#======================================================================= data_global #======================================================================= _audit_creation_method 'Jana2006 Version : 03/11/2014' # 1. PROCESSING SUMMARY (IUCr Office Use Only) _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ; ? ; _journal_techeditor_code ? _journal_paper_category ? _journal_techeditor_notes ; ? ; _journal_coden_ASTM ? _journal_name_full 'Acta Crystallographica Section C' _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #======================================================================= # 2. SUBMISSION DETAILS _publ_contact_author_name ? _publ_contact_author_address ; ? ; _publ_contact_author_email ? _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_requested_journal 'Acta Crystallographica Section C' _publ_requested_category ? _publ_contact_letter ; ? ; #======================================================================= # 3. TITLE AND AUTHOR LIST _publ_section_title ; ? ; _publ_section_title_footnote ; ? ; loop_ _publ_author_name _publ_author_footnote _publ_author_address ; ? # name ; ; ? # footnote ; ; ? # address ; #======================================================================= # 4. TEXT _publ_section_synopsis ; ? ; _publ_section_abstract ; ? ; _publ_section_comment ; ? ; _publ_section_introduction ; ? ; _publ_section_experimental ; ? ; _publ_section_exptl_prep ; ? ; _publ_section_exptl_refinement ; ? ; _publ_section_exptl_solution ; ? ; _publ_section_discussion ; ? ; _publ_section_acknowledgements ; ? ; _publ_section_references ; ; _publ_section_figure_captions ; ? ; _publ_section_table_legends ; ? ; #======================================================================= data_I #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Al1 H7 O8 S1' _chemical_formula_weight 194.1 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _symmetry_cell_setting triclinic _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_Int_Tables_number 2 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z _cell_length_a 5.600(2) _cell_length_b 7.450(3) _cell_length_c 7.671(3) _cell_angle_alpha 74.785(7) _cell_angle_beta 86.042(8) _cell_angle_gamma 75.810(7) _cell_volume 299.4(2) loop_ _twin_individual_id _twin_individual_mass_fraction_refined _twin_individual_twin_matrix_11 _twin_individual_twin_matrix_12 _twin_individual_twin_matrix_13 _twin_individual_twin_matrix_21 _twin_individual_twin_matrix_22 _twin_individual_twin_matrix_23 _twin_individual_twin_matrix_31 _twin_individual_twin_matrix_32 _twin_individual_twin_matrix_33 ? ? ? ? ? ? ? ? ? ? ? _cell_formula_units_Z 2 _cell_measurement_reflns_used 3803 _cell_measurement_theta_min 2.75 _cell_measurement_theta_max 30.95 _cell_measurement_temperature 293 _cell_special_details ; ? ; _exptl_crystal_density_diffrn 2.1531 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 200 _exptl_absorpt_coefficient_mu 0.685 _exptl_crystal_description 'anhedral grain' _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_size_rad ? _exptl_crystal_colour ? _exptl_absorpt_correction_type ? _exptl_absorpt_process_details ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist ? ? ? ? #======================================================================= # 7. EXPERIMENTAL DATA _exptl_special_details ? _diffrn_ambient_temperature 293 _diffrn_source ? _diffrn_source_power ? _diffrn_source_voltage ? _diffrn_source_current ? _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_source 'X-ray tube' _diffrn_radiation_wavelength 0.71069 _diffrn_radiation_monochromator ? _diffrn_measurement_device 'BRUKER SMART APEX2' _diffrn_measurement_device_type ? _diffrn_detector 'CCD' _diffrn_detector_area_resol_mean ? _diffrn_measurement_method ? _diffrn_measurement_specimen_support ? _diffrn_reflns_number 3803 _diffrn_reflns_theta_min 2.75 _diffrn_reflns_theta_max 30.95 _diffrn_reflns_theta_full 25.86 _diffrn_measured_fraction_theta_max 0.97 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.0336 _diffrn_reflns_av_unetI/netI 0.0523 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? _diffrn_radiation_probe X-ray #======================================================================= # 8. REFINEMENT DATA _refine_special_details ; ? ; _reflns_number_total 1814 _reflns_number_gt 1402 _reflns_threshold_expression 'I>2\s(I)' _refine_ls_structure_factor_coef F _refine_ls_R_factor_gt 0.0398 _refine_ls_wR_factor_gt 0.0476 _refine_ls_R_factor_all 0.0565 _refine_ls_wR_factor_ref 0.0515 _refine_ls_goodness_of_fit_ref 0.96 _refine_ls_goodness_of_fit_gt 1.01 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 1814 _refine_ls_number_parameters 113 _refine_ls_number_restraints 10 _refine_ls_number_constraints 7 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'w=1/(\s^2^(F)+0.0008409999F^2^)' _refine_ls_hydrogen_treatment 'refall' _refine_ls_shift/su_max 0.0470 _refine_ls_shift/su_mean 0.0038 _refine_diff_density_max 0.38 _refine_diff_density_min -0.40 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 200(300) _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Al 0.0645 0.0514 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' H 0.0000 0.0000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.0060 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' S 0.1246 0.1234 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement ? _computing_molecular_graphics ? _computing_publication_material ? loop_ _restr_distance_atom_site_label_1 _restr_distance_site_symmetry_1 _restr_distance_atom_site_label_2 _restr_distance_site_symmetry_2 _restr_distance_target _restr_distance_target_weight_param H4_w2 . W2 . 0.98 0.015 H5_w2 . W2 . 0.98 0.015 H6_w3 . W3 . 0.98 0.015 H7_w3 . W3 . 0.98 0.015 H2_w1 . W1 . 0.98 0.015 H3_w1 . W1 . 0.98 0.015 H1_oh . Oh . 0.98 0.015 loop_ _restr_angle_atom_site_label_1 _restr_angle_site_symmetry_1 _restr_angle_atom_site_label_2 _restr_angle_site_symmetry_2 _restr_angle_atom_site_label_3 _restr_angle_site_symmetry_3 _restr_angle_target _restr_angle_target_weight_param H4_w2 . W2 . H5_w2 . 109.4 0.5 H6_w3 . W3 . H7_w3 . 109.4 0.5 H2_w1 . W1 . H3_w1 . 109.4 0.5 loop_ _restr_torsion_atom_site_label_1 _restr_torsion_site_symmetry_1 _restr_torsion_atom_site_label_2 _restr_torsion_site_symmetry_2 _restr_torsion_atom_site_label_3 _restr_torsion_site_symmetry_3 _restr_torsion_atom_site_label_4 _restr_torsion_site_symmetry_4 _restr_torsion_angle_target _restr_torsion_weight_param ? ? ? ? ? ? ? ? ? ? loop_ _restr_equal_distance_atom_site_label_1 _restr_equal_distance_site_symmetry_1 _restr_equal_distance_atom_site_label_2 _restr_equal_distance_site_symmetry_2 _restr_equal_distance_class_class_id _restr_equal_distance_class_target_weight_param ? ? ? ? ? ? loop_ _restr_equal_angle_atom_site_label_1 _restr_equal_angle_site_symmetry_1 _restr_equal_angle_atom_site_label_2 _restr_equal_angle_site_symmetry_2 _restr_equal_angle_atom_site_label_3 _restr_equal_angle_site_symmetry_3 _restr_equal_angle_class_class_id _restr_equal_angle_class_target_weight_param ? ? ? ? ? ? ? ? loop_ _restr_equal_torsion_atom_site_label_1 _restr_equal_torsion_site_symmetry_1 _restr_equal_torsion_atom_site_label_2 _restr_equal_torsion_site_symmetry_2 _restr_equal_torsion_atom_site_label_3 _restr_equal_torsion_site_symmetry_3 _restr_equal_torsion_atom_site_label_4 _restr_equal_torsion_site_symmetry_4 _restr_equal_torsion_class_class_id _restr_equal_torsion_class_target_weight_param ? ? ? ? ? ? ? ? ? ? #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group S S 0.57590(9) 0.22851(7) 0.30004(8) Uani 0.01350(18) 2 1 d . . . Al Al 0.88765(11) 0.87786(8) 0.14873(9) Uani 0.0109(2) 2 1 d . . . W1 O 0.6262(3) 0.7558(2) 0.1668(2) Uani 0.0183(5) 2 1 d . . . O1 O 0.6673(3) 0.1477(3) 0.4838(2) Uani 0.0259(6) 2 1 d . . . Oh O 0.1409(3) 0.0123(2) 0.1041(2) Uani 0.0133(5) 2 1 d . . . O2 O 0.6877(3) 0.3877(2) 0.2052(3) Uani 0.0255(6) 2 1 d . . . W2 O 0.9652(3) 0.7685(2) 0.3935(2) Uani 0.0187(5) 2 1 d . . . W3 O 0.1032(3) 0.6515(2) 0.1061(2) Uani 0.0190(5) 2 1 d . . . O3 O 0.3058(3) 0.2922(2) 0.2986(2) Uani 0.0233(6) 2 1 d . . . O4 O 0.6417(3) 0.0821(2) 0.1942(2) Uani 0.0166(5) 2 1 d . . . H4_w2 H 0.845(4) 0.763(4) 0.490(3) Uiso 0.026885(10) 2 1 d . . . H6_w3 H 0.171(5) 0.634(3) -0.008(2) Uiso 0.034051(10) 2 1 d . . . H5_w2 H 1.109(3) 0.798(4) 0.432(3) Uiso 0.026885(10) 2 1 d . . . H7_w3 H 0.148(5) 0.533(3) 0.196(3) Uiso 0.034051(10) 2 1 d . . . H2_w1 H 0.462(3) 0.824(3) 0.131(4) Uiso 0.020020(9) 2 1 d . . . H1_oh H 0.173(5) 0.088(4) 0.180(3) Uiso 0.020329(9) 2 1 d . . . H3_w1 H 0.642(4) 0.622(2) 0.179(4) Uiso 0.020020(9) 2 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S S 0.0144(3) 0.0097(2) 0.0164(3) -0.00307(18) 0.00326(19) -0.00397(19) Al Al 0.0102(3) 0.0092(3) 0.0131(4) -0.0023(2) 0.0002(2) -0.0023(2) W1 O 0.0133(7) 0.0112(7) 0.0304(10) -0.0036(6) 0.0005(6) -0.0048(6) O1 O 0.0307(9) 0.0309(9) 0.0181(9) -0.0127(8) -0.0033(7) -0.0039(7) Oh O 0.0136(7) 0.0138(7) 0.0140(8) -0.0060(6) -0.0001(6) -0.0034(6) O2 O 0.0351(10) 0.0151(7) 0.0302(11) -0.0134(7) 0.0160(8) -0.0098(7) W2 O 0.0179(8) 0.0221(8) 0.0148(9) -0.0053(6) 0.0014(6) -0.0022(7) W3 O 0.0227(8) 0.0128(7) 0.0164(9) 0.0015(6) 0.0053(7) -0.0017(6) O3 O 0.0167(8) 0.0195(8) 0.0264(10) 0.0029(6) 0.0059(7) -0.0015(7) O4 O 0.0166(7) 0.0126(7) 0.0218(9) -0.0019(6) 0.0014(6) -0.0080(6) loop_ _jana_atom_site_ADP_C_label _jana_atom_site_ADP_C_type_symbol _jana_atom_site_ADP_C_111 _jana_atom_site_ADP_C_112 _jana_atom_site_ADP_C_113 _jana_atom_site_ADP_C_122 _jana_atom_site_ADP_C_123 _jana_atom_site_ADP_C_133 _jana_atom_site_ADP_C_222 _jana_atom_site_ADP_C_223 _jana_atom_site_ADP_C_233 _jana_atom_site_ADP_C_333 ? ? ? ? ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_D_label _jana_atom_site_ADP_D_type_symbol _jana_atom_site_ADP_D_1111 _jana_atom_site_ADP_D_1112 _jana_atom_site_ADP_D_1113 _jana_atom_site_ADP_D_1122 _jana_atom_site_ADP_D_1123 _jana_atom_site_ADP_D_1133 _jana_atom_site_ADP_D_1222 _jana_atom_site_ADP_D_1223 _jana_atom_site_ADP_D_1233 _jana_atom_site_ADP_D_1333 _jana_atom_site_ADP_D_2222 _jana_atom_site_ADP_D_2223 _jana_atom_site_ADP_D_2233 _jana_atom_site_ADP_D_2333 _jana_atom_site_ADP_D_3333 ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_E_label _jana_atom_site_ADP_E_type_symbol _jana_atom_site_ADP_E_11111 _jana_atom_site_ADP_E_11112 _jana_atom_site_ADP_E_11113 _jana_atom_site_ADP_E_11122 _jana_atom_site_ADP_E_11123 _jana_atom_site_ADP_E_11133 _jana_atom_site_ADP_E_11222 _jana_atom_site_ADP_E_11223 _jana_atom_site_ADP_E_11233 _jana_atom_site_ADP_E_11333 _jana_atom_site_ADP_E_12222 _jana_atom_site_ADP_E_12223 _jana_atom_site_ADP_E_12233 _jana_atom_site_ADP_E_12333 _jana_atom_site_ADP_E_13333 _jana_atom_site_ADP_E_22222 _jana_atom_site_ADP_E_22223 _jana_atom_site_ADP_E_22233 _jana_atom_site_ADP_E_22333 _jana_atom_site_ADP_E_23333 _jana_atom_site_ADP_E_33333 ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_F_label _jana_atom_site_ADP_F_type_symbol _jana_atom_site_ADP_F_111111 _jana_atom_site_ADP_F_111112 _jana_atom_site_ADP_F_111113 _jana_atom_site_ADP_F_111122 _jana_atom_site_ADP_F_111123 _jana_atom_site_ADP_F_111133 _jana_atom_site_ADP_F_111222 _jana_atom_site_ADP_F_111223 _jana_atom_site_ADP_F_111233 _jana_atom_site_ADP_F_111333 _jana_atom_site_ADP_F_112222 _jana_atom_site_ADP_F_112223 _jana_atom_site_ADP_F_112233 _jana_atom_site_ADP_F_112333 _jana_atom_site_ADP_F_113333 _jana_atom_site_ADP_F_122222 _jana_atom_site_ADP_F_122223 _jana_atom_site_ADP_F_122233 _jana_atom_site_ADP_F_122333 _jana_atom_site_ADP_F_123333 _jana_atom_site_ADP_F_133333 _jana_atom_site_ADP_F_222222 _jana_atom_site_ADP_F_222223 _jana_atom_site_ADP_F_222233 _jana_atom_site_ADP_F_222333 _jana_atom_site_ADP_F_223333 _jana_atom_site_ADP_F_233333 _jana_atom_site_ADP_F_333333 ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag S O1 . . 1.454(2) ? S O2 . . 1.475(2) ? S O3 . . 1.470(2) ? S O4 . . 1.487(2) ? Al Al . 2_775 2.941(2) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 S O2 . . . 111.15(12) ? O1 S O3 . . . 110.90(11) ? O1 S O4 . . . 110.54(10) ? O2 S O3 . . . 110.58(10) ? O2 S O4 . . . 106.68(11) ? O3 S O4 . . . 106.81(11) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag ? ? ? ? ? ? ? ? ? ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_D _geom_hbond_site_symmetry_H _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag W2 H4_w2 O3 . . 2_666 0.96(2) 1.77(2) 2.714(3) 164.1(18) ? W3 H6_w3 O2 . . 2_665 0.96(2) 1.68(2) 2.640(3) 175(3) ? W2 H5_w2 O1 . . 2_766 0.97(3) 1.63(3) 2.591(3) 174(2) ? W3 H7_w3 O3 . . . 0.957(16) 1.787(17) 2.702(3) 159(2) ? W1 H2_w1 Oh . . 1_565 0.953(16) 1.979(15) 2.902(3) 163(2) ? W1 H2_w1 O4 . . 2_665 0.953(16) 2.48(3) 3.051(3) 118.7(19) ? Oh H1_oh O3 . . . 0.96(3) 2.25(3) 3.193(3) 165(2) ? W1 H3_w1 O2 . . . 0.961(16) 1.659(16) 2.618(3) 176(2) ? #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 65.63 67.92 2.69 o 2 0 0 2.52 3.41 1.09 o 3 0 0 290.36 357.65 8.14 o 4 0 0 1329.13 1315.41 21.79 o 5 0 0 67.81 70.99 5.59 o 6 0 0 29.51 37.29 6.57 o 7 0 0 68.38 76.03 10.12 o -7 1 0 0.61 -0.49 4.13 < -6 1 0 3.45 4.67 3.67 < -5 1 0 69.78 73.30 8.50 o -4 1 0 0.57 1.45 1.47 < -3 1 0 198.77 182.22 5.53 o -2 1 0 812.53 768.02 10.31 o -1 1 0 0.09 -0.56 0.49 < 0 1 0 1249.84 1222.40 16.71 o 1 1 0 142.90 147.18 2.75 o 2 1 0 497.49 509.37 11.75 o 3 1 0 0.04 -1.04 1.01 < 4 1 0 1169.33 1153.28 19.58 o 5 1 0 24.57 24.43 3.58 o 6 1 0 4.22 1.89 3.12 < 7 1 0 8.23 13.42 5.25 o -7 2 0 134.46 128.85 14.31 o -6 2 0 0.03 -0.24 3.45 < -5 2 0 91.92 94.71 7.78 o -4 2 0 35.13 41.37 5.96 o -3 2 0 10.72 15.32 3.54 o -2 2 0 727.60 726.97 16.65 o -1 2 0 835.96 809.97 10.53 o 0 2 0 2309.03 2185.05 29.25 o 1 2 0 269.80 264.62 6.46 o 2 2 0 4664.69 4464.56 57.50 o 3 2 0 957.21 1054.91 16.73 o 4 2 0 39.90 35.13 3.13 o 5 2 0 63.96 58.55 4.32 o 6 2 0 404.76 416.39 13.86 o 7 2 0 8.87 16.38 5.03 o 8 2 0 77.66 56.91 9.69 o -6 3 0 29.05 26.81 6.47 o -5 3 0 14.75 12.77 4.82 o -4 3 0 262.84 268.84 12.24 o -3 3 0 182.38 163.73 8.32 o -2 3 0 44.06 56.70 5.93 o -1 3 0 35.50 43.44 3.13 o 0 3 0 5.21 0.08 0.82 < 1 3 0 745.74 864.36 13.42 o 2 3 0 1296.12 1386.71 24.08 o 4 3 0 797.99 775.86 14.55 o 5 3 0 198.29 187.37 8.74 o 6 3 0 368.30 367.54 13.46 o 7 3 0 78.76 81.68 7.50 o 8 3 0 2.64 9.57 5.88 < -6 4 0 59.02 56.55 9.69 o -5 4 0 369.86 339.35 16.19 o -4 4 0 3.11 2.62 3.50 < -3 4 0 3.97 3.44 2.80 < -2 4 0 7.01 9.30 2.34 o -1 4 0 65.56 68.54 3.58 o 0 4 0 3.21 3.22 1.39 o 1 4 0 684.35 684.32 12.26 o 2 4 0 619.35 646.34 14.92 o 3 4 0 0.07 1.76 1.56 < 4 4 0 147.68 159.69 7.99 o 5 4 0 451.86 436.16 14.47 o 6 4 0 12.61 6.60 3.12 o 7 4 0 38.63 31.52 5.48 o -5 5 0 25.69 22.23 6.57 o -4 5 0 194.61 191.84 11.92 o -3 5 0 87.74 102.71 10.44 o -2 5 0 74.69 75.35 8.25 o -1 5 0 16.68 18.40 2.92 o 0 5 0 15.16 16.21 2.58 o 1 5 0 188.38 185.60 6.09 o 2 5 0 29.06 27.87 2.60 o 3 5 0 59.96 54.86 5.57 o 4 5 0 107.74 102.79 6.81 o 5 5 0 313.27 307.93 12.57 o 6 5 0 70.98 76.13 7.98 o 7 5 0 1.15 7.07 3.41 o -5 6 0 79.32 85.08 11.75 o -4 6 0 7.64 8.04 4.53 < -3 6 0 363.14 367.35 16.14 o -2 6 0 33.41 40.42 6.73 o -1 6 0 0.76 0.43 1.54 < 0 6 0 201.41 201.23 7.23 o 1 6 0 1023.67 1013.20 18.61 o 2 6 0 45.63 46.68 3.98 o 3 6 0 9.44 13.51 3.22 o 4 6 0 3.63 2.98 2.11 < 5 6 0 72.32 72.67 7.51 o 6 6 0 49.72 50.83 6.95 o 7 6 0 45.44 39.95 6.70 o -4 7 0 21.97 19.88 7.02 o -3 7 0 30.49 31.14 7.82 o -2 7 0 403.15 427.68 17.30 o -1 7 0 99.91 104.91 7.73 o 0 7 0 37.07 43.91 4.92 o 1 7 0 111.65 105.58 5.62 o 2 7 0 15.30 10.04 2.94 o 3 7 0 0.40 1.14 2.27 < 4 7 0 26.78 25.53 4.94 o 5 7 0 260.06 262.45 12.97 o 6 7 0 89.21 104.87 10.38 o 7 7 0 33.42 33.14 6.49 o -3 8 0 18.33 25.48 6.96 o -2 8 0 0.85 3.56 3.93 < -1 8 0 86.82 94.47 10.05 o 0 8 0 404.85 409.92 15.24 o 1 8 0 7.81 7.21 2.69 o 2 8 0 79.53 77.34 7.63 o 3 8 0 170.18 167.35 9.87 o 4 8 0 5.09 1.27 2.81 < 5 8 0 39.45 41.65 6.99 o 6 8 0 0.00 -2.03 3.25 < -2 9 0 113.83 127.20 13.77 o -1 9 0 14.32 17.33 5.66 o 0 9 0 220.80 244.35 14.68 o 1 9 0 0.29 2.28 3.04 < 2 9 0 42.19 44.79 6.11 o 3 9 0 152.22 142.02 9.79 o 4 9 0 130.32 141.31 10.07 o 5 9 0 90.06 91.07 10.23 o 0 10 0 1.58 0.76 2.92 < 1 10 0 6.19 8.96 4.83 < 2 10 0 203.97 202.27 14.29 o 3 10 0 0.42 1.42 2.92 < -2 -10 1 0.42 1.55 3.58 < -1 -10 1 132.63 129.07 11.29 o -5 -9 1 11.31 11.84 4.89 o -4 -9 1 30.83 22.18 4.98 o -3 -9 1 429.95 480.62 21.48 o -2 -9 1 22.98 28.46 5.09 o -1 -9 1 46.13 44.15 7.56 o 0 -9 1 11.60 11.85 4.52 o 1 -9 1 106.50 108.37 15.13 o -6 -8 1 69.98 73.12 9.11 o -5 -8 1 149.63 150.94 10.84 o -4 -8 1 111.12 114.63 10.62 o -3 -8 1 122.35 113.64 8.40 o -2 -8 1 83.03 93.07 8.22 o -1 -8 1 24.16 23.47 4.48 o 0 -8 1 14.30 11.68 4.16 o 1 -8 1 531.51 520.67 19.04 o 2 -8 1 12.19 10.63 5.34 < 3 -8 1 27.41 22.50 6.85 o -6 -7 1 2.99 5.34 3.64 < -5 -7 1 0.46 2.78 2.90 < -4 -7 1 164.76 178.78 10.20 o -3 -7 1 1.82 -0.26 2.17 < -2 -7 1 116.49 120.23 7.79 o -1 -7 1 632.76 645.02 15.14 o 0 -7 1 8.50 6.36 2.53 o 1 -7 1 13.33 20.98 8.89 o 2 -7 1 260.89 256.67 13.24 o 3 -7 1 172.88 168.04 11.73 o 4 -7 1 1.77 2.53 5.95 < -7 -6 1 59.62 60.47 8.01 o -6 -6 1 135.19 120.86 8.87 o -5 -6 1 17.84 13.84 4.04 o -4 -6 1 18.89 21.21 4.41 o -3 -6 1 24.45 21.93 4.03 o -2 -6 1 77.04 79.32 4.83 o -1 -6 1 653.41 633.93 13.97 o 0 -6 1 327.99 351.93 10.09 o 1 -6 1 182.98 175.97 7.22 o 2 -6 1 88.51 93.14 9.73 o 3 -6 1 700.86 666.15 22.47 o 4 -6 1 83.69 93.52 12.20 o 5 -6 1 5.50 3.96 5.72 < -7 -5 1 17.92 16.28 4.96 o -6 -5 1 18.98 22.02 4.81 o -5 -5 1 183.21 186.49 9.83 o -4 -5 1 4.51 7.11 2.61 o -3 -5 1 92.55 101.41 6.49 o -2 -5 1 401.62 395.63 9.49 o -1 -5 1 52.19 47.50 3.56 o 0 -5 1 129.28 119.90 5.21 o 1 -5 1 5.36 6.79 2.17 o 2 -5 1 334.37 332.12 13.11 o 3 -5 1 38.05 36.51 6.39 o 4 -5 1 155.62 146.21 10.50 o 5 -5 1 30.71 35.97 8.66 o -7 -4 1 63.86 59.98 7.39 o -6 -4 1 19.72 17.42 4.13 o -5 -4 1 192.48 175.57 9.06 o -4 -4 1 375.83 400.73 13.15 o -3 -4 1 8.52 8.09 2.31 o -2 -4 1 68.31 85.63 5.01 o -1 -4 1 60.06 59.57 3.95 o 0 -4 1 111.04 107.08 4.41 o 1 -4 1 507.17 528.94 11.42 o 2 -4 1 590.16 579.58 12.66 o 3 -4 1 219.98 215.46 10.58 o 4 -4 1 88.53 91.40 10.60 o 5 -4 1 122.06 108.28 12.00 o 6 -4 1 306.83 305.09 16.75 o -7 -3 1 222.46 225.25 11.45 o -6 -3 1 145.42 135.71 8.18 o -5 -3 1 5.71 7.76 2.67 o -4 -3 1 75.88 75.67 4.11 o -3 -3 1 1609.15 1722.92 30.47 o -2 -3 1 323.57 329.10 9.53 o -1 -3 1 464.27 466.70 10.74 o 0 -3 1 286.83 348.91 8.52 o 1 -3 1 173.34 220.33 6.15 o 2 -3 1 3.72 5.82 2.02 o 3 -3 1 1.22 2.08 2.45 < 4 -3 1 46.46 50.82 7.74 o 5 -3 1 15.01 16.63 5.28 o 6 -3 1 215.77 204.84 13.35 o -7 -2 1 18.41 21.31 6.07 o -6 -2 1 102.07 102.03 7.00 o -5 -2 1 687.17 678.22 14.77 o -4 -2 1 682.12 664.33 13.48 o -3 -2 1 168.53 173.55 5.46 o -2 -2 1 21.18 10.47 1.93 o -1 -2 1 460.16 477.10 9.93 o 0 -2 1 370.57 367.31 7.81 o 1 -2 1 151.86 175.13 4.87 o 2 -2 1 590.73 584.01 11.19 o 3 -2 1 92.37 86.29 4.20 o 4 -2 1 427.79 418.58 14.69 o 5 -2 1 1.28 5.70 6.38 < 6 -2 1 65.24 72.42 10.44 o 7 -2 1 1.62 -0.38 4.06 < -7 -1 1 394.90 417.12 19.67 o -6 -1 1 0.63 0.63 2.89 < -5 -1 1 104.93 102.10 5.34 o -4 -1 1 2.46 3.39 1.66 o -3 -1 1 555.96 543.66 10.70 o -2 -1 1 15.57 15.79 1.95 o -1 -1 1 2807.88 2649.12 39.27 o 0 -1 1 318.04 341.54 6.47 o 1 -1 1 337.55 296.17 5.79 o 2 -1 1 498.82 623.37 10.94 o 3 -1 1 287.95 286.41 7.39 o 4 -1 1 14.52 19.03 3.05 o 5 -1 1 0.70 -0.92 2.35 < 6 -1 1 45.81 59.55 8.52 o 7 -1 1 2.83 3.54 4.10 < -7 0 1 20.03 34.05 6.82 o -6 0 1 9.49 13.53 4.66 o -5 0 1 143.16 142.69 6.33 o -4 0 1 183.34 181.61 6.34 o -3 0 1 2544.74 2567.09 35.05 o -2 0 1 985.38 967.52 19.78 o -1 0 1 145.66 142.36 4.66 o 0 0 1 259.69 250.30 4.33 o 1 0 1 2500.21 2508.73 35.67 o 2 0 1 1606.55 1655.41 22.75 o 3 0 1 160.95 152.14 5.03 o 4 0 1 514.61 486.19 11.08 o 5 0 1 46.11 60.10 5.67 o 6 0 1 0.28 0.12 2.66 < 7 0 1 47.26 47.01 7.97 o -7 1 1 34.87 40.45 7.59 o -6 1 1 2.81 2.53 3.78 < -5 1 1 129.37 126.16 8.28 o -4 1 1 458.25 428.14 10.43 o -3 1 1 638.18 672.15 12.54 o -2 1 1 13.27 10.22 1.73 o -1 1 1 2820.04 2756.32 33.34 o 0 1 1 95.29 89.76 2.35 o 2 1 1 856.45 866.79 15.13 o 3 1 1 145.08 154.23 4.95 o 4 1 1 13.52 10.64 2.22 o 5 1 1 38.88 47.90 4.88 o 6 1 1 23.78 27.08 4.55 o 7 1 1 45.45 34.06 7.26 o -7 2 1 0.09 -2.11 3.49 < -6 2 1 16.07 13.97 5.32 o -5 2 1 56.46 58.00 8.08 o -4 2 1 133.39 136.69 8.05 o -3 2 1 1054.53 1079.67 24.11 o -2 2 1 0.10 2.32 1.78 < -1 2 1 2783.35 2706.90 31.04 o 0 2 1 1517.41 1551.39 20.69 o 1 2 1 281.49 299.62 5.60 o 3 2 1 1298.51 1272.81 19.40 o 4 2 1 73.86 79.96 4.10 o 5 2 1 177.71 170.22 6.71 o 6 2 1 57.16 52.86 5.79 o 7 2 1 178.12 186.29 12.77 o 8 2 1 8.94 10.27 5.46 < -6 3 1 333.93 323.28 16.04 o -5 3 1 7.99 7.69 3.93 < -4 3 1 0.01 0.25 2.40 < -3 3 1 0.17 1.05 2.38 < -2 3 1 1134.09 1081.50 23.33 o -1 3 1 455.86 520.08 9.92 o 0 3 1 656.00 616.42 10.64 o 1 3 1 318.08 303.25 6.31 o 2 3 1 521.42 572.75 12.62 o 3 3 1 1277.48 1329.58 19.83 o 4 3 1 235.13 218.18 6.71 o 5 3 1 0.63 1.44 2.00 < 6 3 1 0.02 3.69 2.23 < 7 3 1 252.50 259.00 11.93 o 8 3 1 35.69 35.94 7.83 o -6 4 1 46.96 52.65 10.17 o -5 4 1 9.34 7.61 4.71 < -4 4 1 173.47 163.46 10.27 o -3 4 1 285.88 264.64 11.64 o -2 4 1 457.66 464.94 14.73 o -1 4 1 108.26 111.03 4.54 o 0 4 1 344.47 334.68 7.86 o 1 4 1 309.81 306.38 7.13 o 2 4 1 929.93 953.40 19.27 o 3 4 1 83.23 69.28 4.81 o 4 4 1 189.83 192.35 8.52 o 5 4 1 360.61 346.65 12.47 o 6 4 1 85.17 80.47 8.01 o 7 4 1 6.36 7.59 3.37 o 8 4 1 3.57 -0.19 4.23 < -6 5 1 84.31 87.51 12.56 o -5 5 1 22.55 25.18 7.12 o -4 5 1 52.74 57.18 8.34 o -3 5 1 167.02 162.10 10.04 o -2 5 1 15.76 13.67 4.17 o -1 5 1 24.57 22.00 3.01 o 0 5 1 511.33 510.29 11.21 o 1 5 1 18.98 14.14 2.20 o 2 5 1 1167.30 1172.48 18.64 o 3 5 1 21.14 21.06 3.58 o 4 5 1 388.55 364.11 12.59 o 5 5 1 102.82 99.46 7.10 o 6 5 1 225.66 221.24 11.14 o 7 5 1 2.94 -1.37 2.34 < -5 6 1 0.14 0.90 4.09 < -4 6 1 0.00 -0.95 3.60 < -3 6 1 128.96 124.84 9.62 o -2 6 1 285.41 273.22 12.51 o -1 6 1 419.07 379.85 10.90 o 0 6 1 134.39 132.49 5.80 o 1 6 1 0.57 0.57 1.31 < 2 6 1 451.90 437.37 10.27 o 3 6 1 182.47 174.52 8.67 o 4 6 1 528.83 515.14 16.27 o 5 6 1 1.35 3.46 2.67 < 6 6 1 3.86 2.71 2.92 < 7 6 1 0.78 2.65 2.96 < -4 7 1 0.90 2.50 4.33 < -3 7 1 15.05 16.88 5.71 o -2 7 1 137.64 142.02 9.62 o -1 7 1 7.71 13.04 4.49 o 0 7 1 7.46 8.36 2.57 o 1 7 1 177.74 180.09 7.12 o 2 7 1 614.02 620.74 17.68 o 3 7 1 9.45 9.93 3.19 o 4 7 1 54.83 62.89 7.14 o 5 7 1 9.78 6.46 3.19 o 6 7 1 87.65 84.21 9.17 o 7 7 1 0.08 1.69 3.31 < -3 8 1 107.65 108.53 13.36 o -2 8 1 95.29 103.75 12.13 o -1 8 1 171.20 159.92 9.96 o 0 8 1 56.94 53.06 6.96 o 1 8 1 1.26 1.99 2.13 < 2 8 1 8.23 6.97 2.85 o 3 8 1 5.99 5.87 2.88 o 4 8 1 142.30 138.53 9.51 o 5 8 1 69.82 70.33 8.49 o 6 8 1 127.13 120.47 11.62 o -2 9 1 4.21 2.30 4.26 < -1 9 1 47.34 53.62 8.70 o 0 9 1 89.84 110.49 11.77 o 1 9 1 56.33 52.70 8.88 o 2 9 1 23.49 23.53 4.69 o 3 9 1 91.73 87.08 8.74 o 4 9 1 313.12 313.70 14.76 o 5 9 1 1.11 0.93 3.51 < 0 10 1 9.49 13.30 5.10 o 1 10 1 2.67 2.37 3.21 < 2 10 1 6.24 6.39 3.62 < 3 10 1 6.23 8.39 3.39 o 4 10 1 2.41 2.14 3.86 < -4 -9 2 110.09 109.93 10.95 o -3 -9 2 29.61 33.91 7.78 o -2 -9 2 148.21 151.43 10.36 o -1 -9 2 99.59 100.85 11.39 o 0 -9 2 124.63 105.76 11.66 o 1 -9 2 3.39 1.01 3.34 < -5 -8 2 29.73 38.27 6.82 o -4 -8 2 121.12 137.01 9.97 o -3 -8 2 0.27 -0.57 2.00 < -2 -8 2 163.01 163.79 9.68 o -1 -8 2 12.74 11.74 3.76 o 0 -8 2 3.61 8.35 3.78 o 1 -8 2 3.50 5.61 4.23 < 2 -8 2 124.73 132.13 13.40 o -6 -7 2 19.84 27.39 5.91 o -5 -7 2 6.27 8.62 3.80 o -4 -7 2 222.21 228.74 12.10 o -3 -7 2 149.92 160.50 9.62 o -2 -7 2 46.25 41.96 5.43 o -1 -7 2 129.53 131.87 6.65 o 0 -7 2 251.17 246.62 9.18 o 1 -7 2 70.96 87.16 9.88 o 2 -7 2 189.24 184.14 11.58 o 3 -7 2 3.88 2.82 3.78 < -7 -6 2 3.10 1.11 3.68 < -6 -6 2 35.42 39.76 6.38 o -5 -6 2 406.61 426.00 16.45 o -4 -6 2 80.63 77.28 7.96 o -3 -6 2 0.65 3.06 2.30 < -2 -6 2 73.19 69.78 6.17 o -1 -6 2 2.24 1.49 1.42 < 0 -6 2 659.63 653.32 15.06 o 1 -6 2 39.32 45.03 6.90 o 2 -6 2 114.23 121.28 8.82 o 3 -6 2 33.94 30.61 6.79 o 4 -6 2 147.97 144.23 11.41 o -7 -5 2 57.05 63.54 8.38 o -6 -5 2 8.31 9.16 3.54 o -5 -5 2 380.92 382.20 14.66 o -4 -5 2 9.98 12.98 3.44 o -3 -5 2 3.45 0.64 1.75 < -2 -5 2 102.58 90.49 6.00 o -1 -5 2 1240.88 1225.86 24.58 o 0 -5 2 75.10 79.57 5.03 o 1 -5 2 502.83 491.27 12.30 o 2 -5 2 128.54 119.44 8.07 o 3 -5 2 20.25 25.91 5.91 o 4 -5 2 65.30 64.81 9.60 o 5 -5 2 80.48 85.29 12.22 o -7 -4 2 17.29 21.37 4.87 o -6 -4 2 65.43 66.53 7.22 o -5 -4 2 26.06 25.93 4.56 o -4 -4 2 56.41 59.60 6.10 o -3 -4 2 203.93 204.59 8.72 o -2 -4 2 52.67 52.50 4.99 o -1 -4 2 438.50 413.92 11.38 o 0 -4 2 52.81 54.42 3.85 o 2 -4 2 139.21 133.84 5.90 o 3 -4 2 347.91 369.74 14.65 o 4 -4 2 11.58 12.70 4.85 o 5 -4 2 32.78 32.13 7.46 o 6 -4 2 136.48 139.62 15.12 o -7 -3 2 29.40 29.24 5.58 o -6 -3 2 289.52 280.09 12.12 o -5 -3 2 271.35 249.99 10.60 o -4 -3 2 416.56 418.14 13.11 o -3 -3 2 419.50 405.14 11.88 o -2 -3 2 1487.82 1532.89 27.16 o -1 -3 2 670.16 746.92 15.37 o 0 -3 2 37.40 39.35 2.87 o 1 -3 2 905.22 879.68 16.61 o 2 -3 2 671.38 690.97 14.28 o 3 -3 2 555.88 535.67 12.68 o 4 -3 2 8.47 8.82 3.59 o 5 -3 2 101.11 113.39 11.76 o 6 -3 2 12.57 12.24 5.44 o -7 -2 2 11.45 22.25 5.91 o -6 -2 2 68.45 65.22 6.64 o -5 -2 2 21.62 19.08 3.39 o -4 -2 2 131.43 134.29 5.66 o -3 -2 2 107.45 111.53 4.72 o -2 -2 2 119.73 108.06 5.00 o -1 -2 2 39.06 27.97 2.61 o 0 -2 2 148.96 166.00 5.17 o 1 -2 2 691.61 695.84 12.52 o 2 -2 2 17.06 15.64 2.64 o 3 -2 2 272.64 274.18 8.05 o 4 -2 2 27.30 29.37 5.76 o 5 -2 2 459.22 445.03 17.00 o 6 -2 2 1.67 3.06 3.99 < 7 -2 2 19.73 15.72 6.29 o -7 -1 2 8.12 8.20 4.04 o -6 -1 2 206.13 205.59 10.64 o -5 -1 2 49.59 45.65 4.86 o -4 -1 2 1105.03 1138.65 20.01 o -3 -1 2 42.30 45.00 3.77 o -2 -1 2 102.51 99.07 3.85 o -1 -1 2 370.53 373.35 8.24 o 0 -1 2 902.18 887.31 14.62 o 1 -1 2 36.51 29.20 2.13 o 2 -1 2 77.01 73.71 3.67 o 3 -1 2 957.52 931.32 16.51 o 4 -1 2 152.01 155.27 6.36 o 5 -1 2 98.82 97.91 7.43 o 6 -1 2 119.15 120.93 9.39 o 7 -1 2 67.10 69.76 9.89 o -7 0 2 0.56 1.97 3.68 < -6 0 2 71.75 79.75 9.09 o -5 0 2 98.55 90.98 5.29 o -4 0 2 24.71 22.15 3.34 o -3 0 2 0.34 0.32 1.17 < -2 0 2 331.01 415.83 8.52 o -1 0 2 527.88 541.86 9.25 o 1 0 2 1756.14 1799.00 24.17 o 2 0 2 281.39 317.57 7.26 o 3 0 2 231.82 239.56 6.85 o 4 0 2 464.01 442.15 10.79 o 5 0 2 242.05 223.89 8.05 o 6 0 2 27.81 32.06 6.56 o 7 0 2 105.25 110.61 9.93 o -7 1 2 125.19 129.16 13.59 o -6 1 2 15.22 12.48 5.04 o -5 1 2 11.64 7.31 3.46 o -4 1 2 1080.93 1066.04 19.15 o -3 1 2 7.48 5.92 1.70 o -2 1 2 592.43 584.21 10.79 o -1 1 2 568.97 582.71 9.95 o 0 1 2 1795.20 1808.69 24.49 o 1 1 2 134.61 115.97 3.49 o 3 1 2 4.43 4.34 1.54 o 4 1 2 25.04 27.60 3.48 o 5 1 2 363.69 351.51 10.12 o 6 1 2 61.73 65.98 7.14 o 7 1 2 0.45 1.39 3.37 < -7 2 2 78.04 75.70 11.09 o -6 2 2 80.15 87.26 10.62 o -5 2 2 64.13 53.39 7.45 o -4 2 2 148.04 154.55 8.75 o -3 2 2 179.19 179.58 6.06 o -2 2 2 43.92 40.03 3.42 o -1 2 2 410.23 376.86 7.71 o 0 2 2 540.42 533.22 9.18 o 1 2 2 489.39 462.64 9.57 o 2 2 2 1.92 0.41 0.94 < 3 2 2 4.82 4.87 1.49 o 4 2 2 19.67 22.32 2.97 o 5 2 2 71.65 65.02 4.56 o 6 2 2 157.02 145.35 7.09 o 7 2 2 149.54 161.26 12.02 o 8 2 2 4.41 10.84 6.02 < -6 3 2 60.75 69.52 10.50 o -5 3 2 428.35 417.73 17.07 o -4 3 2 137.97 127.22 8.62 o -3 3 2 516.18 521.57 16.12 o -2 3 2 1528.49 1537.21 19.40 o -1 3 2 3305.74 3447.65 45.83 o 0 3 2 250.57 288.68 6.70 o 1 3 2 1056.48 982.98 15.22 o 2 3 2 0.55 -0.69 0.86 < 3 3 2 725.04 773.15 16.87 o 4 3 2 232.30 211.58 6.72 o 5 3 2 144.74 132.65 6.15 o 6 3 2 13.88 19.05 3.91 o 7 3 2 48.55 42.44 5.85 o 8 3 2 104.28 84.41 11.74 o -6 4 2 10.71 12.42 6.18 o -5 4 2 247.73 221.45 12.76 o -4 4 2 17.53 21.95 5.72 o -3 4 2 123.25 136.49 8.47 o -2 4 2 42.77 54.77 6.45 o -1 4 2 1527.54 1561.69 23.91 o 0 4 2 91.37 88.52 3.89 o 1 4 2 412.69 384.02 8.40 o 2 4 2 424.56 395.70 10.77 o 3 4 2 248.77 234.55 6.32 o 4 4 2 20.91 14.20 3.23 o 5 4 2 74.82 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109.37 12.04 o -4 4 3 528.68 511.31 18.73 o -3 4 3 268.71 259.59 11.88 o -2 4 3 112.92 113.98 5.26 o -1 4 3 82.66 80.95 4.22 o 0 4 3 1324.62 1362.86 21.52 o 1 4 3 75.55 80.56 3.86 o 2 4 3 44.04 41.09 3.86 o 3 4 3 68.12 69.18 4.89 o 4 4 3 22.04 22.46 4.00 o 5 4 3 169.56 171.83 8.94 o 6 4 3 2.60 2.57 2.63 < 7 4 3 63.10 63.05 7.42 o -5 5 3 36.05 49.85 9.11 o -4 5 3 0.16 2.44 4.01 < -3 5 3 0.04 1.55 3.30 < -2 5 3 904.47 908.39 23.65 o -1 5 3 15.23 19.45 3.11 o 0 5 3 225.48 224.00 7.12 o 1 5 3 211.89 200.60 6.52 o 2 5 3 26.10 26.56 3.55 o 3 5 3 6.36 2.93 1.46 o 4 5 3 82.43 89.51 6.39 o 5 5 3 206.64 197.24 9.92 o 6 5 3 4.60 10.75 3.80 o 7 5 3 37.87 26.90 5.15 o -5 6 3 3.81 5.20 4.96 < -4 6 3 74.00 87.27 11.15 o -3 6 3 81.96 90.74 10.81 o -2 6 3 877.83 858.61 24.13 o -1 6 3 32.25 33.52 4.66 o 0 6 3 11.15 11.38 2.46 o 1 6 3 44.40 41.15 4.00 o 2 6 3 1469.88 1456.81 28.71 o 3 6 3 69.04 61.19 6.33 o 4 6 3 169.89 167.13 8.92 o 5 6 3 98.63 100.63 7.64 o 6 6 3 46.46 34.77 6.05 o 7 6 3 1.19 -0.27 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190.21 190.14 7.71 o 5 1 4 22.03 26.07 4.20 o 6 1 4 89.01 89.09 7.86 o 7 1 4 79.13 89.50 10.76 o -6 2 4 69.09 80.90 10.85 o -5 2 4 180.35 174.32 10.78 o -4 2 4 129.47 119.15 7.98 o -3 2 4 148.13 150.39 6.29 o -2 2 4 310.33 303.26 8.42 o -1 2 4 363.03 406.41 9.52 o 0 2 4 186.73 198.87 6.31 o 1 2 4 144.44 172.39 5.68 o 2 2 4 288.70 268.11 7.39 o 3 2 4 472.25 438.17 10.50 o 4 2 4 946.15 937.29 20.72 o 5 2 4 10.86 10.56 3.10 o 6 2 4 23.97 27.63 4.50 o 7 2 4 134.02 144.82 11.35 o -6 3 4 0.04 1.29 4.23 < -5 3 4 190.15 172.44 11.36 o -4 3 4 76.29 80.44 9.53 o -3 3 4 406.85 391.13 14.22 o -2 3 4 116.77 108.86 5.15 o -1 3 4 445.76 444.70 10.40 o 0 3 4 912.69 970.25 17.01 o 1 3 4 640.49 690.16 13.50 o 2 3 4 349.39 337.20 9.99 o 3 3 4 171.33 180.24 7.78 o 4 3 4 46.32 46.30 5.45 o 5 3 4 2.48 2.63 2.50 < 6 3 4 99.67 107.05 8.03 o 7 3 4 7.59 4.65 2.93 < -6 4 4 37.36 45.00 8.95 o -5 4 4 0.28 1.33 4.51 < -4 4 4 15.80 21.15 6.34 o -3 4 4 413.87 420.38 15.86 o -2 4 4 218.76 215.26 7.62 o -1 4 4 44.55 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69.31 4.31 o 1 3 5 75.53 67.42 4.08 o 2 3 5 10.68 9.27 2.25 o 3 3 5 1486.67 1464.41 27.98 o 4 3 5 0.55 -0.64 2.01 < 5 3 5 231.60 244.85 10.97 o 6 3 5 0.64 -2.01 1.88 < 7 3 5 59.80 57.33 7.05 o -5 4 5 2.54 -0.46 3.20 < -4 4 5 20.38 16.14 5.10 o -3 4 5 45.25 45.11 7.18 o -2 4 5 0.04 0.78 1.95 < -1 4 5 0.09 -0.90 1.59 < 0 4 5 109.66 111.47 5.51 o 1 4 5 702.96 706.72 16.23 o 2 4 5 20.42 24.42 3.72 o 3 4 5 468.88 476.12 14.17 o 4 4 5 14.87 9.76 2.83 o 5 4 5 18.29 20.13 4.38 o 6 4 5 4.39 4.16 2.63 < 7 4 5 147.29 160.37 10.28 o -5 5 5 6.26 2.84 5.21 < -4 5 5 41.73 46.91 8.24 o -3 5 5 20.55 24.99 6.41 o -2 5 5 484.09 502.89 17.01 o -1 5 5 33.47 39.86 4.72 o 0 5 5 1.98 2.91 2.11 < 1 5 5 435.63 419.98 12.51 o 2 5 5 109.89 117.69 6.66 o 3 5 5 9.66 6.48 2.42 o 4 5 5 219.51 228.85 10.55 o 5 5 5 716.52 719.81 20.71 o 6 5 5 19.52 19.85 4.69 o 7 5 5 30.55 32.68 6.44 o -4 6 5 33.87 42.63 9.09 o -3 6 5 12.05 9.61 4.88 < -2 6 5 7.86 9.35 4.17 o -1 6 5 8.14 10.15 2.93 o 0 6 5 1.23 1.08 1.97 < 1 6 5 0.96 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6.44 o 3 4 6 11.01 7.50 2.58 o 4 4 6 276.61 278.35 11.81 o 5 4 6 21.19 15.77 4.07 o 6 4 6 0.22 3.03 2.77 < 7 4 6 4.90 9.01 6.38 < -5 5 6 27.80 35.18 7.97 o -4 5 6 18.68 23.58 6.87 o -3 5 6 48.12 52.50 8.41 o -2 5 6 222.73 221.12 11.34 o -1 5 6 106.39 104.93 6.08 o 0 5 6 70.88 72.27 5.30 o 1 5 6 12.94 8.91 2.67 o 2 5 6 1236.91 1257.14 26.41 o 3 5 6 17.90 19.32 4.03 o 4 5 6 38.87 39.41 5.77 o 5 5 6 21.94 25.48 5.00 o 6 5 6 249.58 253.35 12.63 o 7 5 6 4.16 13.95 7.79 < -4 6 6 86.95 98.76 12.89 o -3 6 6 318.99 319.07 15.27 o -2 6 6 2.70 2.10 3.56 < -1 6 6 14.33 18.07 3.75 o 0 6 6 1.97 1.53 2.13 < 1 6 6 108.93 105.18 6.91 o 2 6 6 383.93 366.02 13.09 o 3 6 6 92.51 92.46 7.48 o 4 6 6 63.13 64.41 7.12 o 5 6 6 38.86 45.43 6.85 o 6 6 6 218.76 207.29 11.90 o -3 7 6 4.55 7.63 4.69 < -2 7 6 6.98 8.82 5.02 < -1 7 6 57.77 58.66 7.95 o 0 7 6 16.58 12.64 3.59 o 1 7 6 238.19 239.06 10.55 o 2 7 6 81.99 73.79 7.36 o 3 7 6 47.33 56.56 6.97 o 4 7 6 173.15 171.99 10.14 o 5 7 6 181.43 178.86 11.20 o 6 7 6 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14.79 5.47 o 0 -3 7 119.63 47.09 12.55 o 1 -3 7 12.26 10.92 5.21 o 2 -3 7 4.06 3.24 4.63 < 3 -3 7 258.13 211.66 15.00 o 4 -3 7 0.03 -7.87 10.75 < -5 -2 7 73.92 70.50 13.96 o -4 -2 7 10.09 15.23 5.82 o -3 -2 7 0.73 6.84 5.34 < -1 -2 7 2.68 3.50 3.68 < 1 -2 7 40.19 60.39 9.32 o 2 -2 7 150.40 151.24 11.74 o 3 -2 7 17.31 11.61 4.91 o 4 -2 7 140.29 59.88 13.92 o -5 -1 7 78.83 75.46 12.75 o -3 -1 7 2.78 4.72 4.63 < -2 -1 7 0.53 3.28 3.36 < -1 -1 7 86.83 98.58 8.86 o 0 -1 7 343.77 350.18 15.92 o 1 -1 7 216.88 244.18 13.41 o 2 -1 7 138.66 158.54 11.34 o 3 -1 7 0.66 0.67 3.97 < 4 -1 7 49.31 33.01 7.22 o -5 0 7 30.30 3.39 8.85 < -4 0 7 5.23 3.60 4.55 < 0 0 7 202.64 222.99 12.59 o 1 0 7 206.13 205.78 12.04 o 2 0 7 13.16 22.95 5.94 o 3 0 7 20.86 16.94 5.78 o 4 0 7 107.00 132.55 11.69 o 5 0 7 39.50 34.27 8.68 o -5 1 7 83.47 4.85 9.17 < -2 1 7 15.61 8.83 4.48 < -1 1 7 87.03 61.95 7.88 o 0 1 7 84.24 76.74 8.49 o 1 1 7 30.15 41.72 7.55 o 2 1 7 75.78 90.88 9.00 o 3 1 7 12.25 17.45 6.07 o 4 1 7 256.79 281.65 15.95 o 5 1 7 1.42 2.74 5.31 < 6 1 7 3.23 0.67 10.86 < -5 2 7 109.84 32.59 12.04 o -4 2 7 7.73 4.08 6.97 < -3 2 7 27.57 35.51 8.19 o -2 2 7 10.70 5.94 4.32 < 0 2 7 168.26 160.82 10.64 o 1 2 7 159.90 158.84 10.53 o 2 2 7 5.05 8.99 3.96 o 3 2 7 308.85 317.19 15.28 o 4 2 7 12.79 18.94 6.37 o 5 2 7 31.72 28.27 7.52 o 6 2 7 14.37 6.14 5.75 < -5 3 7 29.35 44.09 14.10 o -4 3 7 7.52 5.37 8.92 < 0 3 7 9.93 8.06 4.21 < 1 3 7 98.60 107.18 8.85 o 2 3 7 192.91 186.62 11.40 o 3 3 7 78.77 74.14 9.17 o 5 3 7 0.14 0.34 4.37 < 6 3 7 20.72 32.57 9.86 o -5 4 7 94.35 110.16 22.35 o -4 4 7 130.85 146.35 18.39 o -3 4 7 77.71 89.17 10.86 o -2 4 7 14.60 12.63 3.25 o 0 4 7 62.42 77.98 11.97 o 1 4 7 554.62 500.41 19.08 o 2 4 7 2.65 2.35 3.58 < 3 4 7 42.21 40.10 6.59 o 4 4 7 15.99 12.06 4.96 o 5 4 7 70.64 83.57 14.47 o 6 4 7 0.79 4.44 5.65 < -4 5 7 25.18 31.30 7.92 o -3 5 7 87.86 98.24 10.85 o -2 5 7 6.19 8.42 4.55 < -1 5 7 268.98 280.15 10.61 o 0 5 7 25.40 30.27 4.27 o 1 5 7 10.98 6.17 3.96 < 2 5 7 5.63 3.99 3.76 < 4 5 7 61.89 65.14 13.09 o 5 5 7 42.77 45.47 11.81 o 6 5 7 51.86 80.70 15.17 o -4 6 7 4.95 6.07 5.08 < -3 6 7 21.21 18.13 5.98 o -2 6 7 469.57 468.30 17.99 o -1 6 7 12.09 10.21 3.33 o 0 6 7 155.67 168.32 8.53 o 1 6 7 115.19 108.24 7.55 o 2 6 7 34.93 30.27 5.74 o 4 6 7 29.01 40.52 11.03 o 5 6 7 19.76 26.86 9.92 o 6 6 7 0.71 2.15 4.81 < -3 7 7 22.98 27.40 8.02 o -2 7 7 189.68 189.99 12.25 o -1 7 7 15.55 20.57 5.48 o 0 7 7 8.83 9.16 3.22 o 1 7 7 69.16 70.74 7.31 o 2 7 7 148.99 167.12 9.55 o 3 7 7 5.71 6.86 3.55 < 4 7 7 72.54 81.54 15.23 o 5 7 7 130.33 153.62 17.92 o -2 8 7 7.16 8.76 4.84 < -1 8 7 0.13 1.41 3.62 < 1 8 7 10.47 8.83 3.04 o 2 8 7 251.74 260.63 12.50 o 3 8 7 20.72 24.43 5.06 o 4 8 7 80.10 96.93 16.65 o 5 8 7 13.73 7.35 7.40 < -1 9 7 56.60 61.51 8.62 o 1 9 7 0.23 1.16 3.19 < 2 9 7 15.55 18.15 4.43 o 3 9 7 22.15 24.24 5.12 o 4 9 7 281.44 285.46 24.47 o -1 -5 8 18.62 8.66 6.39 < 0 -5 8 0.79 -1.43 5.05 < -3 -4 8 35.27 35.60 11.61 o -2 -4 8 24.37 13.20 6.35 o -1 -4 8 35.56 33.14 7.60 o 0 -4 8 35.66 23.45 6.98 o 1 -4 8 37.62 13.86 10.19 < 2 -4 8 107.87 136.17 19.60 o -4 -3 8 6.41 7.89 5.97 < -3 -3 8 24.26 19.29 6.42 o -2 -3 8 0.04 -0.53 3.42 < -1 -3 8 3.05 -0.65 3.91 < 0 -3 8 62.69 68.17 9.85 o 1 -3 8 3.66 4.67 5.04 < 2 -3 8 26.24 26.97 7.58 o 3 -3 8 30.20 15.87 8.27 < -4 -2 8 4.26 4.76 5.45 < -3 -2 8 0.43 0.58 3.79 < -2 -2 8 57.26 67.59 13.91 o 0 -2 8 10.97 7.51 4.43 < 1 -2 8 125.27 142.51 11.73 o 2 -2 8 67.16 66.47 11.09 o 3 -2 8 1.44 -3.24 4.70 < 4 -2 8 24.73 12.10 12.78 < -5 -1 8 7.40 10.39 6.30 < -4 -1 8 53.29 68.47 13.38 o -3 -1 8 232.11 153.99 18.92 o -2 -1 8 9.16 5.97 5.10 < 0 -1 8 1.70 -0.71 3.04 < 1 -1 8 6.11 6.75 4.87 < 2 -1 8 12.19 12.20 6.18 < 3 -1 8 51.41 50.18 9.18 o 4 -1 8 12.15 14.38 7.30 < -5 0 8 51.23 4.55 7.35 < -4 0 8 31.34 22.40 6.64 o -2 0 8 114.17 105.00 12.52 o -1 0 8 71.74 75.50 12.36 o 0 0 8 19.49 18.34 5.09 o 1 0 8 483.99 509.67 20.75 o 2 0 8 95.53 96.31 9.88 o 3 0 8 129.75 148.60 11.95 o 4 0 8 11.02 12.26 5.81 o 5 0 8 23.09 25.29 8.55 o -5 1 8 0.08 6.47 10.75 < -4 1 8 70.64 43.06 8.35 o -3 1 8 51.56 62.85 11.61 o -1 1 8 62.35 53.95 8.12 o 0 1 8 43.46 41.85 7.78 o 1 1 8 169.83 182.82 12.08 o 2 1 8 40.42 48.60 8.60 o 3 1 8 5.10 5.19 4.84 < 4 1 8 1.29 1.38 5.47 < 5 1 8 137.01 112.39 12.45 o -5 2 8 1.47 3.94 10.99 < -3 2 8 71.01 86.87 13.76 o -2 2 8 0.82 -0.28 4.44 < -1 2 8 35.67 22.01 5.45 o 1 2 8 19.91 23.78 6.00 o 2 2 8 38.47 40.24 7.48 o 3 2 8 315.38 357.82 17.42 o 4 2 8 63.48 59.74 9.76 o 5 2 8 73.51 76.29 11.33 o -4 3 8 1.09 3.41 6.27 < -2 3 8 7.11 7.94 4.69 < -1 3 8 0.20 -1.22 3.75 < 0 3 8 120.14 126.11 13.79 o 1 3 8 51.64 52.12 7.86 o 2 3 8 0.57 3.84 4.29 < 3 3 8 40.86 50.96 8.39 o 4 3 8 173.23 179.60 12.90 o 5 3 8 10.84 7.76 5.60 < -4 4 8 65.53 7.39 9.81 < -3 4 8 12.33 -0.63 8.19 < -1 4 8 3.44 1.49 3.89 < 0 4 8 79.67 94.42 13.89 o 1 4 8 44.17 31.25 6.38 o 2 4 8 214.86 216.57 13.36 o 3 4 8 1.89 2.42 3.59 < 4 4 8 9.33 14.27 5.40 o 5 4 8 54.71 73.33 14.84 o 6 4 8 33.09 38.34 11.79 o -3 5 8 80.77 16.13 9.66 < -2 5 8 2.79 8.26 9.03 < 0 5 8 48.04 26.99 6.09 o 1 5 8 11.02 6.02 4.00 < 2 5 8 13.22 5.16 4.26 < 3 5 8 0.68 0.75 3.78 < 4 5 8 5.11 11.07 6.80 < 5 5 8 0.54 2.56 5.85 < -3 6 8 105.25 101.21 22.25 o -1 6 8 13.82 0.45 6.21 < 0 6 8 19.87 8.84 3.92 o 2 6 8 130.11 109.65 9.98 o 3 6 8 1.23 2.25 4.04 < 4 6 8 11.41 11.42 7.26 < 5 6 8 1.06 4.63 5.92 < -2 7 8 0.55 4.15 7.64 < 0 7 8 7.39 6.24 4.09 < 1 7 8 53.05 59.15 11.90 o 2 7 8 52.69 64.50 13.20 o 3 7 8 2.11 1.49 5.33 < 4 7 8 3.32 4.72 5.21 < 5 7 8 12.89 13.31 8.36 < -1 8 8 46.45 -1.64 5.01 < 0 8 8 33.33 4.89 7.55 < 2 8 8 9.73 11.64 6.76 < 3 8 8 125.88 143.05 20.63 o 4 8 8 55.88 70.79 14.76 o 2 9 8 30.48 30.32 9.71 o 3 9 8 53.09 52.91 12.89 o -2 -3 9 48.92 56.01 14.64 o -1 -3 9 6.46 11.62 6.77 < 0 -3 9 77.27 62.16 10.30 o 1 -3 9 19.84 16.01 6.54 o -3 -2 9 0.01 -0.39 4.80 < -2 -2 9 9.57 11.00 6.34 < -1 -2 9 40.46 31.57 7.29 o 0 -2 9 5.42 3.58 4.61 < 1 -2 9 0.29 -2.84 3.72 < 2 -2 9 31.29 34.75 8.80 o -3 -1 9 1.28 3.80 4.94 < -2 -1 9 10.16 7.59 5.26 < -1 -1 9 29.48 19.18 5.70 o 0 -1 9 212.21 214.09 14.40 o 1 -1 9 12.29 16.10 6.13 o 2 -1 9 9.54 9.73 5.65 < 3 -1 9 0.64 -0.70 4.91 < -4 0 9 48.71 28.71 7.52 o -3 0 9 0.49 2.26 5.17 < -1 0 9 1.00 7.63 4.73 < 0 0 9 40.35 30.88 6.82 o 1 0 9 14.89 21.25 6.61 o 2 0 9 79.08 109.17 14.09 o 3 0 9 47.18 77.42 12.57 o 4 0 9 52.54 57.50 10.76 o -4 1 9 116.48 115.32 16.97 o -3 1 9 37.69 23.82 6.41 o -2 1 9 75.70 98.37 15.95 o 0 1 9 81.53 41.28 10.69 o 1 1 9 0.01 1.22 3.57 < 2 1 9 165.68 176.71 12.89 o 3 1 9 0.55 -0.89 4.65 < 4 1 9 3.88 2.90 5.49 < -4 2 9 1.44 -1.07 10.22 < -2 2 9 24.99 17.76 5.67 o -1 2 9 9.67 9.36 5.17 < 1 2 9 6.86 5.64 4.64 < 2 2 9 56.17 65.47 9.61 o 3 2 9 25.12 34.33 8.48 o 4 2 9 238.81 231.36 15.93 o -3 3 9 15.11 4.72 10.05 < -2 3 9 0.03 -0.29 5.09 < 0 3 9 96.73 110.14 15.99 o 1 3 9 165.85 171.52 12.95 o 2 3 9 11.51 10.34 5.13 o 3 3 9 0.45 -2.54 3.79 < 4 3 9 203.34 224.12 15.23 o 5 3 9 18.07 17.45 7.78 o -3 4 9 51.98 7.08 9.83 < -2 4 9 17.33 5.19 5.30 < -1 4 9 72.28 83.18 14.41 o 0 4 9 3.12 0.07 3.76 < 1 4 9 5.76 6.74 4.35 < 2 4 9 76.11 73.37 9.97 o 3 4 9 116.80 120.17 11.83 o 4 4 9 2.31 5.50 4.69 < 5 4 9 85.79 93.01 16.79 o -3 5 9 58.12 0.52 8.67 < -2 5 9 4.60 -2.98 4.38 < -1 5 9 2.81 4.93 4.51 < 0 5 9 78.08 79.21 13.84 o 1 5 9 163.53 182.52 17.88 o 2 5 9 37.29 29.50 6.90 o 3 5 9 78.00 62.82 9.39 o 4 5 9 2.32 1.76 5.46 < 5 5 9 7.48 6.15 6.74 < 0 6 9 71.83 71.14 13.05 o 1 6 9 5.13 3.64 4.11 < 2 6 9 24.52 15.60 5.36 o 3 6 9 11.50 11.39 5.94 < 4 6 9 0.66 5.52 5.81 < -1 7 9 16.73 -0.61 7.29 < 0 7 9 80.55 107.00 16.33 o 1 7 9 31.55 18.40 5.58 o 2 7 9 43.38 61.49 13.51 o 3 7 9 27.61 30.88 11.31 o 4 7 9 5.13 1.29 6.16 < 1 8 9 42.57 24.19 6.82 o 2 8 9 9.28 15.02 7.82 < 3 8 9 2.58 6.70 5.99 < -2 -1 10 11.34 4.18 5.43 < -1 -1 10 20.04 11.90 5.78 o 0 -1 10 1.72 3.51 5.83 < 1 -1 10 106.77 142.54 16.88 o -2 0 10 0.62 5.18 4.73 < -1 0 10 17.69 11.26 5.10 o 0 0 10 133.65 137.64 20.14 o 1 0 10 89.82 91.16 12.13 o 2 0 10 11.88 21.49 8.10 o -2 1 10 0.26 6.53 6.24 < -1 1 10 84.43 80.81 14.98 o 0 1 10 0.36 0.90 3.98 < 1 1 10 2.03 4.90 4.70 < 2 1 10 7.52 12.04 5.87 o 3 1 10 101.05 137.60 17.39 o -2 2 10 27.91 12.58 6.71 < -1 2 10 5.18 3.33 5.69 < 0 2 10 24.55 14.13 5.54 o 1 2 10 61.61 63.48 14.14 o 2 2 10 57.49 71.26 10.88 o 3 2 10 31.04 39.62 9.43 o -2 3 10 31.59 14.34 5.91 o -1 3 10 8.76 6.80 5.95 < 0 3 10 65.36 66.18 13.79 o 1 3 10 112.00 123.00 18.84 o 2 3 10 7.28 3.65 5.08 < 3 3 10 17.10 26.75 7.87 o -2 4 10 5.58 2.24 4.64 < -1 4 10 19.31 10.08 4.96 o 0 4 10 129.18 149.65 17.61 o 1 4 10 0.80 2.01 4.45 < 2 4 10 74.11 65.65 10.18 o 3 4 10 53.07 52.00 9.39 o 4 4 10 0.48 4.49 6.69 < -1 5 10 11.07 9.38 5.36 < 0 5 10 32.34 12.74 5.57 o 1 5 10 0.02 -1.86 3.80 < 2 5 10 68.55 55.08 12.71 o 3 5 10 41.06 26.15 7.24 o 0 6 10 29.92 38.49 11.53 o 1 6 10 35.37 25.27 7.66 o 2 6 10 192.57 209.31 20.77 o 3 6 10 21.27 20.45 9.24 o 1 7 10 29.77 31.41 10.33 o 0 2 11 9.18 2.20 5.57 < 1 2 11 6.89 7.37 8.52 < 0 3 11 29.44 18.94 6.83 o 1 3 11 25.84 18.61 7.71 o 1 4 11 6.60 3.76 6.68 < loop_ _twin_refln_datum_id _twin_refln_individual_id _twin_refln_index_h _twin_refln_index_k _twin_refln_index_l _twin_refln_F_squared_calc _twin_refln_F_squared_meas _twin_refln_F_squared_sigma _twin_refln_include_status ? ? ? ? ? ? ? ? ?