data_shelx
_audit_creation_method SHELXL-97
_chemical_name_systematic
;
?
;
_chemical_name_common 'montbrayite'
_chemical_melting_point ?
_chemical_formula_moiety
'Au2 Bi0 Sb0 Te3'
_chemical_formula_sum
'Au2 Bi0 Sb0 Te3'
_chemical_formula_weight 776.73
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
'Au' 'Au' -2.0133 8.8022
'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'Te' 'Te' -0.5308 1.6751
'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'Sb' 'Sb' -0.5866 1.5461
'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'Bi' 'Bi' -4.1077 10.2566
'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_symmetry_cell_setting 'triclinic'
_symmetry_space_group_name_H-M 'P -1'
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
_cell_length_a 10.8045(6)
_cell_length_b 12.1470(6)
_cell_length_c 13.4480(7)
_cell_angle_alpha 108.091(5)
_cell_angle_beta 104.362(5)
_cell_angle_gamma 97.471(5)
_cell_volume 1583.65(14)
_cell_formula_units_Z 12
_cell_measurement_temperature 293(2)
_cell_measurement_reflns_used 1563
_cell_measurement_theta_min 7.5
_cell_measurement_theta_max 13.1
_exptl_crystal_description block
_exptl_crystal_colour black
_exptl_crystal_size_max 0.085
_exptl_crystal_size_mid 0.065
_exptl_crystal_size_min 0.050
_exptl_crystal_density_meas ?
_exptl_crystal_density_diffrn 9.773
_exptl_crystal_density_method 'not measured'
_exptl_crystal_F_000 3768
_exptl_absorpt_coefficient_mu 71.592
_exptl_absorpt_correction_type 'multi-scan'
_exptl_absorpt_correction_T_min 0.925
_exptl_absorpt_correction_T_max 0.988
_exptl_absorpt_process_details
'(ABSPACK; Oxford Diffraction, 2006)'
_exptl_special_details
;
?
;
_diffrn_ambient_temperature 293(2)
_diffrn_radiation_wavelength 0.71073
_diffrn_radiation_type MoK\a
_diffrn_radiation_source 'fine-focus sealed tube'
_diffrn_radiation_monochromator graphite
_diffrn_measurement_device_type 'Oxford Xcalibur 3'
_diffrn_measurement_method '\w scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number ?
_diffrn_standards_interval_count .
_diffrn_standards_interval_time .
_diffrn_standards_decay_% ?
_diffrn_reflns_number 30597
_diffrn_reflns_av_R_equivalents 0.0702
_diffrn_reflns_av_sigmaI/netI 0.0811
_diffrn_reflns_limit_h_min -15
_diffrn_reflns_limit_h_max 15
_diffrn_reflns_limit_k_min -17
_diffrn_reflns_limit_k_max 17
_diffrn_reflns_limit_l_min -18
_diffrn_reflns_limit_l_max 18
_diffrn_reflns_theta_min 3.99
_diffrn_reflns_theta_max 30.00
_reflns_number_total 9195
_reflns_number_gt 5145
_reflns_threshold_expression >2sigma(I)
_computing_data_collection 'CrysAlis (Oxford Diffraction, 2006)'
_computing_cell_refinement 'CrysAlis (Oxford Diffraction, 2006)'
_computing_data_reduction 'CrysAlis (Oxford Diffraction, 2006)'
_computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)'
_computing_structure_refinement 'SHELXL-97 (Sheldrick, 2008)'
_computing_molecular_graphics 'DIAMOND (Brandenburg, 2001)'
_computing_publication_material 'SHELXL-97 (Sheldrick, 2008)'
_refine_special_details
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type full
_refine_ls_weighting_scheme calc
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0577P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary direct
_atom_sites_solution_secondary difmap
_atom_sites_solution_hydrogens .
_refine_ls_hydrogen_treatment .
_refine_ls_extinction_method SHELXL
_refine_ls_extinction_coef 0.000354(16)
_refine_ls_extinction_expression
'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^'
_refine_ls_number_reflns 9195
_refine_ls_number_parameters 291
_refine_ls_number_restraints 0
_refine_ls_R_factor_all 0.1141
_refine_ls_R_factor_gt 0.0636
_refine_ls_wR_factor_ref 0.1913
_refine_ls_wR_factor_gt 0.1476
_refine_ls_goodness_of_fit_ref 1.020
_refine_ls_restrained_S_all 1.020
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.15833(7) 0.42458(7) 0.32381(6) 0.0129(3) Uani 0.872(9) 1 d P . .
Sb1 Sb 0.15833(7) 0.42458(7) 0.32381(6) 0.0129(3) Uani 0.128(9) 1 d P . .
Au2 Au -0.09742(7) 0.34589(7) 0.01427(6) 0.0133(3) Uani 0.960(9) 1 d P . .
Sb2 Sb -0.09742(7) 0.34589(7) 0.01427(6) 0.0133(3) Uani 0.040(9) 1 d P . .
Au3 Au 0.64203(7) 0.26047(7) 0.69800(6) 0.0137(3) Uani 0.951(9) 1 d P . .
Sb3 Sb 0.64203(7) 0.26047(7) 0.69800(6) 0.0137(3) Uani 0.049(9) 1 d P . .
Au4 Au 0.37677(7) 0.17845(8) 0.38274(6) 0.0131(3) Uani 0.879(9) 1 d P . .
Sb4 Sb 0.37677(7) 0.17845(8) 0.38274(6) 0.0131(3) Uani 0.121(9) 1 d P . .
Au5 Au 0.42152(7) 0.50241(7) 0.63161(6) 0.0138(3) Uani 0.934(10) 1 d P . .
Sb5 Sb 0.42152(7) 0.50241(7) 0.63161(6) 0.0138(3) Uani 0.066(10) 1 d P . .
Au6 Au 0.12410(7) 0.10291(8) 0.07485(6) 0.0136(3) Uani 0.942(9) 1 d P . .
Sb6 Sb 0.12410(7) 0.10291(8) 0.07485(6) 0.0136(3) Uani 0.058(9) 1 d P . .
Au7 Au 0.68990(7) 0.58561(7) 0.93528(6) 0.0131(3) Uani 0.966(10) 1 d P . .
Sb7 Sb 0.68990(7) 0.58561(7) 0.93528(6) 0.0131(3) Uani 0.034(10) 1 d P . .
Au8 Au 0.21231(6) 0.75086(7) 0.56850(6) 0.0131(3) Uani 0.971(10) 1 d P . .
Sb8 Sb 0.21231(6) 0.75086(7) 0.56850(6) 0.0131(3) Uani 0.029(10) 1 d P . .
Au9 Au -0.04847(7) 0.67199(7) 0.25444(6) 0.0137(3) Uani 0.960(10) 1 d P . .
Sb9 Sb -0.04847(7) 0.67199(7) 0.25444(6) 0.0137(3) Uani 0.040(10) 1 d P . .
Au10 Au 0.47876(6) 0.82643(7) 0.87477(6) 0.0132(3) Uani 0.982(10) 1 d P . .
Sb10 Sb 0.47876(6) 0.82643(7) 0.87477(6) 0.0132(3) Uani 0.018(10) 1 d P . .
Au11 Au -0.73828(6) 0.08731(7) -0.18652(6) 0.0128(3) Uani 0.951(10) 1 d P . .
Sb11 Sb -0.73828(6) 0.08731(7) -0.18652(6) 0.0128(3) Uani 0.049(10) 1 d P . .
Au12 Au 0.0000 0.0000 0.5000 0.0147(4) Uani 0.958(13) 2 d SP . .
Sb12 Sb 0.0000 0.0000 0.5000 0.0147(4) Uani 0.042(13) 2 d SP . .
Te1 Te 0.01945(11) 0.56304(12) 0.42757(11) 0.0139(3) Uani 1 1 d . . .
Te2 Te -0.54179(11) 0.26403(12) -0.03781(11) 0.0145(3) Uani 1 1 d . . .
Te3 Te 0.12471(12) 0.53845(12) 0.16493(11) 0.0186(3) Uani 1 1 d . . .
Te4 Te 0.09102(11) 0.24570(12) -0.04981(11) 0.0148(3) Uani 1 1 d . . .
Te5 Te -0.30731(11) -0.00740(12) 0.01131(10) 0.0146(3) Uani 1 1 d . . .
Te6 Te -0.19436(11) 0.82191(12) 0.35247(10) 0.0136(3) Uani 1 1 d . . .
Te7 Te 0.27542(12) 0.64944(13) 0.73849(11) 0.0164(3) Uani 1 1 d . . .
Te8 Te -0.06447(11) 0.09440(12) 0.32360(10) 0.0141(3) Uani 1 1 d . . .
Te9 Te 0.35301(12) 0.33300(14) 0.25998(13) 0.0246(4) Uani 1 1 d . . .
Te10 Te -0.31010(12) 0.16036(12) -0.13046(10) 0.0143(3) Uani 1 1 d . . .
Te11 Te 0.17414(11) -0.17029(12) 0.38476(11) 0.0153(3) Uani 1 1 d . . .
Te12 Te 0.43687(11) -0.09305(12) 0.70308(11) 0.0147(3) Uani 1 1 d . . .
Te13 Te 0.23487(12) 0.31847(13) 0.48178(11) 0.0171(3) Uani 1 1 d . . .
Te14 Te 0.50009(11) 0.40106(12) 0.79286(10) 0.0134(3) Uani 1 1 d . . .
Te15 Te 0.42700(11) 0.07926(12) 0.54567(11) 0.0138(3) Uani 1 1 d . . .
Te16 Te -0.03401(12) 0.22026(13) 0.17294(11) 0.0167(3) Uani 1 1 d . . .
Te17 Te 0.16059(11) -0.00696(12) 0.22455(11) 0.0149(3) Uani 1 1 d . . .
Te18 Te -0.23927(11) 0.48704(12) 0.10831(10) 0.0132(3) Uani 1 1 d . . .
T19T Te 0.60688(9) 0.38095(10) 0.53111(9) 0.0321(4) Uani 0.261(10) 1 d P . .
T19B Bi 0.60688(9) 0.38095(10) 0.53111(9) 0.0321(4) Uani 0.739(10) 1 d P . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Au1 0.0138(4) 0.0125(5) 0.0152(5) 0.0075(4) 0.0058(3) 0.0035(3)
Sb1 0.0138(4) 0.0125(5) 0.0152(5) 0.0075(4) 0.0058(3) 0.0035(3)
Au2 0.0138(4) 0.0118(5) 0.0155(4) 0.0060(3) 0.0049(3) 0.0037(3)
Sb2 0.0138(4) 0.0118(5) 0.0155(4) 0.0060(3) 0.0049(3) 0.0037(3)
Au3 0.0139(4) 0.0116(5) 0.0166(4) 0.0055(3) 0.0059(3) 0.0031(3)
Sb3 0.0139(4) 0.0116(5) 0.0166(4) 0.0055(3) 0.0059(3) 0.0031(3)
Au4 0.0149(4) 0.0118(5) 0.0158(5) 0.0069(4) 0.0069(3) 0.0048(3)
Sb4 0.0149(4) 0.0118(5) 0.0158(5) 0.0069(4) 0.0069(3) 0.0048(3)
Au5 0.0135(4) 0.0107(5) 0.0163(5) 0.0053(3) 0.0033(3) 0.0008(3)
Sb5 0.0135(4) 0.0107(5) 0.0163(5) 0.0053(3) 0.0033(3) 0.0008(3)
Au6 0.0159(4) 0.0128(4) 0.0152(4) 0.0074(3) 0.0061(3) 0.0054(3)
Sb6 0.0159(4) 0.0128(4) 0.0152(4) 0.0074(3) 0.0061(3) 0.0054(3)
Au7 0.0128(4) 0.0105(5) 0.0148(4) 0.0042(3) 0.0033(3) 0.0011(3)
Sb7 0.0128(4) 0.0105(5) 0.0148(4) 0.0042(3) 0.0033(3) 0.0011(3)
Au8 0.0132(4) 0.0117(5) 0.0142(4) 0.0056(3) 0.0037(3) 0.0003(3)
Sb8 0.0132(4) 0.0117(5) 0.0142(4) 0.0056(3) 0.0037(3) 0.0003(3)
Au9 0.0132(4) 0.0107(5) 0.0162(5) 0.0042(3) 0.0037(3) 0.0015(3)
Sb9 0.0132(4) 0.0107(5) 0.0162(5) 0.0042(3) 0.0037(3) 0.0015(3)
Au10 0.0136(4) 0.0123(5) 0.0137(4) 0.0066(3) 0.0033(3) -0.0007(3)
Sb10 0.0136(4) 0.0123(5) 0.0137(4) 0.0066(3) 0.0033(3) -0.0007(3)
Au11 0.0140(4) 0.0105(5) 0.0131(4) 0.0052(3) 0.0028(3) 0.0000(3)
Sb11 0.0140(4) 0.0105(5) 0.0131(4) 0.0052(3) 0.0028(3) 0.0000(3)
Au12 0.0163(5) 0.0113(6) 0.0135(6) 0.0048(5) 0.0005(4) 0.0003(4)
Sb12 0.0163(5) 0.0113(6) 0.0135(6) 0.0048(5) 0.0005(4) 0.0003(4)
Te1 0.0122(5) 0.0125(7) 0.0170(6) 0.0061(5) 0.0049(5) 0.0001(5)
Te2 0.0134(5) 0.0127(7) 0.0172(6) 0.0065(5) 0.0032(5) 0.0025(5)
Te3 0.0232(6) 0.0170(8) 0.0232(7) 0.0148(6) 0.0088(5) 0.0068(6)
Te4 0.0132(5) 0.0128(7) 0.0189(7) 0.0060(6) 0.0059(5) 0.0019(5)
Te5 0.0140(5) 0.0121(7) 0.0167(6) 0.0053(5) 0.0047(5) -0.0013(5)
Te6 0.0142(5) 0.0122(7) 0.0153(6) 0.0068(5) 0.0051(5) 0.0001(5)
Te7 0.0135(5) 0.0154(7) 0.0182(7) 0.0047(6) 0.0035(5) 0.0023(5)
Te8 0.0152(5) 0.0122(7) 0.0152(6) 0.0056(5) 0.0052(5) 0.0007(5)
Te9 0.0159(6) 0.0215(8) 0.0310(8) 0.0018(7) 0.0091(5) 0.0006(6)
Te10 0.0169(6) 0.0140(7) 0.0147(6) 0.0073(5) 0.0060(5) 0.0048(5)
Te11 0.0138(5) 0.0128(7) 0.0188(7) 0.0053(6) 0.0060(5) 0.0000(5)
Te12 0.0131(5) 0.0140(7) 0.0172(6) 0.0064(5) 0.0054(5) -0.0001(5)
Te13 0.0135(6) 0.0137(7) 0.0204(7) 0.0022(6) 0.0045(5) 0.0017(5)
Te14 0.0147(6) 0.0096(6) 0.0150(6) 0.0042(5) 0.0039(5) 0.0015(5)
Te15 0.0153(5) 0.0113(7) 0.0172(6) 0.0076(5) 0.0058(5) 0.0033(5)
Te16 0.0158(6) 0.0177(7) 0.0179(7) 0.0088(6) 0.0053(5) 0.0018(5)
Te17 0.0156(6) 0.0119(7) 0.0162(6) 0.0043(5) 0.0036(5) 0.0038(5)
Te18 0.0137(5) 0.0101(6) 0.0158(6) 0.0043(5) 0.0054(5) 0.0023(5)
T19T 0.0321(6) 0.0339(7) 0.0406(7) 0.0211(6) 0.0172(5) 0.0106(5)
T19B 0.0321(6) 0.0339(7) 0.0406(7) 0.0211(6) 0.0172(5) 0.0106(5)
_geom_special_details
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 Te1 2.6954(15) . ?
Au1 Te9 2.7037(15) . ?
Au1 Te13 2.8221(18) . ?
Au1 Te16 2.8345(15) . ?
Au1 Te3 2.8620(17) . ?
Au1 T19B 2.9910(13) 2_666 ?
Au1 T19T 2.9910(13) 2_666 ?
Au2 Te18 2.6807(15) . ?
Au2 Te4 2.6893(14) . ?
Au2 Te10 2.8032(15) . ?
Au2 Te3 2.9190(15) . ?
Au2 Te16 2.9866(18) . ?
Au2 Te3 3.1188(17) 2_565 ?
Au3 Te14 2.6822(15) . ?
Au3 Te11 2.6997(14) 2_656 ?
Au3 Te15 2.8192(15) . ?
Au3 Te10 2.8951(17) 1_656 ?
Au3 Te3 3.0023(16) 2_666 ?
Au3 T19T 3.0142(15) . ?
Au4 Te13 2.7021(15) . ?
Au4 Te12 2.7230(14) 2_656 ?
Au4 Te15 2.7869(17) . ?
Au4 Te9 2.856(2) . ?
Au4 Te17 2.8714(15) . ?
Au4 T19T 3.0189(14) . ?
Au5 Te13 2.6713(15) . ?
Au5 Te9 2.6867(15) 2_666 ?
Au5 Te14 2.8206(17) . ?
Au5 Te7 2.8305(15) . ?
Au5 T19B 2.9317(15) 2_666 ?
Au5 T19T 2.9317(15) 2_666 ?
Au5 T19T 2.9811(12) . ?
Au6 Te16 2.6969(15) . ?
Au6 Te17 2.7205(18) . ?
Au6 Te5 2.7399(15) 2 ?
Au6 Te4 2.7598(18) . ?
Au6 Sb6 3.1540(16) 2 ?
Au6 Au6 3.1540(16) 2 ?
Au6 Te9 3.3095(16) . ?
Au7 Te14 2.6625(14) . ?
Au7 Te4 2.6728(14) 2_666 ?
Au7 Te2 2.8440(14) 2_566 ?
Au7 Te18 2.9187(17) 1_656 ?
Au7 Te3 2.9937(15) 2_666 ?
Au7 Te9 3.036(2) 2_666 ?
Au8 Te12 2.6928(14) 1_565 ?
Au8 Te1 2.6941(14) . ?
Au8 Te11 2.8741(17) 1_565 ?
Au8 Te7 2.8987(18) . ?
Au8 Te8 2.9029(14) 2_566 ?
Au8 T19B 2.9923(12) 2_666 ?
Au8 T19T 2.9923(12) 2_666 ?
Au9 Te11 2.6744(14) 1_565 ?
Au9 Te18 2.6838(14) . ?
Au9 Te6 2.7974(15) . ?
Au9 Te3 2.8767(14) . ?
Au9 Te1 3.0050(17) . ?
Au9 Te4 3.1597(17) 2_565 ?
Au10 Te7 2.6712(14) . ?
Au10 Te5 2.6772(14) 1_666 ?
Au10 Te2 2.7255(17) 2_566 ?
Au10 Te12 2.7371(17) 1_565 ?
Au10 Te9 3.2722(16) 2_666 ?
Au11 Te8 2.6670(14) 2_455 ?
Au11 Te2 2.6753(14) . ?
Au11 Te6 2.7671(16) 2_465 ?
Au11 Te5 2.7759(16) 2_455 ?
Au11 Te4 3.3001(14) 1_455 ?
Au12 Te6 2.6668(12) 1_545 ?
Au12 Te6 2.6668(12) 2_566 ?
Au12 Te8 2.9163(15) 2_556 ?
Au12 Te8 2.9163(15) . ?
Au12 Te11 3.2694(13) . ?
Au12 Te11 3.2694(13) 2_556 ?
Te1 Te1 2.900(3) 2_566 ?
Te2 Sb10 2.7255(17) 2_566 ?
Te2 Au10 2.7255(17) 2_566 ?
Te2 Au7 2.8440(14) 2_566 ?
Te2 Sb7 2.8440(14) 2_566 ?
Te3 Sb7 2.9937(15) 2_666 ?
Te3 Au7 2.9937(15) 2_666 ?
Te3 Sb3 3.0023(16) 2_666 ?
Te3 Au3 3.0023(16) 2_666 ?
Te3 Au2 3.1188(17) 2_565 ?
Te3 Sb2 3.1188(17) 2_565 ?
Te4 Sb7 2.6728(14) 2_666 ?
Te4 Au7 2.6728(14) 2_666 ?
Te4 Sb9 3.1597(17) 2_565 ?
Te4 Au9 3.1597(17) 2_565 ?
Te4 Au11 3.3001(14) 1_655 ?
Te5 Sb10 2.6772(13) 1_444 ?
Te5 Au10 2.6772(13) 1_444 ?
Te5 Au6 2.7399(15) 2 ?
Te5 Sb6 2.7399(15) 2 ?
Te5 Sb11 2.7759(16) 2_455 ?
Te5 Au11 2.7759(16) 2_455 ?
Te5 Te10 3.192(2) . ?
Te6 Sb12 2.6668(12) 1_565 ?
Te6 Au12 2.6668(12) 1_565 ?
Te6 Sb11 2.7671(16) 2_465 ?
Te6 Au11 2.7671(16) 2_465 ?
Te7 Te18 3.082(2) 2_566 ?
Te8 Sb11 2.6670(14) 2_455 ?
Te8 Au11 2.6670(14) 2_455 ?
Te8 Sb8 2.9029(14) 2_566 ?
Te8 Au8 2.9029(14) 2_566 ?
Te8 Te16 2.945(2) . ?
Te9 Sb5 2.6867(15) 2_666 ?
Te9 Au5 2.6867(15) 2_666 ?
Te9 Sb7 3.036(2) 2_666 ?
Te9 Au7 3.036(2) 2_666 ?
Te9 Sb10 3.2722(16) 2_666 ?
Te9 Au10 3.2722(16) 2_666 ?
Te10 Te17 2.8310(18) 2 ?
Te10 Sb3 2.8951(17) 1_454 ?
Te10 Au3 2.8951(17) 1_454 ?
Te11 Sb9 2.6744(14) 1_545 ?
Te11 Au9 2.6744(14) 1_545 ?
Te11 Sb3 2.6997(14) 2_656 ?
Te11 Au3 2.6997(14) 2_656 ?
Te11 Sb8 2.8741(17) 1_545 ?
Te11 Au8 2.8741(17) 1_545 ?
Te12 Sb8 2.6928(14) 1_545 ?
Te12 Au8 2.6928(14) 1_545 ?
Te12 Au4 2.7230(14) 2_656 ?
Te12 Sb4 2.7230(14) 2_656 ?
Te12 Sb10 2.7371(17) 1_545 ?
Te12 Au10 2.7371(17) 1_545 ?
Te15 Te15 2.826(2) 2_656 ?
Te17 Te10 2.8310(18) 2 ?
Te18 Sb7 2.9188(17) 1_454 ?
Te18 Au7 2.9188(17) 1_454 ?
Te18 Te7 3.082(2) 2_566 ?
T19T Sb5 2.9317(15) 2_666 ?
T19T Au5 2.9317(15) 2_666 ?
T19T Sb1 2.9910(13) 2_666 ?
T19T Au1 2.9910(13) 2_666 ?
T19T Sb8 2.9923(12) 2_666 ?
T19T Au8 2.9923(12) 2_666 ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Te1 Au1 Te9 164.41(5) . . ?
Te1 Au1 Te13 96.97(5) . . ?
Te9 Au1 Te13 80.34(5) . . ?
Te1 Au1 Te16 103.76(5) . . ?
Te9 Au1 Te16 91.77(5) . . ?
Te13 Au1 Te16 94.12(5) . . ?
Te1 Au1 Te3 89.36(5) . . ?
Te9 Au1 Te3 91.72(5) . . ?
Te13 Au1 Te3 170.65(5) . . ?
Te16 Au1 Te3 91.03(5) . . ?
Te1 Au1 T19B 85.73(4) . 2_666 ?
Te9 Au1 T19B 78.73(4) . 2_666 ?
Te13 Au1 T19B 84.19(4) . 2_666 ?
Te16 Au1 T19B 170.50(4) . 2_666 ?
Te3 Au1 T19B 89.45(4) . 2_666 ?
Te1 Au1 T19T 85.73(4) . 2_666 ?
Te9 Au1 T19T 78.73(4) . 2_666 ?
Te13 Au1 T19T 84.19(4) . 2_666 ?
Te16 Au1 T19T 170.50(4) . 2_666 ?
Te3 Au1 T19T 89.45(4) . 2_666 ?
T19B Au1 T19T 0.00(7) 2_666 2_666 ?
Te18 Au2 Te4 166.94(5) . . ?
Te18 Au2 Te10 96.40(4) . . ?
Te4 Au2 Te10 96.65(4) . . ?
Te18 Au2 Te3 83.80(4) . . ?
Te4 Au2 Te3 83.16(4) . . ?
Te10 Au2 Te3 179.78(5) . . ?
Te18 Au2 Te16 99.82(5) . . ?
Te4 Au2 Te16 80.02(5) . . ?
Te10 Au2 Te16 92.91(5) . . ?
Te3 Au2 Te16 86.97(4) . . ?
Te18 Au2 Te3 89.54(5) . 2_565 ?
Te4 Au2 Te3 90.22(5) . 2_565 ?
Te10 Au2 Te3 88.81(4) . 2_565 ?
Te3 Au2 Te3 91.28(4) . 2_565 ?
Te16 Au2 Te3 170.22(4) . 2_565 ?
Te14 Au3 Te11 165.91(5) . 2_656 ?
Te14 Au3 Te15 96.21(4) . . ?
Te11 Au3 Te15 95.85(4) 2_656 . ?
Te14 Au3 Te10 92.30(5) . 1_656 ?
Te11 Au3 Te10 93.30(5) 2_656 1_656 ?
Te15 Au3 Te10 97.57(5) . 1_656 ?
Te14 Au3 Te3 86.13(4) . 2_666 ?
Te11 Au3 Te3 81.02(4) 2_656 2_666 ?
Te15 Au3 Te3 172.51(5) . 2_666 ?
Te10 Au3 Te3 89.42(4) 1_656 2_666 ?
Te14 Au3 T19T 86.66(4) . . ?
Te11 Au3 T19T 86.82(4) 2_656 . ?
Te15 Au3 T19T 86.61(4) . . ?
Te10 Au3 T19T 175.79(5) 1_656 . ?
Te3 Au3 T19T 86.43(4) 2_666 . ?
Te13 Au4 Te12 164.97(6) . 2_656 ?
Te13 Au4 Te15 92.50(5) . . ?
Te12 Au4 Te15 93.49(5) 2_656 . ?
Te13 Au4 Te9 79.77(5) . . ?
Te12 Au4 Te9 91.42(5) 2_656 . ?
Te15 Au4 Te9 166.06(5) . . ?
Te13 Au4 Te17 97.39(4) . . ?
Te12 Au4 Te17 95.40(4) 2_656 . ?
Te15 Au4 Te17 98.12(5) . . ?
Te9 Au4 Te17 94.39(5) . . ?
Te13 Au4 T19T 84.12(4) . . ?
Te12 Au4 T19T 82.43(4) 2_656 . ?
Te15 Au4 T19T 87.09(4) . . ?
Te9 Au4 T19T 80.63(4) . . ?
Te17 Au4 T19T 174.49(5) . . ?
Te13 Au5 Te9 163.36(6) . 2_666 ?
Te13 Au5 Te14 98.88(5) . . ?
Te9 Au5 Te14 85.98(5) 2_666 . ?
Te13 Au5 Te7 102.59(4) . . ?
Te9 Au5 Te7 92.51(5) 2_666 . ?
Te14 Au5 Te7 97.04(5) . . ?
Te13 Au5 T19B 88.06(5) . 2_666 ?
Te9 Au5 T19B 85.08(5) 2_666 2_666 ?
Te14 Au5 T19B 169.11(4) . 2_666 ?
Te7 Au5 T19B 89.55(4) . 2_666 ?
Te13 Au5 T19T 88.06(5) . 2_666 ?
Te9 Au5 T19T 85.08(5) 2_666 2_666 ?
Te14 Au5 T19T 169.11(4) . 2_666 ?
Te7 Au5 T19T 89.55(4) . 2_666 ?
T19B Au5 T19T 0.00(5) 2_666 2_666 ?
Te13 Au5 T19T 85.39(4) . . ?
Te9 Au5 T19T 79.17(4) 2_666 . ?
Te14 Au5 T19T 84.86(4) . . ?
Te7 Au5 T19T 171.35(5) . . ?
T19B Au5 T19T 87.37(4) 2_666 . ?
T19T Au5 T19T 87.37(4) 2_666 . ?
Te16 Au6 Te17 89.30(5) . . ?
Te16 Au6 Te5 173.30(5) . 2 ?
Te17 Au6 Te5 91.78(5) . 2 ?
Te16 Au6 Te4 84.13(5) . . ?
Te17 Au6 Te4 171.13(5) . . ?
Te5 Au6 Te4 94.07(5) 2 . ?
Te16 Au6 Sb6 88.36(4) . 2 ?
Te17 Au6 Sb6 88.97(5) . 2 ?
Te5 Au6 Sb6 98.27(4) 2 2 ?
Te4 Au6 Sb6 96.76(4) . 2 ?
Te16 Au6 Au6 88.36(4) . 2 ?
Te17 Au6 Au6 88.97(5) . 2 ?
Te5 Au6 Au6 98.27(4) 2 2 ?
Te4 Au6 Au6 96.76(4) . 2 ?
Sb6 Au6 Au6 0.00(6) 2 2 ?
Te16 Au6 Te9 82.25(4) . . ?
Te17 Au6 Te9 87.78(5) . . ?
Te5 Au6 Te9 91.18(4) 2 . ?
Te4 Au6 Te9 85.45(5) . . ?
Sb6 Au6 Te9 170.10(5) 2 . ?
Au6 Au6 Te9 170.10(5) 2 . ?
Te14 Au7 Te4 168.07(5) . 2_666 ?
Te14 Au7 Te2 101.01(4) . 2_566 ?
Te4 Au7 Te2 90.05(4) 2_666 2_566 ?
Te14 Au7 Te18 97.27(5) . 1_656 ?
Te4 Au7 Te18 86.03(4) 2_666 1_656 ?
Te2 Au7 Te18 95.39(4) 2_566 1_656 ?
Te14 Au7 Te3 86.65(4) . 2_666 ?
Te4 Au7 Te3 82.01(4) 2_666 2_666 ?
Te2 Au7 Te3 171.28(5) 2_566 2_666 ?
Te18 Au7 Te3 87.70(4) 1_656 2_666 ?
Te14 Au7 Te9 82.20(5) . 2_666 ?
Te4 Au7 Te9 92.68(5) 2_666 2_666 ?
Te2 Au7 Te9 93.82(5) 2_566 2_666 ?
Te18 Au7 Te9 170.71(5) 1_656 2_666 ?
Te3 Au7 Te9 83.01(4) 2_666 2_666 ?
Te12 Au8 Te1 168.30(5) 1_565 . ?
Te12 Au8 Te11 99.43(5) 1_565 1_565 ?
Te1 Au8 Te11 83.80(4) . 1_565 ?
Te12 Au8 Te7 80.11(4) 1_565 . ?
Te1 Au8 Te7 94.98(5) . . ?
Te11 Au8 Te7 171.25(5) 1_565 . ?
Te12 Au8 Te8 89.65(4) 1_565 2_566 ?
Te1 Au8 Te8 101.36(4) . 2_566 ?
Te11 Au8 Te8 94.45(5) 1_565 2_566 ?
Te7 Au8 Te8 94.29(4) . 2_566 ?
Te12 Au8 T19B 83.44(4) 1_565 2_666 ?
Te1 Au8 T19B 85.72(4) . 2_666 ?
Te11 Au8 T19B 84.18(4) 1_565 2_666 ?
Te7 Au8 T19B 87.09(4) . 2_666 ?
Te8 Au8 T19B 172.62(4) 2_566 2_666 ?
Te12 Au8 T19T 83.44(4) 1_565 2_666 ?
Te1 Au8 T19T 85.72(4) . 2_666 ?
Te11 Au8 T19T 84.18(4) 1_565 2_666 ?
Te7 Au8 T19T 87.09(4) . 2_666 ?
Te8 Au8 T19T 172.62(4) 2_566 2_666 ?
T19B Au8 T19T 0.00(7) 2_666 2_666 ?
Te11 Au9 Te18 168.36(5) 1_565 . ?
Te11 Au9 Te6 90.35(4) 1_565 . ?
Te18 Au9 Te6 101.28(4) . . ?
Te11 Au9 Te3 83.82(4) 1_565 . ?
Te18 Au9 Te3 84.57(4) . . ?
Te6 Au9 Te3 174.03(5) . . ?
Te11 Au9 Te1 81.64(4) 1_565 . ?
Te18 Au9 Te1 96.34(5) . . ?
Te6 Au9 Te1 97.15(4) . . ?
Te3 Au9 Te1 83.28(4) . . ?
Te11 Au9 Te4 98.69(5) 1_565 2_565 ?
Te18 Au9 Te4 81.17(4) . 2_565 ?
Te6 Au9 Te4 93.55(4) . 2_565 ?
Te3 Au9 Te4 86.11(4) . 2_565 ?
Te1 Au9 Te4 169.29(4) . 2_565 ?
Te7 Au10 Te5 176.03(5) . 1_666 ?
Te7 Au10 Te2 97.36(5) . 2_566 ?
Te5 Au10 Te2 80.39(5) 1_666 2_566 ?
Te7 Au10 Te12 83.50(5) . 1_565 ?
Te5 Au10 Te12 98.38(5) 1_666 1_565 ?
Te2 Au10 Te12 173.64(5) 2_566 1_565 ?
Te7 Au10 Te9 83.61(4) . 2_666 ?
Te5 Au10 Te9 93.13(4) 1_666 2_666 ?
Te2 Au10 Te9 91.02(5) 2_566 2_666 ?
Te12 Au10 Te9 82.81(5) 1_565 2_666 ?
Te8 Au11 Te2 176.01(5) 2_455 . ?
Te8 Au11 Te6 82.86(4) 2_455 2_465 ?
Te2 Au11 Te6 100.93(5) . 2_465 ?
Te8 Au11 Te5 96.58(5) 2_455 2_455 ?
Te2 Au11 Te5 79.51(4) . 2_455 ?
Te6 Au11 Te5 173.44(5) 2_465 2_455 ?
Te8 Au11 Te4 97.91(4) 2_455 1_455 ?
Te2 Au11 Te4 80.87(4) . 1_455 ?
Te6 Au11 Te4 91.12(4) 2_465 1_455 ?
Te5 Au11 Te4 82.48(4) 2_455 1_455 ?
Te6 Au12 Te6 180.0 1_545 2_566 ?
Te6 Au12 Te8 99.92(4) 1_545 2_556 ?
Te6 Au12 Te8 80.08(4) 2_566 2_556 ?
Te6 Au12 Te8 80.08(4) 1_545 . ?
Te6 Au12 Te8 99.92(4) 2_566 . ?
Te8 Au12 Te8 180.0 2_556 . ?
Te6 Au12 Te11 80.99(3) 1_545 . ?
Te6 Au12 Te11 99.01(3) 2_566 . ?
Te8 Au12 Te11 86.35(4) 2_556 . ?
Te8 Au12 Te11 93.65(4) . . ?
Te6 Au12 Te11 99.01(3) 1_545 2_556 ?
Te6 Au12 Te11 80.99(3) 2_566 2_556 ?
Te8 Au12 Te11 93.65(4) 2_556 2_556 ?
Te8 Au12 Te11 86.35(4) . 2_556 ?
Te11 Au12 Te11 180.0 . 2_556 ?
Au8 Te1 Au1 100.72(4) . . ?
Au8 Te1 Te1 100.52(6) . 2_566 ?
Au1 Te1 Te1 97.96(7) . 2_566 ?
Au8 Te1 Au9 94.57(5) . . ?
Au1 Te1 Au9 93.73(5) . . ?
Te1 Te1 Au9 158.80(7) 2_566 . ?
Au11 Te2 Sb10 100.38(5) . 2_566 ?
Au11 Te2 Au10 100.38(5) . 2_566 ?
Sb10 Te2 Au10 0.00(3) 2_566 2_566 ?
Au11 Te2 Au7 99.36(4) . 2_566 ?
Sb10 Te2 Au7 94.44(5) 2_566 2_566 ?
Au10 Te2 Au7 94.44(5) 2_566 2_566 ?
Au11 Te2 Sb7 99.36(4) . 2_566 ?
Sb10 Te2 Sb7 94.44(5) 2_566 2_566 ?
Au10 Te2 Sb7 94.44(5) 2_566 2_566 ?
Au7 Te2 Sb7 0.00(3) 2_566 2_566 ?
Au1 Te3 Au9 93.07(5) . . ?
Au1 Te3 Au2 91.03(5) . . ?
Au9 Te3 Au2 90.92(4) . . ?
Au1 Te3 Sb7 91.04(4) . 2_666 ?
Au9 Te3 Sb7 175.48(6) . 2_666 ?
Au2 Te3 Sb7 90.89(4) . 2_666 ?
Au1 Te3 Au7 91.04(4) . 2_666 ?
Au9 Te3 Au7 175.48(6) . 2_666 ?
Au2 Te3 Au7 90.89(4) . 2_666 ?
Sb7 Te3 Au7 0.00(4) 2_666 2_666 ?
Au1 Te3 Sb3 93.45(4) . 2_666 ?
Au9 Te3 Sb3 91.40(4) . 2_666 ?
Au2 Te3 Sb3 174.84(6) . 2_666 ?
Sb7 Te3 Sb3 86.48(4) 2_666 2_666 ?
Au7 Te3 Sb3 86.48(4) 2_666 2_666 ?
Au1 Te3 Au3 93.45(4) . 2_666 ?
Au9 Te3 Au3 91.40(4) . 2_666 ?
Au2 Te3 Au3 174.84(6) . 2_666 ?
Sb7 Te3 Au3 86.48(4) 2_666 2_666 ?
Au7 Te3 Au3 86.48(4) 2_666 2_666 ?
Sb3 Te3 Au3 0.00(5) 2_666 2_666 ?
Au1 Te3 Au2 176.87(5) . 2_565 ?
Au9 Te3 Au2 90.05(4) . 2_565 ?
Au2 Te3 Au2 88.72(4) . 2_565 ?
Sb7 Te3 Au2 85.85(4) 2_666 2_565 ?
Au7 Te3 Au2 85.85(4) 2_666 2_565 ?
Sb3 Te3 Au2 86.66(4) 2_666 2_565 ?
Au3 Te3 Au2 86.66(4) 2_666 2_565 ?
Au1 Te3 Sb2 176.87(5) . 2_565 ?
Au9 Te3 Sb2 90.05(4) . 2_565 ?
Au2 Te3 Sb2 88.72(4) . 2_565 ?
Sb7 Te3 Sb2 85.85(4) 2_666 2_565 ?
Au7 Te3 Sb2 85.85(4) 2_666 2_565 ?
Sb3 Te3 Sb2 86.66(4) 2_666 2_565 ?
Au3 Te3 Sb2 86.66(4) 2_666 2_565 ?
Au2 Te3 Sb2 0.00(2) 2_565 2_565 ?
Sb7 Te4 Au7 0.00(5) 2_666 2_666 ?
Sb7 Te4 Au2 103.59(5) 2_666 . ?
Au7 Te4 Au2 103.59(5) 2_666 . ?
Sb7 Te4 Au6 98.15(5) 2_666 . ?
Au7 Te4 Au6 98.15(5) 2_666 . ?
Au2 Te4 Au6 100.15(5) . . ?
Sb7 Te4 Sb9 92.71(5) 2_666 2_565 ?
Au7 Te4 Sb9 92.71(5) 2_666 2_565 ?
Au2 Te4 Sb9 92.70(4) . 2_565 ?
Au6 Te4 Sb9 160.68(5) . 2_565 ?
Sb7 Te4 Au9 92.71(5) 2_666 2_565 ?
Au7 Te4 Au9 92.71(5) 2_666 2_565 ?
Au2 Te4 Au9 92.70(4) . 2_565 ?
Au6 Te4 Au9 160.68(5) . 2_565 ?
Sb9 Te4 Au9 0.00(2) 2_565 2_565 ?
Sb7 Te4 Au11 88.98(4) 2_666 1_655 ?
Au7 Te4 Au11 88.98(4) 2_666 1_655 ?
Au2 Te4 Au11 165.57(5) . 1_655 ?
Au6 Te4 Au11 84.79(4) . 1_655 ?
Sb9 Te4 Au11 79.45(4) 2_565 1_655 ?
Au9 Te4 Au11 79.45(4) 2_565 1_655 ?
Sb10 Te5 Au10 0.00(5) 1_444 1_444 ?
Sb10 Te5 Au6 98.51(5) 1_444 2 ?
Au10 Te5 Au6 98.51(5) 1_444 2 ?
Sb10 Te5 Sb6 98.51(5) 1_444 2 ?
Au10 Te5 Sb6 98.51(5) 1_444 2 ?
Au6 Te5 Sb6 0.00(3) 2 2 ?
Sb10 Te5 Sb11 99.06(5) 1_444 2_455 ?
Au10 Te5 Sb11 99.06(5) 1_444 2_455 ?
Au6 Te5 Sb11 96.19(5) 2 2_455 ?
Sb6 Te5 Sb11 96.19(5) 2 2_455 ?
Sb10 Te5 Au11 99.06(5) 1_444 2_455 ?
Au10 Te5 Au11 99.06(5) 1_444 2_455 ?
Au6 Te5 Au11 96.19(5) 2 2_455 ?
Sb6 Te5 Au11 96.19(5) 2 2_455 ?
Sb11 Te5 Au11 0.00(3) 2_455 2_455 ?
Sb10 Te5 Te10 97.25(5) 1_444 . ?
Au10 Te5 Te10 97.25(5) 1_444 . ?
Au6 Te5 Te10 88.49(5) 2 . ?
Sb6 Te5 Te10 88.49(5) 2 . ?
Sb11 Te5 Te10 162.16(6) 2_455 . ?
Au11 Te5 Te10 162.16(6) 2_455 . ?
Sb12 Te6 Au12 0.0 1_565 1_565 ?
Sb12 Te6 Sb11 100.36(5) 1_565 2_465 ?
Au12 Te6 Sb11 100.36(5) 1_565 2_465 ?
Sb12 Te6 Au11 100.36(5) 1_565 2_465 ?
Au12 Te6 Au11 100.36(5) 1_565 2_465 ?
Sb11 Te6 Au11 0.00(3) 2_465 2_465 ?
Sb12 Te6 Au9 99.82(4) 1_565 . ?
Au12 Te6 Au9 99.82(4) 1_565 . ?
Sb11 Te6 Au9 95.84(5) 2_465 . ?
Au11 Te6 Au9 95.84(5) 2_465 . ?
Au10 Te7 Au5 96.80(4) . . ?
Au10 Te7 Au8 96.08(5) . . ?
Au5 Te7 Au8 93.27(5) . . ?
Au10 Te7 Te18 100.08(5) . 2_566 ?
Au5 Te7 Te18 95.99(5) . 2_566 ?
Au8 Te7 Te18 160.26(6) . 2_566 ?
Sb11 Te8 Au11 0.00(6) 2_455 2_455 ?
Sb11 Te8 Sb8 99.29(4) 2_455 2_566 ?
Au11 Te8 Sb8 99.29(4) 2_455 2_566 ?
Sb11 Te8 Au8 99.29(4) 2_455 2_566 ?
Au11 Te8 Au8 99.29(4) 2_455 2_566 ?
Sb8 Te8 Au8 0.00(3) 2_566 2_566 ?
Sb11 Te8 Au12 96.66(5) 2_455 . ?
Au11 Te8 Au12 96.66(5) 2_455 . ?
Sb8 Te8 Au12 92.80(4) 2_566 . ?
Au8 Te8 Au12 92.80(4) 2_566 . ?
Sb11 Te8 Te16 99.21(5) 2_455 . ?
Au11 Te8 Te16 99.21(5) 2_455 . ?
Sb8 Te8 Te16 95.25(5) 2_566 . ?
Au8 Te8 Te16 95.25(5) 2_566 . ?
Au12 Te8 Te16 160.79(5) . . ?
Sb5 Te9 Au5 0.00(5) 2_666 2_666 ?
Sb5 Te9 Au1 108.03(6) 2_666 . ?
Au5 Te9 Au1 108.03(6) 2_666 . ?
Sb5 Te9 Au4 100.96(5) 2_666 . ?
Au5 Te9 Au4 100.96(5) 2_666 . ?
Au1 Te9 Au4 97.63(6) . . ?
Sb5 Te9 Sb7 91.67(5) 2_666 2_666 ?
Au5 Te9 Sb7 91.67(5) 2_666 2_666 ?
Au1 Te9 Sb7 93.28(5) . 2_666 ?
Au4 Te9 Sb7 159.82(6) . 2_666 ?
Sb5 Te9 Au7 91.67(5) 2_666 2_666 ?
Au5 Te9 Au7 91.67(5) 2_666 2_666 ?
Au1 Te9 Au7 93.28(5) . 2_666 ?
Au4 Te9 Au7 159.82(6) . 2_666 ?
Sb7 Te9 Au7 0.00(3) 2_666 2_666 ?
Sb5 Te9 Sb10 86.78(4) 2_666 2_666 ?
Au5 Te9 Sb10 86.78(4) 2_666 2_666 ?
Au1 Te9 Sb10 164.27(5) . 2_666 ?
Au4 Te9 Sb10 84.31(5) . 2_666 ?
Sb7 Te9 Sb10 80.71(4) 2_666 2_666 ?
Au7 Te9 Sb10 80.71(4) 2_666 2_666 ?
Sb5 Te9 Au10 86.78(4) 2_666 2_666 ?
Au5 Te9 Au10 86.78(4) 2_666 2_666 ?
Au1 Te9 Au10 164.27(5) . 2_666 ?
Au4 Te9 Au10 84.31(5) . 2_666 ?
Sb7 Te9 Au10 80.71(4) 2_666 2_666 ?
Au7 Te9 Au10 80.71(4) 2_666 2_666 ?
Sb10 Te9 Au10 0.00(4) 2_666 2_666 ?
Sb5 Te9 Au6 163.03(6) 2_666 . ?
Au5 Te9 Au6 163.03(6) 2_666 . ?
Au1 Te9 Au6 87.55(4) . . ?
Au4 Te9 Au6 83.05(5) . . ?
Sb7 Te9 Au6 80.50(4) 2_666 . ?
Au7 Te9 Au6 80.50(4) 2_666 . ?
Sb10 Te9 Au6 77.16(4) 2_666 . ?
Au10 Te9 Au6 77.16(4) 2_666 . ?
Au2 Te10 Te17 96.61(5) . 2 ?
Au2 Te10 Sb3 94.99(5) . 1_454 ?
Te17 Te10 Sb3 94.61(5) 2 1_454 ?
Au2 Te10 Au3 94.99(5) . 1_454 ?
Te17 Te10 Au3 94.61(5) 2 1_454 ?
Sb3 Te10 Au3 0.00(3) 1_454 1_454 ?
Au2 Te10 Te5 99.11(5) . . ?
Te17 Te10 Te5 80.98(5) 2 . ?
Sb3 Te10 Te5 165.61(6) 1_454 . ?
Au3 Te10 Te5 165.61(6) 1_454 . ?
Sb9 Te11 Au9 0.00(5) 1_545 1_545 ?
Sb9 Te11 Sb3 103.09(5) 1_545 2_656 ?
Au9 Te11 Sb3 103.09(5) 1_545 2_656 ?
Sb9 Te11 Au3 103.09(5) 1_545 2_656 ?
Au9 Te11 Au3 103.09(5) 1_545 2_656 ?
Sb3 Te11 Au3 0.00(5) 2_656 2_656 ?
Sb9 Te11 Sb8 98.09(5) 1_545 1_545 ?
Au9 Te11 Sb8 98.09(5) 1_545 1_545 ?
Sb3 Te11 Sb8 98.67(5) 2_656 1_545 ?
Au3 Te11 Sb8 98.67(5) 2_656 1_545 ?
Sb9 Te11 Au8 98.09(5) 1_545 1_545 ?
Au9 Te11 Au8 98.09(5) 1_545 1_545 ?
Sb3 Te11 Au8 98.67(5) 2_656 1_545 ?
Au3 Te11 Au8 98.67(5) 2_656 1_545 ?
Sb8 Te11 Au8 0.00(4) 1_545 1_545 ?
Sb9 Te11 Au12 88.82(4) 1_545 . ?
Au9 Te11 Au12 88.82(4) 1_545 . ?
Sb3 Te11 Au12 166.18(5) 2_656 . ?
Au3 Te11 Au12 166.18(5) 2_656 . ?
Sb8 Te11 Au12 86.37(4) 1_545 . ?
Au8 Te11 Au12 86.37(4) 1_545 . ?
Sb8 Te12 Au8 0.00(3) 1_545 1_545 ?
Sb8 Te12 Au4 103.52(5) 1_545 2_656 ?
Au8 Te12 Au4 103.52(5) 1_545 2_656 ?
Sb8 Te12 Sb4 103.52(5) 1_545 2_656 ?
Au8 Te12 Sb4 103.52(5) 1_545 2_656 ?
Au4 Te12 Sb4 0.00(5) 2_656 2_656 ?
Sb8 Te12 Sb10 99.50(5) 1_545 1_545 ?
Au8 Te12 Sb10 99.50(5) 1_545 1_545 ?
Au4 Te12 Sb10 98.11(5) 2_656 1_545 ?
Sb4 Te12 Sb10 98.11(5) 2_656 1_545 ?
Sb8 Te12 Au10 99.50(5) 1_545 1_545 ?
Au8 Te12 Au10 99.50(5) 1_545 1_545 ?
Au4 Te12 Au10 98.11(5) 2_656 1_545 ?
Sb4 Te12 Au10 98.11(5) 2_656 1_545 ?
Sb10 Te12 Au10 0.00(3) 1_545 1_545 ?
Au5 Te13 Au4 102.02(5) . . ?
Au5 Te13 Au1 97.80(6) . . ?
Au4 Te13 Au1 98.48(5) . . ?
Au7 Te14 Au3 100.44(4) . . ?
Au7 Te14 Au5 97.12(5) . . ?
Au3 Te14 Au5 98.96(5) . . ?
Au4 Te15 Au3 97.58(5) . . ?
Au4 Te15 Te15 97.49(7) . 2_656 ?
Au3 Te15 Te15 97.13(6) . 2_656 ?
Au6 Te16 Au1 98.24(4) . . ?
Au6 Te16 Te8 100.69(6) . . ?
Au1 Te16 Te8 99.13(5) . . ?
Au6 Te16 Au2 94.53(5) . . ?
Au1 Te16 Au2 90.20(5) . . ?
Te8 Te16 Au2 160.75(6) . . ?
Au6 Te17 Te10 96.78(6) . 2 ?
Au6 Te17 Au4 94.31(5) . . ?
Te10 Te17 Au4 97.25(5) 2 . ?
Au2 Te18 Au9 100.72(4) . . ?
Au2 Te18 Sb7 95.99(5) . 1_454 ?
Au9 Te18 Sb7 98.09(5) . 1_454 ?
Au2 Te18 Au7 95.99(5) . 1_454 ?
Au9 Te18 Au7 98.09(5) . 1_454 ?
Sb7 Te18 Au7 0.00(3) 1_454 1_454 ?
Au2 Te18 Te7 94.02(5) . 2_566 ?
Au9 Te18 Te7 98.42(5) . 2_566 ?
Sb7 Te18 Te7 158.73(5) 1_454 2_566 ?
Au7 Te18 Te7 158.73(5) 1_454 2_566 ?
Sb5 T19T Au5 0.000(16) 2_666 2_666 ?
Sb5 T19T Au5 92.63(4) 2_666 . ?
Au5 T19T Au5 92.63(4) 2_666 . ?
Sb5 T19T Sb1 88.71(4) 2_666 2_666 ?
Au5 T19T Sb1 88.71(4) 2_666 2_666 ?
Au5 T19T Sb1 93.83(4) . 2_666 ?
Sb5 T19T Au1 88.71(4) 2_666 2_666 ?
Au5 T19T Au1 88.71(4) 2_666 2_666 ?
Au5 T19T Au1 93.83(4) . 2_666 ?
Sb1 T19T Au1 0.00(3) 2_666 2_666 ?
Sb5 T19T Sb8 89.35(4) 2_666 2_666 ?
Au5 T19T Sb8 89.35(4) 2_666 2_666 ?
Au5 T19T Sb8 177.44(5) . 2_666 ?
Sb1 T19T Sb8 87.84(3) 2_666 2_666 ?
Au1 T19T Sb8 87.84(3) 2_666 2_666 ?
Sb5 T19T Au8 89.35(4) 2_666 2_666 ?
Au5 T19T Au8 89.35(4) 2_666 2_666 ?
Au5 T19T Au8 177.44(5) . 2_666 ?
Sb1 T19T Au8 87.84(3) 2_666 2_666 ?
Au1 T19T Au8 87.84(3) 2_666 2_666 ?
Sb8 T19T Au8 0.00(4) 2_666 2_666 ?
Sb5 T19T Au3 178.73(4) 2_666 . ?
Au5 T19T Au3 178.73(4) 2_666 . ?
Au5 T19T Au3 88.51(4) . . ?
Sb1 T19T Au3 90.66(4) 2_666 . ?
Au1 T19T Au3 90.66(4) 2_666 . ?
Sb8 T19T Au3 89.52(4) 2_666 . ?
Au8 T19T Au3 89.52(4) 2_666 . ?
Sb5 T19T Au4 91.88(4) 2_666 . ?
Au5 T19T Au4 91.88(4) 2_666 . ?
Au5 T19T Au4 88.22(3) . . ?
Sb1 T19T Au4 177.83(4) 2_666 . ?
Au1 T19T Au4 177.83(4) 2_666 . ?
Sb8 T19T Au4 90.08(4) 2_666 . ?
Au8 T19T Au4 90.08(4) 2_666 . ?
Au3 T19T Au4 88.71(4) . . ?
_diffrn_measured_fraction_theta_max 0.996
_diffrn_reflns_theta_full 30.00
_diffrn_measured_fraction_theta_full 0.996
_refine_diff_density_max 1.297
_refine_diff_density_min -1.643
_refine_diff_density_rms 0.987