000 10.50000 0.00594 0.00522 = 0.00464 0.00000 0.00163 0.00000 T2 2 0.231301 0.886341 0.124586 11.00000 0.00592 0.00496 = 0.00494 -0.00019 0.00208 -0.00034 O1 1 0.463466 0.715612 0.523561 11.00000 0.00824 0.01085 = 0.00615 -0.00230 0.00237 -0.00135 O2 1 0.106975 0.620706 0.262892 11.00000 0.00748 0.00653 = 0.01534 -0.00096 0.00464 0.00033 O3 1 0.339659 0.670575 0.119670 11.00000 0.01034 0.01021 = 0.00510 -0.00161 0.00251 -0.00316 O4 1 0.116128 0.391696 0.314476 11.00000 0.00608 0.00716 = 0.01772 0.00091 0.00479 0.00074 O5 1 0.215634 0.812512 0.320657 11.00000 0.01048 0.00927 = 0.00678 0.00132 0.00387 -0.00082 O6 1 0.333129 0.503618 0.389002 11.00000 0.01323 0.00573 = 0.01740 0.00116 0.00644 -0.00194 hklf 4 REM Johellerite 4334 REM R1 = 0.0286 for 3063 Fo > 4sig(Fo) and 0.0383 for all 3579 data REM 105 parameters refined using 0 restraints END WGHT 0.0000 5.8258 REM Highest difference peak 0.907, deepest hole -0.993, 1-sigma level 0.200 Q1 1 0.2464 0.9415 0.1490 11.00000 0.05 0.91 Q2 1 0.0000 0.1667 0.2500 10.50000 0.05 0.89 Q3 1 -0.0396 0.6795 0.2105 11.00000 0.05 0.88 Q4 1 0.2935 0.6071 0.3756 11.00000 0.05 0.86 Q5 1 0.2389 0.8185 0.1273 11.00000 0.05 0.83 Q6 1 0.2081 0.8810 -0.0102 11.00000 0.05 0.74 Q7 1 0.0000 0.8095 0.2500 10.50000 0.05 0.74 Q8 1 0.1913 0.3927 0.3836 11.00000 0.05 0.72 Q9 1 0.2563 0.5572 0.3827 11.00000 0.05 0.72 Q10 1 -0.0343 0.7475 0.2083 11.00000 0.05 0.71 Q11 1 0.1734 0.6565 0.3779 11.00000 0.05 0.71 Q12 1 0.1877 0.8497 0.0778 11.00000 0.05 0.69 Q13 1 0.2221 0.6428 0.3183 11.00000 0.05 0.69 Q14 1 0.2976 0.4817 0.3232 11.00000 0.05 0.69 Q15 1 0.3904 0.5017 0.3410 11.00000 0.05 0.68 Q16 1 0.1674 0.9349 0.0556 11.00000 0.05 0.67 Q17 1 0.0762 0.5827 0.2088 11.00000 0.05 0.67 Q18 1 0.1646 0.8875 0.1310 11.00000 0.05 0.67 Q19 1 0.1443 0.4181 0.4973 11.00000 0.05 0.66 Q20 1 0.3695 0.4525 0.3773 11.00000 0.05 0.65 ; _shelx_res_checksum 75860 _shelx_hkl_file ; 2 0 0 209.703 7.027 4 2 0 0 182.629 7.092 9 2 0 0 179.326 5.937 2 -2 0 0 213.732 7.031 4 4 0 0 5555.46 195.42 4 4 0 0 5649.04 197.23 9 -4 0 0 5393.80 162.96 1 -4 0 0 5773.70 195.64 4 4 0 0 5490.54 164.77 2 -6 0 0 319.595 11.696 9 6 0 0 294.744 11.357 4 -6 0 0 298.838 9.503 1 6 0 0 306.928 9.737 2 6 0 0 322.781 11.663 9 -6 0 0 309.158 11.371 4 8 0 0 2322.04 68.50 2 -8 0 0 2311.37 67.54 1 8 0 0 2249.98 80.84 4 8 0 0 2295.92 81.60 9 -8 0 0 2336.95 81.58 9 -8 0 0 2367.24 80.85 4 -10 0 0 580.833 21.213 9 10 0 0 573.286 17.880 2 10 0 0 583.367 20.945 4 10 0 0 556.816 21.221 9 -10 0 0 570.513 20.758 4 -10 0 0 561.037 17.375 1 10 0 0 525.355 20.727 4 -12 0 0 227.309 8.623 1 12 0 0 266.443 9.352 2 12 0 0 257.844 10.619 4 -12 0 0 253.684 10.483 4 14 0 0 383.528 15.741 4 14 0 0 397.702 13.877 2 16 0 0 6.70667 3.76714 2 18 0 0 608.837 21.284 2 -20 0 0 7.70633 5.16361 2 20 0 0 2.48953 5.12699 2 3 -1 0 1653.24 51.23 1 -3 -1 0 1696.76 51.33 1 3 -1 0 1754.18 52.12 2 3 -1 0 1702.71 61.08 4 3 -1 0 1744.57 62.45 9 -3 -1 0 1772.94 61.16 4 -3 1 0 1777.90 60.99 4 3 1 0 1736.28 61.81 4 3 1 0 1781.09 62.68 9 -3 1 0 1731.11 51.06 1 3 1 0 1746.01 61.26 4 3 1 0 1681.66 51.67 2 5 -1 0 670.879 20.228 2 -5 -1 0 655.470 19.942 1 5 -1 0 663.089 24.108 9 -5 -1 0 714.083 23.899 4 5 -1 0 673.307 23.844 4 -5 1 0 645.448 19.892 1 5 1 0 674.794 23.875 4 5 1 0 662.691 20.253 2 5 1 0 671.658 24.162 9 5 1 0 681.751 23.891 4 -5 1 0 698.340 23.851 4 -7 -1 0 1312.33 45.85 9 7 -1 0 1286.08 38.44 2 7 -1 0 1261.36 45.80 9 -7 -1 0 1318.81 45.37 4 7 -1 0 1266.60 45.35 4 -7 -1 0 1258.01 37.89 1 -7 1 0 1340.78 45.36 4 7 1 0 1280.56 45.87 9 7 1 0 1301.88 38.50 2 -7 1 0 1296.88 45.80 9 7 1 0 1257.05 45.36 4 -7 1 0 1270.52 37.86 1 7 1 0 1307.86 45.39 4 9 -1 0 4.90726 1.33631 4 9 -1 0 4.12939 1.52040 2 -9 -1 0 3.38874 1.56138 9 -9 -1 0 4.62132 1.29821 1 9 -1 0 2.99412 1.57623 9 -9 -1 0 5.30039 1.47141 4 9 1 0 4.81438 1.54711 2 -9 1 0 6.03050 1.30869 1 9 1 0 5.84632 1.61182 4 -9 1 0 3.16351 1.51955 9 9 1 0 7.16178 1.45335 4 -9 1 0 5.79860 1.51644 4 9 1 0 3.88746 1.24608 9 -11 -1 0 735.874 27.892 4 11 -1 0 793.073 24.049 2 11 -1 0 786.445 28.115 4 -11 -1 0 751.185 23.414 1 -11 1 0 746.419 23.365 1 11 1 0 778.528 28.140 4 11 1 0 790.845 24.048 2 -11 1 0 775.511 27.957 4 13 -1 0 127.725 6.337 2 13 -1 0 130.860 6.857 4 13 1 0 131.984 6.326 2 -13 1 0 126.563 6.459 4 13 1 0 132.578 6.868 4 15 -1 0 319.780 12.105 2 15 1 0 316.001 12.128 2 17 -1 0 -0.6784 3.9361 2 17 1 0 0.13023 3.99691 2 19 -1 0 71.0851 6.6167 2 19 1 0 77.5964 6.7351 2 -19 1 0 79.1515 6.7750 2 0 -2 0 272.490 9.339 4 0 2 0 256.939 9.409 9 0 2 0 286.223 9.349 4 0 2 0 243.882 7.897 2 2 -2 0 75.3206 2.5346 2 -2 -2 0 76.4171 3.0405 4 2 -2 0 83.3380 2.9906 4 2 -2 0 71.2850 2.5172 1 2 -2 0 74.4576 3.0638 9 2 2 0 74.8337 3.1053 9 -2 2 0 83.8955 2.9855 4 2 2 0 79.1074 3.0498 4 2 2 0 82.9201 3.0298 4 2 2 0 71.2880 2.5699 2 -2 2 0 74.8339 3.0084 9 -2 2 0 74.9825 2.5414 2 4 -2 0 196.096 6.584 1 4 -2 0 203.357 7.925 9 4 -2 0 214.763 7.775 4 -4 -2 0 203.102 6.550 1 4 -2 0 212.866 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0 225.728 7.040 1 3 3 0 237.604 8.518 4 3 3 0 233.588 8.550 4 3 3 0 229.328 8.647 9 5 -3 0 1128.03 39.70 9 5 -3 0 1162.31 33.32 2 5 -3 0 1081.84 32.96 1 5 -3 0 1078.81 39.28 4 -5 -3 0 1098.59 32.91 1 -5 3 0 1127.13 39.28 4 -5 3 0 1147.55 39.69 9 5 3 0 1115.34 33.38 2 -5 3 0 1154.65 39.63 9 5 3 0 1068.18 39.34 4 -5 3 0 1091.46 32.79 1 5 3 0 1162.35 39.43 4 5 3 0 1145.23 39.79 9 7 -3 0 844.583 25.151 2 -7 -3 0 826.572 30.080 9 7 -3 0 795.605 29.923 9 -7 -3 0 826.246 24.807 1 7 -3 0 822.504 29.577 4 -7 3 0 842.212 29.947 9 7 3 0 828.273 29.653 4 7 3 0 816.219 25.216 2 -7 3 0 885.852 29.605 4 7 3 0 809.981 30.022 9 -7 3 0 826.406 29.829 9 7 3 0 858.295 29.711 4 -7 3 0 825.794 24.690 1 9 -3 0 277.167 11.274 9 9 -3 0 271.122 10.999 4 -9 -3 0 285.831 9.289 1 9 -3 0 292.776 9.573 2 -9 -3 0 277.071 11.298 9 -9 3 0 287.564 10.950 4 9 3 0 286.230 11.389 9 9 3 0 292.335 11.125 4 9 3 0 270.647 10.947 4 9 3 0 287.138 9.623 2 -9 3 0 281.462 11.078 9 -9 3 0 275.239 9.127 1 -9 3 0 284.506 11.159 9 -11 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4 0 169.083 5.588 2 -4 4 0 166.101 5.327 1 4 4 0 158.056 6.429 4 6 -4 0 4000.50 116.39 2 6 -4 0 3919.56 137.97 9 6 -4 0 3847.86 135.81 4 -6 -4 0 3898.95 114.27 1 6 -4 0 3805.20 113.11 1 6 4 0 3867.75 139.10 9 6 4 0 3907.70 116.57 2 6 4 0 3669.70 136.47 4 6 4 0 4106.65 137.92 4 -6 4 0 3923.10 112.91 1 -6 4 0 3959.01 138.35 9 -6 4 0 3851.86 139.10 9 -6 4 0 3868.98 135.75 4 -8 -4 0 24.2028 2.5021 9 -8 -4 0 24.9585 1.9487 1 8 -4 0 22.8995 2.2293 4 8 -4 0 26.0370 2.0988 2 8 -4 0 25.4162 2.5734 9 -8 4 0 24.5555 2.4900 9 8 4 0 24.3979 2.4749 4 -8 4 0 25.6347 2.2643 9 8 4 0 26.1066 2.1841 2 8 4 0 24.8339 2.5369 9 -8 4 0 27.0178 2.0150 1 8 4 0 23.4197 2.2284 4 -8 4 0 22.7234 2.2922 4 10 -4 0 380.788 11.990 2 -10 -4 0 343.583 14.184 9 -10 -4 0 359.851 11.610 1 -10 4 0 366.164 13.711 4 10 4 0 364.962 12.045 2 -10 4 0 348.404 13.943 9 10 4 0 333.332 13.689 4 -10 4 0 344.805 11.407 1 10 4 0 374.776 13.925 4 -12 -4 0 338.782 13.250 1 12 -4 0 409.103 13.535 2 12 4 0 423.492 13.676 2 -12 4 0 393.992 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43.49 2 -5 -5 0 1483.15 43.04 1 -5 5 0 1515.52 43.54 2 5 5 0 1458.58 51.95 9 -5 5 0 1454.96 42.86 1 -5 5 0 1487.08 51.83 9 5 5 0 1432.63 51.42 4 5 5 0 1464.79 43.61 2 5 5 0 1463.91 51.47 4 -5 5 0 1498.51 51.35 4 -5 5 0 1482.63 51.76 9 7 -5 0 21.1259 2.0269 4 7 -5 0 23.1386 1.8800 2 -7 -5 0 22.1530 2.1767 9 -7 -5 0 24.2862 1.9787 1 7 -5 0 21.2096 0.9752 8 7 -5 0 20.0428 1.8413 1 7 5 0 18.4063 2.0780 9 -7 5 0 23.8954 1.9681 2 -7 5 0 23.1810 2.1414 9 -7 5 0 23.2270 2.0810 4 7 5 0 21.8683 2.0626 4 -7 5 0 21.5245 1.7899 1 7 5 0 23.4941 1.9989 2 -7 5 0 20.7271 2.0340 9 7 5 0 19.4439 1.9853 4 -9 -5 0 1172.19 34.95 1 9 -5 0 1222.38 35.47 2 9 -5 0 1107.72 41.59 4 9 -5 0 1059.51 38.25 8 -9 -5 0 1190.42 42.29 9 9 -5 0 1201.46 42.24 9 -9 5 0 1240.59 35.51 2 9 5 0 1175.49 42.30 9 -9 5 0 1122.47 41.94 9 9 5 0 1181.07 35.55 2 9 5 0 1120.86 41.67 4 -9 5 0 1182.64 34.76 1 -9 5 0 1197.92 41.62 4 -9 5 0 1187.91 42.16 9 9 5 0 1210.30 41.81 4 -11 -5 0 0.60966 1.62327 1 11 -5 0 4.05083 2.10688 2 -11 5 0 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9.26454 1.32792 4 4 6 0 9.75386 1.40505 9 4 6 0 10.2791 1.2467 2 -4 6 0 10.1372 1.1342 9 -4 6 0 10.5457 1.1994 2 -4 6 0 10.0629 1.0301 1 6 -6 0 454.326 17.739 4 -6 -6 0 462.448 17.891 4 6 -6 0 503.624 15.160 1 -6 -6 0 492.162 15.057 1 6 -6 0 490.297 15.189 2 -6 6 0 517.304 15.274 2 6 6 0 498.222 15.358 2 6 6 0 469.140 17.842 4 -6 6 0 485.587 14.843 1 6 6 0 487.975 18.242 9 -6 6 0 491.914 18.005 9 -6 6 0 495.173 18.107 9 6 6 0 498.583 17.972 4 -6 6 0 502.948 17.790 4 -8 -6 0 64.2298 3.9077 9 8 -6 0 55.8809 3.3758 1 8 -6 0 66.8208 3.6116 4 8 -6 0 63.3879 3.4329 2 -8 -6 0 65.5704 3.2666 1 -8 6 0 57.2986 3.5440 9 -8 6 0 57.7610 3.4804 9 -8 6 0 56.4455 3.3437 2 8 6 0 68.4278 3.6409 4 8 6 0 66.4516 4.0462 4 8 6 0 66.9189 3.5704 2 8 6 0 60.4236 3.8806 9 -8 6 0 71.6401 3.6854 4 -8 6 0 63.8030 3.0272 1 10 -6 0 92.0863 4.5541 2 -10 -6 0 86.2803 4.2075 1 10 6 0 89.9228 4.6640 2 -10 6 0 93.5672 4.8773 4 10 6 0 93.9101 5.0245 4 -10 6 0 83.9811 3.9542 1 -10 6 0 88.6646 4.5289 2 12 -6 0 7.30400 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0 533.168 16.173 2 5 7 0 548.211 19.082 4 5 7 0 532.668 16.277 2 -5 7 0 517.318 19.193 9 -5 7 0 544.492 18.913 4 -5 7 0 510.165 15.751 1 -5 7 0 513.153 17.073 6 5 7 0 507.701 18.930 4 -7 -7 0 7.30654 1.73104 9 -7 -7 0 7.35805 1.50552 4 -7 -7 0 10.0744 1.5889 1 7 -7 0 8.64008 1.47379 4 7 -7 0 7.27074 1.56259 1 7 7 0 9.12361 1.78166 9 -7 7 0 8.36657 1.73863 9 -7 7 0 10.9293 1.6248 9 7 7 0 8.89495 1.73851 4 -7 7 0 8.03658 1.56949 4 -7 7 0 10.5846 1.7053 2 7 7 0 9.63449 1.72215 2 7 7 0 8.98938 1.49231 4 -7 7 0 9.22602 1.37012 1 -9 -7 0 146.447 5.838 1 9 -7 0 161.084 6.089 2 9 -7 0 145.674 6.089 1 -9 7 0 148.398 6.070 2 9 7 0 155.190 6.917 4 9 7 0 151.123 6.195 2 9 7 0 144.544 6.723 4 -9 7 0 159.862 6.749 4 -9 7 0 151.657 5.601 1 11 -7 0 1.75981 2.22730 2 -11 -7 0 1.78397 1.80810 1 11 7 0 0.92197 2.23585 2 -11 7 0 -0.0163 2.2273 2 -11 7 0 3.47007 2.06012 4 11 7 0 2.14160 2.06255 4 13 -7 0 176.036 7.822 2 13 7 0 167.936 8.696 4 -13 7 0 166.739 8.241 2 13 7 0 168.914 7.776 2 15 -7 0 1.97654 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48.5815 6.3329 6 -16 4 -3 51.8031 5.3818 2 -18 -4 -3 0.08695 4.65895 3 21 5 -3 5.58729 4.73009 2 -21 5 3 20.8372 5.4796 2 19 5 -3 20.4195 5.5034 8 -19 5 3 9.77768 5.36609 2 19 5 -3 9.67762 4.38595 2 17 -5 -3 70.3997 6.1250 5 -17 -5 3 71.0600 5.6830 1 17 -5 -3 83.1138 6.2089 7 17 5 -3 77.0132 5.7523 7 17 5 -3 70.6320 6.5214 8 -17 5 3 69.1120 5.5741 1 17 5 -3 70.9161 5.9699 2 15 -5 -3 34.3293 3.7674 7 15 -5 -3 33.4671 3.6632 5 -15 -5 3 25.1628 3.3627 1 15 5 -3 34.0587 3.7221 7 15 5 -3 30.0083 3.5997 2 15 5 -3 30.6456 4.2573 8 -15 5 3 28.4125 3.5029 4 -15 5 3 32.6965 3.4010 1 -13 -5 3 155.382 6.556 1 13 -5 -3 156.783 7.202 4 13 -5 -3 164.978 6.980 7 -13 5 3 157.810 7.302 4 13 5 -3 160.398 7.802 8 13 5 -3 158.154 6.918 7 13 5 -3 159.209 6.935 4 -13 5 3 158.493 6.472 1 13 5 -3 148.060 6.616 2 -11 -5 3 89.7593 4.6910 4 11 -5 -3 92.7615 3.8001 8 -11 -5 3 94.0793 4.2506 1 11 -5 -3 92.9757 4.7252 4 11 -5 -3 91.9651 4.3968 7 -11 -5 3 88.9570 5.1366 9 -11 5 3 99.3596 4.2266 1 -11 5 3 88.2375 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9.57263 1.26123 9 5 -5 -3 12.9771 1.0942 7 -5 -5 3 12.6414 1.1111 1 5 -5 -3 11.6944 0.9074 3 5 -5 -3 12.1216 1.0778 8 5 -5 -3 11.3127 1.4048 5 -5 5 3 10.8271 1.1438 4 5 5 -3 9.83319 0.89300 2 5 5 -3 8.73903 0.92568 9 5 5 -3 13.5102 1.4696 8 -5 5 3 8.14398 0.99274 2 5 5 -3 12.5033 1.0671 7 -5 5 3 9.33690 1.23364 9 -3 -5 3 58.9763 2.8057 9 -3 -5 3 63.7698 2.6197 4 -3 -5 3 57.4995 2.2506 1 3 -5 -3 64.4725 2.7408 5 3 -5 -3 61.0964 2.2530 6 3 -5 -3 64.5764 2.3542 3 3 -5 -3 66.4112 2.4735 7 3 5 -3 63.3398 2.0121 2 3 5 -3 67.5627 2.8368 8 3 5 -3 60.9446 2.3275 9 3 5 -3 63.2071 3.0552 6 -3 5 3 54.1533 2.3476 2 3 5 -3 67.3372 2.4415 7 3 5 -3 59.1815 2.3083 9 3 5 -3 67.3345 2.5546 3 3 5 -3 63.1947 1.9874 2 -3 5 3 68.8119 2.8471 4 -3 5 3 60.7030 2.8734 9 1 -5 -3 10.9337 0.9337 6 1 -5 -3 14.8124 1.2024 5 -1 -5 3 10.4704 1.0847 9 -1 -5 3 11.6963 0.9292 1 -1 -5 3 14.4487 1.0060 4 1 -5 -3 14.4902 1.1030 3 1 -5 -3 11.0720 0.9767 9 1 5 -3 14.5490 1.1006 3 -1 5 3 11.3212 1.1703 9 -1 5 3 14.2511 1.4295 4 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1.01206 2 5 5 3 4.97375 1.27143 2 -5 5 -3 2.96771 1.63398 6 7 -5 3 63.1991 3.6623 1 7 -5 3 60.6457 3.3527 2 7 -5 3 65.2537 4.0684 9 -7 5 -3 58.5641 3.0277 3 -7 5 -3 65.5488 3.3115 2 -7 5 -3 69.8995 4.2003 6 7 5 3 47.3029 3.3155 2 7 5 3 52.3970 3.8128 4 7 5 3 46.0747 3.8614 9 -9 5 -3 6.75266 2.02656 3 -9 5 -3 4.76178 2.59917 6 -9 5 -3 8.13159 1.91061 2 9 5 3 9.87657 2.33589 2 -11 5 -3 28.7391 2.9624 3 11 5 3 34.3016 3.6835 2 -11 5 -3 26.4950 3.4589 2 -13 5 -3 1.47444 2.39712 3 -13 5 -3 3.45747 4.00206 6 13 5 3 -0.5408 3.4321 2 -13 5 -3 0.36377 3.62045 2 -15 -5 -3 1.58392 4.30120 3 -15 5 -3 0.22461 3.41989 2 -15 5 -3 1.24651 4.53255 6 -17 -5 -3 22.3051 5.4268 3 -17 5 -3 20.3253 4.5580 2 20 6 -3 169.877 9.852 2 -20 6 3 151.140 9.618 2 18 -6 -3 49.0903 4.6005 5 18 -6 -3 44.2234 4.8759 7 18 6 -3 37.4174 4.3813 7 18 6 -3 59.0546 5.8956 8 18 6 -3 43.9584 5.0054 2 -18 6 3 45.0536 5.1942 2 -16 -6 3 243.301 10.490 1 16 -6 -3 250.953 10.644 7 16 -6 -3 263.687 10.428 5 16 6 -3 258.253 10.800 2 16 6 -3 270.974 11.898 8 16 6 -3 266.046 10.593 7 -16 6 3 239.987 10.502 2 -16 6 3 261.424 10.005 1 -14 -6 3 10.4753 2.7464 1 14 -6 -3 8.33281 2.25047 4 14 -6 -3 10.6391 2.7035 7 -14 6 3 9.71303 2.46833 4 -14 6 3 11.0065 2.8210 2 14 6 -3 11.1907 2.6455 7 -14 6 3 17.1536 2.8494 1 14 6 -3 8.81188 2.76758 2 14 6 -3 9.43006 2.28304 4 14 6 -3 14.2931 3.5652 8 12 -6 -3 294.259 11.517 4 12 -6 -3 293.740 10.605 7 -12 -6 3 303.406 10.194 1 -12 6 3 316.129 10.137 1 -12 6 3 281.365 11.748 4 12 6 -3 303.307 10.292 2 12 6 -3 286.070 10.662 7 12 6 -3 276.534 11.751 8 12 6 -3 295.515 11.371 4 -10 -6 3 23.5888 2.6360 9 10 -6 -3 29.8907 1.7084 8 10 -6 -3 32.5309 2.4354 7 10 -6 -3 30.3495 2.4567 4 -10 -6 3 25.9002 2.2530 1 -10 6 3 22.4439 2.4678 9 10 6 -3 27.5103 2.2007 4 10 6 -3 26.7209 2.5013 4 -10 6 3 26.4772 2.7159 9 -10 6 3 26.5102 2.2198 1 10 6 -3 30.6310 3.1248 8 -10 6 3 30.2032 2.7282 4 10 6 -3 25.1198 2.2144 2 -10 6 3 24.8049 2.3278 2 10 6 -3 29.7998 2.5166 7 8 -6 -3 208.463 7.583 8 8 -6 -3 213.071 8.375 4 -8 -6 3 219.365 7.356 1 -8 -6 3 229.260 9.070 9 8 -6 -3 219.444 7.601 7 8 6 -3 230.267 7.507 2 -8 6 3 232.062 8.846 9 8 6 -3 217.298 7.653 7 8 6 -3 215.601 8.791 9 -8 6 3 213.897 8.730 4 -8 6 3 222.624 8.977 9 -8 6 3 230.082 7.339 1 8 6 -3 210.654 8.573 8 -8 6 3 226.903 7.592 2 8 6 -3 217.728 8.177 4 8 6 -3 214.930 8.129 4 -6 -6 3 300.052 11.484 9 6 -6 -3 309.423 9.831 7 6 -6 -3 299.585 10.957 4 -6 -6 3 306.142 9.419 1 6 -6 -3 310.618 10.201 8 6 -6 -3 286.325 9.944 5 -6 6 3 289.183 9.591 2 6 6 -3 305.818 9.840 7 -6 6 3 299.967 11.405 9 -6 6 3 310.118 11.233 4 6 6 -3 301.172 10.764 8 6 6 -3 299.811 9.421 2 6 6 -3 281.385 11.182 9 4 -6 -3 191.343 6.611 5 4 -6 -3 186.476 6.140 3 4 -6 -3 196.466 7.096 4 4 -6 -3 194.698 6.389 7 -4 -6 3 198.523 7.526 9 -4 -6 3 188.639 6.160 1 4 6 -3 189.040 7.201 9 -4 6 3 196.709 7.389 4 4 6 -3 192.280 6.354 7 4 6 -3 184.887 7.042 8 4 6 -3 196.455 6.089 2 -4 6 3 195.935 7.519 9 -4 6 3 183.607 6.272 2 2 -6 -3 995.618 30.726 3 -2 -6 3 1006.68 29.62 1 -2 -6 3 955.979 35.356 4 2 -6 -3 982.063 30.050 5 -2 -6 3 1022.64 35.79 9 2 -6 -3 989.197 35.653 9 2 -6 -3 1032.25 35.24 4 2 -6 -3 1004.02 32.17 6 2 -6 -3 1032.20 31.32 7 2 6 -3 1018.94 33.30 8 2 6 -3 1027.39 31.27 7 2 6 -3 1003.59 35.42 9 2 6 -3 981.101 35.487 9 2 6 -3 1004.83 29.83 2 2 6 -3 1024.53 29.76 2 -2 6 3 965.451 30.085 2 -2 6 3 1041.31 35.62 4 2 6 -3 1037.71 30.81 3 2 6 -3 1035.41 32.86 6 -2 6 3 1060.26 35.90 9 0 -6 -3 33.1291 1.8415 9 0 -6 -3 36.6079 1.8042 3 0 -6 -3 32.4608 1.7618 5 0 -6 3 34.2441 1.7130 1 0 -6 3 31.5180 1.9610 9 0 6 -3 33.8370 1.6237 3 0 6 -3 30.4370 1.6483 9 0 6 -3 34.6591 2.0499 6 0 6 3 34.2079 2.1948 9 0 6 3 34.9408 2.3038 4 0 6 -3 34.2964 1.6760 9 0 6 -3 33.4043 1.4435 2 0 6 3 31.6634 1.8637 2 0 6 -3 33.0302 1.5429 2 0 6 -3 32.8965 1.8479 8 -2 -6 -3 841.396 30.142 9 2 -6 3 899.766 25.051 1 -2 -6 -3 834.433 25.031 5 2 -6 3 870.735 30.195 9 2 -6 3 828.339 25.323 2 -2 -6 -3 846.435 26.240 3 -2 6 -3 821.285 25.851 3 -2 6 -3 826.179 29.930 9 2 6 3 883.047 30.442 9 -2 6 -3 817.814 29.885 9 -2 6 -3 866.661 27.773 6 2 6 3 842.171 30.132 4 -2 6 -3 871.099 25.163 2 2 6 3 794.723 25.474 2 -2 6 -3 837.267 27.768 8 4 -6 3 65.8034 3.0336 2 4 -6 3 71.9996 3.8163 9 4 -6 3 73.6668 3.1781 1 -4 -6 -3 65.8222 3.5027 9 4 6 3 68.8832 3.7358 4 4 6 3 65.5427 3.1732 2 -4 6 -3 66.3095 2.8179 3 -4 6 -3 67.0469 2.8839 2 4 6 3 70.2658 3.9199 9 -4 6 -3 70.4795 3.7087 6 6 -6 3 883.507 32.081 9 6 -6 3 874.821 26.875 2 6 -6 3 907.787 26.756 1 6 6 3 913.382 31.905 4 6 6 3 857.979 32.166 9 -6 6 -3 835.715 27.188 3 -6 6 -3 894.817 26.636 2 6 6 3 861.428 27.029 2 -6 6 -3 899.178 29.391 6 8 -6 3 126.452 6.099 1 8 -6 3 116.784 5.810 2 8 6 3 133.234 5.664 2 8 6 3 125.726 6.384 4 -8 6 -3 130.223 6.378 6 -8 6 -3 123.061 5.033 3 -8 6 -3 131.456 5.214 2 -10 6 -3 341.988 11.635 2 -10 6 -3 332.749 11.597 3 10 6 3 339.622 12.169 2 -10 6 -3 346.567 13.115 6 -12 6 -3 46.1718 3.7258 3 12 6 3 52.4995 4.5560 2 -12 6 -3 50.6855 4.6030 6 -12 6 -3 45.9044 3.9096 2 -14 6 -3 230.582 11.447 6 -14 6 -3 232.675 9.525 2 -16 -6 -3 5.64423 4.88849 3 -16 6 -3 1.40952 4.32734 2 -16 6 -3 3.68280 4.70221 6 -18 -6 -3 31.5336 5.7720 3 21 7 -3 5.93976 5.70931 2 21 7 -3 4.66303 4.63255 8 -21 7 3 8.89231 5.32968 2 19 -7 -3 21.9302 4.9379 5 19 7 -3 22.4372 5.2033 8 19 7 -3 21.7874 4.7378 2 -19 7 3 16.8808 4.9413 2 17 -7 -3 22.6206 4.1653 5 17 -7 -3 20.3584 3.6977 7 -17 -7 3 12.9036 4.3245 1 17 7 -3 18.5035 4.6919 8 -17 7 3 15.0183 4.0296 2 17 7 -3 15.0964 3.3165 7 17 7 -3 15.3900 4.0447 2 15 -7 -3 23.0977 3.3028 7 -15 -7 3 15.5121 3.1479 1 15 7 -3 19.4193 4.2999 8 15 7 -3 10.2310 3.2395 2 15 7 -3 17.6464 3.5292 7 -15 7 3 12.3094 3.2724 2 -15 7 3 11.5571 3.0391 1 13 -7 -3 186.084 8.243 4 -13 -7 3 193.579 7.663 1 13 -7 -3 199.688 7.841 7 13 7 -3 205.740 7.923 7 13 7 -3 184.455 8.016 4 -13 7 3 197.052 7.929 2 13 7 -3 187.877 7.701 2 -13 7 3 187.092 7.511 1 13 7 -3 194.058 9.181 8 -13 7 3 183.049 8.546 4 11 -7 -3 71.9823 3.7302 7 -11 -7 3 66.4007 3.8700 1 -11 7 3 66.5211 4.1627 4 11 7 -3 67.9675 3.7443 4 -11 7 3 63.8876 3.6093 2 11 7 -3 72.6677 4.0982 7 11 7 -3 66.8907 3.8781 2 -11 7 3 68.9201 3.8389 1 11 7 -3 62.6186 4.6195 8 9 -7 -3 548.976 20.948 4 -9 -7 3 571.075 17.911 1 9 -7 -3 594.447 18.733 7 -9 -7 3 567.403 21.715 9 9 -7 -3 565.044 19.185 8 -9 7 3 584.980 21.291 4 9 7 -3 576.066 18.095 2 -9 7 3 576.005 21.659 9 9 7 -3 566.902 20.800 4 -9 7 3 590.924 17.843 1 9 7 -3 609.342 20.806 4 -9 7 3 603.801 18.298 2 9 7 -3 567.792 20.481 8 -9 7 3 581.832 21.592 9 9 7 -3 606.801 18.847 7 -7 -7 3 571.433 21.267 9 7 -7 -3 572.235 20.640 4 -7 -7 3 581.235 17.554 1 7 -7 -3 598.981 18.337 7 -7 7 3 585.323 21.281 9 7 7 -3 591.664 20.343 4 7 7 -3 563.026 17.665 2 -7 7 3 568.816 17.834 2 7 7 -3 569.293 19.963 8 7 7 -3 582.412 20.288 4 7 7 -3 584.810 18.327 7 7 7 -3 527.955 21.006 9 -7 7 3 580.581 20.903 4 -7 7 3 579.726 21.171 9 5 -7 -3 1934.17 58.41 5 5 -7 -3 1958.33 59.51 3 -5 -7 3 1994.96 69.67 9 5 -7 -3 1985.00 61.43 7 5 -7 -3 1979.27 68.84 4 -5 -7 3 1996.78 57.73 1 5 7 -3 1873.34 69.39 9 5 7 -3 1979.37 60.83 7 -5 7 3 1947.47 58.48 2 5 7 -3 1985.84 64.85 8 -5 7 3 2019.15 69.64 9 -5 7 3 2045.98 69.12 4 5 7 -3 1989.29 58.32 2 3 -7 -3 807.681 24.333 5 3 -7 -3 823.906 25.090 7 -3 -7 3 817.039 23.887 1 3 -7 -3 831.077 28.407 4 -3 -7 3 824.350 28.877 9 3 -7 -3 791.780 24.545 3 3 7 -3 790.245 23.927 2 3 7 -3 824.777 25.049 7 -3 7 3 841.442 28.690 4 -3 7 3 760.601 24.239 2 3 7 -3 773.746 28.616 9 3 7 -3 807.092 26.824 8 3 7 -3 797.100 24.061 2 -3 7 3 799.888 28.883 9 1 -7 -3 1435.70 43.06 5 1 -7 -3 1432.81 51.43 9 1 -7 -3 1446.09 46.48 6 -1 -7 3 1479.40 51.54 9 1 -7 -3 1476.79 50.96 4 -1 -7 3 1450.71 42.70 1 1 -7 -3 1467.22 44.29 3 1 7 -3 1512.76 44.28 3 1 7 -3 1499.76 47.13 6 1 7 -3 1465.52 43.11 2 1 7 -3 1412.83 51.29 9 1 7 -3 1456.43 43.00 2 -1 7 3 1389.34 43.33 2 -1 7 3 1492.74 51.66 9 -1 7 3 1541.72 51.34 4 1 7 -3 1488.17 47.81 8 1 7 -3 1390.99 51.20 9 1 -7 3 243.349 7.710 1 1 -7 3 241.847 9.272 9 -1 -7 -3 242.793 9.210 9 -1 -7 -3 247.080 8.083 3 -1 -7 -3 241.142 7.648 5 -1 7 -3 232.859 8.980 9 -1 7 -3 247.803 7.632 2 -1 7 -3 226.741 7.573 2 1 7 3 250.845 9.499 9 1 7 3 247.482 9.381 4 -1 7 -3 229.748 8.941 9 -1 7 -3 254.909 8.772 6 -1 7 -3 241.650 8.348 8 -1 7 -3 244.121 7.771 3 1 7 3 231.613 7.948 2 -3 -7 -3 206.853 7.261 3 3 -7 3 191.687 6.705 2 3 -7 3 210.815 6.756 1 -3 -7 -3 185.812 7.949 9 3 -7 3 202.523 8.025 9 3 7 3 200.202 8.298 9 -3 7 -3 199.621 6.615 3 -3 7 -3 197.613 7.591 6 3 7 3 207.523 8.181 4 3 7 3 199.268 6.944 2 -3 7 -3 201.536 6.596 2 5 -7 3 15.8648 1.8014 2 5 -7 3 14.7613 1.8745 1 -5 7 -3 14.5964 1.3682 3 -5 7 -3 16.4298 1.5461 2 5 7 3 15.9215 1.9322 2 5 7 3 19.5166 2.2917 9 5 7 3 12.7746 1.9914 4 -5 7 -3 14.7185 2.1641 6 7 -7 3 20.5441 2.4796 2 7 -7 3 21.3537 2.5874 1 -7 7 -3 22.5535 2.0038 3 -7 7 -3 20.5925 2.2834 2 -7 7 -3 17.5832 2.6757 6 7 7 3 22.5882 2.6593 4 7 7 3 19.4734 2.4483 2 9 -7 3 84.7773 5.0833 1 -9 7 -3 80.6848 3.9011 3 -9 7 -3 89.9897 4.8159 2 9 7 3 81.2210 4.8221 2 -9 7 -3 83.5438 4.8229 6 -11 7 -3 100.962 4.878 3 -11 7 -3 113.314 5.599 2 -11 7 -3 116.166 6.904 6 11 7 3 103.543 6.175 2 13 7 3 237.761 10.474 2 -13 7 -3 250.095 10.136 2 -13 7 -3 243.249 11.398 6 -15 -7 -3 46.1378 5.8363 3 -15 7 -3 48.1692 5.7404 6 -15 7 -3 44.3203 5.1573 2 -17 -7 -3 102.161 8.473 3 20 8 -3 3.92127 4.69549 8 -20 8 3 0.71449 4.89813 2 20 8 -3 3.74730 4.41872 2 18 -8 -3 79.2010 6.1552 5 18 8 -3 78.9093 7.0727 8 18 8 -3 73.1813 6.6010 2 -18 8 3 67.3848 6.2460 2 -16 -8 3 20.4290 3.7319 1 16 -8 -3 15.2702 3.2811 7 16 -8 -3 23.2175 4.3434 5 -16 8 3 17.0509 3.5491 1 -16 8 3 20.9451 4.0429 2 16 8 -3 26.3648 3.9189 7 16 8 -3 22.3569 4.8089 8 16 8 -3 14.9340 4.4985 2 -14 -8 3 228.524 9.012 1 14 -8 -3 237.466 9.071 7 14 8 -3 226.399 9.006 7 14 8 -3 236.932 9.085 2 -14 8 3 225.892 9.280 1 -14 8 3 209.362 9.163 2 14 8 -3 231.013 10.773 8 -14 8 3 213.219 9.986 4 12 -8 -3 12.4526 2.1719 7 -12 -8 3 14.0396 2.5276 1 12 8 -3 11.8289 2.4178 2 12 8 -3 12.0398 2.0276 4 -12 8 3 12.7383 2.6011 2 12 8 -3 11.4062 2.1371 7 12 8 -3 12.3954 3.1639 8 -12 8 3 11.0387 2.3911 1 -12 8 3 9.01951 2.30526 4 -10 -8 3 330.387 11.002 1 10 -8 -3 338.970 11.318 7 -10 8 3 330.962 12.910 4 10 8 -3 334.836 11.384 7 -10 8 3 332.106 10.896 1 10 8 -3 314.494 12.735 8 10 8 -3 329.436 11.127 2 10 8 -3 331.740 12.353 4 -10 8 3 329.560 11.300 2 -8 -8 3 -0.1495 1.4845 9 -8 -8 3 1.25063 1.43328 1 8 -8 -3 1.12166 1.02672 7 8 -8 -3 0.04029 1.02386 4 8 8 -3 1.24594 1.80609 8 8 8 -3 0.66784 1.07524 4 8 8 -3 0.72575 0.98352 7 -8 8 3 -0.6787 1.4009 2 8 8 -3 1.22759 1.30745 2 -8 8 3 2.45171 1.44548 4 -8 8 3 1.55515 1.52229 9 8 8 -3 1.35281 0.98037 4 -8 8 3 4.33650 1.47758 1 -8 8 3 1.98821 1.61161 9 6 -8 -3 487.088 15.230 7 -6 -8 3 472.806 17.846 9 6 -8 -3 462.252 17.252 4 -6 -8 3 478.908 14.743 1 6 8 -3 464.011 14.849 2 -6 8 3 483.859 17.555 4 6 8 -3 494.590 16.781 8 6 8 -3 473.383 16.840 4 -6 8 3 472.735 14.987 2 6 8 -3 481.704 16.907 4 6 8 -3 480.128 15.206 7 -6 8 3 479.233 17.788 9 4 -8 -3 265.719 10.478 9 4 -8 -3 280.017 9.301 5 -4 -8 3 279.169 8.909 1 4 -8 -3 278.526 10.343 4 4 -8 -3 288.437 9.008 7 4 -8 -3 275.098 8.690 3 -4 -8 3 279.036 10.732 9 -4 8 3 267.629 9.021 2 4 8 -3 266.330 10.508 9 4 8 -3 273.667 8.890 2 -4 8 3 285.654 10.764 9 4 8 -3 287.596 8.971 7 4 8 -3 275.610 9.978 8 -4 8 3 287.681 10.618 4 2 -8 -3 12.9633 1.1402 3 2 -8 -3 13.6289 1.3783 4 2 -8 -3 11.3318 1.2980 9 2 8 -3 11.4651 1.2942 9 -2 8 3 13.4169 1.5456 4 2 8 -3 16.4321 1.5291 8 -2 8 3 12.9592 1.5160 2 -2 8 3 11.2591 1.5806 9 0 -8 -3 1039.77 31.08 5 0 -8 -3 1036.12 36.84 4 0 -8 -3 1015.62 32.02 3 0 -8 3 1027.10 30.91 1 0 -8 3 1043.99 37.31 9 0 -8 -3 1024.85 37.24 9 0 8 -3 1065.62 34.42 8 0 8 -3 1069.41 31.89 3 0 8 3 1010.71 31.44 2 0 8 -3 1052.76 31.18 2 0 8 3 1083.59 37.50 9 0 8 -3 1055.12 34.14 6 0 8 3 1090.80 37.23 4 2 -8 3 81.3232 3.3891 1 -2 -8 -3 88.7228 3.6398 3 -2 -8 -3 82.4702 3.1270 5 2 -8 3 77.3876 3.9575 9 -2 -8 -3 73.0589 3.8778 9 2 8 3 81.1968 3.7287 2 -2 8 -3 85.0433 3.2218 8 -2 8 -3 78.4837 3.9085 6 -2 8 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77.2827 4.8998 4 -7 9 -3 75.9905 4.3009 2 -7 9 -3 67.1331 4.6180 6 7 9 3 75.5407 4.4037 2 9 -9 3 6.66557 2.85544 1 -9 9 -3 9.54933 2.79993 2 9 9 3 8.74737 3.20277 2 -9 9 -3 8.66365 2.81035 6 11 9 3 27.3287 3.9457 2 -11 9 -3 20.6886 3.1922 2 -11 9 -3 29.5944 3.9938 6 13 9 3 27.3052 4.4946 2 -13 9 -3 30.3187 4.5935 6 -13 9 -3 31.1983 4.3890 2 -15 -9 -3 9.31550 4.86847 3 -15 9 -3 6.51700 4.12472 2 -15 9 -3 4.09684 4.13642 6 -17 -9 -3 11.6738 3.9458 3 20 -10 -3 10.2224 4.7422 5 20 10 -3 7.66801 4.39029 2 20 10 -3 14.8949 4.1838 8 -20 10 3 13.9598 5.2761 2 18 -10 -3 129.942 8.753 5 18 10 -3 131.763 7.765 2 -18 10 3 109.233 8.294 2 18 10 -3 118.883 9.054 8 16 -10 -3 34.1718 3.6815 7 -16 -10 3 37.8445 4.3781 1 16 10 -3 43.5202 5.7961 8 16 10 -3 37.6480 4.6031 2 -16 10 3 44.6581 5.0470 2 -14 -10 3 139.672 6.992 1 14 -10 -3 140.336 6.620 7 14 10 -3 143.334 7.629 2 14 10 -3 138.716 6.607 7 14 10 -3 146.654 8.613 8 -14 10 3 125.029 7.273 2 -14 10 3 144.581 6.945 1 -12 -10 3 18.3130 2.9623 1 12 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354.412 12.599 9 7 3 -4 337.201 11.118 7 -7 3 4 327.081 12.230 4 7 3 -4 333.478 10.474 5 7 3 -4 326.880 11.872 8 5 -3 -4 203.168 6.959 5 5 -3 -4 208.461 6.812 3 5 -3 -4 221.018 7.056 7 -5 -3 4 194.115 6.095 1 -5 -3 4 206.682 7.367 4 -5 -3 4 193.884 7.348 4 5 -3 -4 211.925 7.391 8 -5 -3 4 196.193 7.657 9 5 3 -4 215.788 7.577 8 5 3 -4 211.644 7.014 7 -5 3 4 204.676 7.751 9 5 3 -4 210.632 6.936 3 -5 3 4 209.925 7.562 4 3 -3 -4 52.8470 2.3373 6 -3 -3 4 53.9696 2.1326 9 3 -3 -4 52.2216 2.3634 7 3 -3 -4 48.9261 2.4861 8 3 -3 -4 53.5253 2.3709 5 3 -3 -4 51.2603 2.2997 3 -3 3 4 50.5654 1.7799 1 3 3 -4 50.2084 2.5756 8 3 3 -4 59.6597 2.8860 6 3 3 -4 49.5434 2.3399 3 -3 3 4 54.3746 2.3189 9 3 3 -4 51.6387 2.3208 7 -3 3 4 51.9891 2.1421 4 1 -3 -4 49.1035 2.2970 3 1 -3 -4 44.3783 2.3514 6 1 -3 -4 51.5746 2.3559 5 -1 -3 4 45.4615 2.0103 9 -1 -3 4 47.8076 2.0688 9 -1 3 4 45.7322 2.2329 9 1 3 -4 50.9817 2.1623 3 1 3 -4 51.1433 2.4154 8 -1 3 4 50.7631 2.0868 4 1 3 -4 48.1774 2.7665 6 -1 3 4 44.2229 1.6498 1 1 -3 4 55.2338 2.7026 9 1 -3 4 58.8722 2.1271 1 -1 -3 -4 61.5195 2.8392 3 -1 -3 -4 59.0741 3.0306 6 1 -3 4 57.2122 2.7385 9 -1 3 -4 58.6329 3.2696 6 -1 3 -4 67.5193 2.7719 3 1 3 4 56.5042 2.8624 9 -1 3 -4 65.3515 2.7781 8 -3 -3 -4 308.672 9.548 2 3 -3 4 314.055 9.820 1 3 -3 4 328.910 11.934 9 -3 -3 -4 311.864 10.617 3 3 3 4 321.875 12.043 9 -3 3 -4 305.267 10.356 3 -3 3 -4 314.253 11.354 6 5 -3 4 258.326 10.649 9 5 -3 4 248.018 8.938 1 -5 -3 -4 279.852 9.567 3 5 3 4 275.263 10.838 9 -5 3 -4 266.451 8.341 2 5 3 4 272.569 10.499 4 -5 3 -4 276.249 9.245 3 -5 3 -4 271.621 10.261 6 7 -3 4 169.806 7.795 9 -7 -3 -4 167.283 7.193 3 7 -3 4 171.415 6.720 1 -7 3 -4 170.292 6.707 3 -7 3 -4 170.703 5.941 2 -7 3 -4 167.699 7.722 6 -9 -3 -4 203.708 8.790 3 -9 3 -4 194.063 9.383 6 -9 3 -4 201.328 8.045 3 -9 3 -4 206.664 7.389 2 -11 -3 -4 66.9565 5.0092 3 -11 3 -4 69.7344 5.0519 3 -11 3 -4 62.4785 4.5312 2 -11 3 -4 76.6976 6.7874 6 -13 -3 -4 39.1855 3.8687 2 -13 -3 -4 47.0053 5.4728 3 -13 3 -4 56.4757 4.7575 3 -13 3 -4 43.2940 4.3568 2 -13 3 -4 54.2874 6.1506 6 -15 -3 -4 -1.7161 4.4475 3 -15 -3 -4 7.25976 3.69814 2 -15 3 -4 3.02112 3.60111 2 -15 3 -4 5.06961 3.56727 3 -15 3 -4 8.75100 5.28407 6 -17 -3 -4 6.96419 4.93584 3 20 4 -4 0.13753 3.83728 2 20 4 -4 2.78155 4.00878 8 18 -4 -4 235.950 9.676 5 -18 -4 4 234.243 10.036 1 18 -4 -4 241.360 10.818 7 18 4 -4 244.125 10.688 7 18 4 -4 232.949 11.233 8 -18 4 4 232.589 10.543 1 18 4 -4 244.233 10.377 2 16 -4 -4 45.8697 3.9105 5 16 -4 -4 48.4567 4.5206 7 -16 -4 4 38.9390 3.9711 1 -16 4 4 43.3461 4.0258 1 16 4 -4 40.7468 4.1970 2 16 4 -4 44.7697 4.4270 7 16 4 -4 52.4817 5.1054 8 14 -4 -4 569.797 20.801 4 14 -4 -4 620.940 18.696 5 -14 -4 4 592.353 18.359 1 14 -4 -4 559.303 19.621 8 14 -4 -4 591.552 19.602 7 14 4 -4 562.320 18.261 2 -14 4 4 595.078 18.279 1 14 4 -4 549.861 19.524 7 14 4 -4 516.634 20.197 4 14 4 -4 587.747 20.903 8 12 -4 -4 131.678 5.248 4 12 -4 -4 126.531 5.627 7 -12 -4 4 126.576 5.343 1 -12 -4 4 121.989 6.339 9 12 -4 -4 124.626 5.624 5 12 -4 -4 123.238 5.116 8 12 4 -4 120.728 4.984 2 -12 4 4 116.709 6.146 4 -12 4 4 127.886 5.270 1 12 4 -4 124.793 5.716 7 12 4 -4 131.842 6.294 8 -10 -4 4 66.6265 3.1714 1 10 -4 -4 69.9115 2.7452 4 10 -4 -4 73.3469 3.8570 5 -10 -4 4 73.4187 4.0934 9 10 -4 -4 63.5637 3.4496 7 10 -4 -4 62.5069 2.6750 4 -10 -4 4 64.8637 3.5562 4 10 -4 -4 70.4234 3.2364 8 10 4 -4 69.4379 3.5807 7 10 4 -4 66.0437 3.9577 8 -10 4 4 68.0354 3.9311 9 -10 4 4 71.0193 3.2826 1 10 4 -4 67.3264 3.1299 2 10 4 -4 66.9150 2.7855 5 -10 4 4 63.6910 3.5684 4 -10 4 4 73.3682 4.1133 9 8 -4 -4 1429.70 46.78 8 -8 -4 4 1398.16 41.77 1 -8 -4 4 1428.63 50.57 9 8 -4 -4 1434.58 44.41 7 8 -4 -4 1396.93 42.56 5 -8 -4 4 1393.92 49.97 4 8 4 -4 1400.21 47.20 8 -8 4 4 1421.88 50.55 9 8 4 -4 1460.62 44.46 7 8 4 -4 1421.12 41.91 2 -8 4 4 1409.69 50.03 4 8 4 -4 1446.21 41.98 5 -8 4 4 1495.23 50.57 9 6 -4 -4 54.0414 2.5945 7 6 -4 -4 54.4022 2.6268 8 6 -4 -4 58.2361 3.0051 5 -6 -4 4 58.4879 2.1809 1 -6 -4 4 60.5202 2.9845 9 6 -4 -4 54.4886 2.3960 3 -6 -4 4 52.0828 2.5274 4 6 4 -4 53.6616 2.9525 8 -6 4 4 68.1336 2.9706 9 -6 4 4 53.4877 2.7155 4 6 4 -4 55.9554 2.5871 7 -4 -4 4 3535.90 124.65 4 4 -4 -4 3571.38 113.97 6 -4 -4 4 3311.90 124.54 4 4 -4 -4 3623.55 107.94 3 4 -4 -4 3534.28 117.85 8 -4 -4 4 3614.01 127.01 9 4 -4 -4 3568.31 104.77 5 4 -4 -4 3661.40 112.73 7 -4 -4 4 3525.76 104.01 1 4 4 -4 3625.28 110.25 3 4 4 -4 3635.31 116.08 6 4 4 -4 3680.41 111.86 7 -4 4 4 3681.96 127.45 9 -4 4 4 3637.50 125.77 4 4 4 -4 3603.21 119.33 8 2 -4 -4 124.663 4.219 3 -2 -4 4 108.016 4.090 4 2 -4 -4 106.987 4.291 6 2 -4 -4 126.991 4.263 7 2 -4 -4 116.155 4.270 5 -2 -4 4 108.859 4.423 9 2 4 -4 125.297 4.238 3 -2 4 4 114.702 4.502 4 2 4 -4 106.765 4.729 6 2 4 -4 123.141 4.211 7 -2 4 4 104.092 4.576 9 2 4 -4 126.258 4.594 8 0 -4 4 3350.12 100.08 1 0 -4 4 3597.92 122.05 9 0 -4 -4 3364.48 104.51 3 0 -4 4 3427.08 121.73 9 0 -4 -4 3503.24 100.28 5 0 -4 -4 3463.27 110.80 6 0 -4 4 3213.72 99.79 1 0 4 -4 3502.41 110.96 6 0 4 4 3427.08 120.58 4 0 4 -4 3358.74 105.65 3 0 4 4 3547.71 120.53 9 0 4 -4 3487.60 112.85 8 -2 -4 -4 10.1614 1.4721 3 2 -4 4 9.06012 1.03609 1 2 -4 4 8.24103 1.13367 9 2 -4 4 6.87336 1.20485 9 -2 -4 -4 7.54820 0.69414 2 2 4 4 7.81231 1.13373 2 -2 4 -4 13.2228 1.3784 3 2 4 4 6.12837 1.45901 9 -2 4 -4 7.20036 1.38967 6 2 4 4 10.7987 1.3913 4 4 -4 4 2748.00 96.07 9 -4 -4 -4 2735.03 83.16 3 4 -4 4 2771.52 79.71 1 4 4 4 2757.65 95.44 4 -4 4 -4 2692.46 82.73 3 4 4 4 2738.49 96.22 9 -4 4 -4 2708.45 87.76 6 -4 4 -4 2707.00 80.00 2 6 -4 4 5.42610 1.70280 1 -6 -4 -4 4.67268 2.01314 3 6 -4 4 3.00848 1.75466 9 -6 4 -4 4.74375 1.30606 2 6 4 4 5.97165 1.91409 9 -6 4 -4 3.58257 1.50559 3 -6 4 -4 4.63599 2.26408 6 -8 -4 -4 470.681 16.747 3 -8 4 -4 488.221 15.129 2 -8 4 -4 494.365 17.716 6 -8 4 -4 475.242 15.950 3 -10 -4 -4 92.9819 6.3364 3 -10 4 -4 97.7745 5.3532 3 -10 4 -4 114.191 7.315 6 -10 4 -4 104.692 5.087 2 -12 -4 -4 109.218 7.422 3 -12 4 -4 97.8617 5.5821 2 -12 4 -4 105.639 6.911 6 -12 4 -4 105.922 6.513 3 -14 -4 -4 136.419 8.914 3 -14 -4 -4 131.532 7.121 2 -14 4 -4 131.767 7.220 3 -14 4 -4 138.755 9.489 6 -14 4 -4 124.542 6.791 2 -16 -4 -4 -2.5808 4.7464 3 -16 -4 -4 5.78054 4.07161 2 21 5 -4 1.68005 4.37529 8 21 5 -4 4.66020 4.70460 2 -19 -5 4 233.495 10.355 1 19 5 -4 238.790 10.645 2 19 5 -4 243.237 11.712 8 17 -5 -4 4.26747 3.33201 7 17 -5 -4 2.38683 3.69562 5 -17 -5 4 3.76530 3.27720 1 17 5 -4 -0.4257 3.6467 2 17 5 -4 6.06142 3.19097 7 -17 5 4 6.12302 3.34891 1 17 5 -4 4.86337 3.93723 8 15 -5 -4 773.200 25.046 7 -15 -5 4 758.481 23.544 1 15 -5 -4 750.446 23.812 5 15 5 -4 748.721 26.771 8 15 5 -4 693.708 23.420 2 -15 5 4 747.564 23.390 1 15 5 -4 745.676 25.009 7 -13 -5 4 23.4854 2.7510 1 13 -5 -4 24.3888 2.8525 7 13 -5 -4 18.2474 2.9212 5 13 -5 -4 19.4355 2.0276 4 13 -5 -4 19.2455 2.0788 8 -13 5 4 18.2481 2.5729 1 13 5 -4 20.6852 2.7934 7 13 5 -4 17.9628 2.5740 2 13 5 -4 19.3609 3.3217 8 11 -5 -4 1049.66 34.63 8 -11 -5 4 1025.60 37.99 9 11 -5 -4 1001.61 36.72 4 -11 -5 4 1084.14 31.43 1 11 -5 -4 1058.28 33.27 7 11 -5 -4 1057.76 32.12 5 11 -5 -4 1058.80 36.79 4 -11 5 4 1048.42 37.93 9 11 5 -4 1058.91 33.38 7 11 5 -4 1056.07 35.63 8 -11 5 4 1061.18 31.35 1 -11 5 4 1030.94 37.94 9 -11 5 4 1008.81 37.38 4 11 5 -4 1062.33 31.56 2 -9 -5 4 1.74483 1.47848 1 9 -5 -4 4.33978 1.34479 7 -9 -5 4 5.73986 1.85083 9 -9 -5 4 2.15323 1.13241 4 9 -5 -4 2.23687 1.62476 5 9 -5 -4 3.45443 1.04382 8 9 5 -4 3.19931 1.73640 8 -9 5 4 1.95043 1.42751 9 9 5 -4 3.56502 1.35992 7 -9 5 4 3.07754 1.29187 1 -9 5 4 2.23179 1.21673 4 -9 5 4 2.90909 1.57646 9 9 5 -4 2.53469 1.01604 2 7 -5 -4 2037.93 61.41 7 7 -5 -4 1990.11 64.78 8 -7 -5 4 2070.72 69.99 9 -7 -5 4 1925.54 69.23 4 7 -5 -4 1983.34 58.79 5 -7 -5 4 1993.94 57.87 1 -7 5 4 1932.27 58.73 2 -7 5 4 1968.43 69.31 4 7 5 -4 1923.55 58.05 2 -7 5 4 2085.09 69.95 9 7 5 -4 1987.85 61.39 7 7 5 -4 1924.95 65.20 8 5 -5 -4 337.988 11.369 8 5 -5 -4 321.279 10.689 5 -5 -5 4 326.628 9.965 1 5 -5 -4 343.360 10.811 7 -5 -5 4 345.450 12.279 9 -5 -5 4 319.333 11.896 4 5 -5 -4 338.822 10.493 3 -5 5 4 341.259 12.299 9 -5 5 4 303.788 10.243 2 5 5 -4 326.435 11.623 8 5 5 -4 320.690 10.742 7 -5 5 4 338.094 12.066 4 3 -5 -4 485.877 15.736 3 3 -5 -4 494.836 16.427 6 3 -5 -4 489.383 15.571 5 -3 -5 4 487.562 14.859 1 3 -5 -4 509.715 16.086 7 -3 -5 4 527.419 18.149 9 3 5 -4 500.753 17.134 8 3 5 -4 523.224 17.103 6 3 5 -4 506.816 15.836 3 -3 5 4 506.901 18.064 4 3 5 -4 512.383 16.064 7 -3 5 4 523.737 18.259 9 1 -5 -4 110.028 4.209 3 -1 -5 4 110.284 3.664 1 -1 -5 4 114.090 4.584 9 1 -5 -4 115.364 4.375 6 1 -5 -4 116.367 4.249 5 1 5 -4 110.377 4.168 3 -1 5 4 115.084 4.715 4 1 5 -4 116.614 4.502 8 -1 5 4 119.117 4.772 9 1 5 -4 118.070 4.900 6 1 -5 4 565.720 19.675 9 1 -5 4 562.390 19.751 9 1 -5 4 560.371 16.253 1 -1 -5 -4 550.471 16.588 5 -1 -5 -4 539.241 16.252 2 -1 -5 -4 534.001 17.288 3 -1 5 -4 541.247 17.109 3 -1 5 -4 551.907 18.450 6 1 5 4 503.396 16.636 2 1 5 4 552.740 19.696 4 1 5 4 551.026 19.907 9 -1 5 -4 539.052 18.314 8 -3 -5 -4 383.634 13.019 3 3 -5 4 381.307 12.099 1 3 -5 4 407.103 14.731 9 -3 5 -4 384.125 12.614 3 -3 5 -4 406.016 13.918 6 3 5 4 385.888 14.857 9 3 5 4 396.798 14.678 4 -5 -5 -4 67.9667 4.0002 3 5 -5 4 61.5884 3.9627 9 5 -5 4 61.8103 3.4189 1 -5 5 -4 69.5557 2.7137 2 5 5 4 65.9485 4.1878 9 -5 5 -4 71.1250 4.3164 6 5 5 4 67.5360 3.9095 4 -5 5 -4 70.2889 3.3504 3 -7 -5 -4 595.339 20.396 3 7 -5 4 627.197 19.355 1 -7 5 -4 596.971 19.548 3 -7 5 -4 615.990 21.435 6 -7 5 -4 616.253 18.697 2 -9 -5 -4 8.28339 3.02699 3 -9 5 -4 11.9024 2.2045 2 -9 5 -4 13.3659 3.4500 6 -9 5 -4 10.0520 2.2015 3 -11 -5 -4 678.770 23.298 3 -11 5 -4 688.397 24.480 6 -11 5 -4 645.454 21.907 3 -13 -5 -4 1.79106 4.12987 3 -13 5 -4 0.25556 2.73642 3 -13 5 -4 3.00028 4.47315 6 -13 5 -4 -1.7137 3.3509 2 -15 -5 -4 275.894 10.843 2 -15 -5 -4 304.814 13.124 3 -15 5 -4 256.064 10.143 2 -15 5 -4 285.879 13.736 6 -17 -5 -4 3.98889 4.89761 3 20 6 -4 1.51051 4.49318 2 20 6 -4 -4.5553 5.1912 8 -18 -6 4 7.59711 3.79080 1 18 -6 -4 5.88114 3.47639 5 18 -6 -4 4.52889 3.68109 7 18 6 -4 5.30215 3.35070 7 -18 6 4 -1.9704 4.3297 1 18 6 -4 12.9268 4.5421 8 18 6 -4 4.35360 4.19548 2 16 -6 -4 76.9566 5.4875 7 16 -6 -4 68.2215 5.5734 5 -16 -6 4 70.1265 5.5427 1 -16 6 4 69.0979 5.3986 1 16 6 -4 69.5668 5.3146 7 16 6 -4 66.7966 6.4676 8 16 6 -4 58.4345 4.8955 2 14 -6 -4 7.12883 3.02536 5 14 -6 -4 8.10777 2.56953 7 -14 -6 4 7.88453 3.11325 1 14 -6 -4 7.26817 1.94911 4 14 6 -4 6.62536 2.76773 2 14 6 -4 6.89902 2.50031 7 -14 6 4 7.80822 2.74718 1 14 6 -4 6.26789 3.20321 8 -12 -6 4 31.8829 2.8328 1 12 -6 -4 35.9620 2.9325 7 12 -6 -4 35.4628 2.8337 4 12 -6 -4 35.0271 3.0679 5 12 6 -4 33.2808 3.6705 8 12 6 -4 30.3253 2.5194 2 -12 6 4 33.4450 2.8264 1 12 6 -4 33.7614 2.9415 7 10 -6 -4 10.1094 1.3957 4 -10 -6 4 7.96897 1.96101 9 10 -6 -4 12.9075 1.2584 4 -10 -6 4 9.08010 1.73581 1 10 -6 -4 12.3521 2.3230 5 -10 -6 4 8.00661 1.73666 4 10 -6 -4 15.5739 1.8577 7 10 -6 -4 12.8430 1.5140 8 -10 6 4 8.41382 1.66647 2 10 6 -4 12.7974 1.8321 7 10 6 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1.8536 3 2 -6 -4 35.2965 1.7497 6 -2 -6 4 36.4243 2.0030 9 -2 -6 4 34.1356 1.6280 1 2 -6 -4 37.5651 2.2360 5 -2 6 4 31.5578 1.7577 2 2 6 -4 36.2905 1.9520 3 2 6 -4 37.3354 2.6634 6 2 6 -4 34.5170 2.1375 8 -2 6 4 35.0920 2.2345 9 -2 6 4 34.0185 2.2467 4 0 -6 4 9.31040 1.20361 9 0 -6 -4 10.8125 1.3457 6 0 -6 -4 12.0857 1.4694 3 0 -6 4 9.97337 1.03976 1 0 -6 -4 9.03819 0.82718 2 0 -6 -4 12.0893 1.4560 5 0 6 -4 12.5818 1.2838 8 0 6 4 9.18984 1.12424 2 0 6 4 10.7139 1.4249 9 0 6 -4 9.61595 1.73311 6 0 6 4 10.1248 1.3001 4 0 6 -4 11.4702 1.2031 3 -2 -6 -4 26.0028 2.2567 3 2 -6 4 26.4004 1.9409 1 2 -6 4 25.2966 2.0262 9 2 6 4 23.6450 2.0404 2 -2 6 -4 25.8650 1.8507 3 2 6 4 29.7035 2.4233 9 -2 6 -4 30.7099 2.7146 6 -2 6 -4 25.6911 1.7449 8 2 6 4 26.6587 2.2680 4 -4 -6 -4 160.921 6.632 3 4 -6 4 171.985 7.227 9 4 -6 4 168.113 5.992 1 4 6 4 161.862 7.330 9 -4 6 -4 159.675 5.968 3 -4 6 -4 173.815 7.128 6 -4 6 -4 170.679 5.435 2 4 6 4 164.144 7.165 4 6 -6 4 76.4788 4.7916 9 6 -6 4 85.0542 4.3791 1 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523.666 16.530 2 -5 9 4 558.995 20.360 9 5 9 -4 537.921 18.935 8 5 9 -4 549.667 17.382 7 -5 9 4 560.433 20.126 4 -5 9 4 550.390 17.129 2 3 -9 -4 273.212 8.757 3 3 -9 -4 276.122 9.155 5 -3 -9 4 268.053 8.704 1 -3 -9 4 280.372 10.561 9 3 9 -4 249.173 8.252 2 -3 9 4 274.700 10.675 9 -3 9 4 254.126 8.916 2 3 9 -4 271.298 9.777 8 3 9 -4 267.911 8.239 2 -3 9 4 281.828 10.629 4 3 9 -4 282.301 10.083 6 -1 -9 4 493.586 17.714 9 1 -9 -4 479.076 14.884 5 -1 -9 4 501.479 14.682 1 1 -9 -4 470.088 15.106 3 -1 9 4 462.997 15.033 2 1 9 -4 487.685 16.281 8 -1 9 4 490.090 17.915 9 1 9 -4 489.597 16.530 6 -1 9 4 476.313 17.711 4 1 9 -4 478.756 15.032 3 1 9 -4 428.146 14.268 2 1 -9 4 265.473 8.389 1 1 -9 4 254.329 10.038 9 -1 -9 -4 253.505 8.761 3 -1 -9 -4 250.002 8.339 5 -1 9 -4 250.077 8.356 3 -1 9 -4 238.193 8.898 8 1 9 4 248.546 8.656 2 1 9 4 250.988 10.177 4 1 9 4 262.594 10.370 9 -1 9 -4 250.066 7.948 2 -1 9 -4 274.019 9.709 6 3 -9 4 88.0715 4.2049 1 -3 -9 -4 82.6096 4.2305 3 3 -9 4 77.1594 4.2679 9 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3.8325 2 17 -5 -5 45.3312 4.4153 5 17 -5 -5 40.3296 4.4999 7 -17 -5 5 43.9515 4.5278 1 17 5 -5 42.6600 5.2343 8 17 5 -5 40.5419 4.4169 7 -17 5 5 46.7604 4.4588 1 17 5 -5 35.6054 3.4546 2 15 -5 -5 4.10160 2.79003 7 -15 -5 5 1.69792 2.76332 1 15 -5 -5 4.68039 2.96109 5 15 5 -5 1.13191 3.33894 8 15 5 -5 1.16061 1.99911 2 -15 5 5 8.18352 2.87723 1 15 5 -5 4.71649 2.80077 7 13 -5 -5 5.58987 2.53884 5 13 -5 -5 3.99056 1.64715 8 13 -5 -5 5.47340 2.27684 7 -13 -5 5 8.75448 2.29313 1 13 5 -5 3.99653 1.46544 2 13 5 -5 5.03064 2.24226 7 -13 5 5 4.39280 2.17236 1 13 5 -5 8.23923 2.91136 8 -11 -5 5 28.6113 2.3685 1 11 -5 -5 34.0401 2.7443 7 11 -5 -5 32.4257 2.8099 8 -11 -5 5 26.3517 2.7216 9 11 -5 -5 29.6031 3.0196 5 -11 5 5 25.8414 2.8064 9 11 5 -5 35.4579 2.8269 7 -11 5 5 28.8041 2.4478 1 -11 5 5 27.7137 2.7518 9 11 5 -5 32.9547 3.3247 8 9 -5 -5 20.4656 1.9837 7 -9 -5 5 11.5705 2.0394 9 9 -5 -5 16.4546 2.3626 5 -9 -5 5 10.8730 1.4053 1 9 -5 -5 16.9445 1.7399 8 9 5 -5 15.2453 2.2612 8 9 5 -5 18.4528 1.9191 7 -9 5 5 10.2223 1.7844 9 -9 5 5 12.1110 1.9056 9 7 -5 -5 33.2313 2.3110 8 -7 -5 5 31.0758 1.7931 1 -7 -5 5 30.8415 2.3174 9 7 -5 -5 31.8113 2.0180 3 7 -5 -5 32.9041 2.8395 5 7 -5 -5 34.4254 2.2867 7 -7 -5 5 32.4568 2.0119 4 7 5 -5 35.8919 2.7265 8 7 5 -5 35.3881 2.2617 7 -7 5 5 33.1086 2.1228 4 -7 5 5 31.5588 2.6964 9 5 -5 -5 9.46404 1.68548 5 -5 -5 5 7.09012 0.84589 4 5 -5 -5 7.60538 1.32372 7 -5 -5 5 8.94877 0.78391 1 -5 -5 5 9.52227 1.11225 9 5 -5 -5 8.51925 1.45478 8 5 -5 -5 7.22131 1.17546 3 -5 5 5 7.92737 1.10645 4 5 5 -5 8.62556 1.30674 7 -5 5 5 10.5590 1.2863 9 5 5 -5 9.10154 1.84225 6 5 5 -5 7.80168 1.40462 3 5 5 -5 8.46010 1.61636 8 3 -5 -5 93.9074 3.8310 7 -3 -5 5 90.0896 2.9498 1 3 -5 -5 95.5084 3.8609 6 3 -5 -5 98.9907 4.1003 5 -3 -5 5 98.3271 3.9724 9 -3 -5 5 91.6439 3.0014 1 3 -5 -5 97.0536 3.8292 3 3 5 -5 95.7928 4.2175 8 3 5 -5 95.6110 3.8834 3 3 5 -5 93.0577 4.3148 6 -3 5 5 99.7183 4.0583 4 3 5 -5 92.8678 3.8032 7 -3 5 5 96.9475 4.1076 9 1 -5 -5 8.52223 1.40508 3 -1 -5 5 11.1343 1.1557 9 1 -5 -5 12.8972 1.4719 6 -1 -5 5 10.7202 0.8466 1 1 -5 -5 12.5234 1.5920 5 1 5 -5 8.78963 1.35422 3 1 5 -5 9.97092 1.98372 6 -1 5 5 12.1875 1.3737 9 -1 5 5 8.85348 1.10309 4 1 5 -5 9.37387 1.47810 8 1 -5 5 19.2262 1.4907 1 1 -5 5 19.1660 1.8435 9 1 -5 5 20.2614 1.7232 9 -1 -5 -5 20.5045 2.0032 3 -1 -5 -5 23.5591 2.1619 6 -1 5 -5 18.7582 1.9304 8 -1 5 -5 17.5012 1.7719 3 -1 5 -5 16.3804 2.4028 6 1 5 5 19.6074 2.0563 9 1 5 5 16.6246 1.7514 4 -3 -5 -5 10.3935 2.2398 6 3 -5 5 7.53958 1.38285 1 3 -5 5 7.78786 1.88405 9 -3 -5 -5 10.4721 2.0125 3 3 5 5 9.07772 1.83147 9 -3 5 -5 9.21821 2.35241 6 -3 5 -5 9.22985 1.70612 3 5 -5 5 16.8957 2.2051 1 5 -5 5 15.7400 2.2906 9 -5 -5 -5 17.7149 2.7305 3 -5 5 -5 17.5490 2.2185 3 5 5 5 15.5052 2.4497 9 -5 5 -5 19.9717 2.6113 6 -7 -5 -5 6.62862 2.14977 3 7 -5 5 3.87979 2.32031 1 -7 5 -5 4.03847 3.03543 6 -7 5 -5 6.30038 2.13453 3 -9 -5 -5 25.9217 4.0604 3 -9 5 -5 37.5826 4.8291 6 -9 5 -5 29.0873 3.2343 3 -11 -5 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1.7225 8 4 6 -5 12.0754 1.5345 3 -2 -6 5 462.045 13.985 1 2 -6 -5 466.166 15.594 6 2 -6 -5 460.799 14.984 3 2 -6 -5 472.071 14.741 5 -2 -6 5 484.661 17.027 9 2 6 -5 474.178 16.172 8 -2 6 5 480.846 17.235 9 -2 6 5 463.067 17.067 4 2 6 -5 465.602 14.967 3 2 6 -5 467.510 16.289 6 0 -6 -5 45.4984 2.6513 5 0 -6 -5 44.2535 2.6428 6 0 -6 5 43.4596 2.5908 9 0 -6 -5 40.7601 2.6831 3 0 -6 5 42.5832 2.0553 1 0 6 -5 42.7338 2.5175 3 0 6 5 44.3469 2.8034 9 0 6 5 42.2782 2.5895 4 0 6 -5 42.0605 2.5757 8 0 6 -5 43.6821 3.4339 6 2 -6 5 299.781 9.479 1 2 -6 5 306.835 11.431 9 -2 -6 -5 293.649 10.355 3 -2 -6 -5 290.805 10.879 6 2 -6 5 302.065 11.578 9 -2 6 -5 295.714 9.980 3 2 6 5 292.437 11.707 9 -2 6 -5 291.980 11.187 6 4 -6 5 31.0325 2.6908 1 -4 -6 -5 36.4051 3.2250 3 4 -6 5 32.0804 3.1075 9 4 6 5 31.8592 3.2122 9 -4 6 -5 34.6969 3.4450 6 -4 6 -5 32.1958 2.7179 3 -6 -6 -5 230.889 9.195 3 6 -6 5 207.051 8.178 1 -6 6 -5 218.780 8.084 3 -6 6 -5 217.220 9.638 6 -8 -6 -5 46.0278 4.5943 3 8 -6 5 46.2274 4.0910 1 -8 6 -5 48.9646 3.7272 3 -8 6 -5 46.5169 4.9205 6 -10 -6 -5 12.8161 4.1130 3 -10 6 -5 14.8696 3.4322 6 -10 6 -5 20.3278 3.3593 3 -12 -6 -5 102.365 5.056 2 -12 -6 -5 114.073 8.606 3 -12 6 -5 115.712 7.473 6 -14 -6 -5 7.75345 5.01568 3 -14 6 -5 3.67365 5.13140 6 21 7 -5 116.582 8.903 8 19 -7 -5 41.6806 5.0212 5 -19 -7 5 49.4063 5.3175 1 19 7 -5 39.3426 6.1412 8 19 7 -5 37.3993 4.0456 2 -19 7 5 44.5993 5.1237 1 17 -7 -5 133.370 7.736 5 -17 -7 5 137.818 7.509 1 17 -7 -5 130.572 7.219 7 17 7 -5 131.699 8.782 8 -17 7 5 136.256 7.297 1 17 7 -5 130.277 6.996 7 17 7 -5 102.374 5.766 2 15 -7 -5 77.1734 6.1380 5 -15 -7 5 79.6875 5.5263 1 15 -7 -5 73.6834 5.1555 7 -15 7 5 88.5284 5.5313 1 15 7 -5 77.6358 6.7178 8 15 7 -5 62.9150 4.2716 2 15 7 -5 74.0614 5.1158 7 13 -7 -5 313.955 11.445 7 13 -7 -5 330.075 11.861 5 -13 -7 5 323.085 10.946 1 13 7 -5 320.146 12.880 8 -13 7 5 316.540 11.129 1 13 7 -5 302.604 11.480 7 13 7 -5 278.362 9.951 2 11 -7 -5 40.2414 2.5838 8 11 -7 -5 39.2997 3.6973 5 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2.65638 3.53743 3 1 11 -9 6.73019 3.15661 3 1 11 -9 2.10753 4.75639 6 1 -11 9 366.332 13.446 1 -1 -11 -9 377.303 14.461 3 -1 11 -9 345.691 15.832 6 3 -11 9 58.4610 5.3173 1 -3 -11 -9 67.3603 6.2729 3 -3 11 -9 54.2412 6.8167 6 5 -11 9 299.766 13.159 1 -18 -12 9 -3.0842 5.7317 1 -18 12 9 -10.505 4.810 1 -16 -12 9 18.3594 5.2975 1 16 -12 -9 7.45356 4.40408 5 16 12 -9 7.19821 5.84544 8 -16 12 9 3.47869 4.58543 1 14 -12 -9 1.46221 5.59166 5 -14 -12 9 8.25696 3.78143 1 -14 12 9 2.33194 4.19667 1 14 12 -9 6.31292 5.40330 8 12 -12 -9 68.1222 7.1413 5 -12 -12 9 70.5544 5.6172 1 -12 12 9 77.8348 6.1628 1 12 12 -9 78.7334 7.1523 8 -10 -12 9 104.815 6.549 1 10 -12 -9 114.350 8.493 5 10 12 -9 112.040 8.003 8 -8 -12 9 126.134 6.189 1 8 -12 -9 147.602 8.563 5 8 12 -9 131.868 8.138 8 6 -12 -9 128.914 7.766 5 -6 -12 9 124.119 6.270 1 6 12 -9 117.596 7.422 8 -4 -12 9 145.911 6.964 1 4 -12 -9 153.066 7.880 5 -2 -12 9 105.587 6.212 1 2 12 -9 98.8488 8.5425 6 0 -12 9 27.9527 4.3820 1 0 -12 -9 24.9425 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108.309 7.128 5 -3 -15 9 -2.5796 3.3478 1 -1 -15 9 239.570 10.899 1 1 -15 9 18.0633 4.5045 1 -14 16 9 -3.1391 4.9017 1 -12 -16 9 108.193 7.352 1 12 -16 -9 120.929 9.309 5 -12 16 9 105.807 8.880 1 -10 -16 9 12.0553 4.0052 1 10 -16 -9 11.5708 5.2368 5 10 16 -9 10.9895 4.5799 8 8 -16 -9 134.057 8.391 5 -8 -16 9 139.314 8.340 1 6 -16 -9 14.4440 4.2211 5 -6 -16 9 17.7566 4.7053 1 -4 -16 9 232.031 10.496 1 -2 -16 9 27.8260 5.3644 1 0 -16 9 60.5961 5.7676 1 11 -17 -9 16.5854 5.4614 5 -11 -17 9 10.0403 5.1608 1 -11 17 9 0.27811 4.73109 1 -9 -17 9 5.36144 4.86205 1 9 -17 -9 5.67954 4.74398 5 -7 -17 9 4.77905 3.95365 1 7 -17 -9 5.34027 3.96854 5 -5 -17 9 11.6579 4.9165 1 -3 -17 9 15.8158 4.4026 1 -1 -17 9 13.0751 4.5913 1 -8 -18 9 68.1675 5.7744 1 8 -18 -9 59.2937 5.7678 5 -6 -18 9 -0.9244 5.0816 1 -4 -18 9 81.8064 7.0017 1 -20 0 10 111.183 7.643 1 -18 0 10 3.60630 4.70179 1 18 0 -10 0.96930 4.51729 8 16 0 -10 324.628 14.387 8 -16 0 10 341.605 12.256 1 14 0 -10 3.73139 4.37733 8 -14 0 10 -2.2545 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