data_4338_ _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'Al0.16 As3 Cu1.30 Fe0.32 Mg1.58 Na1.17 O12 Zn0.32' _chemical_formula_weight 607.78 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'As' 'As' 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Mg' 'Mg' 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Zn' 'Zn' 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Na' 'Na' 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Al' 'Al' 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_H-M_alt 'C 2/c' _space_group_name_Hall '-C 2yc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 11.9073(4) _cell_length_b 12.7384(4) _cell_length_c 6.7197(2) _cell_angle_alpha 90 _cell_angle_beta 113.2724(16) _cell_angle_gamma 90 _cell_volume 936.31(5) _cell_formula_units_Z 4 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 4.312 _exptl_crystal_F_000 1138 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_absorpt_coefficient_mu 15.042 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 24225 _diffrn_reflns_av_unetI/netI 0.0217 _diffrn_reflns_av_R_equivalents 0.0343 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_theta_min 2.454 _diffrn_reflns_theta_max 40.281 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 2958 _reflns_number_gt 2675 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+15.4165P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick 2014' _refine_ls_extinction_coef 0.00049(9) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_number_reflns 2958 _refine_ls_number_parameters 105 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0420 _refine_ls_R_factor_gt 0.0362 _refine_ls_wR_factor_ref 0.0858 _refine_ls_wR_factor_gt 0.0846 _refine_ls_goodness_of_fit_ref 1.345 _refine_ls_restrained_S_all 1.345 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group A2' Na 0.0000 -0.0066(3) 0.2500 0.0260(10) Uani 0.837(13) 2 d S T P . . A1' Cu 0.0000 0.50405(6) 0.2500 0.0090(2) Uani 0.677(4) 2 d S T P . . A1 Na 0.5000 0.0000 0.0000 0.019(2) Uani 0.333(12) 2 d S . P . . M1 Mg 0.0000 0.26355(9) 0.2500 0.0112(3) Uani 1.478(10) 2 d S T P . . M2 Mg 0.28483(6) 0.65622(5) 0.37364(11) 0.00524(16) Uani 1.629(7) 1 d . . P . . T1 As 0.0000 0.71475(3) 0.2500 0.00657(8) Uani 1 2 d S T P . . T2 As 0.23250(3) 0.88704(2) 0.12515(5) 0.00729(7) Uani 1 1 d . . . . . O1 O 0.4618(2) 0.71314(19) 0.5248(4) 0.0112(4) Uani 1 1 d . . . . . O2 O 0.1068(2) 0.62304(18) 0.2604(4) 0.0117(4) Uani 1 1 d . . . . . O3 O 0.3395(2) 0.67008(19) 0.1193(4) 0.0118(4) Uani 1 1 d . . . . . O4 O 0.1160(2) 0.39350(19) 0.3128(4) 0.0134(4) Uani 1 1 d . . . . . O5 O 0.2170(2) 0.81315(19) 0.3209(4) 0.0114(4) Uani 1 1 d . . . . . O6 O 0.3332(3) 0.50375(19) 0.3897(5) 0.0154(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 A2' 0.0144(14) 0.040(2) 0.0195(15) 0.000 0.0019(10) 0.000 A1' 0.0082(3) 0.0044(3) 0.0150(4) 0.000 0.0051(3) 0.000 A1 0.025(4) 0.005(2) 0.016(3) 0.0008(19) -0.006(2) -0.003(2) M1 0.0085(5) 0.0118(5) 0.0171(6) 0.000 0.0091(4) 0.000 M2 0.0045(3) 0.0041(3) 0.0076(3) -0.00032(18) 0.0029(2) -0.00038(17) T1 0.00696(16) 0.00567(15) 0.00586(15) 0.000 0.00125(12) 0.000 T2 0.00870(12) 0.00576(11) 0.00676(11) -0.00002(8) 0.00237(9) -0.00031(9) O1 0.0097(9) 0.0131(9) 0.0086(8) -0.0038(7) 0.0014(7) -0.0006(7) O2 0.0087(8) 0.0078(8) 0.0174(10) -0.0029(7) 0.0039(7) 0.0013(7) O3 0.0156(10) 0.0109(9) 0.0071(8) -0.0014(7) 0.0027(7) -0.0017(7) O4 0.0091(9) 0.0098(9) 0.0216(11) 0.0009(8) 0.0062(8) 0.0012(7) O5 0.0123(9) 0.0126(9) 0.0092(8) 0.0013(7) 0.0042(7) -0.0024(7) O6 0.0186(11) 0.0076(9) 0.0193(11) 0.0015(8) 0.0067(9) -0.0023(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag A2' O6 2.451(3) 7_556 ? A2' O6 2.451(3) 8_455 ? A2' O6 2.513(3) 4_545 ? A2' O6 2.513(3) 3_445 ? A2' O3 2.857(4) 4_545 ? A2' O3 2.857(4) 3_445 ? A2' O1 2.979(4) 8_455 ? A2' O1 2.979(4) 7_556 ? A2' T2 3.2899(18) 6_566 ? A2' T2 3.2899(18) 5_565 ? A2' A2' 3.3640(4) 5_556 ? A2' A2' 3.3640(4) 5 ? A1' A1 1.68071(6) 4 ? A1' A1 1.68071(6) 3_455 ? A1' O4 1.899(2) 2 ? A1' O4 1.899(2) . ? A1' O2 1.962(2) 2 ? A1' O2 1.962(2) . ? A1' T1 2.6840(9) . ? A1' M1 3.0636(14) . ? A1 A1' 1.68071(6) 7 ? A1 A1' 1.68071(6) 3_545 ? A1 O2 2.319(2) 7 ? A1 O2 2.319(2) 3_545 ? A1 O4 2.423(3) 7 ? A1 O4 2.423(3) 3_545 ? A1 O4 2.589(3) 8 ? A1 O4 2.589(3) 4_545 ? A1 O2 2.878(3) 8 ? A1 O2 2.878(3) 4_545 ? A1 T1 3.2102(4) 3_545 ? A1 T1 3.2102(4) 7 ? M1 O4 2.089(3) . ? M1 O4 2.089(3) 2 ? M1 O3 2.125(3) 3_445 ? M1 O3 2.125(3) 4_545 ? M1 O1 2.166(3) 4_545 ? M1 O1 2.166(3) 3_445 ? M1 M2 3.2872(8) 3_445 ? M1 M2 3.2872(8) 4_545 ? M1 A1 3.4488(11) 4 ? M1 A1 3.4488(11) 3_455 ? M2 O2 1.994(2) . ? M2 O6 2.016(3) . ? M2 O3 2.063(3) . ? M2 O1 2.075(2) . ? M2 O5 2.098(3) 7_566 ? M2 O5 2.133(3) . ? M2 M2 3.2239(13) 7_566 ? M2 T1 3.2438(6) . ? M2 T1 3.2468(7) 7_566 ? M2 M1 3.2872(8) 3 ? M2 A2' 3.387(2) 7_556 ? M2 A2' 3.638(2) 3 ? T1 O1 1.672(2) 7_566 ? T1 O1 1.672(2) 8_465 ? T1 O2 1.708(2) . ? T1 O2 1.708(2) 2 ? T1 A1 3.2103(4) 3_455 ? T1 A1 3.2103(4) 4 ? T1 M2 3.2438(6) 2 ? T1 M2 3.2468(7) 7_566 ? T1 M2 3.2468(7) 8_465 ? T1 A2' 3.550(4) 1_565 ? T2 O6 1.665(2) 4 ? T2 O5 1.686(2) . ? T2 O4 1.686(2) 4 ? T2 O3 1.688(2) 7_565 ? T2 A2' 3.2899(18) 5_565 ? T2 A2' 3.4697(16) 1_565 ? T2 A1 3.4958(3) 2_665 ? O1 T1 1.672(2) 7_566 ? O1 M1 2.166(3) 3 ? O1 A2' 2.979(4) 7_556 ? O2 A1 2.319(2) 3_455 ? O2 A1 2.878(3) 4 ? O3 T2 1.688(2) 7_565 ? O3 M1 2.125(3) 3 ? O3 A2' 2.857(4) 3 ? O4 T2 1.686(2) 4_545 ? O4 A1 2.423(3) 3_455 ? O4 A1 2.589(3) 4 ? O5 M2 2.098(3) 7_566 ? O6 T2 1.665(2) 4_545 ? O6 A2' 2.451(3) 7_556 ? O6 A2' 2.513(3) 3 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O6 A2' O6 178.3(2) 7_556 8_455 ? O6 A2' O6 85.22(9) 7_556 4_545 ? O6 A2' O6 94.70(9) 8_455 4_545 ? O6 A2' O6 94.70(9) 7_556 3_445 ? O6 A2' O6 85.22(9) 8_455 3_445 ? O6 A2' O6 174.0(2) 4_545 3_445 ? O6 A2' O3 60.14(9) 7_556 4_545 ? O6 A2' O3 118.33(14) 8_455 4_545 ? O6 A2' O3 62.76(9) 4_545 4_545 ? O6 A2' O3 112.03(13) 3_445 4_545 ? O6 A2' O3 118.33(14) 7_556 3_445 ? O6 A2' O3 60.14(9) 8_455 3_445 ? O6 A2' O3 112.03(13) 4_545 3_445 ? O6 A2' O3 62.76(9) 3_445 3_445 ? O3 A2' O3 76.05(14) 4_545 3_445 ? O6 A2' O1 114.60(14) 7_556 8_455 ? O6 A2' O1 67.03(9) 8_455 8_455 ? O6 A2' O1 80.87(10) 4_545 8_455 ? O6 A2' O1 104.56(12) 3_445 8_455 ? O3 A2' O1 143.25(7) 4_545 8_455 ? O3 A2' O1 126.17(7) 3_445 8_455 ? O6 A2' O1 67.03(9) 7_556 7_556 ? O6 A2' O1 114.60(14) 8_455 7_556 ? O6 A2' O1 104.56(12) 4_545 7_556 ? O6 A2' O1 80.87(10) 3_445 7_556 ? O3 A2' O1 126.17(7) 4_545 7_556 ? O3 A2' O1 143.25(7) 3_445 7_556 ? O1 A2' O1 55.95(11) 8_455 7_556 ? O6 A2' T2 29.33(6) 7_556 6_566 ? O6 A2' T2 149.11(15) 8_455 6_566 ? O6 A2' T2 73.26(7) 4_545 6_566 ? O6 A2' T2 103.86(8) 3_445 6_566 ? O3 A2' T2 30.86(5) 4_545 6_566 ? O3 A2' T2 97.42(11) 3_445 6_566 ? O1 A2' T2 135.35(8) 8_455 6_566 ? O1 A2' T2 96.10(5) 7_556 6_566 ? O6 A2' T2 149.11(15) 7_556 5_565 ? O6 A2' T2 29.33(6) 8_455 5_565 ? O6 A2' T2 103.86(8) 4_545 5_565 ? O6 A2' T2 73.26(7) 3_445 5_565 ? O3 A2' T2 97.42(11) 4_545 5_565 ? O3 A2' T2 30.86(5) 3_445 5_565 ? O1 A2' T2 96.10(5) 8_455 5_565 ? O1 A2' T2 135.35(8) 7_556 5_565 ? T2 A2' T2 124.85(12) 6_566 5_565 ? O6 A2' A2' 48.12(7) 7_556 5_556 ? O6 A2' A2' 131.77(7) 8_455 5_556 ? O6 A2' A2' 133.01(7) 4_545 5_556 ? O6 A2' A2' 46.57(7) 3_445 5_556 ? O3 A2' A2' 85.27(11) 4_545 5_556 ? O3 A2' A2' 90.22(12) 3_445 5_556 ? O1 A2' A2' 119.42(17) 8_455 5_556 ? O1 A2' A2' 66.24(11) 7_556 5_556 ? T2 A2' A2' 62.85(5) 6_566 5_556 ? T2 A2' A2' 114.21(9) 5_565 5_556 ? O6 A2' A2' 131.77(7) 7_556 5 ? O6 A2' A2' 48.12(7) 8_455 5 ? O6 A2' A2' 46.57(7) 4_545 5 ? O6 A2' A2' 133.01(7) 3_445 5 ? O3 A2' A2' 90.22(12) 4_545 5 ? O3 A2' A2' 85.27(11) 3_445 5 ? O1 A2' A2' 66.24(11) 8_455 5 ? O1 A2' A2' 119.42(17) 7_556 5 ? T2 A2' A2' 114.21(9) 6_566 5 ? T2 A2' A2' 62.85(5) 5_565 5 ? A2' A2' A2' 174.3(3) 5_556 5 ? A1 A1' A1 176.48(5) 4 3_455 ? A1 A1' O4 84.96(9) 4 2 ? A1 A1' O4 92.43(9) 3_455 2 ? A1 A1' O4 92.43(9) 4 . ? A1 A1' O4 84.96(9) 3_455 . ? O4 A1' O4 84.29(15) 2 . ? A1 A1' O2 78.66(8) 4 2 ? A1 A1' O2 104.12(8) 3_455 2 ? O4 A1' O2 99.25(10) 2 2 ? O4 A1' O2 170.01(11) . 2 ? A1 A1' O2 104.12(8) 4 . ? A1 A1' O2 78.66(8) 3_455 . ? O4 A1' O2 170.01(11) 2 . ? O4 A1' O2 99.25(10) . . ? O2 A1' O2 78.83(14) 2 . ? A1 A1' T1 91.76(3) 4 . ? A1 A1' T1 91.76(3) 3_455 . ? O4 A1' T1 137.85(8) 2 . ? O4 A1' T1 137.85(8) . . ? O2 A1' T1 39.42(7) 2 . ? O2 A1' T1 39.41(7) . . ? A1 A1' M1 88.24(3) 4 . ? A1 A1' M1 88.24(3) 3_455 . ? O4 A1' M1 42.15(8) 2 . ? O4 A1' M1 42.15(8) . . ? O2 A1' M1 140.58(7) 2 . ? O2 A1' M1 140.59(7) . . ? T1 A1' M1 180.0 . . ? A1' A1 A1' 180.00(5) 7 3_545 ? A1' A1 O2 56.05(7) 7 7 ? A1' A1 O2 123.95(7) 3_545 7 ? A1' A1 O2 123.95(7) 7 3_545 ? A1' A1 O2 56.05(7) 3_545 3_545 ? O2 A1 O2 180.00(8) 7 3_545 ? A1' A1 O4 51.33(6) 7 7 ? A1' A1 O4 128.67(6) 3_545 7 ? O2 A1 O4 76.65(9) 7 7 ? O2 A1 O4 103.35(9) 3_545 7 ? A1' A1 O4 128.67(6) 7 3_545 ? A1' A1 O4 51.33(6) 3_545 3_545 ? O2 A1 O4 103.35(9) 7 3_545 ? O2 A1 O4 76.65(9) 3_545 3_545 ? O4 A1 O4 180.00(10) 7 3_545 ? A1' A1 O4 47.14(6) 7 8 ? A1' A1 O4 132.86(6) 3_545 8 ? O2 A1 O4 103.08(9) 7 8 ? O2 A1 O4 76.92(9) 3_545 8 ? O4 A1 O4 61.03(10) 7 8 ? O4 A1 O4 118.97(10) 3_545 8 ? A1' A1 O4 132.86(6) 7 4_545 ? A1' A1 O4 47.14(6) 3_545 4_545 ? O2 A1 O4 76.92(9) 7 4_545 ? O2 A1 O4 103.08(9) 3_545 4_545 ? O4 A1 O4 118.97(10) 7 4_545 ? O4 A1 O4 61.03(10) 3_545 4_545 ? O4 A1 O4 180.00(12) 8 4_545 ? A1' A1 O2 41.38(5) 7 8 ? A1' A1 O2 138.62(5) 3_545 8 ? O2 A1 O2 56.06(10) 7 8 ? O2 A1 O2 123.94(10) 3_545 8 ? O4 A1 O2 92.64(8) 7 8 ? O4 A1 O2 87.36(8) 3_545 8 ? O4 A1 O2 64.86(7) 8 8 ? O4 A1 O2 115.14(7) 4_545 8 ? A1' A1 O2 138.62(5) 7 4_545 ? A1' A1 O2 41.38(5) 3_545 4_545 ? O2 A1 O2 123.94(10) 7 4_545 ? O2 A1 O2 56.06(10) 3_545 4_545 ? O4 A1 O2 87.36(8) 7 4_545 ? O4 A1 O2 92.64(8) 3_545 4_545 ? O4 A1 O2 115.14(7) 8 4_545 ? O4 A1 O2 64.86(7) 4_545 4_545 ? O2 A1 O2 180.00(9) 8 4_545 ? A1' A1 T1 123.31(3) 7 3_545 ? A1' A1 T1 56.69(3) 3_545 3_545 ? O2 A1 T1 149.03(6) 7 3_545 ? O2 A1 T1 30.97(6) 3_545 3_545 ? O4 A1 T1 81.89(6) 7 3_545 ? O4 A1 T1 98.11(6) 3_545 3_545 ? O4 A1 T1 85.30(6) 8 3_545 ? O4 A1 T1 94.70(6) 4_545 3_545 ? O2 A1 T1 148.01(5) 8 3_545 ? O2 A1 T1 31.99(5) 4_545 3_545 ? A1' A1 T1 56.69(3) 7 7 ? A1' A1 T1 123.31(3) 3_545 7 ? O2 A1 T1 30.97(6) 7 7 ? O2 A1 T1 149.03(6) 3_545 7 ? O4 A1 T1 98.11(6) 7 7 ? O4 A1 T1 81.89(6) 3_545 7 ? O4 A1 T1 94.70(6) 8 7 ? O4 A1 T1 85.30(6) 4_545 7 ? O2 A1 T1 31.99(5) 8 7 ? O2 A1 T1 148.01(5) 4_545 7 ? T1 A1 T1 180.0 3_545 7 ? O4 M1 O4 75.18(14) . 2 ? O4 M1 O3 160.43(10) . 3_445 ? O4 M1 O3 86.90(10) 2 3_445 ? O4 M1 O3 86.89(10) . 4_545 ? O4 M1 O3 160.42(10) 2 4_545 ? O3 M1 O3 111.84(15) 3_445 4_545 ? O4 M1 O1 93.58(10) . 4_545 ? O4 M1 O1 114.04(10) 2 4_545 ? O3 M1 O1 86.50(10) 3_445 4_545 ? O3 M1 O1 74.27(9) 4_545 4_545 ? O4 M1 O1 114.04(10) . 3_445 ? O4 M1 O1 93.58(10) 2 3_445 ? O3 M1 O1 74.27(9) 3_445 3_445 ? O3 M1 O1 86.50(10) 4_545 3_445 ? O1 M1 O1 145.51(14) 4_545 3_445 ? O4 M1 A1' 37.59(7) . . ? O4 M1 A1' 37.59(7) 2 . ? O3 M1 A1' 124.08(7) 3_445 . ? O3 M1 A1' 124.08(7) 4_545 . ? O1 M1 A1' 107.24(7) 4_545 . ? O1 M1 A1' 107.24(7) 3_445 . ? O4 M1 M2 142.89(8) . 3_445 ? O4 M1 M2 82.05(7) 2 3_445 ? O3 M1 M2 37.63(7) 3_445 3_445 ? O3 M1 M2 109.02(8) 4_545 3_445 ? O1 M1 M2 122.63(7) 4_545 3_445 ? O1 M1 M2 38.20(6) 3_445 3_445 ? A1' M1 M2 114.58(2) . 3_445 ? O4 M1 M2 82.05(7) . 4_545 ? O4 M1 M2 142.89(8) 2 4_545 ? O3 M1 M2 109.02(8) 3_445 4_545 ? O3 M1 M2 37.63(7) 4_545 4_545 ? O1 M1 M2 38.20(6) 4_545 4_545 ? O1 M1 M2 122.63(7) 3_445 4_545 ? A1' M1 M2 114.58(2) . 4_545 ? M2 M1 M2 130.85(4) 3_445 4_545 ? O4 M1 A2' 142.41(7) . . ? O4 M1 A2' 142.41(7) 2 . ? O3 M1 A2' 55.92(7) 3_445 . ? O3 M1 A2' 55.92(7) 4_545 . ? O1 M1 A2' 72.76(7) 4_545 . ? O1 M1 A2' 72.76(7) 3_445 . ? A1' M1 A2' 180.0 . . ? M2 M1 A2' 65.42(2) 3_445 . ? M2 M1 A2' 65.42(2) 4_545 . ? O4 M1 A1 48.46(7) . 4 ? O4 M1 A1 43.87(7) 2 4 ? O3 M1 A1 121.18(7) 3_445 4 ? O3 M1 A1 117.46(7) 4_545 4 ? O1 M1 A1 135.60(8) 4_545 4 ? O1 M1 A1 78.65(7) 3_445 4 ? A1' M1 A1 29.150(10) . 4 ? M2 M1 A1 95.171(16) 3_445 4 ? M2 M1 A1 129.52(2) 4_545 4 ? A2' M1 A1 150.850(10) . 4 ? O4 M1 A1 43.87(7) . 3_455 ? O4 M1 A1 48.46(7) 2 3_455 ? O3 M1 A1 117.46(7) 3_445 3_455 ? O3 M1 A1 121.18(7) 4_545 3_455 ? O1 M1 A1 78.65(7) 4_545 3_455 ? O1 M1 A1 135.60(8) 3_445 3_455 ? A1' M1 A1 29.150(10) . 3_455 ? M2 M1 A1 129.52(2) 3_445 3_455 ? M2 M1 A1 95.171(16) 4_545 3_455 ? A2' M1 A1 150.850(10) . 3_455 ? A1 M1 A1 58.30(2) 4 3_455 ? O2 M2 O6 93.11(11) . . ? O2 M2 O3 109.75(11) . . ? O6 M2 O3 87.12(11) . . ? O2 M2 O1 168.98(10) . . ? O6 M2 O1 95.57(11) . . ? O3 M2 O1 77.51(10) . . ? O2 M2 O5 89.55(10) . 7_566 ? O6 M2 O5 103.89(11) . 7_566 ? O3 M2 O5 157.43(10) . 7_566 ? O1 M2 O5 81.79(10) . 7_566 ? O2 M2 O5 81.93(10) . . ? O6 M2 O5 173.28(11) . . ? O3 M2 O5 90.28(10) . . ? O1 M2 O5 89.91(10) . . ? O5 M2 O5 80.71(10) 7_566 . ? O2 M2 M2 84.38(7) . 7_566 ? O6 M2 M2 144.41(9) . 7_566 ? O3 M2 M2 127.16(8) . 7_566 ? O1 M2 M2 84.61(7) . 7_566 ? O5 M2 M2 40.75(7) 7_566 7_566 ? O5 M2 M2 39.95(7) . 7_566 ? O2 M2 T1 26.46(7) . . ? O6 M2 T1 118.86(8) . . ? O3 M2 T1 114.11(7) . . ? O1 M2 T1 143.30(7) . . ? O5 M2 T1 78.10(7) 7_566 . ? O5 M2 T1 56.84(7) . . ? M2 M2 T1 60.26(2) 7_566 . ? O2 M2 T1 142.86(8) . 7_566 ? O6 M2 T1 108.98(8) . 7_566 ? O3 M2 T1 101.06(7) . 7_566 ? O1 M2 T1 26.58(7) . 7_566 ? O5 M2 T1 56.90(7) 7_566 7_566 ? O5 M2 T1 77.60(7) . 7_566 ? M2 M2 T1 60.17(2) 7_566 7_566 ? T1 M2 T1 120.44(2) . 7_566 ? O2 M2 M1 143.99(8) . 3 ? O6 M2 M1 100.34(9) . 3 ? O3 M2 M1 38.95(7) . 3 ? O1 M2 M1 40.21(7) . 3 ? O5 M2 M1 118.71(7) 7_566 3 ? O5 M2 M1 81.37(7) . 3 ? M2 M2 M1 102.32(3) 7_566 3 ? T1 M2 M1 132.85(3) . 3 ? T1 M2 M1 62.117(14) 7_566 3 ? O2 M2 A2' 122.82(9) . 7_556 ? O6 M2 A2' 45.76(10) . 7_556 ? O3 M2 A2' 105.87(7) . 7_556 ? O1 M2 A2' 60.59(9) . 7_556 ? O5 M2 A2' 70.82(8) 7_566 7_556 ? O5 M2 A2' 140.95(9) . 7_556 ? M2 M2 A2' 107.45(5) 7_566 7_556 ? T1 M2 A2' 136.59(3) . 7_556 ? T1 M2 A2' 64.66(6) 7_566 7_556 ? M1 M2 A2' 89.29(3) 3 7_556 ? O2 M2 A2' 122.03(8) . 3 ? O6 M2 A2' 41.51(10) . 3 ? O3 M2 A2' 51.56(8) . 3 ? O1 M2 A2' 68.93(8) . 3 ? O5 M2 A2' 127.59(7) 7_566 3 ? O5 M2 A2' 138.68(8) . 3 ? M2 M2 A2' 153.34(4) 7_566 3 ? T1 M2 A2' 146.29(3) . 3 ? T1 M2 A2' 93.23(3) 7_566 3 ? M1 M2 A2' 59.33(5) 3 3 ? A2' M2 A2' 57.083(10) 7_556 3 ? O1 T1 O1 113.37(18) 7_566 8_465 ? O1 T1 O2 114.00(12) 7_566 . ? O1 T1 O2 110.17(13) 8_465 . ? O1 T1 O2 110.17(13) 7_566 2 ? O1 T1 O2 114.00(12) 8_465 2 ? O2 T1 O2 93.67(16) . 2 ? O1 T1 A1' 123.32(9) 7_566 . ? O1 T1 A1' 123.32(9) 8_465 . ? O2 T1 A1' 46.84(8) . . ? O2 T1 A1' 46.84(8) 2 . ? O1 T1 A1 152.29(9) 7_566 3_455 ? O1 T1 A1 92.91(9) 8_465 3_455 ? O2 T1 A1 44.32(8) . 3_455 ? O2 T1 A1 63.23(9) 2 3_455 ? A1' T1 A1 31.554(4) . 3_455 ? O1 T1 A1 92.91(9) 7_566 4 ? O1 T1 A1 152.29(9) 8_465 4 ? O2 T1 A1 63.23(9) . 4 ? O2 T1 A1 44.32(8) 2 4 ? A1' T1 A1 31.554(4) . 4 ? A1 T1 A1 63.107(8) 3_455 4 ? O1 T1 M2 103.95(9) 7_566 2 ? O1 T1 M2 90.65(8) 8_465 2 ? O2 T1 M2 122.65(8) . 2 ? O2 T1 M2 31.35(8) 2 2 ? A1' T1 M2 76.711(13) . 2 ? A1 T1 M2 83.470(14) 3_455 2 ? A1 T1 M2 73.857(13) 4 2 ? O1 T1 M2 90.65(8) 7_566 . ? O1 T1 M2 103.95(9) 8_465 . ? O2 T1 M2 31.35(8) . . ? O2 T1 M2 122.65(8) 2 . ? A1' T1 M2 76.711(13) . . ? A1 T1 M2 73.857(13) 3_455 . ? A1 T1 M2 83.469(14) 4 . ? M2 T1 M2 153.42(3) 2 . ? O1 T1 M2 33.72(9) 7_566 7_566 ? O1 T1 M2 106.00(9) 8_465 7_566 ? O2 T1 M2 88.21(8) . 7_566 ? O2 T1 M2 136.38(9) 2 7_566 ? A1' T1 M2 120.413(13) . 7_566 ? A1 T1 M2 132.519(13) 3_455 7_566 ? A1 T1 M2 100.773(12) 4 7_566 ? M2 T1 M2 137.67(2) 2 7_566 ? M2 T1 M2 59.56(2) . 7_566 ? O1 T1 M2 106.00(9) 7_566 8_465 ? O1 T1 M2 33.72(9) 8_465 8_465 ? O2 T1 M2 136.38(9) . 8_465 ? O2 T1 M2 88.21(8) 2 8_465 ? A1' T1 M2 120.413(13) . 8_465 ? A1 T1 M2 100.773(12) 3_455 8_465 ? A1 T1 M2 132.519(13) 4 8_465 ? M2 T1 M2 59.56(2) 2 8_465 ? M2 T1 M2 137.67(2) . 8_465 ? M2 T1 M2 119.17(3) 7_566 8_465 ? O1 T1 A2' 56.68(9) 7_566 1_565 ? O1 T1 A2' 56.68(9) 8_465 1_565 ? O2 T1 A2' 133.16(8) . 1_565 ? O2 T1 A2' 133.16(8) 2 1_565 ? A1' T1 A2' 180.0 . 1_565 ? A1 T1 A2' 148.446(4) 3_455 1_565 ? A1 T1 A2' 148.446(4) 4 1_565 ? M2 T1 A2' 103.289(13) 2 1_565 ? M2 T1 A2' 103.289(13) . 1_565 ? M2 T1 A2' 59.587(13) 7_566 1_565 ? M2 T1 A2' 59.587(13) 8_465 1_565 ? O6 T2 O5 110.59(14) 4 . ? O6 T2 O4 113.76(13) 4 4 ? O5 T2 O4 105.70(13) . 4 ? O6 T2 O3 106.31(13) 4 7_565 ? O5 T2 O3 110.39(12) . 7_565 ? O4 T2 O3 110.14(13) 4 7_565 ? O6 T2 A2' 46.17(11) 4 5_565 ? O5 T2 A2' 122.55(9) . 5_565 ? O4 T2 A2' 131.40(10) 4 5_565 ? O3 T2 A2' 60.25(10) 7_565 5_565 ? O6 T2 A2' 42.66(12) 4 1_565 ? O5 T2 A2' 71.68(10) . 1_565 ? O4 T2 A2' 143.07(10) 4 1_565 ? O3 T2 A2' 104.86(9) 7_565 1_565 ? A2' T2 A2' 59.620(9) 5_565 1_565 ? O6 T2 A1 87.03(10) 4 2_665 ? O5 T2 A1 90.97(8) . 2_665 ? O4 T2 A1 38.76(9) 4 2_665 ? O3 T2 A1 147.83(9) 7_565 2_665 ? A2' T2 A1 127.80(6) 5_565 2_665 ? A2' T2 A1 104.59(3) 1_565 2_665 ? T1 O1 M2 119.70(14) 7_566 . ? T1 O1 M1 122.33(14) 7_566 3 ? M2 O1 M1 101.59(10) . 3 ? T1 O1 A2' 95.34(11) 7_566 7_556 ? M2 O1 A2' 82.06(8) . 7_556 ? M1 O1 A2' 130.80(11) 3 7_556 ? T1 O2 A1' 93.75(11) . . ? T1 O2 M2 122.19(13) . . ? A1' O2 M2 138.91(13) . . ? T1 O2 A1 104.71(11) . 3_455 ? A1' O2 A1 45.29(5) . 3_455 ? M2 O2 A1 127.91(12) . 3_455 ? T1 O2 A1 84.78(10) . 4 ? A1' O2 A1 34.49(5) . 4 ? M2 O2 A1 122.69(11) . 4 ? A1 O2 A1 79.76(7) 3_455 4 ? T2 O3 M2 124.32(14) 7_565 . ? T2 O3 M1 132.23(14) 7_565 3 ? M2 O3 M1 103.42(10) . 3 ? T2 O3 A2' 88.89(10) 7_565 3 ? M2 O3 A2' 93.98(9) . 3 ? M1 O3 A2' 86.06(10) 3 3 ? T2 O4 A1' 134.77(15) 4_545 . ? T2 O4 M1 124.66(14) 4_545 . ? A1' O4 M1 100.26(11) . . ? T2 O4 A1 115.43(13) 4_545 3_455 ? A1' O4 A1 43.70(5) . 3_455 ? M1 O4 A1 99.43(10) . 3_455 ? T2 O4 A1 129.02(14) 4_545 4 ? A1' O4 A1 40.44(5) . 4 ? M1 O4 A1 94.39(9) . 4 ? A1 O4 A1 84.12(7) 3_455 4 ? T2 O5 M2 134.93(14) . 7_566 ? T2 O5 M2 120.13(14) . . ? M2 O5 M2 99.29(10) 7_566 . ? T2 O6 M2 137.69(17) 4_545 . ? T2 O6 A2' 104.50(15) 4_545 7_556 ? M2 O6 A2' 98.13(14) . 7_556 ? T2 O6 A2' 110.66(16) 4_545 3 ? M2 O6 A2' 106.36(14) . 3 ? A2' O6 A2' 85.30(9) 7_556 3 ? _refine_diff_density_max 1.905 _refine_diff_density_min -1.249 _refine_diff_density_rms 0.244 _shelx_res_file ; 4338_.res created by SHELXL-2014/7 TITL Johellerite 4338 CELL 0.7107300 11.90727 12.73845 6.71966 90.0000 113.2724 90.0000 ZERR 4 0.00040 0.00041 0.00022 0.0000 0.0016 0.0000 LATT 7 SYMM -X, Y, 0.5-Z SFAC O As Mg Fe Cu Zn Na Al UNIT 48 12 6.32 1.28 5.2 1.28 4.68 0.64 L.S. 14 BOND FMAP 2 PLAN 20 acta WGHT 0.000000 15.416492 EXTI 0.000486 FVAR 0.18136 0.83684 0.67699 0.33343 1.47805 1.62912 A2' 7 0.000000 -0.006594 0.250000 20.50000 0.01436 0.03985 = 0.01949 0.00000 0.00194 0.00000 A1' 5 0.000000 0.504049 0.250000 30.50000 0.00821 0.00437 = 0.01495 0.00000 0.00506 0.00000 A1 7 0.500000 0.000000 0.000000 40.50000 0.02475 0.00504 = 0.01564 0.00077 -0.00588 -0.00310 M1 3 0.000000 0.263547 0.250000 50.50000 0.00852 0.01182 = 0.01705 0.00000 0.00912 0.00000 M2 3 0.284828 0.656218 0.373636 61.00000 0.00450 0.00407 = 0.00762 -0.00032 0.00289 -0.00038 T1 2 0.000000 0.714753 0.250000 10.50000 0.00696 0.00567 = 0.00586 0.00000 0.00125 0.00000 T2 2 0.232497 0.887038 0.125154 11.00000 0.00870 0.00576 = 0.00676 -0.00002 0.00237 -0.00031 O1 1 0.461789 0.713138 0.524792 11.00000 0.00974 0.01306 = 0.00858 -0.00383 0.00137 -0.00058 O2 1 0.106803 0.623041 0.260424 11.00000 0.00866 0.00780 = 0.01744 -0.00287 0.00393 0.00131 O3 1 0.339518 0.670085 0.119255 11.00000 0.01563 0.01094 = 0.00712 -0.00141 0.00269 -0.00165 O4 1 0.115962 0.393498 0.312780 11.00000 0.00906 0.00982 = 0.02161 0.00093 0.00623 0.00121 O5 1 0.217015 0.813154 0.320927 11.00000 0.01229 0.01261 = 0.00921 0.00129 0.00417 -0.00240 O6 1 0.333188 0.503752 0.389650 11.00000 0.01863 0.00757 = 0.01928 0.00154 0.00669 -0.00231 hklf 4 REM Johellerite 4338 REM R1 = 0.0362 for 2675 Fo > 4sig(Fo) and 0.0420 for all 2958 data REM 105 parameters refined using 0 restraints END WGHT 0.0000 15.4147 REM Highest difference peak 1.905, deepest hole -1.249, 1-sigma level 0.244 Q1 1 0.0282 0.2845 0.3338 11.00000 0.05 1.90 Q2 1 0.2766 0.8816 0.0956 11.00000 0.05 1.42 Q3 1 0.2769 0.6013 0.3839 11.00000 0.05 1.30 Q4 1 0.0455 0.5006 0.2261 11.00000 0.05 1.15 Q5 1 0.2514 0.6497 0.2821 11.00000 0.05 1.13 Q6 1 0.0000 0.2205 0.2500 10.50000 0.05 1.10 Q7 1 0.2151 0.8375 0.1430 11.00000 0.05 1.03 Q8 1 0.0000 0.7965 0.2500 10.50000 0.05 0.97 Q9 1 0.2634 0.8601 0.3570 11.00000 0.05 0.88 Q10 1 0.2183 0.8800 0.2384 11.00000 0.05 0.83 Q11 1 0.4052 0.5007 0.3834 11.00000 0.05 0.81 Q12 1 0.1218 0.3826 0.2378 11.00000 0.05 0.80 Q13 1 0.2978 0.6591 0.5016 11.00000 0.05 0.75 Q14 1 0.1571 0.6204 0.3384 11.00000 0.05 0.75 Q15 1 0.2164 0.5023 0.1311 11.00000 0.05 0.75 Q16 1 0.4373 0.7297 0.6319 11.00000 0.05 0.74 Q17 1 -0.0184 0.7237 0.1265 11.00000 0.05 0.74 Q18 1 0.2513 0.8162 0.2634 11.00000 0.05 0.72 Q19 1 0.2416 0.5538 0.3938 11.00000 0.05 0.72 Q20 1 0.1818 0.8898 0.1533 11.00000 0.05 0.71 ; _shelx_res_checksum 45038 _shelx_hkl_file ; 2 0 0 324.209 11.4101 12 -2 0 0 326.542 11.4604 5 -2 0 0 305.713 11.4604 8 -2 0 0 317.444 11.4032 12 2 0 0 317.390 11.3826 1 2 0 0 324.472 11.3754 7 4 0 0 6200.00 219.729 1 -4 0 0 6160.09 220.769 8 -4 0 0 6197.42 220.751 5 6 0 0 201.477 7.86762 1 6 0 0 209.155 7.95075 12 6 0 0 206.131 7.84165 7 -6 0 0 223.827 8.99997 10 -6 0 0 215.102 8.15094 5 -6 0 0 217.800 8.25235 8 -8 0 0 2423.64 87.6899 5 8 0 0 2410.20 87.7990 7 -8 0 0 2589.87 89.0804 10 8 0 0 2495.83 87.3965 1 -8 0 0 2436.20 87.8530 8 8 0 0 2406.62 87.4627 12 -10 0 0 606.034 21.8528 10 10 0 0 531.251 19.9590 4 10 0 0 504.848 19.7528 7 10 0 0 523.204 19.8117 1 -10 0 0 548.244 20.5830 8 10 0 0 528.989 19.9389 12 12 0 0 222.782 9.31689 1 -12 0 0 238.901 10.5700 8 12 0 0 244.717 9.71794 4 12 0 0 235.779 9.54734 12 12 0 0 225.101 9.23852 7 14 0 0 353.689 14.5677 1 14 0 0 373.485 14.8136 12 14 0 0 380.688 14.8310 4 14 0 0 361.935 14.4127 7 -14 0 0 406.792 16.1230 8 16 0 0 0.02219 2.92719 12 16 0 0 7.21126 3.04754 1 -16 0 0 -3.5453 4.54733 8 16 0 0 3.18023 2.82446 4 -18 0 0 538.861 21.9895 8 18 0 0 487.658 20.2614 1 1 -1 0 102.798 3.62589 1 1 -1 0 102.636 3.83376 6 -1 -1 0 106.374 3.68249 8 1 -1 0 108.494 3.77030 10 -1 -1 0 97.8040 3.62867 12 -1 1 0 83.2210 3.62267 12 -3 -1 0 1625.80 59.3174 10 -3 -1 0 1462.38 54.9970 12 3 -1 0 1491.94 55.3883 12 3 -1 0 1555.35 56.1919 6 -3 -1 0 1549.71 55.2932 5 -3 -1 0 1621.34 55.1320 8 3 -1 0 1499.60 55.2382 1 -3 -1 0 1525.07 55.2967 11 3 -1 0 1510.09 55.0856 7 3 1 0 1570.32 55.4348 4 3 1 0 1588.36 55.2079 7 3 1 0 1565.41 55.0260 12 -3 1 0 1611.41 54.6718 5 -3 1 0 1536.89 55.0924 8 3 1 0 1525.07 55.1769 1 -3 1 0 1395.46 54.6955 12 5 -1 0 883.455 30.9467 12 -5 -1 0 863.513 32.1015 10 -5 -1 0 861.427 31.0247 5 -5 -1 0 857.710 31.1561 8 5 -1 0 870.120 30.8593 7 5 -1 0 863.466 30.8845 1 5 1 0 868.918 30.9430 12 5 1 0 877.771 30.8813 1 5 1 0 890.986 30.8622 7 -5 1 0 825.667 31.0710 8 5 1 0 865.479 30.9582 4 -5 1 0 864.158 31.0994 5 7 -1 0 1179.41 43.2312 7 -7 -1 0 1227.03 45.0438 10 -7 -1 0 1190.27 43.6897 8 7 -1 0 1203.83 43.3536 12 7 -1 0 1189.34 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612.604 22.1586 7 4 8 0 581.174 23.3780 9 -4 8 0 605.702 22.4044 5 4 8 0 618.742 22.1372 3 4 8 0 587.322 22.4863 4 4 8 0 625.308 22.1191 7 -4 8 0 614.545 22.3768 12 4 8 0 612.888 22.1637 1 -4 8 0 591.212 22.6383 3 -4 8 0 569.445 21.8118 8 -4 8 0 568.638 23.4375 9 4 8 0 619.714 22.3418 12 -6 -8 0 40.4046 2.80873 11 6 -8 0 36.7549 2.47311 1 -6 -8 0 31.0850 3.25259 6 6 -8 0 42.9854 3.79835 9 -6 -8 0 35.0546 2.80293 8 6 -8 0 33.8132 2.95426 10 6 -8 0 40.9490 2.75280 12 6 -8 0 34.2648 3.96802 6 6 -8 0 35.9966 2.59694 7 -6 8 0 33.1983 3.09192 3 -6 8 0 34.6302 2.57983 12 6 8 0 36.5953 2.40620 1 -6 8 0 34.5964 3.35655 10 -6 8 0 29.5683 1.93946 8 6 8 0 38.0214 2.26701 7 6 8 0 41.3497 2.18540 3 6 8 0 32.8574 2.85750 4 -6 8 0 36.5735 2.89636 5 6 8 0 40.2340 2.69092 12 8 -8 0 616.511 24.1135 9 -8 -8 0 608.533 23.4759 6 8 -8 0 608.579 22.9109 12 8 -8 0 608.127 22.7559 1 -8 -8 0 615.929 23.0664 11 8 -8 0 601.339 24.6007 6 -8 -8 0 596.464 23.1033 8 8 -8 0 622.989 22.7581 7 8 8 0 599.252 22.8003 12 8 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8 -13 -5 2 146.076 7.73337 8 13 -5 -2 149.602 7.17627 12 13 -5 -2 152.782 6.93255 1 -13 5 2 166.096 7.84441 8 13 5 -2 152.442 6.89160 4 13 5 -2 141.363 6.94140 12 -13 5 2 153.201 8.02088 5 13 5 -2 143.493 6.66628 1 -11 -5 2 303.510 12.0542 11 11 -5 -2 307.226 11.9925 1 11 -5 -2 298.926 11.8183 7 -11 -5 2 304.324 12.4865 8 11 -5 -2 315.884 12.6331 9 11 -5 -2 310.909 12.1836 12 11 5 -2 302.220 12.0521 4 11 5 -2 315.353 12.1090 12 -11 5 2 327.448 12.2993 8 -11 5 2 322.626 12.7791 5 11 5 -2 306.370 11.8472 1 -11 5 2 307.350 13.0603 10 9 -5 -2 54.7089 2.90006 7 9 -5 -2 52.8518 3.42656 9 -9 -5 2 51.2716 3.37877 8 -9 -5 2 51.9597 2.93881 11 9 -5 -2 54.9967 2.91313 1 9 -5 -2 54.6295 3.20565 12 -9 5 2 46.8853 3.82453 5 9 5 -2 55.4492 3.04671 12 -9 5 2 50.4232 3.89021 10 9 5 -2 53.0813 2.81490 1 9 5 -2 47.2527 2.15973 3 9 5 -2 45.4695 2.95917 4 -9 5 2 51.7549 3.27360 3 9 5 -2 42.2548 3.85326 9 9 5 -2 46.7559 2.48453 7 -9 5 2 49.1410 3.16870 8 7 -5 -2 1981.27 69.2812 12 7 -5 -2 1916.77 69.0465 7 -7 -5 2 1984.82 69.2419 11 7 -5 -2 2072.76 69.7127 9 7 -5 -2 1928.53 69.1350 1 7 -5 -2 1871.05 70.3709 6 -7 -5 2 1992.82 69.2872 8 7 5 -2 1878.38 69.2780 4 7 5 -2 1975.54 69.0346 1 -7 5 2 1884.59 69.4930 5 7 5 -2 1855.91 68.7343 3 -7 5 2 1987.41 70.4836 10 7 5 -2 2010.77 69.1820 12 7 5 -2 1891.85 70.0847 9 -7 5 2 1943.17 69.3438 3 -7 5 2 1892.87 69.2128 8 5 -5 -2 28.0846 2.17094 9 5 -5 -2 24.2320 1.60254 1 5 -5 -2 25.2508 1.31419 11 5 -5 -2 22.7957 1.85597 12 -5 -5 2 24.6712 2.45057 9 5 -5 -2 21.8824 1.49015 7 -5 -5 2 21.8419 1.62655 8 -5 -5 2 24.8777 1.72948 11 5 -5 -2 22.1937 2.56949 6 5 5 -2 22.1828 2.36760 9 -5 5 2 21.0607 1.76691 3 -5 5 2 23.9068 2.57812 10 5 5 -2 24.2543 1.53987 12 5 5 -2 17.8918 1.19819 3 5 5 -2 26.4705 2.08666 4 -5 5 2 22.3977 1.90808 5 -5 5 2 23.5344 1.87790 9 5 5 -2 25.3488 1.40873 1 3 -5 -2 3227.58 116.432 1 -3 -5 2 3262.43 116.614 8 3 -5 -2 3335.45 120.115 10 -3 -5 2 3250.47 116.505 11 3 -5 -2 3367.90 117.854 12 3 -5 -2 3344.75 116.513 11 3 -5 -2 3264.73 119.538 6 3 -5 -2 3467.81 119.504 9 -3 -5 2 3386.39 117.768 9 3 -5 -2 3133.82 115.758 7 -3 5 2 3385.23 115.828 12 3 5 -2 3194.95 116.416 1 -3 5 2 3221.40 115.678 4 -3 5 2 3146.28 115.877 5 -3 5 2 3267.50 115.816 3 3 5 -2 3113.12 116.810 9 3 5 -2 3390.60 115.637 3 3 5 -2 3252.28 116.498 12 3 5 -2 3064.84 115.966 4 -3 5 2 3318.64 124.156 10 -3 5 2 3206.27 119.024 9 1 -5 -2 165.909 8.25789 10 -1 -5 2 155.112 6.04834 12 1 -5 -2 160.970 6.15725 1 -1 -5 2 162.632 5.91670 8 -1 -5 2 156.578 6.14647 12 -1 -5 2 174.511 7.25655 9 -1 -5 2 154.921 6.37043 11 1 -5 -2 169.913 7.05187 6 1 -5 -2 161.599 6.23279 12 1 -5 -2 165.113 6.10383 11 -1 5 2 157.446 6.21042 3 -1 5 2 167.937 6.69751 9 -1 5 2 163.154 6.20891 4 -1 5 2 170.959 7.93471 10 1 5 -2 164.870 6.04127 12 -1 5 2 159.356 6.27413 12 1 5 -2 148.195 7.21045 9 1 -5 2 2983.23 105.516 12 1 -5 2 2987.61 105.413 6 -1 -5 -2 3001.57 104.405 6 -1 -5 -2 2860.93 104.692 11 1 -5 2 3042.12 108.240 9 1 -5 2 2951.68 103.957 1 1 -5 2 2822.81 103.793 12 -1 -5 -2 2811.57 104.150 1 1 -5 2 3009.08 104.137 7 1 -5 2 2773.83 103.637 8 -1 -5 -2 2828.60 106.437 10 1 5 2 2972.53 104.673 12 -1 5 -2 2908.29 103.950 12 -1 5 -2 2865.38 104.971 9 1 5 2 2919.88 104.459 7 1 5 2 2923.37 104.649 3 1 5 2 3021.66 109.928 10 1 5 2 3037.57 104.833 4 1 5 2 2973.76 106.320 9 1 5 2 2913.37 104.343 1 3 -5 2 50.9642 2.22260 7 3 -5 2 44.3406 2.18205 1 3 -5 2 50.0784 3.28932 6 3 -5 2 45.8860 2.26419 12 -3 -5 -2 46.2376 2.53690 11 -3 -5 -2 49.5663 2.49310 6 -3 -5 -2 44.3663 2.27001 1 3 -5 2 47.9069 2.58039 10 3 -5 2 46.1728 3.44098 9 -3 -5 -2 38.5585 4.53885 10 3 5 2 47.1288 4.65413 10 3 5 2 48.7463 2.20065 7 3 5 2 49.7052 2.53142 4 3 5 2 44.0182 2.20393 1 3 5 2 49.3728 2.40618 12 -3 5 -2 49.2869 2.36974 12 5 -5 2 2087.04 74.9245 9 5 -5 2 2081.67 73.5151 7 -5 -5 -2 2048.89 77.0706 10 5 -5 2 2051.15 74.4834 6 5 -5 2 2059.78 73.5871 12 5 -5 2 2080.48 73.5422 1 -5 5 -2 2092.10 73.5646 12 5 5 2 2054.76 73.5067 1 5 5 2 2096.56 73.6334 12 5 5 2 1986.89 73.4303 7 5 5 2 2103.90 73.8218 4 5 5 2 2077.89 76.3719 10 7 -5 2 14.9755 1.55935 1 7 -5 2 16.0022 1.53025 7 7 -5 2 12.4114 2.33731 6 7 -5 2 15.4780 2.82207 9 -7 -5 -2 5.68245 3.31327 10 7 -5 2 18.4042 1.96298 12 7 5 2 13.5729 1.50873 1 7 5 2 15.4158 1.64098 7 7 5 2 15.8098 1.74404 12 7 5 2 16.4836 2.04114 4 9 -5 2 351.836 12.9543 7 9 -5 2 344.880 13.0975 12 9 -5 2 336.130 14.8379 9 9 -5 2 336.247 12.9644 1 9 5 2 341.315 13.3901 4 9 5 2 339.027 13.0930 12 9 5 2 333.676 12.8778 7 9 5 2 337.787 12.9067 1 11 -5 2 51.2711 3.68041 1 11 -5 2 52.1391 4.41497 12 11 -5 2 51.5115 4.08599 7 11 5 2 53.0467 3.78667 1 11 5 2 53.2048 4.06250 7 11 5 2 60.3888 4.47260 12 11 5 2 58.1475 4.53306 4 13 -5 2 118.724 6.33407 7 13 -5 2 131.243 6.49420 1 13 -5 2 119.695 6.52374 12 13 5 2 121.260 6.31537 1 13 5 2 114.458 6.46427 7 13 5 2 102.212 6.32512 12 13 5 2 131.696 7.23567 4 15 -5 2 51.1050 4.62941 1 15 -5 2 53.8070 4.55565 7 15 -5 2 48.5576 4.83094 12 15 5 2 60.3211 4.76035 1 15 5 2 53.8421 4.34381 7 15 5 2 66.9738 6.33799 4 15 5 2 57.4090 4.96364 12 17 -5 2 4.55012 3.65689 1 17 -5 2 3.70123 4.18098 4 17 5 2 8.02490 4.32538 4 17 5 2 6.43459 3.78579 1 20 -6 -2 34.0013 4.12294 1 -20 -6 2 40.1312 7.65961 8 20 6 -2 38.1876 4.77765 1 18 -6 -2 36.9797 4.76753 1 -18 -6 2 45.2381 6.91182 8 18 6 -2 37.5066 4.65680 12 18 6 -2 34.5740 4.27900 1 -18 6 2 25.5041 6.73285 5 -16 -6 2 49.7708 5.88339 8 16 -6 -2 39.7252 4.43778 12 16 -6 -2 43.8239 4.40070 1 16 6 -2 39.9945 4.15153 4 -16 6 2 54.2862 5.22689 5 -16 6 2 50.2120 4.83451 8 16 6 -2 41.9955 4.29884 12 16 6 -2 44.6402 4.02178 1 14 -6 -2 86.9033 5.31386 1 14 -6 -2 84.5740 5.51813 12 -14 -6 2 85.2520 6.31924 8 14 6 -2 82.8941 5.00718 1 -14 6 2 83.5254 6.82257 5 14 6 -2 87.7800 5.29052 12 -14 6 2 92.3085 6.28798 8 14 6 -2 81.0364 5.56067 4 12 -6 -2 38.4162 3.87607 9 12 -6 -2 40.0551 3.00392 7 12 -6 -2 44.1767 3.26370 1 -12 -6 2 40.6573 3.83172 8 -12 -6 2 44.7479 3.47511 11 12 -6 -2 39.3095 3.45609 12 -12 6 2 42.9612 3.74196 5 12 6 -2 40.7744 3.50398 12 12 6 -2 45.3607 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11 6 -6 -2 40.6888 2.53565 12 -6 -6 2 41.9684 2.43145 11 6 6 -2 32.3602 3.04733 9 -6 6 2 35.5382 2.85654 5 -6 6 2 34.5970 2.16026 8 6 6 -2 38.1875 2.06542 1 6 6 -2 37.1541 1.98092 7 -6 6 2 38.1071 2.59585 3 -6 6 2 39.7619 3.34108 10 6 6 -2 29.4854 1.73002 3 6 6 -2 42.8342 2.30400 12 6 6 -2 36.5827 2.56052 4 -4 -6 2 120.690 5.74594 9 4 -6 -2 125.436 5.52957 9 4 -6 -2 115.507 4.71474 1 4 -6 -2 123.183 4.91705 12 4 -6 -2 107.781 4.59623 7 4 -6 -2 107.960 6.38476 10 -4 -6 2 113.502 4.88887 11 -4 -6 2 117.270 4.60161 8 4 -6 -2 106.944 5.89361 6 4 -6 -2 121.498 4.57955 11 -4 6 2 112.488 4.95690 5 4 6 -2 114.730 4.61505 12 4 6 -2 111.846 4.54061 3 -4 6 2 112.162 5.27874 9 -4 6 2 120.423 4.88366 12 -4 6 2 120.978 6.37712 10 4 6 -2 115.477 5.05349 4 -4 6 2 115.346 4.91282 3 4 6 -2 120.778 4.54657 1 4 6 -2 113.644 5.92313 9 2 -6 -2 60.7395 2.70918 1 2 -6 -2 64.3704 2.63147 7 2 -6 -2 55.5056 2.81363 12 -2 -6 2 60.6012 2.69529 12 -2 -6 2 53.8344 2.91973 11 2 -6 -2 62.6480 3.40909 9 2 -6 -2 60.8981 2.63293 11 2 -6 -2 65.9143 4.73252 10 -2 -6 2 61.0226 2.43873 8 2 -6 -2 60.2824 3.80212 6 -2 -6 2 53.3673 3.67850 9 -2 6 2 62.3309 2.90791 12 -2 6 2 58.6340 2.70154 4 2 6 -2 54.1370 3.93292 9 -2 6 2 55.4666 3.30342 9 -2 6 2 57.9379 2.88229 5 -2 6 2 64.5583 4.37917 10 2 6 -2 54.0389 2.66465 3 2 6 -2 63.6636 2.59152 12 -2 6 2 52.1310 2.66404 3 0 -6 -2 19.6711 3.39769 10 0 -6 2 21.9917 2.59757 9 0 -6 2 19.3358 1.39541 12 0 -6 -2 19.2774 2.12947 6 0 -6 2 18.0971 1.20726 1 0 -6 2 18.8817 2.24252 10 0 -6 -2 19.1597 1.39931 1 0 -6 2 18.8351 2.16349 6 0 -6 2 17.0816 0.82373 8 0 -6 -2 23.6217 1.56258 12 0 -6 2 19.5725 1.73984 11 0 -6 -2 18.8482 1.40432 11 0 6 -2 20.6942 2.60500 9 0 6 2 19.6199 1.27549 7 0 6 2 21.9315 1.64100 12 0 6 -2 19.4017 1.38585 12 0 6 2 23.6250 1.56870 4 0 6 2 23.1245 2.08573 9 0 6 2 24.3470 1.59872 3 0 6 2 20.8569 3.00644 10 2 -6 2 29.0608 2.42284 10 -2 -6 -2 31.9817 1.73881 1 2 -6 2 30.8727 1.82064 12 -2 -6 -2 30.3723 4.29577 10 2 -6 2 33.1817 1.70560 1 2 -6 2 31.1382 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376.581 18.8681 10 6 8 4 389.117 14.4778 1 6 8 4 379.747 15.0131 4 8 -8 4 13.1589 2.19326 1 8 -8 4 13.3010 2.37129 12 8 -8 4 10.2994 2.47444 7 8 8 4 11.8310 2.37950 1 8 8 4 14.6189 2.58638 12 8 8 4 17.8990 2.40401 7 8 8 4 13.7716 3.18829 4 10 -8 4 140.646 7.37608 12 10 -8 4 148.488 7.37472 7 10 -8 4 141.011 6.92964 1 10 8 4 141.298 7.05326 1 10 8 4 147.707 6.89144 7 10 8 4 134.204 7.02120 12 10 8 4 137.931 8.04675 4 12 -8 4 0.22634 2.75179 1 12 -8 4 3.20527 3.61534 7 12 -8 4 2.52301 3.66702 12 12 8 4 4.62499 4.26422 4 12 8 4 3.57748 3.65070 7 12 8 4 2.38724 3.06685 1 14 -8 4 4.43921 3.23012 1 14 -8 4 10.2260 4.27767 7 14 8 4 9.41194 3.70762 1 14 8 4 7.57055 4.20718 3 14 8 4 12.4283 4.96105 4 14 8 4 11.4700 4.27474 7 19 -9 -4 7.39390 4.23060 1 -19 -9 4 2.73879 5.92805 8 -19 9 4 1.99165 7.01018 5 17 -9 -4 446.701 19.2057 12 17 -9 -4 470.090 19.8763 2 -17 -9 4 440.886 19.7631 8 17 -9 -4 472.612 19.1239 1 -17 9 4 529.374 20.7685 5 15 -9 -4 16.9694 4.27353 2 -15 -9 4 22.3204 3.59098 11 -15 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6.24264 3.39537 9 5 -5 5 6.14427 1.32452 7 5 5 5 7.36684 2.28689 4 5 5 5 5.76989 3.50345 10 5 5 5 5.35637 1.49144 7 5 5 5 7.97489 1.61185 12 5 5 5 7.36052 1.47942 1 7 -5 5 2.22114 1.67649 7 7 -5 5 0.98470 1.29902 1 7 -5 5 1.25493 1.80080 12 7 5 5 2.79600 2.04576 1 7 5 5 0.60100 2.55828 4 7 5 5 0.01900 1.88936 7 7 5 5 1.23731 1.70830 12 9 -5 5 18.8794 2.75523 7 9 -5 5 14.1193 2.17546 1 9 -5 5 17.4096 2.45959 12 9 5 5 20.5434 2.57277 7 9 5 5 21.4272 3.11378 12 9 5 5 19.2672 2.62623 1 9 5 5 18.7758 3.79585 4 11 -5 5 21.5016 3.51537 12 11 -5 5 16.4269 2.73301 1 11 -5 5 23.8817 3.13503 7 11 5 5 20.8769 3.11944 12 11 5 5 22.9949 4.68092 4 11 5 5 19.1165 3.08469 1 11 5 5 19.1300 3.61863 7 13 -5 5 34.9350 3.73995 1 13 -5 5 41.8002 4.81846 7 13 5 5 53.6436 4.46549 1 13 5 5 44.8230 4.27114 7 13 5 5 47.6800 5.94054 4 -20 -6 5 0.81959 6.51656 8 20 -6 -5 4.57115 6.77006 2 -20 6 5 1.41243 4.68391 5 -20 6 5 1.33467 6.76691 8 18 -6 -5 113.089 7.42627 1 18 -6 -5 128.515 10.3593 2 -18 -6 5 118.965 9.34997 8 -18 6 5 139.213 10.1539 5 -18 6 5 142.288 9.27894 8 16 -6 -5 12.2819 3.45662 12 16 -6 -5 19.3510 5.30951 2 -16 -6 5 7.83271 4.50092 8 16 -6 -5 3.61344 3.41853 1 -16 6 5 15.5275 4.57592 8 -16 6 5 16.7941 5.30659 5 14 -6 -5 449.777 18.2523 2 -14 -6 5 416.306 17.1782 8 14 -6 -5 405.164 16.8512 12 14 -6 -5 415.213 16.5414 1 -14 -6 5 403.863 16.3242 11 -14 6 5 455.011 17.4802 8 -14 6 5 477.690 17.9633 5 -12 -6 5 26.0007 3.19545 8 12 -6 -5 24.6624 2.89771 12 12 -6 -5 30.0940 2.84603 1 12 -6 -5 27.5712 4.03859 2 -12 -6 5 27.1153 2.41701 11 12 6 -5 17.3455 2.42282 12 -12 6 5 28.9965 3.17146 3 -12 6 5 20.6572 4.69183 10 -12 6 5 27.0323 3.54670 8 -12 6 5 22.9505 3.73240 5 -10 -6 5 480.035 18.2032 8 10 -6 -5 483.288 18.1587 12 10 -6 -5 485.362 17.8282 1 -10 -6 5 476.998 17.9341 11 10 -6 -5 501.053 19.2151 2 -10 6 5 481.258 20.8935 10 -10 6 5 480.441 18.7459 5 -10 6 5 491.501 18.5544 8 10 6 -5 460.940 17.8504 12 -10 6 5 474.475 18.0897 3 8 -6 -5 105.599 5.09210 12 8 -6 -5 101.838 6.06666 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13.9894 8 -2 -6 5 383.600 13.8351 1 2 -6 -5 376.673 15.0232 2 -2 -6 5 377.612 13.9430 12 -2 -6 5 388.367 15.9765 9 -2 6 5 380.531 17.3673 10 2 6 -5 395.485 14.8821 2 -2 6 5 373.642 14.8549 9 -2 6 5 391.729 14.1834 4 -2 6 5 384.440 14.0205 7 -2 6 5 393.763 14.4107 3 -2 6 5 395.613 14.2994 12 0 -6 5 34.6135 4.22585 9 0 -6 5 38.1179 2.15322 12 0 -6 5 35.8608 1.87259 1 0 -6 -5 42.7406 3.61565 2 0 6 5 36.8765 2.57174 4 0 6 5 35.7854 2.49571 12 0 6 5 40.4195 2.20250 7 0 6 5 36.9130 5.66873 10 0 6 -5 38.8551 3.36022 2 0 6 5 39.0272 2.95093 3 2 -6 5 246.975 9.44260 1 2 -6 5 261.362 11.1272 6 2 -6 5 256.120 9.62276 12 -2 -6 -5 255.960 11.0619 2 2 -6 5 253.456 9.36373 7 2 -6 5 252.948 11.9515 9 2 -6 5 240.788 11.4772 10 2 6 5 246.781 13.2716 10 -2 6 -5 265.651 10.4653 2 2 6 5 259.500 10.2047 4 2 6 5 251.554 9.78066 12 2 6 5 256.561 9.65045 1 2 6 5 252.402 9.53771 7 4 -6 5 26.7636 2.02422 1 4 -6 5 26.5469 2.20719 12 4 -6 5 20.8452 2.99229 6 4 -6 5 24.0865 1.91846 7 -4 -6 -5 32.1769 4.16130 2 4 -6 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6 36.9201 3.31869 1 9 3 6 41.2340 3.54477 7 11 -3 6 17.7814 2.65848 1 11 -3 6 25.9664 3.75583 7 11 3 6 21.7746 3.73210 7 11 3 6 18.8109 2.88188 1 11 3 6 25.0626 5.15383 4 -20 -4 6 86.9836 8.49507 8 20 -4 -6 81.8928 10.0464 2 -20 4 6 85.9925 8.00815 8 -20 4 6 77.9110 8.00281 5 18 -4 -6 5.74620 6.72631 2 -18 -4 6 -2.8216 5.42182 8 -18 4 6 3.83698 5.50077 8 -18 4 6 6.07185 4.06079 5 16 -4 -6 486.992 21.9795 2 -16 -4 6 483.468 20.1992 8 -16 4 6 508.014 20.4694 5 -16 4 6 507.630 20.4490 8 -14 -4 6 10.2335 3.71205 8 -14 -4 6 6.31847 2.31647 5 14 -4 -6 9.67879 4.69383 2 14 4 -6 -1.8432 5.26418 2 -14 4 6 9.48437 4.02615 5 -14 4 6 5.93692 3.93274 8 12 -4 -6 972.408 37.3066 2 -12 -4 6 1022.22 36.1102 8 -12 -4 6 968.093 35.4320 5 -12 4 6 1015.92 36.4188 5 12 4 -6 921.911 37.8772 2 -12 4 6 1017.58 36.3708 8 -12 4 6 927.720 39.0780 10 -10 -4 6 80.7233 4.90653 8 -10 -4 6 80.4029 3.83805 11 -10 -4 6 85.3586 3.95923 5 10 -4 -6 76.4826 5.86940 2 -10 4 6 86.3231 5.46896 8 -10 4 6 80.7269 8.16815 10 -10 4 6 76.6637 4.16347 3 10 4 -6 66.9277 6.38185 2 -10 4 6 88.8765 5.47652 5 -8 -4 6 1941.57 68.8865 8 -8 -4 6 1905.36 68.5755 11 8 -4 -6 1912.93 69.8260 2 -8 -4 6 1925.14 69.2183 9 -8 4 6 1902.38 68.6404 3 -8 4 6 1987.78 72.4180 10 -8 4 6 1860.55 69.1842 5 8 4 -6 1939.75 69.9796 2 -6 -4 6 13.8468 1.68756 5 6 -4 -6 18.5198 3.05939 2 -6 -4 6 13.2335 1.94344 8 -6 -4 6 16.1406 2.39700 9 -6 -4 6 13.4531 1.75697 11 -6 4 6 10.9586 3.69130 10 6 4 -6 16.5284 3.03477 2 -6 4 6 12.8947 2.05854 5 -6 4 6 16.0889 1.61772 9 -6 4 6 12.7570 1.71185 3 4 -4 -6 890.473 34.4071 2 -4 -4 6 932.108 33.7020 11 -4 -4 6 943.092 34.8786 9 -4 4 6 930.737 33.1428 4 -4 4 6 935.725 33.4536 3 4 4 -6 917.100 34.2860 2 -4 4 6 926.265 33.3243 12 -4 4 6 920.659 36.8260 10 -2 -4 6 77.6518 5.44334 9 -2 -4 6 76.9734 2.94921 1 2 -4 -6 77.3801 5.03551 2 -2 4 6 77.0699 6.76554 10 -2 4 6 74.9113 3.25017 7 -2 4 6 77.8913 3.59472 4 2 4 -6 78.0503 4.89658 2 -2 4 6 79.1424 4.03511 3 -2 4 6 75.5974 3.47531 12 0 -4 -6 267.993 11.2571 2 0 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4 6 56.8166 4.31810 7 8 4 6 49.8989 3.74669 12 8 4 6 55.4256 4.25883 1 8 4 6 61.3027 5.27710 4 10 -4 6 450.284 16.8281 7 10 -4 6 404.001 16.3463 1 10 4 6 442.064 18.1212 4 10 4 6 435.534 16.5749 1 10 4 6 431.950 16.5973 7 10 4 6 411.747 16.5975 12 12 -4 6 5.93769 3.71541 7 12 -4 6 -0.0315 2.28388 1 12 4 6 5.28978 4.74900 4 12 4 6 3.07358 3.79302 7 12 4 6 10.8571 3.36705 1 -21 5 6 7.31763 6.17149 8 -19 -5 6 126.184 9.83824 8 19 -5 -6 108.350 10.4562 2 -19 5 6 119.959 9.69737 8 -19 5 6 139.147 10.2630 5 17 -5 -6 69.4633 8.09106 2 -17 -5 6 58.3912 6.46821 8 -17 5 6 71.7255 6.98944 5 -17 5 6 73.1037 6.80751 8 -15 -5 6 171.632 9.32322 8 15 -5 -6 162.193 10.5423 2 -15 5 6 172.776 9.88493 5 -15 5 6 183.925 9.82897 8 13 -5 -6 183.012 10.2104 2 -13 -5 6 172.698 8.44997 8 -13 5 6 180.933 8.92799 8 13 5 -6 166.854 10.9565 2 -13 5 6 179.225 8.99487 5 -13 5 6 143.672 12.6310 10 11 -5 -6 11.2763 3.58021 2 -11 -5 6 7.29507 1.74766 11 -11 -5 6 7.08134 2.67851 8 -11 5 6 9.70293 3.03920 8 -11 5 6 7.97979 2.41177 5 11 5 -6 7.37274 4.13249 2 -11 5 6 8.76743 2.20353 3 -11 5 6 6.54039 4.72512 10 -9 -5 6 646.335 23.2788 11 -9 -5 6 622.375 24.0371 9 9 -5 -6 629.195 24.5838 2 -9 -5 6 650.795 23.6096 8 -9 -5 6 589.155 23.4378 5 -9 5 6 626.836 23.3792 3 -9 5 6 649.727 24.1466 5 9 5 -6 657.856 24.9697 2 -9 5 6 646.490 26.9511 10 -7 -5 6 12.8485 2.33591 8 -7 -5 6 10.4605 1.37954 5 7 -5 -6 12.7902 2.92419 2 -7 -5 6 9.52183 1.96766 11 -7 -5 6 10.0402 2.42973 9 -7 5 6 10.2813 2.05397 3 -7 5 6 13.3200 4.59670 10 7 5 -6 12.7043 3.12509 2 -7 5 6 10.6070 2.57947 5 -5 -5 6 953.188 35.6469 8 -5 -5 6 990.913 37.0826 9 -5 -5 6 990.219 35.9111 11 -5 -5 6 942.775 35.4503 5 -5 -5 6 958.450 35.1713 7 5 -5 -6 970.940 36.6426 2 -5 5 6 1007.57 39.3479 10 -5 5 6 1009.67 35.6695 12 5 5 -6 1010.92 36.5379 2 -5 5 6 941.537 35.2948 4 -5 5 6 1019.92 36.3041 5 -5 5 6 1054.04 35.7446 3 3 -5 -6 24.3379 3.16495 2 -3 -5 6 21.0664 3.21092 9 -3 5 6 22.7195 4.88829 10 3 5 -6 22.3551 3.07274 2 -3 5 6 19.6347 1.99010 12 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6.07051 2 9 5 -10 5.47955 6.54804 2 -9 5 10 -0.3076 4.99060 5 7 -5 -10 191.752 12.4434 2 -7 -5 10 199.682 10.0530 8 -7 5 10 203.417 11.3242 5 7 5 -10 211.349 12.4047 2 5 -5 -10 4.21889 5.94437 2 5 5 -10 -0.5904 5.78299 2 -5 5 10 2.24920 3.09021 3 -5 5 10 -7.0108 4.97641 5 3 -5 -10 183.661 12.1930 2 3 5 -10 193.542 11.6349 2 -3 5 10 181.046 9.02020 3 -1 -5 10 2.64669 1.08109 7 1 -5 -10 1.61575 6.23292 2 -1 5 10 -0.4806 3.59500 3 1 5 -10 5.29493 5.99976 2 1 -5 10 217.287 8.42082 7 -1 -5 -10 236.934 14.1808 2 1 5 10 219.805 10.8732 3 -1 5 -10 244.284 14.2691 2 1 5 10 214.113 9.14451 7 3 -5 10 0.74953 1.87003 7 3 5 10 0.74293 2.66125 7 3 5 10 4.10939 3.36371 3 16 -6 -10 16.8672 7.93454 2 -16 -6 10 24.1749 5.64288 8 -16 6 10 33.7933 7.68401 8 16 6 -10 20.8848 9.00990 2 -16 6 10 29.2536 6.82706 5 -14 -6 10 16.8961 4.97430 8 14 -6 -10 8.16584 7.06340 2 -14 6 10 16.9377 6.98406 8 -14 6 10 7.45508 6.02808 5 14 6 -10 16.4574 8.05816 2 -12 -6 10 21.3475 5.35479 8 12 -6 -10 9.89955 6.95417 2 -12 6 10 14.8471 3.90477 12 -12 6 10 8.66637 6.48362 8 -12 6 10 10.1384 5.64185 5 12 6 -10 16.5874 7.48465 2 -10 -6 10 -0.0963 3.59730 8 10 -6 -10 -3.2518 6.06211 2 10 6 -10 8.54850 6.78916 2 -10 6 10 6.34028 5.46751 5 8 -6 -10 6.33975 5.95671 2 8 6 -10 5.90808 6.17451 2 -8 6 10 2.38713 5.20881 5 6 -6 -10 25.5654 6.48801 2 -6 6 10 23.9713 3.65125 3 6 6 -10 22.8442 6.51887 2 -6 6 10 22.2149 5.59974 5 4 -6 -10 -1.8928 5.83055 2 -4 6 10 -2.1492 5.31876 5 4 6 -10 5.68962 5.80054 2 -4 6 10 -2.0642 3.24293 3 -2 -6 10 0.58049 4.38599 11 2 -6 -10 5.56717 6.27166 2 -2 -6 10 2.52653 1.16708 7 -2 6 10 1.02858 3.66296 3 2 6 -10 -0.3149 5.53333 2 0 -6 -10 0.32088 6.61106 2 0 -6 10 3.58372 1.38147 7 0 6 10 1.09373 3.96806 3 0 6 -10 -0.3427 5.86860 2 0 6 10 2.85528 2.45935 7 2 -6 10 -0.0979 1.70753 7 -2 -6 -10 0.96677 7.30307 2 -2 6 -10 -1.1760 6.34724 2 2 6 10 1.24264 4.27592 3 2 6 10 1.33052 2.36749 7 15 -7 -10 -1.5087 6.99822 2 -15 -7 10 7.67923 4.78454 8 15 7 -10 4.64681 8.12934 2 -15 7 10 1.33629 6.28159 5 -15 7 10 2.19008 6.95835 8 13 -7 -10 35.8840 7.52467 2 -13 -7 10 36.5320 5.87305 8 -13 7 10 48.0698 6.96144 5 -13 7 10 44.7184 7.52241 8 13 7 -10 44.1842 8.51663 2 11 -7 -10 -1.3257 6.19395 2 -11 -7 10 1.61439 3.69311 8 -11 7 10 0.21749 5.53386 5 11 7 -10 -0.6453 6.62576 2 -11 7 10 -0.6030 6.28157 8 -11 7 10 2.34716 2.98068 12 9 -7 -10 18.1923 6.45608 2 9 7 -10 23.7731 6.93919 2 -9 7 10 16.9516 4.37749 5 7 -7 -10 26.9472 6.62041 2 7 7 -10 29.2932 6.58213 2 -7 7 10 27.7287 6.08130 5 5 -7 -10 0.00661 5.85928 2 5 7 -10 0.89069 5.70656 2 -5 7 10 3.02344 4.10795 3 -5 7 10 2.55360 5.53377 5 -3 -7 10 93.8552 8.77397 6 3 -7 -10 88.6869 9.05692 2 -3 -7 10 93.7220 9.45754 11 -3 7 10 93.4262 6.66695 3 3 7 -10 108.131 9.00329 2 1 -7 -10 7.26389 6.52795 2 -1 -7 10 7.21292 1.67856 7 -1 -7 10 3.36858 4.86167 11 1 7 -10 7.32170 6.94242 2 -1 7 10 3.58816 4.07029 3 -1 -7 -10 94.8672 9.82722 2 1 -7 10 92.9348 4.42172 7 1 7 10 82.5259 6.68925 3 -1 7 -10 81.3113 8.05453 2 1 7 10 92.9501 5.61367 7 -16 -8 10 88.9058 7.64607 8 16 -8 -10 90.1441 9.63447 2 16 8 -10 80.7600 10.5415 2 -16 8 10 103.022 10.5008 8 -16 8 10 86.9980 8.73082 5 -14 -8 10 17.2973 4.69280 8 14 -8 -10 25.9913 7.31981 2 -14 8 10 18.0686 7.14070 8 -14 8 10 37.4354 7.04984 5 14 8 -10 31.4069 8.22735 2 12 -8 -10 89.9449 9.09164 2 12 8 -10 117.448 10.6238 2 -12 8 10 106.192 8.99047 8 10 -8 -10 5.50459 5.97739 2 10 8 -10 10.6232 6.75073 2 -10 8 10 5.10095 3.85531 12 -10 8 10 11.9999 5.96926 5 8 -8 -10 42.6862 7.16671 2 8 8 -10 46.5132 7.18687 2 -8 8 10 56.8125 6.98221 5 6 -8 -10 8.39462 5.98254 2 6 8 -10 8.58017 7.03873 2 -6 8 10 11.3222 5.96821 5 -6 8 10 8.86284 3.62983 3 4 -8 -10 43.6520 7.16274 2 -4 -8 10 24.9401 5.83048 6 -4 8 10 44.0936 6.86108 5 4 8 -10 43.2590 6.51097 2 -4 8 10 42.0421 4.72400 3 -2 -8 10 2.95812 1.77097 7 2 -8 -10 0.12010 6.10117 2 -2 -8 10 0.79402 4.83802 11 -2 8 10 -5.6526 3.83598 3 2 8 -10 -2.0631 5.37503 2 0 -8 10 7.43291 1.98342 7 0 -8 -10 5.65138 6.87880 2 0 -8 10 11.1839 5.33412 11 0 8 10 -0.8837 4.26266 3 0 8 -10 4.21402 6.76786 2 -2 -8 -10 15.4821 7.74083 2 2 -8 10 13.8879 2.29690 7 2 8 10 9.55076 5.42362 3 15 -9 -10 19.8100 7.21933 2 15 9 -10 24.8542 8.26112 2 -15 9 10 27.0881 7.40252 8 -15 9 10 25.2754 7.19991 5 13 -9 -10 161.485 11.9661 2 -13 9 10 174.833 11.9362 5 13 9 -10 174.090 13.8343 2 -13 9 10 196.393 12.1836 8 11 -9 -10 -2.0816 5.95748 2 11 9 -10 0.85184 6.70901 2 -11 9 10 -4.3353 6.34731 8 -11 9 10 4.91289 6.12233 5 9 -9 -10 173.782 11.7554 2 -9 9 10 200.021 11.8731 5 9 9 -10 193.006 12.9285 2 7 -9 -10 4.31548 5.79346 2 -7 9 10 3.82755 3.63185 3 7 9 -10 2.57085 5.74690 2 -7 9 10 0.60599 5.83621 5 -5 -9 10 149.972 11.3906 6 5 -9 -10 144.095 10.8791 2 5 9 -10 147.741 10.8356 2 -5 9 10 145.828 8.30747 3 -5 9 10 144.111 10.6994 5 -3 -9 10 0.03077 4.63556 6 -3 -9 10 -2.8463 5.84198 11 -3 -9 10 2.24701 1.99395 7 3 -9 -10 4.36262 5.95823 2 -3 9 10 2.52409 4.08290 3 -3 9 10 -1.3041 5.99434 5 3 9 -10 1.48456 6.42803 2 -1 -9 10 201.475 11.1830 11 -1 -9 10 212.322 8.26836 7 1 -9 -10 197.027 12.9559 2 -1 9 10 191.918 10.4612 3 -1 -9 -10 5.84024 7.21246 2 1 -9 10 6.09513 6.22873 11 1 -9 10 4.50486 2.16641 7 1 9 10 1.09632 3.29633 3 14 -10 -10 12.9712 7.92653 2 14 10 -10 5.03479 7.28977 2 -14 10 10 13.9111 6.76012 8 -14 10 10 -6.2571 6.67299 5 12 -10 -10 86.3751 8.50136 2 -12 10 10 84.0429 8.50466 8 12 10 -10 102.177 10.2182 2 -12 10 10 77.0817 8.36720 5 10 -10 -10 -0.0062 5.80213 2 10 10 -10 2.12377 6.26312 2 -10 10 10 9.82658 6.55115 5 8 -10 -10 33.2534 6.59181 2 -8 10 10 46.2788 7.11798 5 -8 10 10 34.6730 4.67381 3 8 10 -10 44.9861 8.49246 2 -6 -10 10 16.3553 7.51622 6 6 -10 -10 13.2896 6.07713 2 -6 10 10 13.9174 5.06809 3 -6 10 10 14.7315 6.44919 5 4 -10 -10 40.9587 7.01380 2 -4 -10 10 44.4397 5.92733 11 -4 -10 10 51.9496 3.65636 7 -4 -10 10 30.4265 6.33962 6 -4 10 10 47.2747 5.22673 3 -4 10 10 58.0267 7.49473 5 2 -10 -10 15.6729 6.50533 2 -2 -10 10 16.1367 2.35209 7 -2 -10 10 6.28775 4.88225 6 -2 -10 10 16.1143 5.60044 11 -2 10 10 13.8115 6.65981 5 -2 10 10 13.9316 4.66222 3 0 -10 10 12.6991 2.48102 7 0 -10 10 14.6225 6.64837 11 0 -10 -10 12.0296 6.98692 2 0 10 10 5.59228 3.39484 3 13 -11 -10 5.08800 5.76917 2 13 11 -10 -1.4577 6.52757 2 -13 11 10 5.09912 6.89402 5 -13 11 10 -1.0000 6.47701 8 11 -11 -10 9.20140 5.87896 2 -11 11 10 6.85881 6.60435 8 -11 11 10 6.24445 4.79007 5 9 -11 -10 6.67415 5.70616 2 -9 -11 10 10.0833 6.90773 6 -9 11 10 20.5596 6.84415 5 -7 -11 10 4.34042 6.34138 6 7 -11 -10 8.72765 5.66918 2 -7 11 10 9.19610 6.45223 5 -7 11 10 10.4875 4.27048 3 5 -11 -10 3.51052 5.71892 2 -5 -11 10 -0.4291 5.66742 6 -5 11 10 -2.6164 6.24040 5 -5 11 10 -4.5871 4.09658 3 3 -11 -10 14.5719 6.19418 2 -3 -11 10 16.7831 2.68373 7 -3 -11 10 17.8969 5.53812 11 -3 -11 10 12.6752 5.50078 6 -3 11 10 25.1378 6.88340 5 -3 11 10 11.5779 4.61791 3 1 -11 -10 7.80694 6.63540 2 -1 -11 10 5.09175 2.33979 7 -1 11 10 3.90704 4.51415 3 -1 11 10 1.21488 6.69458 5 10 -12 -10 -1.0675 5.33851 2 -10 -12 10 4.81903 7.08855 6 -10 12 10 -6.0575 6.54972 5 -8 -12 10 10.8376 6.92582 6 8 -12 -10 12.2037 5.42596 2 -8 12 10 9.02427 4.37559 3 -8 12 10 -4.4798 6.40696 5 -6 -12 10 5.41293 7.65512 6 6 -12 -10 7.04399 6.65603 2 -6 12 10 18.6679 6.88293 5 -6 12 10 10.1958 4.59448 3 -4 -12 10 7.45605 2.86856 7 -4 -12 10 6.03820 5.43447 11 4 -12 -10 3.67954 5.65505 2 -4 -12 10 5.16127 5.59605 6 -4 12 10 7.86052 6.79342 5 -4 12 10 4.82548 4.52665 3 9 -13 -10 12.3356 5.32907 2 -9 13 10 13.9629 5.29033 5 7 -13 -10 85.7888 9.00777 2 -7 -13 10 118.444 11.9755 6 -7 13 10 120.163 8.38232 3 -7 13 10 134.843 8.94424 5 5 -13 -10 10.2768 5.65848 2 -5 -13 10 3.20564 5.96537 6 -5 13 10 3.72523 7.73451 5 -5 13 10 9.55311 4.98127 3 -16 0 11 -2.5753 6.59968 8 16 0 -11 -0.1306 8.45286 2 -14 0 11 0.23627 6.11282 8 14 0 -11 -0.8715 7.96219 2 12 0 -11 -0.1898 7.62731 2 -12 0 11 5.96588 5.76232 8 -10 0 11 -2.5199 5.24103 8 10 0 -11 3.01925 7.38031 2 -8 0 11 -3.1175 4.93565 8 8 0 -11 -6.8858 6.89658 2 6 0 -11 -1.2009 6.81170 2 -4 0 11 0.67236 5.08162 5 4 0 -11 2.47295 6.81520 2 2 0 -11 -2.4770 6.70328 2 0 0 11 -1.5466 5.00710 3 0 0 11 0.19900 1.30175 7 0 0 -11 6.21081 7.36485 2 -15 -1 11 54.5461 7.34322 8 15 -1 -11 34.6593 9.37864 2 -15 1 11 56.3971 7.71561 8 15 1 -11 37.6348 9.58013 2 -13 -1 11 3.84443 5.78061 8 13 -1 -11 7.94711 7.70443 2 13 1 -11 -1.5289 7.69696 2 -13 1 11 5.75159 6.16497 8 11 -1 -11 113.613 11.4488 2 -11 -1 11 132.965 9.31855 8 11 1 -11 132.566 12.2530 2 -11 1 11 122.805 9.88914 8 -9 -1 11 -2.0771 4.77109 8 9 -1 -11 -0.7275 7.10016 2 -9 1 11 1.22522 5.35280 8 9 1 -11 1.93024 7.07051 2 -9 1 11 -2.1204 4.54030 5 7 -1 -11 68.2415 9.12476 2 -7 -1 11 63.8831 6.09770 8 -7 1 11 56.6285 6.03305 5 7 1 -11 58.0908 8.63194 2 5 -1 -11 -1.5162 6.62290 2 -5 1 11 -0.5939 4.44057 5 5 1 -11 -3.6544 6.64524 2 3 -1 -11 39.3808 7.98074 2 3 1 -11 29.3271 7.54269 2 1 -1 -11 0.00042 7.10144 2 -1 -1 11 0.70349 1.21857 7 -1 1 11 -0.0419 3.58464 3 1 1 -11 -2.9627 6.79745 2 -16 -2 11 28.2216 6.68620 8 16 -2 -11 16.2004 8.69609 2 16 2 -11 16.5863 8.98488 2 14 -2 -11 22.2519 8.52163 2 -14 -2 11 17.6057 6.09389 8 -14 2 11 20.4470 7.04894 8 14 2 -11 12.2286 8.63415 2 -12 -2 11 -3.8524 5.27074 8 12 -2 -11 3.53682 7.56769 2 -12 2 11 3.13034 6.19572 8 12 2 -11 -0.5748 7.68003 2 -10 -2 11 12.2976 5.02553 8 10 -2 -11 11.7211 7.56873 2 10 2 -11 17.5070 7.87108 2 -10 2 11 16.8056 6.14468 8 -10 2 11 11.6831 4.86832 5 8 -2 -11 11.4916 7.26896 2 -8 -2 11 13.0230 4.65253 8 8 2 -11 9.50072 7.24892 2 -8 2 11 11.9357 4.94353 5 6 -2 -11 4.51470 6.96001 2 -6 -2 11 10.4884 4.19581 8 6 2 -11 7.19091 6.95322 2 -6 2 11 3.56833 4.77531 5 4 -2 -11 24.4148 7.58473 2 4 2 -11 19.3247 7.29452 2 -4 2 11 28.6473 5.71306 5 2 -2 -11 -4.4141 6.77376 2 2 2 -11 1.78234 6.69240 2 0 -2 -11 30.7906 8.24326 2 0 2 -11 27.9202 7.82960 2 0 2 11 37.1353 4.72727 3 0 2 11 40.0018 2.86621 7 15 -3 -11 2.32487 8.16264 2 -15 -3 11 1.85672 5.79986 8 -15 3 11 5.41122 7.10975 8 15 3 -11 5.80962 8.41544 2 -13 -3 11 114.691 8.57795 8 13 -3 -11 84.0929 10.5977 2 -13 3 11 87.0511 8.31154 5 -13 3 11 97.6482 8.95337 8 13 3 -11 101.607 11.1582 2 -11 -3 11 38.4321 5.58054 8 11 -3 -11 24.0183 8.07231 2 -11 3 11 40.3975 7.00296 8 11 3 -11 31.3311 6.56567 2 -11 3 11 33.1526 5.74429 5 9 -3 -11 103.009 10.3863 2 -9 -3 11 118.972 7.97894 8 -9 3 11 98.7213 8.56952 5 9 3 -11 120.791 11.2170 2 -9 3 11 113.880 9.62533 8 7 -3 -11 4.21946 6.96522 2 -7 -3 11 19.6660 4.34005 8 7 3 -11 21.4279 7.50925 2 -7 3 11 13.1633 5.23898 5 5 -3 -11 117.380 10.9340 2 -5 3 11 106.367 8.94382 5 5 3 -11 126.257 11.0033 2 3 -3 -11 21.2755 7.51394 2 3 3 -11 30.2719 7.53223 2 1 -3 -11 29.3019 7.97991 2 -1 3 11 39.2848 4.62570 3 1 3 -11 38.3059 7.74360 2 -14 -4 11 -0.9595 5.20098 8 14 -4 -11 2.39968 7.69010 2 -14 4 11 1.12962 5.46843 5 14 4 -11 -6.1054 8.02456 2 -14 4 11 -0.5665 6.87500 8 -12 -4 11 18.4119 5.07977 8 12 -4 -11 20.0970 7.98595 2 -12 4 11 26.5059 7.13184 8 -12 4 11 15.1453 5.60958 5 12 4 -11 21.8022 8.31380 2 10 -4 -11 0.32457 7.13624 2 -10 -4 11 -1.0693 4.24490 8 10 4 -11 4.50087 7.51717 2 -10 4 11 -4.3228 5.99421 8 -10 4 11 -7.6012 5.08699 5 -8 -4 11 14.7174 6.69407 8 8 -4 -11 25.7098 7.80739 2 8 4 -11 21.6813 7.54496 2 -8 4 11 13.4022 5.49196 5 6 -4 -11 8.33044 6.95974 2 -6 4 11 3.45222 5.34208 5 6 4 -11 10.0872 6.94226 2 4 -4 -11 10.2090 7.07303 2 -4 4 11 -5.3259 5.35733 5 4 4 -11 4.38838 6.80702 2 2 -4 -11 52.4770 8.46692 2 2 4 -11 52.1014 7.96398 2 -2 4 11 63.3675 5.18548 3 0 -4 -11 -7.1451 7.05974 2 0 4 -11 4.25978 6.90745 2 0 4 11 -1.5919 3.79104 3 -15 -5 11 1.95080 5.22305 8 15 -5 -11 7.91192 7.93924 2 -15 5 11 8.92474 7.63174 8 -15 5 11 6.64025 5.93996 5 15 5 -11 -4.2841 8.61400 2 13 -5 -11 17.9227 7.84272 2 -13 -5 11 32.2367 5.49283 8 13 5 -11 32.9106 8.80770 2 -13 5 11 26.6235 6.25650 5 -13 5 11 35.0303 7.54141 8 11 -5 -11 13.7847 7.47048 2 -11 -5 11 2.27755 4.34985 8 -11 5 11 4.30631 5.43612 5 11 5 -11 10.1692 7.92725 2 -11 5 11 11.9282 6.67630 8 9 -5 -11 6.75215 7.06873 2 9 5 -11 15.2459 7.48458 2 -9 5 11 20.2889 5.81331 5 7 -5 -11 5.53020 6.78875 2 7 5 -11 -3.3060 6.81428 2 -7 5 11 -0.2007 5.35564 5 5 -5 -11 8.89923 7.04974 2 5 5 -11 1.76878 6.74067 2 -5 5 11 9.86234 5.72028 5 3 -5 -11 13.5425 7.10826 2 -3 5 11 -0.4916 3.44646 3 3 5 -11 2.78689 6.45557 2 -3 5 11 1.87125 5.85269 5 1 -5 -11 -2.5539 7.02145 2 1 5 -11 4.15291 6.69302 2 -1 5 11 1.89815 3.75323 3 -14 -6 11 3.82771 4.85393 8 14 -6 -11 -7.0728 7.14399 2 -14 6 11 4.97717 7.44408 8 -14 6 11 0.48191 5.92592 5 14 6 -11 -2.4914 8.11172 2 12 -6 -11 22.1109 7.91574 2 -12 6 11 24.1826 7.20086 8 12 6 -11 28.6858 8.57700 2 -12 6 11 24.9093 6.41755 5 10 -6 -11 -5.8577 6.88751 2 -10 6 11 3.32144 6.52337 8 -10 6 11 3.23094 5.80472 5 10 6 -11 2.38044 7.15660 2 8 -6 -11 3.35181 6.99092 2 -8 6 11 5.29279 5.80815 5 8 6 -11 9.68336 7.13812 2 6 6 -11 64.2525 8.42861 2 -6 6 11 59.1146 7.34234 5 4 -6 -11 10.0963 6.98982 2 -4 6 11 -0.7587 3.68805 3 4 6 -11 3.22087 6.52985 2 -4 6 11 2.54038 5.83175 5 2 -6 -11 74.1408 9.22515 2 -2 6 11 74.0841 5.96672 3 2 6 -11 77.5437 8.39574 2 13 -7 -11 58.5548 8.95015 2 -13 7 11 77.7594 8.93907 8 13 7 -11 80.3195 9.94722 2 -13 7 11 78.0506 8.03109 5 11 -7 -11 38.4210 8.08590 2 11 7 -11 54.4125 8.78515 2 -11 7 11 46.0904 7.03258 5 -11 7 11 54.2336 7.86577 8 9 -7 -11 79.2800 9.31929 2 9 7 -11 115.995 10.5819 2 -9 7 11 93.1946 8.49270 5 7 -7 -11 62.8587 8.52511 2 7 7 -11 55.4569 8.17113 2 -7 7 11 58.8165 7.36326 5 5 -7 -11 192.867 13.2908 2 5 7 -11 213.127 12.5929 2 -5 7 11 192.732 12.1031 5 -3 -7 11 94.6055 4.16009 7 3 -7 -11 85.2165 9.51134 2 3 7 -11 102.184 9.50037 2 -3 7 11 100.883 8.65558 5 -3 7 11 88.1749 6.87373 3 12 -8 -11 3.31105 6.90175 2 -12 8 11 10.2372 6.40980 5 12 8 -11 16.6955 7.78179 2 -12 8 11 7.35242 7.24519 8 10 -8 -11 48.4904 8.16936 2 -10 8 11 58.7910 7.57041 5 10 8 -11 64.9275 8.59392 2 8 -8 -11 8.52401 6.78306 2 -8 8 11 -0.5870 5.95650 5 8 8 -11 1.11371 6.64448 2 6 -8 -11 33.5024 7.50239 2 -6 8 11 38.0866 6.92555 5 6 8 -11 35.8756 7.22842 2 4 -8 -11 30.5735 7.49536 2 -4 -8 11 14.8171 6.30698 6 -4 -8 11 30.3198 2.31481 7 -4 8 11 21.2476 4.45082 3 -4 8 11 40.6110 6.99630 5 4 8 -11 21.6835 6.68794 2 11 -9 -11 3.23348 6.64478 2 -11 9 11 5.31177 6.49692 5 11 9 -11 6.02009 7.12597 2 -11 9 11 -4.6360 6.97699 8 9 -9 -11 5.98524 6.63068 2 -9 9 11 -0.6298 4.48680 5 9 9 -11 7.90708 6.73827 2 -7 -9 11 7.75051 6.28105 6 7 -9 -11 6.20528 6.46069 2 7 9 -11 14.5524 6.69557 2 -7 9 11 3.74478 4.51503 5 -5 -9 11 1.48180 5.44477 6 5 -9 -11 0.29253 6.48201 2 -5 9 11 6.55780 4.01473 3 -5 9 11 -3.9980 6.22605 5 8 -10 -11 6.02442 6.34470 2 -12 0 12 60.9810 8.32388 8 12 0 -12 51.3534 9.87028 2 10 0 -12 63.3341 9.92765 2 -10 0 12 91.6040 7.73479 8 -8 0 12 16.4827 5.46476 8 8 0 -12 9.81479 7.96083 2 6 0 -12 151.713 12.6596 2 -6 0 12 134.749 9.17099 8 -11 -1 12 17.5931 5.83856 8 11 -1 -12 8.02785 8.16239 2 11 1 -12 6.46895 8.16843 2 -11 1 12 16.5942 6.29399 8 -9 -1 12 83.1816 7.11466 8 9 -1 -12 67.7489 9.95001 2 -9 1 12 93.0485 7.86602 8 9 1 -12 50.7558 9.53701 2 7 -1 -12 1.09100 7.72438 2 -7 -1 12 13.7290 4.94060 8 -7 1 12 17.1361 5.38608 8 7 1 -12 13.9072 7.99926 2 5 -1 -12 50.6630 8.89699 2 5 1 -12 47.4853 8.86730 2 10 -2 -12 3.74991 7.93246 2 -10 -2 12 4.67639 4.99298 8 10 2 -12 -12.172 7.47057 2 -10 2 12 -2.8090 5.98306 8 -8 -2 12 20.6686 7.62445 8 8 -2 -12 3.53645 7.68569 2 -8 2 12 13.0533 5.95829 8 8 2 -12 4.49374 7.88375 2 6 -2 -12 -4.3456 7.46661 2 6 2 -12 -3.6328 7.46439 2 -11 -3 12 16.2232 5.26668 8 11 -3 -12 9.84987 8.24018 2 11 3 -12 8.52462 8.46273 2 -11 3 12 25.7327 7.88711 8 9 -3 -12 41.9148 7.07147 2 -9 3 12 45.3922 8.55861 5 9 3 -12 50.9063 9.14185 2 -9 3 12 64.4258 7.67206 8 7 -3 -12 2.10099 7.40468 2 7 3 -12 3.41781 7.57078 2 -7 3 12 1.58901 5.15537 5 8 -4 -12 72.4983 9.74552 2 -8 4 12 101.305 8.83912 5 8 4 -12 90.4227 10.0732 2 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details 'SADABS 2014/4' _exptl_absorpt_correction_type multiscan _exptl_absorpt_correction_T_max 0.7479 _exptl_absorpt_correction_T_min 0.3851 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 0.71074 11.915 12.737 6.715 90.001 113.295 90.004 ) ; _shelx_hkl_checksum 34150