data_jo45 _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'H4 Al0 Be2.40 Ca1.60 Na0.80 O12.80 Si3.20 Sr0' _chemical_formula_weight 402.86 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Be' 'Be' 0.0005 0.0002 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Na' 'Na' 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ca' 'Ca' 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Sr' 'Sr' -1.5307 3.2498 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Al' 'Al' 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting ? _symmetry_space_group_name_H-M ? loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 7.1222(4) _cell_length_b 19.8378(11) _cell_length_c 9.8071(5) _cell_angle_alpha 90.00 _cell_angle_beta 111.2870(10) _cell_angle_gamma 90.00 _cell_volume 1291.10(12) _cell_formula_units_Z 5 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 2.591 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 1008 _exptl_absorpt_coefficient_mu 1.385 _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 6089 _diffrn_reflns_av_R_equivalents 0.0177 _diffrn_reflns_av_sigmaI/netI 0.0268 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_theta_min 1.03 _diffrn_reflns_theta_max 22.53 _reflns_number_total 3388 _reflns_number_gt 3283 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0860P)^2^+2.6452P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.00 _refine_ls_number_reflns 3388 _refine_ls_number_parameters 243 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0476 _refine_ls_R_factor_gt 0.0462 _refine_ls_wR_factor_ref 0.1270 _refine_ls_wR_factor_gt 0.1234 _refine_ls_goodness_of_fit_ref 1.093 _refine_ls_restrained_S_all 1.093 _refine_ls_shift/su_max 0.347 _refine_ls_shift/su_mean 0.039 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Ca1 Ca 0.89757(13) 0.5000 0.00230(17) 0.0185(2) Uani 1 1 d . . . Ca2 Ca 0.7780(2) 0.50207(9) 0.42026(15) 0.0328(4) Uani 1 1 d . . . Ca3 Ca 0.12972(17) 0.74715(8) 0.35603(14) 0.0167(3) Uani 1 1 d . . . Ca4 Ca 0.7858(3) 0.74839(8) 0.64373(14) 0.0269(4) Uani 1 1 d . . . Na1 Na 0.3865(3) 0.26159(12) -0.0032(4) 0.0332(7) Uani 1 1 d . . . Na2 Ca 0.3576(3) 0.50196(11) 0.58439(18) 0.0171(4) Uani 0.75 1 d P . . Si1 Si 0.5275(2) 0.62592(8) 0.82772(17) 0.0079(4) Uiso 1 1 d . . . Si2 Si 0.1005(2) 0.62791(9) 0.61553(18) 0.0104(4) Uiso 1 1 d . . . Si3 Si 0.6911(3) 0.37417(9) 0.16563(18) 0.0097(4) Uiso 1 1 d . . . Si4 Si 0.5079(3) 0.37408(10) 0.39840(19) 0.0112(4) Uiso 1 1 d . . . Si5 Si 0.6965(3) 0.62780(10) 0.1717(2) 0.0153(5) Uiso 1 1 d . . . Si6 Si 0.4881(3) 0.62929(10) 0.3880(2) 0.0145(4) Uiso 1 1 d . . . Si7 Si 0.5233(3) 0.37478(10) 0.8338(2) 0.0162(5) Uiso 1 1 d . . . Si8 Si 1.1111(3) 0.37306(10) 0.6080(2) 0.0127(4) Uiso 1 1 d . . . Be1 Be 0.3433(11) 0.2500(5) 0.6789(7) 0.0072(14) Uiso 1 1 d . . . Be2 Be 0.0913(12) 0.4239(4) 0.3217(8) 0.0080(17) Uiso 1 1 d . . . Be3 Be -0.2455(13) 0.5752(4) 0.6661(8) 0.0078(17) Uiso 1 1 d . . . Be4 Be 0.6498(13) 0.2482(6) 0.3082(9) 0.0175(19) Uiso 1 1 d . . . Be5 Be 0.7870(15) 0.4209(4) 0.6835(9) 0.0136(19) Uiso 1 1 d . . . Be6 Be 0.0850(13) 0.5775(4) 0.3131(8) 0.0055(17) Uiso 1 1 d . . . O1 O 0.5465(5) 0.63182(17) 0.0017(5) 0.0142(8) Uiso 1 1 d . . . O2 O 0.6915(6) 0.5734(2) 0.8170(4) 0.0085(9) Uiso 1 1 d . . . O3 O 0.3013(6) 0.5920(2) 0.7373(4) 0.0089(9) Uiso 1 1 d . . . O4 O 0.5370(7) 0.7008(2) 0.7675(4) 0.0109(10) Uiso 1 1 d . . . O5 O -0.0717(7) 0.6332(2) 0.6877(5) 0.0152(10) Uiso 1 1 d . . . O6 O 0.1578(7) 0.7047(2) 0.5851(4) 0.0093(10) Uiso 1 1 d . . . O7 O 0.0389(6) 0.5797(2) 0.4780(4) 0.0136(10) Uiso 1 1 d . . . O8 O 0.8937(7) 0.4140(2) 0.1772(5) 0.0160(11) Uiso 1 1 d . . . O9 O 0.5914(7) 0.4096(2) 0.2703(5) 0.0135(10) Uiso 1 1 d . . . O10 O 0.7249(8) 0.2977(2) 0.2030(5) 0.0242(12) Uiso 1 1 d . . . O11 O 0.5207(6) 0.38707(19) 0.9964(6) 0.0213(9) Uiso 1 1 d . . . O12 O 0.5939(6) 0.2979(2) 0.4299(4) 0.0048(9) Uiso 1 1 d . . . O13 O 0.2618(7) 0.3669(2) 0.3277(5) 0.0137(11) Uiso 1 1 d . . . O14 O 0.5860(7) 0.4239(3) 0.5310(5) 0.0195(11) Uiso 1 1 d . . . O15 O 0.7712(8) 0.7024(2) 0.2299(5) 0.0189(12) Uiso 1 1 d . . . O16 O 0.8734(8) 0.5756(3) 0.1872(5) 0.0241(13) Uiso 1 1 d . . . O17 O 0.5550(8) 0.5956(2) 0.2555(5) 0.0185(11) Uiso 1 1 d . . . O18 O 0.5749(8) 0.7035(2) 0.4185(5) 0.0161(11) Uiso 1 1 d . . . O19 O 0.2492(9) 0.6348(3) 0.3315(6) 0.0301(14) Uiso 1 1 d . . . O20 O 0.5863(7) 0.5767(3) 0.5268(5) 0.0141(11) Uiso 1 1 d . . . O21 O 0.7094(7) 0.4162(2) 0.8224(5) 0.0128(11) Uiso 1 1 d . . . O22 O 0.3090(8) 0.4105(2) 0.7240(5) 0.0141(11) Uiso 1 1 d . . . O23 O 0.5038(7) 0.2940(2) 0.8110(4) 0.0110(10) Uiso 1 1 d . . . O24 O 0.0450(8) 0.4250(3) 0.4695(5) 0.0168(11) Uiso 1 1 d . . . O25 O 0.1702(10) 0.2997(3) 0.5724(6) 0.0322(14) Uiso 1 1 d . . . O26 O 0.9476(8) 0.3687(2) 0.6862(5) 0.0226(13) Uiso 1 1 d . . . OH27 O -0.1154(6) 0.5001(2) 0.6929(4) 0.0157(9) Uiso 1 1 d . . . OH28 O 0.1868(6) 0.5005(3) 0.3118(4) 0.0146(10) Uiso 1 1 d . . . OW1 O 0.1538(8) 0.4286(3) 0.9894(7) 0.0521(14) Uiso 1 1 d . . . OW2 O 0.1373(7) 0.5905(2) 0.0008(7) 0.0397(11) Uiso 1 1 d . . . OW3 O 0.1506(12) 0.7373(4) 0.1235(8) 0.0329(9) Uiso 0.67 1 d P . . OW4 O 0.8794(10) 0.7883(4) 0.9036(7) 0.0329(9) Uiso 0.77 1 d P . . OW5 O 0.0375(15) 0.7283(5) 0.8731(10) 0.0329(9) Uiso 0.56 1 d P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ca1 0.0145(4) 0.0207(5) 0.0212(5) 0.0014(7) 0.0077(6) 0.0007(5) Ca2 0.0301(7) 0.0303(8) 0.0359(7) 0.0011(8) 0.0093(6) -0.0017(9) Ca3 0.0025(5) 0.0185(6) 0.0264(6) -0.0035(6) 0.0018(5) 0.0044(7) Ca4 0.0594(9) 0.0117(6) 0.0097(6) 0.0013(7) 0.0127(7) 0.0104(9) Na1 0.0308(12) 0.0314(12) 0.0271(12) -0.0053(15) -0.0019(17) -0.0111(11) Na2 0.0173(8) 0.0188(9) 0.0213(8) 0.0016(9) 0.0143(7) -0.0049(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ca1 OW1 2.350(6) 1_654 ? Ca1 O2 2.375(4) 1_554 ? Ca1 O16 2.407(5) . ? Ca1 O8 2.426(5) . ? Ca1 O21 2.441(4) 1_554 ? Ca1 OW2 2.482(5) 1_655 ? Ca1 OH28 2.986(4) 1_655 ? Ca1 OH27 3.002(4) 1_654 ? Ca1 Be6 3.238(8) 1_655 ? Ca1 Be2 3.295(8) 1_655 ? Ca1 Be5 3.327(9) 1_554 ? Ca1 Be3 3.420(8) 1_654 ? Ca2 O7 2.320(5) 1_655 ? Ca2 O24 2.350(6) 1_655 ? Ca2 O9 2.424(4) . ? Ca2 O20 2.487(5) . ? Ca2 OH27 2.501(4) 1_655 ? Ca2 O14 2.555(6) . ? Ca2 O17 2.591(5) . ? Ca2 Be3 2.871(8) 1_655 ? Ca2 O16 2.990(6) . ? Ca2 Be5 3.024(9) . ? Ca2 Be6 3.129(9) 1_655 ? Ca2 Be2 3.144(9) 1_655 ? Ca3 O6 2.338(4) . ? Ca3 OW3 2.347(8) . ? Ca3 O19 2.428(6) . ? Ca3 O26 2.475(5) 2_656 ? Ca3 O12 2.509(4) 2_656 ? Ca3 O15 2.558(6) 1_455 ? Ca3 O25 2.690(7) 2_556 ? Ca3 Be4 3.091(8) 2_656 ? Ca3 Si8 3.122(2) 2_656 ? Ca3 O18 3.125(6) . ? Ca3 Be1 3.261(8) 2_556 ? Ca3 Si6 3.391(2) . ? Ca4 OW5 2.346(9) 1_655 ? Ca4 O18 2.349(5) . ? Ca4 O13 2.406(5) 2_656 ? Ca4 O25 2.472(6) 2_656 ? Ca4 O5 2.473(5) 1_655 ? Ca4 OW4 2.516(7) . ? Ca4 O4 2.658(5) . ? Ca4 O12 2.717(4) 2_656 ? Ca4 Be1 2.957(7) 2_656 ? Ca4 O6 3.034(5) 1_655 ? Ca4 Si4 3.184(2) 2_656 ? Ca4 Be4 3.303(10) 2_656 ? Na1 O23 2.353(6) 1_554 ? Na1 O15 2.402(6) 2_645 ? Na1 OW4 2.483(8) 2_646 ? Na1 O4 2.487(5) 2_646 ? Na1 O1 2.617(4) 2_645 ? Na1 O10 2.621(5) . ? Na1 O11 2.667(4) 1_554 ? Na1 Be4 2.960(8) . ? Na1 Be1 3.028(8) 1_554 ? Na1 Si5 3.068(3) 2_645 ? Na1 Si7 3.110(4) 1_554 ? Na1 Si1 3.133(3) 2_646 ? Na2 O22 2.374(5) . ? Na2 O20 2.417(5) . ? Na2 O14 2.436(6) . ? Na2 O3 2.457(5) . ? Na2 OH28 2.503(4) . ? Na2 O24 2.596(5) . ? Na2 O7 2.627(5) . ? Na2 O2 2.988(4) . ? Na2 Be2 3.015(7) . ? Na2 Be3 3.016(9) 1_655 ? Na2 Be6 3.057(8) . ? Na2 Si8 3.158(3) 1_455 ? Si1 O2 1.597(5) . ? Si1 O4 1.609(4) . ? Si1 O1 1.666(5) 1_556 ? Si1 O3 1.672(4) . ? Si1 Na1 3.133(3) 2_656 ? Si1 Ca1 3.5837(18) 1_556 ? Si2 O7 1.580(5) . ? Si2 O5 1.627(5) . ? Si2 O6 1.633(4) . ? Si2 O3 1.655(4) . ? Si2 OH27 3.196(5) . ? Si2 Ca4 3.356(2) 1_455 ? Si2 OW5 3.372(10) . ? Si2 Ca2 3.461(2) 1_455 ? Si3 O10 1.560(5) . ? Si3 O9 1.606(5) . ? Si3 O8 1.613(5) . ? Si3 O11 1.682(5) 1_554 ? Si3 OW5 3.576(10) 2_646 ? Si4 O14 1.566(5) . ? Si4 O12 1.619(4) . ? Si4 O13 1.640(5) . ? Si4 O9 1.724(5) . ? Si4 Ca4 3.184(2) 2_646 ? Si4 OH28 3.291(5) . ? Si4 OW4 3.653(7) 2_646 ? Si5 O16 1.595(6) . ? Si5 O15 1.605(5) . ? Si5 O1 1.623(5) . ? Si5 O17 1.643(6) . ? Si5 Na1 3.068(3) 2_655 ? Si6 O18 1.583(5) . ? Si6 O19 1.591(7) . ? Si6 O20 1.655(5) . ? Si6 O17 1.677(6) . ? Si6 OH28 3.245(5) . ? Si6 OW3 3.546(7) . ? Si7 O21 1.597(5) . ? Si7 O23 1.617(5) . ? Si7 O11 1.620(6) . ? Si7 O22 1.673(5) . ? Si7 Na1 3.110(4) 1_556 ? Si7 OW3 3.507(8) 2_646 ? Si7 Ca1 3.579(2) 1_556 ? Si7 OW1 3.648(7) . ? Si8 O25 1.588(6) 1_655 ? Si8 O26 1.613(6) . ? Si8 O24 1.632(5) 1_655 ? Si8 O22 1.633(5) 1_655 ? Si8 Ca3 3.122(2) 2_646 ? Si8 Na2 3.158(3) 1_655 ? Si8 OH27 3.260(5) 1_655 ? Be1 O18 1.584(10) 2_646 ? Be1 O25 1.627(10) . ? Be1 O23 1.634(8) . ? Be1 O15 1.700(10) 2_646 ? Be1 Ca4 2.957(7) 2_646 ? Be1 Na1 3.028(8) 1_556 ? Be1 Ca3 3.261(8) 2_546 ? Be1 OW3 3.426(10) 2_646 ? Be2 O24 1.599(10) . ? Be2 O8 1.606(8) 1_455 ? Be2 O13 1.644(9) . ? Be2 OH28 1.683(9) . ? Be2 Ca2 3.144(9) 1_455 ? Be2 Ca1 3.295(8) 1_455 ? Be2 OW1 3.447(11) 1_554 ? Be2 OW4 3.535(11) 2_646 ? Be2 Ca4 3.575(8) 2_646 ? Be3 O20 1.454(8) 1_455 ? Be3 O5 1.647(10) . ? Be3 O2 1.695(10) 1_455 ? Be3 OH27 1.723(9) . ? Be3 Ca2 2.871(8) 1_455 ? Be3 Na2 3.016(9) 1_455 ? Be3 Ca1 3.420(8) 1_456 ? Be3 OW2 3.435(9) 1_556 ? Be3 Ca4 3.455(8) 1_455 ? Be4 O4 1.578(11) 2_646 ? Be4 O6 1.636(10) 2_646 ? Be4 O10 1.647(11) . ? Be4 O12 1.701(11) . ? Be4 Ca3 3.091(8) 2_646 ? Be4 Ca4 3.303(9) 2_646 ? Be4 OW5 3.340(14) 2_646 ? Be5 O26 1.535(11) . ? Be5 O21 1.648(11) . ? Be5 O14 1.654(9) . ? Be5 OH27 1.707(10) 1_655 ? Be5 OW1 3.187(10) 1_655 ? Be5 Ca1 3.327(9) 1_556 ? Be5 Ca3 3.542(9) 2_646 ? Be6 O16 1.564(9) 1_455 ? Be6 O19 1.593(10) . ? Be6 OH28 1.693(10) . ? Be6 O7 1.763(9) . ? Be6 Ca2 3.129(9) 1_455 ? Be6 OW2 3.228(11) . ? Be6 Ca1 3.238(8) 1_455 ? O1 Si1 1.666(5) 1_554 ? O1 Na1 2.617(4) 2_655 ? O1 OW2 3.024(6) . ? O2 Be3 1.695(10) 1_655 ? O2 Ca1 2.375(4) 1_556 ? O2 OH27 2.588(6) 1_655 ? O2 OW2 3.048(6) 1_656 ? O4 Be4 1.578(11) 2_656 ? O4 Na1 2.487(5) 2_656 ? O4 OW4 2.894(8) . ? O5 Ca4 2.473(5) 1_455 ? O5 OW5 2.538(10) . ? O5 OH27 2.662(7) . ? O5 OW2 3.007(7) 1_556 ? O6 Be4 1.636(10) 2_656 ? O6 Ca4 3.034(5) 1_455 ? O7 Ca2 2.320(5) 1_455 ? O7 OH28 2.735(7) . ? O7 OH27 3.135(6) . ? O8 Be2 1.606(8) 1_655 ? O8 OH28 2.654(6) 1_655 ? O8 OW1 3.063(9) 1_654 ? O10 OW5 2.497(12) 2_646 ? O11 Si3 1.682(5) 1_556 ? O11 Na1 2.667(5) 1_556 ? O11 OW1 2.717(7) . ? O12 Ca3 2.509(4) 2_646 ? O12 Ca4 2.717(4) 2_646 ? O13 Ca4 2.406(5) 2_646 ? O13 OW4 2.633(8) 2_646 ? O13 OH28 2.697(7) . ? O14 OH27 2.622(6) 1_655 ? O15 Be1 1.700(10) 2_656 ? O15 Na1 2.402(6) 2_655 ? O15 Ca3 2.558(5) 1_655 ? O16 Be6 1.564(9) 1_655 ? O16 OH28 2.591(7) 1_655 ? O16 OW2 3.075(9) 1_655 ? O17 OW2 3.115(7) . ? O18 Be1 1.584(10) 2_656 ? O19 OH28 2.696(7) . ? O19 OW3 2.784(9) . ? O20 Be3 1.454(8) 1_655 ? O20 OH27 2.639(6) 1_655 ? O21 Ca1 2.441(4) 1_556 ? O21 OH27 2.663(7) 1_655 ? O21 OW1 3.000(7) 1_655 ? O22 Si8 1.633(5) 1_455 ? O23 Na1 2.353(6) 1_556 ? O23 OW3 2.567(9) 2_646 ? O24 Si8 1.632(5) 1_455 ? O24 Ca2 2.350(6) 1_455 ? O24 OH28 2.606(7) . ? O25 Si8 1.588(6) 1_455 ? O25 Ca4 2.472(6) 2_646 ? O25 Ca3 2.690(7) 2_546 ? O26 Ca3 2.475(5) 2_646 ? O26 OH27 2.649(7) 1_655 ? O26 OW1 3.039(8) 1_655 ? OH27 Be5 1.707(10) 1_455 ? OH27 Ca2 2.501(4) 1_455 ? OH27 O2 2.588(6) 1_455 ? OH27 O14 2.622(6) 1_455 ? OH27 O20 2.639(6) 1_455 ? OH27 O26 2.649(7) 1_455 ? OH27 O21 2.663(7) 1_455 ? OH27 Ca1 3.002(4) 1_456 ? OH27 OW1 3.177(7) . ? OH28 O16 2.591(7) 1_455 ? OH28 O8 2.654(6) 1_455 ? OH28 Ca1 2.986(4) 1_455 ? OW1 Ca1 2.350(6) 1_456 ? OW1 O21 3.000(7) 1_455 ? OW1 OW4 3.014(9) 2_647 ? OW1 O26 3.039(8) 1_455 ? OW1 O8 3.063(9) 1_456 ? OW1 Be5 3.187(10) 1_455 ? OW1 OW2 3.218(7) 1_556 ? OW1 OH28 3.398(8) 1_556 ? OW1 Be2 3.447(11) 1_556 ? OW2 Ca1 2.482(5) 1_455 ? OW2 OW5 2.983(11) 1_554 ? OW2 O5 3.007(7) 1_554 ? OW2 O2 3.048(6) 1_454 ? OW2 O16 3.075(9) 1_455 ? OW2 OW3 3.139(9) . ? OW2 OW1 3.218(7) 1_554 ? OW2 OH27 3.410(7) 1_554 ? OW2 Be3 3.435(9) 1_554 ? OW3 OW5 2.296(10) 1_554 ? OW3 OW4 2.526(9) 1_454 ? OW3 O23 2.567(9) 2_656 ? OW3 Be1 3.426(10) 2_656 ? OW3 Si7 3.507(8) 2_656 ? OW3 Na1 3.603(8) 2 ? OW3 Na1 3.913(9) 2_655 ? OW3 OW1 4.311(9) 2_556 ? OW4 OW5 1.737(12) 1_655 ? OW4 Na1 2.483(8) 2_656 ? OW4 OW3 2.526(9) 1_656 ? OW4 O13 2.633(8) 2_656 ? OW4 OW1 3.014(9) 2_657 ? OW4 Be2 3.535(11) 2_656 ? OW4 Si4 3.653(7) 2_656 ? OW4 Ca3 4.218(7) 1_656 ? OW4 OW2 4.290(9) 1_656 ? OW4 Ca1 4.467(7) 2_756 ? OW5 OW4 1.737(12) 1_455 ? OW5 OW3 2.296(10) 1_556 ? OW5 Ca4 2.346(9) 1_455 ? OW5 O10 2.497(12) 2_656 ? OW5 OW2 2.983(11) 1_556 ? OW5 Be4 3.340(14) 2_656 ? OW5 Si3 3.576(10) 2_656 ? OW5 Na1 3.739(11) 2_556 ? OW5 Na1 3.885(10) 2_656 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag OW1 Ca1 O2 127.2(2) 1_654 1_554 ? OW1 Ca1 O16 133.3(2) 1_654 . ? O2 Ca1 O16 90.06(14) 1_554 . ? OW1 Ca1 O8 79.8(2) 1_654 . ? O2 Ca1 O8 144.06(16) 1_554 . ? O16 Ca1 O8 83.30(17) . . ? OW1 Ca1 O21 77.51(18) 1_654 1_554 ? O2 Ca1 O21 80.79(14) 1_554 1_554 ? O16 Ca1 O21 142.98(19) . 1_554 ? O8 Ca1 O21 83.56(13) . 1_554 ? OW1 Ca1 OW2 83.47(17) 1_654 1_655 ? O2 Ca1 OW2 77.71(16) 1_554 1_655 ? O16 Ca1 OW2 77.9(2) . 1_655 ? O8 Ca1 OW2 134.21(18) . 1_655 ? O21 Ca1 OW2 133.4(2) 1_554 1_655 ? OW1 Ca1 OH28 78.12(18) 1_654 1_655 ? O2 Ca1 OH28 141.48(14) 1_554 1_655 ? O16 Ca1 OH28 56.20(16) . 1_655 ? O8 Ca1 OH28 57.62(14) . 1_655 ? O21 Ca1 OH28 137.07(14) 1_554 1_655 ? OW2 Ca1 OH28 77.38(17) 1_655 1_655 ? OW1 Ca1 OH27 71.67(19) 1_654 1_654 ? O2 Ca1 OH27 56.11(14) 1_554 1_654 ? O16 Ca1 OH27 140.95(16) . 1_654 ? O8 Ca1 OH27 135.31(15) . 1_654 ? O21 Ca1 OH27 57.49(15) 1_554 1_654 ? OW2 Ca1 OH27 76.24(18) 1_655 1_654 ? OH28 Ca1 OH27 141.65(10) 1_655 1_654 ? OW1 Ca1 Be6 105.9(2) 1_654 1_655 ? O2 Ca1 Be6 110.99(17) 1_554 1_655 ? O16 Ca1 Be6 27.5(2) . 1_655 ? O8 Ca1 Be6 76.99(18) . 1_655 ? O21 Ca1 Be6 159.16(19) 1_554 1_655 ? OW2 Ca1 Be6 67.2(2) 1_655 1_655 ? OH28 Ca1 Be6 31.24(17) 1_655 1_655 ? OH27 Ca1 Be6 143.34(18) 1_654 1_655 ? OW1 Ca1 Be2 73.1(2) 1_654 1_655 ? O2 Ca1 Be2 159.65(19) 1_554 1_655 ? O16 Ca1 Be2 71.90(19) . 1_655 ? O8 Ca1 Be2 27.63(17) . 1_655 ? O21 Ca1 Be2 107.78(17) 1_554 1_655 ? OW2 Ca1 Be2 106.6(2) 1_655 1_655 ? OH28 Ca1 Be2 30.58(16) 1_655 1_655 ? OH27 Ca1 Be2 144.07(17) 1_654 1_655 ? Be6 Ca1 Be2 55.64(18) 1_655 1_655 ? OW1 Ca1 Be5 65.7(2) 1_654 1_554 ? O2 Ca1 Be5 72.57(18) 1_554 1_554 ? O16 Ca1 Be5 160.8(2) . 1_554 ? O8 Ca1 Be5 105.85(19) . 1_554 ? O21 Ca1 Be5 28.2(2) 1_554 1_554 ? OW2 Ca1 Be5 105.3(2) 1_655 1_554 ? OH28 Ca1 Be5 142.87(19) 1_655 1_554 ? OH27 Ca1 Be5 30.75(19) 1_654 1_554 ? Be6 Ca1 Be5 170.0(2) 1_655 1_554 ? Be2 Ca1 Be5 123.47(18) 1_655 1_554 ? OW1 Ca1 Be3 100.2(2) 1_654 1_654 ? O2 Ca1 Be3 27.09(19) 1_554 1_654 ? O16 Ca1 Be3 112.13(18) . 1_654 ? O8 Ca1 Be3 155.83(17) . 1_654 ? O21 Ca1 Be3 72.97(17) 1_554 1_654 ? OW2 Ca1 Be3 69.1(2) 1_655 1_654 ? OH28 Ca1 Be3 146.38(17) 1_655 1_654 ? OH27 Ca1 Be3 30.24(17) 1_654 1_654 ? Be6 Ca1 Be3 125.26(17) 1_655 1_654 ? Be2 Ca1 Be3 172.6(2) 1_655 1_654 ? Be5 Ca1 Be3 54.1(2) 1_554 1_654 ? O7 Ca2 O24 82.27(17) 1_655 1_655 ? O7 Ca2 O9 149.85(19) 1_655 . ? O24 Ca2 O9 81.75(18) 1_655 . ? O7 Ca2 O20 90.87(17) 1_655 . ? O24 Ca2 O20 145.91(17) 1_655 . ? O9 Ca2 O20 116.23(18) . . ? O7 Ca2 OH27 81.03(15) 1_655 1_655 ? O24 Ca2 OH27 82.04(16) 1_655 1_655 ? O9 Ca2 OH27 121.59(17) . 1_655 ? O20 Ca2 OH27 63.89(15) . 1_655 ? O7 Ca2 O14 143.50(16) 1_655 . ? O24 Ca2 O14 92.06(19) 1_655 . ? O9 Ca2 O14 62.53(16) . . ? O20 Ca2 O14 73.89(16) . . ? OH27 Ca2 O14 62.47(15) 1_655 . ? O7 Ca2 O17 86.11(17) 1_655 . ? O24 Ca2 O17 149.47(19) 1_655 . ? O9 Ca2 O17 94.96(14) . . ? O20 Ca2 O17 61.95(16) . . ? OH27 Ca2 O17 123.87(17) 1_655 . ? O14 Ca2 O17 113.43(18) . . ? O7 Ca2 Be3 75.2(2) 1_655 1_655 ? O24 Ca2 Be3 116.5(2) 1_655 1_655 ? O9 Ca2 Be3 134.9(2) . 1_655 ? O20 Ca2 Be3 30.44(19) . 1_655 ? OH27 Ca2 Be3 36.61(19) 1_655 1_655 ? O14 Ca2 Be3 75.3(2) . 1_655 ? O17 Ca2 Be3 87.3(2) . 1_655 ? O7 Ca2 O16 58.57(14) 1_655 . ? O24 Ca2 O16 94.76(17) 1_655 . ? O9 Ca2 O16 97.58(16) . . ? O20 Ca2 O16 110.02(16) . . ? OH27 Ca2 O16 139.46(16) 1_655 . ? O14 Ca2 O16 157.79(15) . . ? O17 Ca2 O16 55.39(17) . . ? Be3 Ca2 O16 119.6(2) 1_655 . ? O7 Ca2 Be5 112.2(2) 1_655 . ? O24 Ca2 Be5 73.3(2) 1_655 . ? O9 Ca2 Be5 87.3(2) . . ? O20 Ca2 Be5 78.7(2) . . ? OH27 Ca2 Be5 34.4(2) 1_655 . ? O14 Ca2 Be5 33.2(2) . . ? O17 Ca2 Be5 137.1(2) . . ? Be3 Ca2 Be5 62.7(2) 1_655 . ? O16 Ca2 Be5 166.5(2) . . ? O7 Ca2 Be6 33.81(17) 1_655 1_655 ? O24 Ca2 Be6 76.6(2) 1_655 1_655 ? O9 Ca2 Be6 117.0(2) . 1_655 ? O20 Ca2 Be6 114.4(2) . 1_655 ? OH27 Ca2 Be6 112.87(18) 1_655 1_655 ? O14 Ca2 Be6 168.5(2) . 1_655 ? O17 Ca2 Be6 78.1(2) . 1_655 ? Be3 Ca2 Be6 107.5(2) 1_655 1_655 ? O16 Ca2 Be6 29.50(17) . 1_655 ? Be5 Ca2 Be6 137.8(2) . 1_655 ? O7 Ca2 Be2 78.92(19) 1_655 1_655 ? O24 Ca2 Be2 29.58(18) 1_655 1_655 ? O9 Ca2 Be2 74.57(19) . 1_655 ? O20 Ca2 Be2 169.15(19) . 1_655 ? OH27 Ca2 Be2 110.33(17) 1_655 1_655 ? O14 Ca2 Be2 112.4(2) . 1_655 ? O17 Ca2 Be2 120.29(19) . 1_655 ? Be3 Ca2 Be2 140.5(2) 1_655 1_655 ? O16 Ca2 Be2 67.80(18) . 1_655 ? Be5 Ca2 Be2 101.7(2) . 1_655 ? Be6 Ca2 Be2 58.2(2) 1_655 1_655 ? O6 Ca3 OW3 152.9(2) . . ? O6 Ca3 O19 81.62(18) . . ? OW3 Ca3 O19 71.3(2) . . ? O6 Ca3 O26 116.59(17) . 2_656 ? OW3 Ca3 O26 90.4(2) . 2_656 ? O19 Ca3 O26 160.4(2) . 2_656 ? O6 Ca3 O12 64.70(14) . 2_656 ? OW3 Ca3 O12 122.6(2) . 2_656 ? O19 Ca3 O12 104.73(17) . 2_656 ? O26 Ca3 O12 78.97(15) 2_656 2_656 ? O6 Ca3 O15 93.54(16) . 1_455 ? OW3 Ca3 O15 84.6(2) . 1_455 ? O19 Ca3 O15 87.56(19) . 1_455 ? O26 Ca3 O15 97.76(16) 2_656 1_455 ? O12 Ca3 O15 152.36(17) 2_656 1_455 ? O6 Ca3 O25 71.81(17) . 2_556 ? OW3 Ca3 O25 128.5(2) . 2_556 ? O19 Ca3 O25 136.2(2) . 2_556 ? O26 Ca3 O25 61.06(19) 2_656 2_556 ? O12 Ca3 O25 94.71(17) 2_656 2_556 ? O15 Ca3 O25 60.86(17) 1_455 2_556 ? O6 Ca3 Be4 31.3(2) . 2_656 ? OW3 Ca3 Be4 148.1(3) . 2_656 ? O19 Ca3 Be4 92.9(2) . 2_656 ? O26 Ca3 Be4 99.7(2) 2_656 2_656 ? O12 Ca3 Be4 33.4(2) 2_656 2_656 ? O15 Ca3 Be4 123.3(2) 1_455 2_656 ? O25 Ca3 Be4 82.2(2) 2_556 2_656 ? O6 Ca3 Si8 92.18(12) . 2_656 ? OW3 Ca3 Si8 114.06(19) . 2_656 ? O19 Ca3 Si8 166.44(17) . 2_656 ? O26 Ca3 Si8 30.83(14) 2_656 2_656 ? O12 Ca3 Si8 83.16(11) 2_656 2_656 ? O15 Ca3 Si8 80.77(12) 1_455 2_656 ? O25 Ca3 Si8 30.57(13) 2_556 2_656 ? Be4 Ca3 Si8 87.8(2) 2_656 2_656 ? O6 Ca3 O18 89.14(16) . . ? OW3 Ca3 O18 75.5(2) . . ? O19 Ca3 O18 53.01(17) . . ? O26 Ca3 O18 116.81(16) 2_656 . ? O12 Ca3 O18 60.99(13) 2_656 . ? O15 Ca3 O18 139.64(15) 1_455 . ? O25 Ca3 O18 154.37(14) 2_556 . ? Be4 Ca3 O18 72.9(2) 2_656 . ? Si8 Ca3 O18 139.41(10) 2_656 . ? O6 Ca3 Be1 80.33(17) . 2_556 ? OW3 Ca3 Be1 109.1(2) . 2_556 ? O19 Ca3 Be1 113.0(2) . 2_556 ? O26 Ca3 Be1 78.9(2) 2_656 2_556 ? O12 Ca3 Be1 123.20(18) 2_656 2_556 ? O15 Ca3 Be1 31.09(19) 1_455 2_556 ? O25 Ca3 Be1 29.82(19) 2_556 2_556 ? Be4 Ca3 Be1 102.6(2) 2_656 2_556 ? Si8 Ca3 Be1 53.75(18) 2_656 2_556 ? O18 Ca3 Be1 164.0(2) . 2_556 ? O6 Ca3 Si6 82.19(12) . . ? OW3 Ca3 Si6 73.82(19) . . ? O19 Ca3 Si6 25.50(15) . . ? O26 Ca3 Si6 143.28(15) 2_656 . ? O12 Ca3 Si6 82.16(11) 2_656 . ? O15 Ca3 Si6 113.01(12) 1_455 . ? O25 Ca3 Si6 152.36(14) 2_556 . ? Be4 Ca3 Si6 80.3(2) 2_656 . ? Si8 Ca3 Si6 165.30(6) 2_656 . ? O18 Ca3 Si6 27.73(9) . . ? Be1 Ca3 Si6 137.41(19) 2_556 . ? OW5 Ca4 O18 147.4(3) 1_655 . ? OW5 Ca4 O13 98.4(3) 1_655 2_656 ? O18 Ca4 O13 114.25(16) . 2_656 ? OW5 Ca4 O25 127.0(3) 1_655 2_656 ? O18 Ca4 O25 65.60(18) . 2_656 ? O13 Ca4 O25 76.36(18) 2_656 2_656 ? OW5 Ca4 O5 63.5(3) 1_655 1_655 ? O18 Ca4 O5 84.02(16) . 1_655 ? O13 Ca4 O5 161.52(15) 2_656 1_655 ? O25 Ca4 O5 111.02(19) 2_656 1_655 ? OW5 Ca4 OW4 41.7(3) 1_655 . ? O18 Ca4 OW4 156.2(2) . . ? O13 Ca4 OW4 64.63(19) 2_656 . ? O25 Ca4 OW4 132.0(2) 2_656 . ? O5 Ca4 OW4 99.94(19) 1_655 . ? OW5 Ca4 O4 84.6(3) 1_655 . ? O18 Ca4 O4 89.43(17) . . ? O13 Ca4 O4 98.53(16) 2_656 . ? O25 Ca4 O4 148.31(18) 2_656 . ? O5 Ca4 O4 83.77(16) 1_655 . ? OW4 Ca4 O4 67.95(19) . . ? OW5 Ca4 O12 131.0(3) 1_655 2_656 ? O18 Ca4 O12 69.64(16) . 2_656 ? O13 Ca4 O12 60.61(14) 2_656 2_656 ? O25 Ca4 O12 92.71(19) 2_656 2_656 ? O5 Ca4 O12 133.30(16) 1_655 2_656 ? OW4 Ca4 O12 91.58(18) . 2_656 ? O4 Ca4 O12 59.02(13) . 2_656 ? OW5 Ca4 Be1 149.4(3) 1_655 2_656 ? O18 Ca4 Be1 32.2(2) . 2_656 ? O13 Ca4 Be1 96.4(2) 2_656 2_656 ? O25 Ca4 Be1 33.4(2) 2_656 2_656 ? O5 Ca4 Be1 98.4(2) 1_655 2_656 ? OW4 Ca4 Be1 161.0(3) . 2_656 ? O4 Ca4 Be1 119.51(19) . 2_656 ? O12 Ca4 Be1 79.56(18) 2_656 2_656 ? OW5 Ca4 O6 73.6(3) 1_655 1_655 ? O18 Ca4 O6 91.02(17) . 1_655 ? O13 Ca4 O6 118.07(16) 2_656 1_655 ? O25 Ca4 O6 64.14(17) 2_656 1_655 ? O5 Ca4 O6 55.83(15) 1_655 1_655 ? OW4 Ca4 O6 110.69(18) . 1_655 ? O4 Ca4 O6 139.28(13) . 1_655 ? O12 Ca4 O6 154.99(12) 2_656 1_655 ? Be1 Ca4 O6 75.77(17) 2_656 1_655 ? OW5 Ca4 Si4 119.6(2) 1_655 2_656 ? O18 Ca4 Si4 90.52(13) . 2_656 ? O13 Ca4 Si4 30.25(11) 2_656 2_656 ? O25 Ca4 Si4 81.25(15) 2_656 2_656 ? O5 Ca4 Si4 162.68(14) 1_655 2_656 ? OW4 Ca4 Si4 78.76(17) . 2_656 ? O4 Ca4 Si4 79.74(11) . 2_656 ? O12 Ca4 Si4 30.55(9) 2_656 2_656 ? Be1 Ca4 Si4 85.30(18) 2_656 2_656 ? O6 Ca4 Si4 140.96(10) 1_655 2_656 ? OW5 Ca4 Be4 107.1(3) 1_655 2_656 ? O18 Ca4 Be4 79.7(2) . 2_656 ? O13 Ca4 Be4 78.7(2) 2_656 2_656 ? O25 Ca4 Be4 122.7(2) 2_656 2_656 ? O5 Ca4 Be4 108.7(2) 1_655 2_656 ? OW4 Ca4 Be4 76.9(2) . 2_656 ? O4 Ca4 Be4 28.1(2) . 2_656 ? O12 Ca4 Be4 30.9(2) 2_656 2_656 ? Be1 Ca4 Be4 102.1(2) 2_656 2_656 ? O6 Ca4 Be4 163.1(2) 1_655 2_656 ? Si4 Ca4 Be4 54.0(2) 2_656 2_656 ? O23 Na1 O15 66.13(19) 1_554 2_645 ? O23 Na1 OW4 141.5(2) 1_554 2_646 ? O15 Na1 OW4 107.5(2) 2_645 2_646 ? O23 Na1 O4 146.42(19) 1_554 2_646 ? O15 Na1 O4 119.62(16) 2_645 2_646 ? OW4 Na1 O4 71.2(2) 2_646 2_646 ? O23 Na1 O1 99.10(18) 1_554 2_645 ? O15 Na1 O1 63.09(16) 2_645 2_645 ? OW4 Na1 O1 111.8(2) 2_646 2_645 ? O4 Na1 O1 62.59(16) 2_646 2_645 ? O23 Na1 O10 92.15(16) 1_554 . ? O15 Na1 O10 146.9(2) 2_645 . ? OW4 Na1 O10 104.9(2) 2_646 . ? O4 Na1 O10 65.49(17) 2_646 . ? O1 Na1 O10 98.59(16) 2_645 . ? O23 Na1 O11 61.04(17) 1_554 1_554 ? O15 Na1 O11 120.2(2) 2_645 1_554 ? OW4 Na1 O11 97.3(2) 2_646 1_554 ? O4 Na1 O11 119.75(19) 2_646 1_554 ? O1 Na1 O11 148.59(16) 2_645 1_554 ? O10 Na1 O11 61.10(16) . 1_554 ? O23 Na1 Be4 123.6(2) 1_554 . ? O15 Na1 Be4 145.0(3) 2_645 . ? OW4 Na1 Be4 84.3(3) 2_646 . ? O4 Na1 Be4 32.2(2) 2_646 . ? O1 Na1 Be4 82.0(3) 2_645 . ? O10 Na1 Be4 33.6(2) . . ? O11 Na1 Be4 89.5(3) 1_554 . ? O23 Na1 Be1 32.37(19) 1_554 1_554 ? O15 Na1 Be1 34.1(2) 2_645 1_554 ? OW4 Na1 Be1 127.9(2) 2_646 1_554 ? O4 Na1 Be1 145.8(2) 2_646 1_554 ? O1 Na1 Be1 83.2(2) 2_645 1_554 ? O10 Na1 Be1 122.4(2) . 1_554 ? O11 Na1 Be1 88.4(2) 1_554 1_554 ? Be4 Na1 Be1 147.7(2) . 1_554 ? O23 Na1 Si5 82.68(15) 1_554 2_645 ? O15 Na1 Si5 31.20(12) 2_645 2_645 ? OW4 Na1 Si5 111.78(18) 2_646 2_645 ? O4 Na1 Si5 90.89(12) 2_646 2_645 ? O1 Na1 Si5 31.94(11) 2_645 2_645 ? O10 Na1 Si5 126.52(15) . 2_645 ? O11 Na1 Si5 143.69(19) 1_554 2_645 ? Be4 Na1 Si5 113.9(2) . 2_645 ? Be1 Na1 Si5 56.8(2) 1_554 2_645 ? O23 Na1 Si7 30.62(12) 1_554 1_554 ? O15 Na1 Si7 90.36(17) 2_645 1_554 ? OW4 Na1 Si7 118.31(19) 2_646 1_554 ? O4 Na1 Si7 145.49(14) 2_646 1_554 ? O1 Na1 Si7 128.50(16) 2_645 1_554 ? O10 Na1 Si7 80.07(13) . 1_554 ? O11 Na1 Si7 31.39(13) 1_554 1_554 ? Be4 Na1 Si7 113.3(2) . 1_554 ? Be1 Na1 Si7 57.3(2) 1_554 1_554 ? Si5 Na1 Si7 112.51(13) 2_645 1_554 ? O23 Na1 Si1 127.35(15) 1_554 2_646 ? O15 Na1 Si1 91.19(13) 2_645 2_646 ? OW4 Na1 Si1 89.53(19) 2_646 2_646 ? O4 Na1 Si1 30.61(10) 2_646 2_646 ? O1 Na1 Si1 32.11(12) 2_645 2_646 ? O10 Na1 Si1 82.46(14) . 2_646 ? O11 Na1 Si1 143.49(15) 1_554 2_646 ? Be4 Na1 Si1 55.4(2) . 2_646 ? Be1 Na1 Si1 115.3(2) 1_554 2_646 ? Si5 Na1 Si1 60.91(6) 2_645 2_646 ? Si7 Na1 Si1 150.12(10) 1_554 2_646 ? O22 Na2 O20 148.89(18) . . ? O22 Na2 O14 83.53(19) . . ? O20 Na2 O14 77.31(18) . . ? O22 Na2 O3 96.51(16) . . ? O20 Na2 O3 88.26(17) . . ? O14 Na2 O3 149.64(16) . . ? O22 Na2 OH28 119.42(17) . . ? O20 Na2 OH28 82.24(16) . . ? O14 Na2 OH28 82.33(16) . . ? O3 Na2 OH28 122.44(16) . . ? O22 Na2 O24 61.23(16) . . ? O20 Na2 O24 143.54(16) . . ? O14 Na2 O24 93.86(18) . . ? O3 Na2 O24 112.85(17) . . ? OH28 Na2 O24 61.43(16) . . ? O22 Na2 O7 113.06(18) . . ? O20 Na2 O7 96.05(17) . . ? O14 Na2 O7 146.70(16) . . ? O3 Na2 O7 60.43(14) . . ? OH28 Na2 O7 64.39(15) . . ? O24 Na2 O7 72.04(15) . . ? O22 Na2 O2 99.47(14) . . ? O20 Na2 O2 58.02(14) . . ? O14 Na2 O2 93.28(15) . . ? O3 Na2 O2 56.65(13) . . ? OH28 Na2 O2 139.85(16) . . ? O24 Na2 O2 158.43(16) . . ? O7 Na2 O2 110.99(14) . . ? O22 Na2 Be2 85.5(2) . . ? O20 Na2 Be2 112.6(2) . . ? O14 Na2 Be2 75.6(2) . . ? O3 Na2 Be2 134.7(2) . . ? OH28 Na2 Be2 33.93(19) . . ? O24 Na2 Be2 32.0(2) . . ? O7 Na2 Be2 77.14(18) . . ? O2 Na2 Be2 167.3(2) . . ? O22 Na2 Be3 122.28(19) . 1_655 ? O20 Na2 Be3 28.41(17) . 1_655 ? O14 Na2 Be3 74.3(2) . 1_655 ? O3 Na2 Be3 80.4(2) . 1_655 ? OH28 Na2 Be3 109.6(2) . 1_655 ? O24 Na2 Be3 166.4(2) . 1_655 ? O7 Na2 Be3 114.5(2) . 1_655 ? O2 Na2 Be3 32.80(18) . 1_655 ? Be2 Na2 Be3 135.5(2) . 1_655 ? O22 Na2 Be6 134.2(2) . . ? O20 Na2 Be6 76.4(2) . . ? O14 Na2 Be6 112.8(2) . . ? O3 Na2 Be6 88.95(19) . . ? OH28 Na2 Be6 33.62(19) . . ? O24 Na2 Be6 74.7(2) . . ? O7 Na2 Be6 35.13(19) . . ? O2 Na2 Be6 120.66(18) . . ? Be2 Na2 Be6 60.3(2) . . ? Be3 Na2 Be6 103.5(2) 1_655 . ? O22 Na2 Si8 30.34(12) . 1_455 ? O20 Na2 Si8 162.56(15) . 1_455 ? O14 Na2 Si8 86.20(14) . 1_455 ? O3 Na2 Si8 109.02(13) . 1_455 ? OH28 Na2 Si8 90.07(13) . 1_455 ? O24 Na2 Si8 31.04(11) . 1_455 ? O7 Na2 Si8 94.66(12) . 1_455 ? O2 Na2 Si8 129.62(11) . 1_455 ? Be2 Na2 Si8 56.79(17) . 1_455 ? Be3 Na2 Si8 149.65(16) 1_655 1_455 ? Be6 Na2 Si8 105.44(17) . 1_455 ? O2 Si1 O4 116.7(3) . . ? O2 Si1 O1 108.9(2) . 1_556 ? O4 Si1 O1 108.2(2) . 1_556 ? O2 Si1 O3 106.8(2) . . ? O4 Si1 O3 109.7(2) . . ? O1 Si1 O3 106.0(2) 1_556 . ? O2 Si1 Na1 126.49(16) . 2_656 ? O4 Si1 Na1 51.90(17) . 2_656 ? O1 Si1 Na1 56.63(14) 1_556 2_656 ? O3 Si1 Na1 126.57(18) . 2_656 ? O2 Si1 Na2 63.61(15) . . ? O4 Si1 Na2 118.09(16) . . ? O1 Si1 Na2 131.19(14) 1_556 . ? O3 Si1 Na2 45.09(16) . . ? Na1 Si1 Na2 167.14(8) 2_656 . ? O2 Si1 Ca1 31.56(15) . 1_556 ? O4 Si1 Ca1 134.19(19) . 1_556 ? O1 Si1 Ca1 77.72(13) 1_556 1_556 ? O3 Si1 Ca1 111.88(15) . 1_556 ? Na1 Si1 Ca1 111.90(7) 2_656 1_556 ? Na2 Si1 Ca1 80.83(5) . 1_556 ? O7 Si2 O5 113.0(2) . . ? O7 Si2 O6 114.8(2) . . ? O5 Si2 O6 107.3(2) . . ? O7 Si2 O3 104.8(2) . . ? O5 Si2 O3 107.7(2) . . ? O6 Si2 O3 109.0(2) . . ? O7 Si2 Na2 55.48(17) . . ? O5 Si2 Na2 130.15(18) . . ? O6 Si2 Na2 121.68(19) . . ? O3 Si2 Na2 49.72(15) . . ? O7 Si2 OH27 73.4(2) . . ? O5 Si2 OH27 56.25(19) . . ? O6 Si2 OH27 163.2(2) . . ? O3 Si2 OH27 81.48(18) . . ? Na2 Si2 OH27 75.11(10) . . ? O7 Si2 Ca4 120.96(18) . 1_455 ? O5 Si2 Ca4 44.47(16) . 1_455 ? O6 Si2 Ca4 64.48(18) . 1_455 ? O3 Si2 Ca4 132.48(17) . 1_455 ? Na2 Si2 Ca4 173.43(7) . 1_455 ? OH27 Si2 Ca4 98.74(10) . 1_455 ? O7 Si2 OW5 157.8(3) . . ? O5 Si2 OW5 46.3(2) . . ? O6 Si2 OW5 72.3(2) . . ? O3 Si2 OW5 91.7(2) . . ? Na2 Si2 OW5 140.76(16) . . ? OH27 Si2 OW5 94.8(2) . . ? Ca4 Si2 OW5 40.82(16) 1_455 . ? O7 Si2 Ca2 33.73(18) . 1_455 ? O5 Si2 Ca2 80.44(16) . 1_455 ? O6 Si2 Ca2 137.02(15) . 1_455 ? O3 Si2 Ca2 108.35(16) . 1_455 ? Na2 Si2 Ca2 70.70(6) . 1_455 ? OH27 Si2 Ca2 43.90(7) . 1_455 ? Ca4 Si2 Ca2 103.32(6) 1_455 1_455 ? OW5 Si2 Ca2 126.75(19) . 1_455 ? O7 Si2 Ca3 82.01(18) . . ? O5 Si2 Ca3 121.37(17) . . ? O6 Si2 Ca3 32.87(15) . . ? O3 Si2 Ca3 123.08(18) . . ? Na2 Si2 Ca3 105.68(6) . . ? OH27 Si2 Ca3 149.40(8) . . ? Ca4 Si2 Ca3 78.37(5) 1_455 . ? OW5 Si2 Ca3 101.69(17) . . ? Ca2 Si2 Ca3 106.55(5) 1_455 . ? O10 Si3 O9 110.0(3) . . ? O10 Si3 O8 113.7(3) . . ? O9 Si3 O8 109.4(3) . . ? O10 Si3 O11 112.0(2) . 1_554 ? O9 Si3 O11 103.6(2) . 1_554 ? O8 Si3 O11 107.6(2) . 1_554 ? O10 Si3 Na1 56.56(19) . . ? O9 Si3 Na1 105.54(19) . . ? O8 Si3 Na1 144.7(2) . . ? O11 Si3 Na1 58.28(15) 1_554 . ? O10 Si3 Ca2 124.96(19) . . ? O9 Si3 Ca2 38.87(17) . . ? O8 Si3 Ca2 70.63(18) . . ? O11 Si3 Ca2 118.49(16) 1_554 . ? Na1 Si3 Ca2 144.41(9) . . ? O10 Si3 Ca1 137.3(2) . . ? O9 Si3 Ca1 109.34(17) . . ? O8 Si3 Ca1 35.19(16) . . ? O11 Si3 Ca1 73.59(15) 1_554 . ? Na1 Si3 Ca1 125.56(9) . . ? Ca2 Si3 Ca1 79.36(5) . . ? O10 Si3 OW5 36.3(3) . 2_646 ? O9 Si3 OW5 143.4(2) . 2_646 ? O8 Si3 OW5 84.2(2) . 2_646 ? O11 Si3 OW5 104.0(2) 1_554 2_646 ? Na1 Si3 OW5 70.40(16) . 2_646 ? Ca2 Si3 OW5 135.17(15) . 2_646 ? Ca1 Si3 OW5 101.07(17) . 2_646 ? O14 Si4 O12 115.9(2) . . ? O14 Si4 O13 114.1(3) . . ? O12 Si4 O13 105.8(2) . . ? O14 Si4 O9 103.6(3) . . ? O12 Si4 O9 108.3(2) . . ? O13 Si4 O9 109.0(2) . . ? O14 Si4 Ca2 53.8(2) . . ? O12 Si4 Ca2 124.15(17) . . ? O13 Si4 Ca2 129.21(18) . . ? O9 Si4 Ca2 49.86(15) . . ? O14 Si4 Ca4 128.4(2) . 2_646 ? O12 Si4 Ca4 58.56(16) . 2_646 ? O13 Si4 Ca4 47.64(16) . 2_646 ? O9 Si4 Ca4 127.59(16) . 2_646 ? Ca2 Si4 Ca4 176.19(7) . 2_646 ? O14 Si4 OH28 74.7(2) . . ? O12 Si4 OH28 160.1(2) . . ? O13 Si4 OH28 54.64(18) . . ? O9 Si4 OH28 83.78(18) . . ? Ca2 Si4 OH28 75.70(10) . . ? Ca4 Si4 OH28 101.59(10) 2_646 . ? O14 Si4 Na2 36.45(19) . . ? O12 Si4 Na2 137.87(17) . . ? O13 Si4 Na2 78.57(17) . . ? O9 Si4 Na2 109.52(16) . . ? Ca2 Si4 Na2 71.07(6) . . ? Ca4 Si4 Na2 108.87(7) 2_646 . ? OH28 Si4 Na2 43.03(7) . . ? O14 Si4 OW4 154.6(2) . 2_646 ? O12 Si4 OW4 80.88(18) . 2_646 ? O13 Si4 OW4 40.6(2) . 2_646 ? O9 Si4 OW4 87.62(19) . 2_646 ? Ca2 Si4 OW4 133.98(13) . 2_646 ? Ca4 Si4 OW4 42.50(12) 2_646 2_646 ? OH28 Si4 OW4 84.05(14) . 2_646 ? Na2 Si4 OW4 118.36(13) . 2_646 ? O16 Si5 O15 114.6(3) . . ? O16 Si5 O1 109.4(3) . . ? O15 Si5 O1 109.2(2) . . ? O16 Si5 O17 107.9(3) . . ? O15 Si5 O17 111.4(3) . . ? O1 Si5 O17 103.8(2) . . ? O16 Si5 Na1 127.1(2) . 2_655 ? O15 Si5 Na1 50.84(18) . 2_655 ? O1 Si5 Na1 58.53(14) . 2_655 ? O17 Si5 Na1 124.9(2) . 2_655 ? O16 Si5 Ca2 62.0(2) . . ? O15 Si5 Ca2 118.34(19) . . ? O1 Si5 Ca2 130.72(16) . . ? O17 Si5 Ca2 47.92(18) . . ? Na1 Si5 Ca2 166.83(10) 2_655 . ? O16 Si5 Ca1 32.22(18) . . ? O15 Si5 Ca1 132.6(2) . . ? O1 Si5 Ca1 77.54(15) . . ? O17 Si5 Ca1 112.07(18) . . ? Na1 Si5 Ca1 113.06(9) 2_655 . ? Ca2 Si5 Ca1 79.67(5) . . ? O18 Si6 O19 107.3(3) . . ? O18 Si6 O20 114.3(3) . . ? O19 Si6 O20 114.2(3) . . ? O18 Si6 O17 108.4(3) . . ? O19 Si6 O17 109.0(3) . . ? O20 Si6 O17 103.4(3) . . ? O18 Si6 Ca2 121.4(2) . . ? O19 Si6 Ca2 131.2(2) . . ? O20 Si6 Ca2 50.00(19) . . ? O17 Si6 Ca2 53.71(17) . . ? O18 Si6 OH28 163.0(2) . . ? O19 Si6 OH28 55.9(2) . . ? O20 Si6 OH28 74.92(19) . . ? O17 Si6 OH28 81.8(2) . . ? Ca2 Si6 OH28 75.58(10) . . ? O18 Si6 Ca3 66.8(2) . . ? O19 Si6 Ca3 41.1(2) . . ? O20 Si6 Ca3 126.1(2) . . ? O17 Si6 Ca3 128.27(18) . . ? Ca2 Si6 Ca3 171.50(8) . . ? OH28 Si6 Ca3 96.25(10) . . ? O18 Si6 Na2 136.9(2) . . ? O19 Si6 Na2 77.1(2) . . ? O20 Si6 Na2 37.82(18) . . ? O17 Si6 Na2 110.21(19) . . ? Ca2 Si6 Na2 70.57(6) . . ? OH28 Si6 Na2 43.36(8) . . ? Ca3 Si6 Na2 101.95(7) . . ? O18 Si6 Ca4 31.99(17) . . ? O19 Si6 Ca4 119.4(2) . . ? O20 Si6 Ca4 82.66(18) . . ? O17 Si6 Ca4 123.4(2) . . ? Ca2 Si6 Ca4 104.92(6) . . ? OH28 Si6 Ca4 149.94(10) . . ? Ca3 Si6 Ca4 80.92(5) . . ? Na2 Si6 Ca4 107.60(6) . . ? O18 Si6 OW3 72.0(2) . . ? O19 Si6 OW3 49.3(2) . . ? O20 Si6 OW3 162.7(3) . . ? O17 Si6 OW3 89.0(2) . . ? Ca2 Si6 OW3 142.19(15) . . ? OH28 Si6 OW3 95.24(15) . . ? Ca3 Si6 OW3 39.47(14) . . ? Na2 Si6 OW3 126.42(15) . . ? Ca4 Si6 OW3 100.82(13) . . ? O21 Si7 O23 122.1(3) . . ? O21 Si7 O11 107.4(2) . . ? O23 Si7 O11 104.7(2) . . ? O21 Si7 O22 108.9(3) . . ? O23 Si7 O22 108.5(2) . . ? O11 Si7 O22 103.6(2) . . ? O21 Si7 Na1 146.10(19) . 1_556 ? O23 Si7 Na1 47.83(18) . 1_556 ? O11 Si7 Na1 59.02(16) . 1_556 ? O22 Si7 Na1 104.7(2) . 1_556 ? O21 Si7 Na2 69.47(17) . . ? O23 Si7 Na2 130.03(17) . . ? O11 Si7 Na2 118.02(17) . . ? O22 Si7 Na2 39.49(19) . . ? Na1 Si7 Na2 144.15(8) 1_556 . ? O21 Si7 OW3 83.0(2) . 2_646 ? O23 Si7 OW3 42.8(2) . 2_646 ? O11 Si7 OW3 104.1(2) . 2_646 ? O22 Si7 OW3 144.7(2) . 2_646 ? Na1 Si7 OW3 72.23(15) 1_556 2_646 ? Na2 Si7 OW3 134.59(15) . 2_646 ? O21 Si7 Ca1 34.69(17) . 1_556 ? O23 Si7 Ca1 139.82(18) . 1_556 ? O11 Si7 Ca1 73.38(15) . 1_556 ? O22 Si7 Ca1 110.85(18) . 1_556 ? Na1 Si7 Ca1 125.71(9) 1_556 1_556 ? Na2 Si7 Ca1 79.83(5) . 1_556 ? OW3 Si7 Ca1 97.74(13) 2_646 1_556 ? O21 Si7 OW1 128.5(2) . . ? O23 Si7 OW1 108.0(2) . . ? O11 Si7 OW1 43.64(18) . . ? O22 Si7 OW1 61.1(2) . . ? Na1 Si7 OW1 65.69(11) 1_556 . ? Na2 Si7 OW1 88.23(11) . . ? OW3 Si7 OW1 136.44(17) 2_646 . ? Ca1 Si7 OW1 97.66(10) 1_556 . ? O25 Si8 O26 110.5(3) 1_655 . ? O25 Si8 O24 114.5(3) 1_655 1_655 ? O26 Si8 O24 112.9(3) . 1_655 ? O25 Si8 O22 109.8(3) 1_655 1_655 ? O26 Si8 O22 106.4(3) . 1_655 ? O24 Si8 O22 102.0(3) 1_655 1_655 ? O25 Si8 Ca3 59.5(3) 1_655 2_646 ? O26 Si8 Ca3 51.86(19) . 2_646 ? O24 Si8 Ca3 126.5(2) 1_655 2_646 ? O22 Si8 Ca3 130.94(18) 1_655 2_646 ? O25 Si8 Na2 121.8(3) 1_655 1_655 ? O26 Si8 Na2 126.5(2) . 1_655 ? O24 Si8 Na2 55.12(19) 1_655 1_655 ? O22 Si8 Na2 47.23(17) 1_655 1_655 ? Ca3 Si8 Na2 177.75(8) 2_646 1_655 ? O25 Si8 OH27 163.7(3) 1_655 1_655 ? O26 Si8 OH27 53.8(2) . 1_655 ? O24 Si8 OH27 72.8(2) 1_655 1_655 ? O22 Si8 OH27 81.5(2) 1_655 1_655 ? Ca3 Si8 OH27 104.27(10) 2_646 1_655 ? Na2 Si8 OH27 74.49(10) 1_655 1_655 ? O25 Si8 Ca2 137.1(2) 1_655 . ? O26 Si8 Ca2 79.72(19) . . ? O24 Si8 Ca2 33.9(2) 1_655 . ? O22 Si8 Ca2 106.32(18) 1_655 . ? Ca3 Si8 Ca2 110.31(6) 2_646 . ? Na2 Si8 Ca2 70.13(6) 1_655 . ? OH27 Si8 Ca2 43.07(7) 1_655 . ? O18 Be1 O25 109.0(5) 2_646 . ? O18 Be1 O23 119.0(5) 2_646 . ? O25 Be1 O23 109.5(6) . . ? O18 Be1 O15 110.2(6) 2_646 2_646 ? O25 Be1 O15 106.2(5) . 2_646 ? O23 Be1 O15 102.2(4) . 2_646 ? O18 Be1 Ca4 52.2(2) 2_646 2_646 ? O25 Be1 Ca4 56.7(3) . 2_646 ? O23 Be1 Ca4 135.3(5) . 2_646 ? O15 Be1 Ca4 122.3(4) 2_646 2_646 ? O18 Be1 Na1 138.0(5) 2_646 1_556 ? O25 Be1 Na1 112.6(5) . 1_556 ? O23 Be1 Na1 50.4(3) . 1_556 ? O15 Be1 Na1 52.4(2) 2_646 1_556 ? Ca4 Be1 Na1 168.0(3) 2_646 1_556 ? O18 Be1 Ca3 121.2(4) 2_646 2_546 ? O25 Be1 Ca3 55.3(3) . 2_546 ? O23 Be1 Ca3 119.4(4) . 2_546 ? O15 Be1 Ca3 51.0(3) 2_646 2_546 ? Ca4 Be1 Ca3 88.82(17) 2_646 2_546 ? Na1 Be1 Ca3 79.88(19) 1_556 2_546 ? O18 Be1 OW3 75.9(3) 2_646 2_646 ? O25 Be1 OW3 143.5(5) . 2_646 ? O23 Be1 OW3 45.7(3) . 2_646 ? O15 Be1 OW3 105.6(4) 2_646 2_646 ? Ca4 Be1 OW3 117.3(3) 2_646 2_646 ? Na1 Be1 OW3 74.4(2) 1_556 2_646 ? Ca3 Be1 OW3 153.2(3) 2_546 2_646 ? O24 Be2 O8 113.5(6) . 1_455 ? O24 Be2 O13 111.7(5) . . ? O8 Be2 O13 110.3(5) 1_455 . ? O24 Be2 OH28 105.1(5) . . ? O8 Be2 OH28 107.6(5) 1_455 . ? O13 Be2 OH28 108.3(5) . . ? O24 Be2 Na2 59.4(3) . . ? O8 Be2 Na2 153.5(5) 1_455 . ? O13 Be2 Na2 95.5(3) . . ? OH28 Be2 Na2 56.1(2) . . ? O24 Be2 Ca2 46.5(3) . 1_455 ? O8 Be2 Ca2 80.7(4) 1_455 1_455 ? O13 Be2 Ca2 157.7(5) . 1_455 ? OH28 Be2 Ca2 85.3(3) . 1_455 ? Na2 Be2 Ca2 77.30(19) . 1_455 ? O24 Be2 Ca1 134.6(4) . 1_455 ? O8 Be2 Ca1 44.5(3) 1_455 1_455 ? O13 Be2 Ca1 113.5(4) . 1_455 ? OH28 Be2 Ca1 64.5(3) . 1_455 ? Na2 Be2 Ca1 119.5(2) . 1_455 ? Ca2 Be2 Ca1 88.11(19) 1_455 1_455 ? O24 Be2 OW1 175.2(5) . 1_554 ? O8 Be2 OW1 62.7(3) 1_455 1_554 ? O13 Be2 OW1 72.9(3) . 1_554 ? OH28 Be2 OW1 74.2(3) . 1_554 ? Na2 Be2 OW1 122.5(3) . 1_554 ? Ca2 Be2 OW1 128.8(2) 1_455 1_554 ? Ca1 Be2 OW1 40.71(13) 1_455 1_554 ? O24 Be2 OW4 131.0(4) . 2_646 ? O8 Be2 OW4 65.6(3) 1_455 2_646 ? O13 Be2 OW4 44.7(3) . 2_646 ? OH28 Be2 OW4 122.3(4) . 2_646 ? Na2 Be2 OW4 139.8(3) . 2_646 ? Ca2 Be2 OW4 141.0(3) 1_455 2_646 ? Ca1 Be2 OW4 81.6(2) 1_455 2_646 ? OW1 Be2 OW4 51.14(19) 1_554 2_646 ? O24 Be2 Ca4 93.0(4) . 2_646 ? O8 Be2 Ca4 94.1(3) 1_455 2_646 ? O13 Be2 Ca4 34.4(2) . 2_646 ? OH28 Be2 Ca4 142.7(4) . 2_646 ? Na2 Be2 Ca4 111.3(2) . 2_646 ? Ca2 Be2 Ca4 128.9(3) 1_455 2_646 ? Ca1 Be2 Ca4 122.7(2) 1_455 2_646 ? OW1 Be2 Ca4 90.3(2) 1_554 2_646 ? OW4 Be2 Ca4 41.45(15) 2_646 2_646 ? O20 Be3 O5 115.5(6) 1_455 . ? O20 Be3 O2 115.6(6) 1_455 1_455 ? O5 Be3 O2 109.1(5) . 1_455 ? O20 Be3 OH27 112.0(5) 1_455 . ? O5 Be3 OH27 104.3(5) . . ? O2 Be3 OH27 98.4(4) 1_455 . ? O20 Be3 Ca2 60.0(3) 1_455 1_455 ? O5 Be3 Ca2 101.0(4) . 1_455 ? O2 Be3 Ca2 146.8(4) 1_455 1_455 ? OH27 Be3 Ca2 59.9(3) . 1_455 ? O20 Be3 Na2 52.2(3) 1_455 1_455 ? O5 Be3 Na2 163.5(4) . 1_455 ? O2 Be3 Na2 72.7(3) 1_455 1_455 ? OH27 Be3 Na2 91.4(4) . 1_455 ? Ca2 Be3 Na2 82.4(2) 1_455 1_455 ? O20 Be3 Ca1 140.4(5) 1_455 1_456 ? O5 Be3 Ca1 103.5(3) . 1_456 ? O2 Be3 Ca1 39.6(2) 1_455 1_456 ? OH27 Be3 Ca1 61.3(3) . 1_456 ? Ca2 Be3 Ca1 120.1(3) 1_455 1_456 ? Na2 Be3 Ca1 88.2(2) 1_455 1_456 ? O20 Be3 OW2 173.4(5) 1_455 1_556 ? O5 Be3 OW2 61.1(3) . 1_556 ? O2 Be3 OW2 62.5(3) 1_455 1_556 ? OH27 Be3 OW2 74.6(3) . 1_556 ? Ca2 Be3 OW2 125.4(3) 1_455 1_556 ? Na2 Be3 OW2 129.7(3) 1_455 1_556 ? Ca1 Be3 OW2 42.46(12) 1_456 1_556 ? O20 Be3 Ca4 88.3(4) 1_455 1_455 ? O5 Be3 Ca4 41.4(3) . 1_455 ? O2 Be3 Ca4 96.9(4) 1_455 1_455 ? OH27 Be3 Ca4 145.7(4) . 1_455 ? Ca2 Be3 Ca4 115.1(3) 1_455 1_455 ? Na2 Be3 Ca4 122.5(3) 1_455 1_455 ? Ca1 Be3 Ca4 119.4(2) 1_456 1_455 ? OW2 Be3 Ca4 85.72(19) 1_556 1_455 ? O4 Be4 O6 110.7(7) 2_646 2_646 ? O4 Be4 O10 118.0(5) 2_646 . ? O6 Be4 O10 109.1(6) 2_646 . ? O4 Be4 O12 107.6(6) 2_646 . ? O6 Be4 O12 102.2(5) 2_646 . ? O10 Be4 O12 107.9(7) . . ? O4 Be4 Na1 57.2(3) 2_646 . ? O6 Be4 Na1 141.0(5) 2_646 . ? O10 Be4 Na1 61.8(3) . . ? O12 Be4 Na1 116.7(5) . . ? O4 Be4 Ca3 120.8(5) 2_646 2_646 ? O6 Be4 Ca3 48.0(3) 2_646 2_646 ? O10 Be4 Ca3 121.1(5) . 2_646 ? O12 Be4 Ca3 54.2(2) . 2_646 ? Na1 Be4 Ca3 170.6(4) . 2_646 ? O4 Be4 Ca4 52.6(3) 2_646 2_646 ? O6 Be4 Ca4 121.4(5) 2_646 2_646 ? O10 Be4 Ca4 128.6(5) . 2_646 ? O12 Be4 Ca4 55.1(3) . 2_646 ? Na1 Be4 Ca4 82.6(2) . 2_646 ? Ca3 Be4 Ca4 89.3(2) 2_646 2_646 ? O4 Be4 OW5 106.9(5) 2_646 2_646 ? O6 Be4 OW5 73.3(4) 2_646 2_646 ? O10 Be4 OW5 46.0(4) . 2_646 ? O12 Be4 OW5 144.4(5) . 2_646 ? Na1 Be4 OW5 75.9(2) . 2_646 ? Ca3 Be4 OW5 112.8(3) 2_646 2_646 ? Ca4 Be4 OW5 156.7(3) 2_646 2_646 ? O26 Be5 O21 114.7(6) . . ? O26 Be5 O14 115.8(6) . . ? O21 Be5 O14 108.0(6) . . ? O26 Be5 OH27 109.5(7) . 1_655 ? O21 Be5 OH27 105.1(5) . 1_655 ? O14 Be5 OH27 102.5(5) . 1_655 ? O26 Be5 Ca2 99.1(5) . . ? O21 Be5 Ca2 145.7(5) . . ? O14 Be5 Ca2 57.7(3) . . ? OH27 Be5 Ca2 55.8(3) 1_655 . ? O26 Be5 OW1 70.4(4) . 1_655 ? O21 Be5 OW1 68.4(3) . 1_655 ? O14 Be5 OW1 173.8(6) . 1_655 ? OH27 Be5 OW1 74.1(3) 1_655 1_655 ? Ca2 Be5 OW1 122.3(3) . 1_655 ? O26 Be5 Na2 161.0(5) . . ? O21 Be5 Na2 73.5(4) . . ? O14 Be5 Na2 46.0(3) . . ? OH27 Be5 Na2 83.2(4) 1_655 . ? Ca2 Be5 Na2 75.9(2) . . ? OW1 Be5 Na2 127.9(3) 1_655 . ? O26 Be5 Ca1 112.4(4) . 1_556 ? O21 Be5 Ca1 44.5(3) . 1_556 ? O14 Be5 Ca1 131.6(5) . 1_556 ? OH27 Be5 Ca1 64.0(3) 1_655 1_556 ? Ca2 Be5 Ca1 118.4(3) . 1_556 ? OW1 Be5 Ca1 42.22(15) 1_655 1_556 ? Na2 Be5 Ca1 85.7(2) . 1_556 ? O26 Be5 Ca3 36.2(3) . 2_646 ? O21 Be5 Ca3 98.9(4) . 2_646 ? O14 Be5 Ca3 93.5(4) . 2_646 ? OH27 Be5 Ca3 145.1(5) 1_655 2_646 ? Ca2 Be5 Ca3 112.2(3) . 2_646 ? OW1 Be5 Ca3 92.1(2) 1_655 2_646 ? Na2 Be5 Ca3 128.4(3) . 2_646 ? Ca1 Be5 Ca3 124.7(3) 1_556 2_646 ? O16 Be6 O19 124.3(6) 1_455 . ? O16 Be6 OH28 105.4(5) 1_455 . ? O19 Be6 OH28 110.2(6) . . ? O16 Be6 O7 106.2(6) 1_455 . ? O19 Be6 O7 104.6(5) . . ? OH28 Be6 O7 104.6(5) . . ? O16 Be6 Na2 143.2(5) 1_455 . ? O19 Be6 Na2 92.5(4) . . ? OH28 Be6 Na2 54.9(2) . . ? O7 Be6 Na2 59.0(3) . . ? O16 Be6 Ca2 70.3(4) 1_455 1_455 ? O19 Be6 Ca2 151.3(5) . 1_455 ? OH28 Be6 Ca2 85.7(4) . 1_455 ? O7 Be6 Ca2 47.0(3) . 1_455 ? Na2 Be6 Ca2 76.93(19) . 1_455 ? O16 Be6 OW2 70.3(4) 1_455 . ? O19 Be6 OW2 73.6(4) . . ? OH28 Be6 OW2 82.4(3) . . ? O7 Be6 OW2 172.9(4) . . ? Na2 Be6 OW2 127.5(3) . . ? Ca2 Be6 OW2 133.8(3) 1_455 . ? O16 Be6 Ca1 45.2(3) 1_455 1_455 ? O19 Be6 Ca1 118.7(5) . 1_455 ? OH28 Be6 Ca1 66.2(3) . 1_455 ? O7 Be6 Ca1 136.4(4) . 1_455 ? Na2 Be6 Ca1 120.1(3) . 1_455 ? Ca2 Be6 Ca1 89.4(2) 1_455 1_455 ? OW2 Be6 Ca1 45.15(14) . 1_455 ? O16 Be6 Ca3 98.2(4) 1_455 . ? O19 Be6 Ca3 41.1(3) . . ? OH28 Be6 Ca3 151.0(5) . . ? O7 Be6 Ca3 84.4(3) . . ? Na2 Be6 Ca3 112.2(2) . . ? Ca2 Be6 Ca3 118.6(3) 1_455 . ? OW2 Be6 Ca3 90.0(2) . . ? Ca1 Be6 Ca3 125.2(2) 1_455 . ? Si5 O1 Si1 145.8(2) . 1_554 ? Si5 O1 Na1 89.53(18) . 2_655 ? Si1 O1 Na1 91.25(19) 1_554 2_655 ? Si5 O1 OW2 105.3(3) . . ? Si1 O1 OW2 104.9(2) 1_554 . ? Na1 O1 OW2 116.10(16) 2_655 . ? Si1 O2 Be3 118.4(4) . 1_655 ? Si1 O2 Ca1 127.8(2) . 1_556 ? Be3 O2 Ca1 113.3(3) 1_655 1_556 ? Si1 O2 OH27 157.4(2) . 1_655 ? Be3 O2 OH27 41.2(3) 1_655 1_655 ? Ca1 O2 OH27 74.29(15) 1_556 1_655 ? Si1 O2 Na2 87.78(17) . . ? Be3 O2 Na2 74.5(3) 1_655 . ? Ca1 O2 Na2 113.13(15) 1_556 . ? OH27 O2 Na2 77.64(14) 1_655 . ? Si1 O2 OW2 121.2(2) . 1_656 ? Be3 O2 OW2 88.0(3) 1_655 1_656 ? Ca1 O2 OW2 52.72(13) 1_556 1_656 ? OH27 O2 OW2 73.95(18) 1_655 1_656 ? Na2 O2 OW2 150.90(19) . 1_656 ? Si2 O3 Si1 128.6(3) . . ? Si2 O3 Na2 99.36(18) . . ? Si1 O3 Na2 106.1(2) . . ? Be4 O4 Si1 125.6(5) 2_656 . ? Be4 O4 Na1 90.6(4) 2_656 2_656 ? Si1 O4 Na1 97.5(2) . 2_656 ? Be4 O4 Ca4 99.3(4) 2_656 . ? Si1 O4 Ca4 128.3(3) . . ? Na1 O4 Ca4 107.16(17) 2_656 . ? Be4 O4 OW4 106.5(5) 2_656 . ? Si1 O4 OW4 121.7(2) . . ? Na1 O4 OW4 54.32(18) 2_656 . ? Ca4 O4 OW4 53.70(17) . . ? Si2 O5 Be3 123.3(4) . . ? Si2 O5 Ca4 108.1(2) . 1_455 ? Be3 O5 Ca4 112.4(4) . 1_455 ? Si2 O5 OW5 106.1(3) . . ? Be3 O5 OW5 129.2(5) . . ? Ca4 O5 OW5 55.8(2) 1_455 . ? Si2 O5 OH27 93.2(2) . . ? Be3 O5 OH27 38.8(3) . . ? Ca4 O5 OH27 151.2(2) 1_455 . ? OW5 O5 OH27 137.0(3) . . ? Si2 O5 OW2 104.7(2) . 1_556 ? Be3 O5 OW2 90.3(3) . 1_556 ? Ca4 O5 OW2 117.26(19) 1_455 1_556 ? OW5 O5 OW2 64.4(2) . 1_556 ? OH27 O5 OW2 73.68(16) . 1_556 ? Si2 O6 Be4 125.6(4) . 2_656 ? Si2 O6 Ca3 124.9(2) . . ? Be4 O6 Ca3 100.6(4) 2_656 . ? Si2 O6 Ca4 86.5(2) . 1_455 ? Be4 O6 Ca4 108.3(4) 2_656 1_455 ? Ca3 O6 Ca4 107.66(15) . 1_455 ? Si2 O7 Be6 135.3(4) . . ? Si2 O7 Ca2 124.0(3) . 1_455 ? Be6 O7 Ca2 99.1(3) . 1_455 ? Si2 O7 Na2 94.82(18) . . ? Be6 O7 Na2 85.9(3) . . ? Ca2 O7 Na2 101.95(18) 1_455 . ? Si2 O7 OH28 144.0(3) . . ? Be6 O7 OH28 36.8(3) . . ? Ca2 O7 OH28 85.45(18) 1_455 . ? Na2 O7 OH28 55.60(13) . . ? Si2 O7 OH27 77.7(2) . . ? Be6 O7 OH27 146.3(4) . . ? Ca2 O7 OH27 52.00(12) 1_455 . ? Na2 O7 OH27 84.29(15) . . ? OH28 O7 OH27 114.6(2) . . ? Be2 O8 Si3 126.6(4) 1_655 . ? Be2 O8 Ca1 107.9(4) 1_655 . ? Si3 O8 Ca1 122.3(2) . . ? Be2 O8 OH28 37.2(3) 1_655 1_655 ? Si3 O8 OH28 150.9(3) . 1_655 ? Ca1 O8 OH28 71.85(16) . 1_655 ? Be2 O8 OW1 89.5(4) 1_655 1_654 ? Si3 O8 OW1 136.5(3) . 1_654 ? Ca1 O8 OW1 49.01(14) . 1_654 ? OH28 O8 OW1 72.54(19) 1_655 1_654 ? Si3 O9 Si4 129.5(3) . . ? Si3 O9 Ca2 116.5(3) . . ? Si4 O9 Ca2 97.2(2) . . ? Si3 O10 Be4 132.0(5) . . ? Si3 O10 OW5 122.0(4) . 2_646 ? Be4 O10 OW5 105.6(5) . 2_646 ? Si3 O10 Na1 93.7(2) . . ? Be4 O10 Na1 84.5(4) . . ? OW5 O10 Na1 98.7(3) 2_646 . ? Si7 O11 Si3 133.3(3) . 1_556 ? Si7 O11 Na1 89.6(2) . 1_556 ? Si3 O11 Na1 89.3(2) 1_556 1_556 ? Si7 O11 OW1 112.1(3) . . ? Si3 O11 OW1 114.5(3) 1_556 . ? Na1 O11 OW1 86.64(17) 1_556 . ? Si4 O12 Be4 125.1(4) . . ? Si4 O12 Ca3 131.4(2) . 2_646 ? Be4 O12 Ca3 92.4(3) . 2_646 ? Si4 O12 Ca4 90.89(18) . 2_646 ? Be4 O12 Ca4 93.9(4) . 2_646 ? Ca3 O12 Ca4 118.71(16) 2_646 2_646 ? Si4 O13 Be2 128.1(4) . . ? Si4 O13 Ca4 102.1(2) . 2_646 ? Be2 O13 Ca4 122.8(4) . 2_646 ? Si4 O13 OW4 115.5(3) . 2_646 ? Be2 O13 OW4 109.3(3) . 2_646 ? Ca4 O13 OW4 59.71(19) 2_646 2_646 ? Si4 O13 OH28 95.6(2) . . ? Be2 O13 OH28 36.3(3) . . ? Ca4 O13 OH28 159.0(2) 2_646 . ? OW4 O13 OH28 121.8(2) 2_646 . ? Si4 O14 Be5 131.1(5) . . ? Si4 O14 Na2 121.1(3) . . ? Be5 O14 Na2 104.8(4) . . ? Si4 O14 Ca2 96.5(2) . . ? Be5 O14 Ca2 89.2(4) . . ? Na2 O14 Ca2 102.0(2) . . ? Si4 O14 OH27 146.3(3) . 1_655 ? Be5 O14 OH27 39.5(3) . 1_655 ? Na2 O14 OH27 87.8(2) . 1_655 ? Ca2 O14 OH27 57.75(15) . 1_655 ? Si5 O15 Be1 122.6(5) . 2_656 ? Si5 O15 Na1 98.0(2) . 2_655 ? Be1 O15 Na1 93.6(3) 2_656 2_655 ? Si5 O15 Ca3 129.5(3) . 1_655 ? Be1 O15 Ca3 97.9(3) 2_656 1_655 ? Na1 O15 Ca3 109.1(2) 2_655 1_655 ? Be6 O16 Si5 124.1(5) 1_655 . ? Be6 O16 Ca1 107.4(4) 1_655 . ? Si5 O16 Ca1 127.1(3) . . ? Be6 O16 OH28 39.1(3) 1_655 1_655 ? Si5 O16 OH28 159.0(3) . 1_655 ? Ca1 O16 OH28 73.28(18) . 1_655 ? Be6 O16 Ca2 80.2(4) 1_655 . ? Si5 O16 Ca2 89.9(3) . . ? Ca1 O16 Ca2 111.72(19) . . ? OH28 O16 Ca2 75.81(17) 1_655 . ? Be6 O16 OW2 81.1(4) 1_655 1_655 ? Si5 O16 OW2 120.9(3) . 1_655 ? Ca1 O16 OW2 52.12(15) . 1_655 ? OH28 O16 OW2 74.2(2) 1_655 1_655 ? Ca2 O16 OW2 149.2(2) . 1_655 ? Si5 O17 Si6 129.1(3) . . ? Si5 O17 Ca2 104.0(3) . . ? Si6 O17 Ca2 94.8(2) . . ? Si5 O17 OW2 101.1(2) . . ? Si6 O17 OW2 100.2(3) . . ? Ca2 O17 OW2 131.9(2) . . ? Si6 O18 Be1 129.2(4) . 2_656 ? Si6 O18 Ca4 127.1(3) . . ? Be1 O18 Ca4 95.5(3) 2_656 . ? Si6 O18 Ca3 85.5(2) . . ? Be1 O18 Ca3 106.8(4) 2_656 . ? Ca4 O18 Ca3 109.65(19) . . ? Si6 O19 Be6 129.7(5) . . ? Si6 O19 Ca3 113.4(3) . . ? Be6 O19 Ca3 113.4(5) . . ? Si6 O19 OH28 94.8(3) . . ? Be6 O19 OH28 36.1(3) . . ? Ca3 O19 OH28 149.2(3) . . ? Si6 O19 OW3 105.0(3) . . ? Be6 O19 OW3 117.3(4) . . ? Ca3 O19 OW3 53.0(2) . . ? OH28 O19 OW3 132.7(3) . . ? Be3 O20 Si6 138.1(5) 1_655 . ? Be3 O20 Na2 99.3(4) 1_655 . ? Si6 O20 Na2 117.4(2) . . ? Be3 O20 Ca2 89.5(4) 1_655 . ? Si6 O20 Ca2 99.4(2) . . ? Na2 O20 Ca2 104.6(2) . . ? Be3 O20 OH27 37.3(4) 1_655 1_655 ? Si6 O20 OH27 151.2(3) . 1_655 ? Na2 O20 OH27 87.82(19) . 1_655 ? Ca2 O20 OH27 58.32(15) . 1_655 ? Si7 O21 Be5 128.6(4) . . ? Si7 O21 Ca1 123.4(3) . 1_556 ? Be5 O21 Ca1 107.3(4) . 1_556 ? Si7 O21 OH27 154.1(3) . 1_655 ? Be5 O21 OH27 38.2(3) . 1_655 ? Ca1 O21 OH27 71.89(15) 1_556 1_655 ? Si7 O21 OW1 137.9(3) . 1_655 ? Be5 O21 OW1 80.9(4) . 1_655 ? Ca1 O21 OW1 49.88(14) 1_556 1_655 ? OH27 O21 OW1 67.96(18) 1_655 1_655 ? Si8 O22 Si7 127.7(3) 1_455 . ? Si8 O22 Na2 102.4(2) 1_455 . ? Si7 O22 Na2 113.9(3) . . ? Si7 O23 Be1 129.7(4) . . ? Si7 O23 Na1 101.6(2) . 1_556 ? Be1 O23 Na1 97.2(4) . 1_556 ? Si7 O23 OW3 111.9(3) . 2_646 ? Be1 O23 OW3 107.2(4) . 2_646 ? Na1 O23 OW3 105.3(2) 1_556 2_646 ? Be2 O24 Si8 130.8(5) . 1_455 ? Be2 O24 Ca2 103.9(4) . 1_455 ? Si8 O24 Ca2 123.3(3) 1_455 1_455 ? Be2 O24 Na2 88.6(4) . . ? Si8 O24 Na2 93.8(2) 1_455 . ? Ca2 O24 Na2 102.1(2) 1_455 . ? Be2 O24 OH28 38.6(3) . . ? Si8 O24 OH28 143.1(3) 1_455 . ? Ca2 O24 OH28 87.9(2) 1_455 . ? Na2 O24 OH28 57.52(15) . . ? Si8 O25 Be1 127.8(5) 1_455 . ? Si8 O25 Ca4 133.8(3) 1_455 2_646 ? Be1 O25 Ca4 89.9(4) . 2_646 ? Si8 O25 Ca3 89.9(3) 1_455 2_546 ? Be1 O25 Ca3 94.9(4) . 2_546 ? Ca4 O25 Ca3 115.1(2) 2_646 2_546 ? Be5 O26 Si8 128.2(5) . . ? Be5 O26 Ca3 122.3(5) . 2_646 ? Si8 O26 Ca3 97.3(2) . 2_646 ? Be5 O26 OH27 37.4(4) . 1_655 ? Si8 O26 OH27 96.8(3) . 1_655 ? Ca3 O26 OH27 158.9(2) 2_646 1_655 ? Be5 O26 OW1 81.1(4) . 1_655 ? Si8 O26 OW1 105.6(3) . 1_655 ? Ca3 O26 OW1 122.9(2) 2_646 1_655 ? OH27 O26 OW1 67.51(17) 1_655 1_655 ? Be5 OH27 Be3 127.0(5) 1_455 . ? Be5 OH27 Ca2 89.8(3) 1_455 1_455 ? Be3 OH27 Ca2 83.5(3) . 1_455 ? Be5 OH27 O2 105.5(4) 1_455 1_455 ? Be3 OH27 O2 40.4(3) . 1_455 ? Ca2 OH27 O2 119.16(18) 1_455 1_455 ? Be5 OH27 O14 38.0(3) 1_455 1_455 ? Be3 OH27 O14 97.6(3) . 1_455 ? Ca2 OH27 O14 59.78(14) 1_455 1_455 ? O2 OH27 O14 99.0(2) 1_455 1_455 ? Be5 OH27 O20 106.0(4) 1_455 1_455 ? Be3 OH27 O20 30.7(3) . 1_455 ? Ca2 OH27 O20 57.79(14) 1_455 1_455 ? O2 OH27 O20 61.38(17) 1_455 1_455 ? O14 OH27 O20 70.36(17) 1_455 1_455 ? Be5 OH27 O26 33.1(4) 1_455 1_455 ? Be3 OH27 O26 158.9(4) . 1_455 ? Ca2 OH27 O26 88.69(18) 1_455 1_455 ? O2 OH27 O26 133.5(2) 1_455 1_455 ? O14 OH27 O26 61.68(19) 1_455 1_455 ? O20 OH27 O26 131.1(2) 1_455 1_455 ? Be5 OH27 O5 163.8(4) 1_455 . ? Be3 OH27 O5 36.8(3) . . ? Ca2 OH27 O5 87.50(17) 1_455 . ? O2 OH27 O5 62.45(18) 1_455 . ? O14 OH27 O5 129.4(2) 1_455 . ? O20 OH27 O5 59.36(17) 1_455 . ? O26 OH27 O5 162.4(2) 1_455 . ? Be5 OH27 O21 36.7(4) 1_455 1_455 ? Be3 OH27 O21 107.1(4) . 1_455 ? Ca2 OH27 O21 120.44(19) 1_455 1_455 ? O2 OH27 O21 72.92(18) 1_455 1_455 ? O14 OH27 O21 60.73(17) 1_455 1_455 ? O20 OH27 O21 104.1(2) 1_455 1_455 ? O26 OH27 O21 60.63(19) 1_455 1_455 ? O5 OH27 O21 135.1(2) . 1_455 ? Be5 OH27 Ca1 85.2(3) 1_455 1_456 ? Be3 OH27 Ca1 88.4(3) . 1_456 ? Ca2 OH27 Ca1 165.20(18) 1_455 1_456 ? O2 OH27 Ca1 49.60(11) 1_455 1_456 ? O14 OH27 Ca1 109.42(19) 1_455 1_456 ? O20 OH27 Ca1 110.31(19) 1_455 1_456 ? O26 OH27 Ca1 94.64(17) 1_455 1_456 ? O5 OH27 Ca1 93.39(16) . 1_456 ? O21 OH27 Ca1 50.62(12) 1_455 1_456 ? Be5 OH27 O7 131.5(4) 1_455 . ? Be3 OH27 O7 76.3(3) . . ? Ca2 OH27 O7 46.97(11) 1_455 . ? O2 OH27 O7 114.1(2) 1_455 . ? O14 OH27 O7 106.75(18) 1_455 . ? O20 OH27 O7 72.23(18) 1_455 . ? O26 OH27 O7 112.0(2) 1_455 . ? O5 OH27 O7 54.22(16) . . ? O21 OH27 O7 167.1(2) 1_455 . ? Ca1 OH27 O7 142.22(18) 1_456 . ? Be5 OH27 OW1 74.7(3) 1_455 . ? Be3 OH27 OW1 129.6(3) . . ? Ca2 OH27 OW1 146.5(2) 1_455 . ? O2 OH27 OW1 93.88(18) 1_455 . ? O14 OH27 OW1 112.6(2) 1_455 . ? O20 OH27 OW1 154.9(2) 1_455 . ? O26 OH27 OW1 62.10(17) 1_455 . ? O5 OH27 OW1 115.12(18) . . ? O21 OH27 OW1 61.06(16) 1_455 . ? Ca1 OH27 OW1 44.59(12) 1_456 . ? O7 OH27 OW1 126.71(19) . . ? Be2 OH28 Be6 129.2(5) . . ? Be2 OH28 Na2 89.9(3) . . ? Be6 OH28 Na2 91.4(3) . . ? Be2 OH28 O16 104.5(3) . 1_455 ? Be6 OH28 O16 35.6(3) . 1_455 ? Na2 OH28 O16 119.9(2) . 1_455 ? Be2 OH28 O24 36.3(3) . . ? Be6 OH28 O24 104.8(4) . . ? Na2 OH28 O24 61.05(14) . . ? O16 OH28 O24 99.1(2) 1_455 . ? Be2 OH28 O8 35.2(3) . 1_455 ? Be6 OH28 O8 109.0(4) . 1_455 ? Na2 OH28 O8 121.9(2) . 1_455 ? O16 OH28 O8 75.51(18) 1_455 1_455 ? O24 OH28 O8 61.25(18) . 1_455 ? Be2 OH28 O19 161.5(4) . . ? Be6 OH28 O19 33.7(3) . . ? Na2 OH28 O19 84.76(17) . . ? O16 OH28 O19 63.7(2) 1_455 . ? O24 OH28 O19 128.0(2) . . ? O8 OH28 O19 138.9(2) 1_455 . ? Be2 OH28 O13 35.4(3) . . ? Be6 OH28 O13 164.3(4) . . ? Na2 OH28 O13 86.58(16) . . ? O16 OH28 O13 135.3(2) 1_455 . ? O24 OH28 O13 60.79(19) . . ? O8 OH28 O13 59.80(17) 1_455 . ? O19 OH28 O13 160.5(2) . . ? Be2 OH28 O7 103.5(4) . . ? Be6 OH28 O7 38.6(3) . . ? Na2 OH28 O7 60.01(13) . . ? O16 OH28 O7 59.91(18) 1_455 . ? O24 OH28 O7 70.17(18) . . ? O8 OH28 O7 105.3(2) 1_455 . ? O19 OH28 O7 58.6(2) . . ? O13 OH28 O7 129.9(2) . . ? Be2 OH28 Ca1 84.9(3) . 1_455 ? Be6 OH28 Ca1 82.6(3) . 1_455 ? Na2 OH28 Ca1 166.9(2) . 1_455 ? O16 OH28 Ca1 50.52(13) 1_455 1_455 ? O24 OH28 Ca1 109.16(18) . 1_455 ? O8 OH28 Ca1 50.54(12) 1_455 1_455 ? O19 OH28 Ca1 96.37(17) . 1_455 ? O13 OH28 Ca1 96.00(16) . 1_455 ? O7 OH28 Ca1 109.56(17) . 1_455 ? Be2 OH28 Si6 161.0(3) . . ? Be6 OH28 Si6 62.4(3) . . ? Na2 OH28 Si6 73.77(12) . . ? O16 OH28 Si6 92.31(19) 1_455 . ? O24 OH28 Si6 133.06(18) . . ? O8 OH28 Si6 163.47(19) 1_455 . ? O19 OH28 Si6 29.25(15) . . ? O13 OH28 Si6 131.29(18) . . ? O7 OH28 Si6 77.06(16) . . ? Ca1 OH28 Si6 113.03(15) 1_455 . ? Be2 OH28 Si4 63.5(3) . . ? Be6 OH28 Si4 160.9(3) . . ? Na2 OH28 Si4 73.17(12) . . ? O16 OH28 Si4 163.5(2) 1_455 . ? O24 OH28 Si4 77.97(17) . . ? O8 OH28 Si4 89.03(17) 1_455 . ? O19 OH28 Si4 130.8(2) . . ? O13 OH28 Si4 29.74(11) . . ? O7 OH28 Si4 131.76(16) . . ? Ca1 OH28 Si4 114.71(14) 1_455 . ? Si6 OH28 Si4 101.60(12) . . ? Ca1 OW1 O11 160.1(3) 1_456 . ? Ca1 OW1 O21 52.61(14) 1_456 1_455 ? O11 OW1 O21 143.5(3) . 1_455 ? Ca1 OW1 OW4 112.2(3) 1_456 2_647 ? O11 OW1 OW4 84.7(2) . 2_647 ? O21 OW1 OW4 85.0(2) 1_455 2_647 ? Ca1 OW1 O26 100.3(2) 1_456 1_455 ? O11 OW1 O26 91.4(2) . 1_455 ? O21 OW1 O26 52.72(17) 1_455 1_455 ? OW4 OW1 O26 84.8(2) 2_647 1_455 ? Ca1 OW1 O8 51.21(15) 1_456 1_456 ? O11 OW1 O8 137.9(3) . 1_456 ? O21 OW1 O8 64.66(16) 1_455 1_456 ? OW4 OW1 O8 64.1(2) 2_647 1_456 ? O26 OW1 O8 111.6(2) 1_455 1_456 ? Ca1 OW1 OH27 63.75(16) 1_456 . ? O11 OW1 OH27 114.5(3) . . ? O21 OW1 OH27 50.98(15) 1_455 . ? OW4 OW1 OH27 129.3(2) 2_647 . ? O26 OW1 OH27 50.39(16) 1_455 . ? O8 OW1 OH27 107.26(19) 1_456 . ? Ca1 OW1 Be5 72.1(2) 1_456 1_455 ? O11 OW1 Be5 117.5(3) . 1_455 ? O21 OW1 Be5 30.7(2) 1_455 1_455 ? OW4 OW1 Be5 98.2(3) 2_647 1_455 ? O26 OW1 Be5 28.4(2) 1_455 1_455 ? O8 OW1 Be5 95.4(3) 1_456 1_455 ? OH27 OW1 Be5 31.12(19) . 1_455 ? Ca1 OW1 OW2 50.03(14) 1_456 1_556 ? O11 OW1 OW2 110.4(2) . 1_556 ? O21 OW1 OW2 93.24(19) 1_455 1_556 ? OW4 OW1 OW2 154.3(3) 2_647 1_556 ? O26 OW1 OW2 114.4(2) 1_455 1_556 ? O8 OW1 OW2 92.1(2) 1_456 1_556 ? OH27 OW1 OW2 64.44(18) . 1_556 ? Be5 OW1 OW2 93.0(2) 1_455 1_556 ? Ca1 OW1 OH28 59.31(16) 1_456 1_556 ? O11 OW1 OH28 111.3(2) . 1_556 ? O21 OW1 OH28 104.2(2) 1_455 1_556 ? OW4 OW1 OH28 92.9(2) 2_647 1_556 ? O26 OW1 OH28 156.9(2) 1_455 1_556 ? O8 OW1 OH28 48.15(15) 1_456 1_556 ? OH27 OW1 OH28 118.62(19) . 1_556 ? Be5 OW1 OH28 130.7(3) 1_455 1_556 ? OW2 OW1 OH28 62.60(18) 1_556 1_556 ? Ca1 OW1 Be2 66.2(2) 1_456 1_556 ? O11 OW1 Be2 114.9(3) . 1_556 ? O21 OW1 Be2 92.4(2) 1_455 1_556 ? OW4 OW1 Be2 65.9(2) 2_647 1_556 ? O26 OW1 Be2 137.0(3) 1_455 1_556 ? O8 OW1 Be2 27.76(16) 1_456 1_556 ? OH27 OW1 Be2 129.4(2) . 1_556 ? Be5 OW1 Be2 123.1(3) 1_455 1_556 ? OW2 OW1 Be2 88.6(2) 1_556 1_556 ? OH28 OW1 Be2 28.45(16) 1_556 1_556 ? Ca1 OW1 Si7 153.0(2) 1_456 . ? O11 OW1 Si7 24.30(14) . . ? O21 OW1 Si7 121.7(2) 1_455 . ? OW4 OW1 Si7 92.0(2) 2_647 . ? O26 OW1 Si7 69.04(17) 1_455 . ? O8 OW1 Si7 155.4(2) 1_456 . ? OH27 OW1 Si7 92.03(19) . . ? Be5 OW1 Si7 93.5(3) 1_455 . ? OW2 OW1 Si7 110.3(2) 1_556 . ? OH28 OW1 Si7 134.04(18) 1_556 . ? Be2 OW1 Si7 138.4(2) 1_556 . ? Ca1 OW2 OW5 127.3(3) 1_455 1_554 ? Ca1 OW2 O5 97.08(19) 1_455 1_554 ? OW5 OW2 O5 50.1(2) 1_554 1_554 ? Ca1 OW2 O1 149.4(2) 1_455 . ? OW5 OW2 O1 80.6(3) 1_554 . ? O5 OW2 O1 92.6(2) 1_554 . ? Ca1 OW2 O2 49.57(12) 1_455 1_454 ? OW5 OW2 O2 79.4(2) 1_554 1_454 ? O5 OW2 O2 53.43(15) 1_554 1_454 ? O1 OW2 O2 145.9(3) . 1_454 ? Ca1 OW2 O16 49.94(14) 1_455 1_455 ? OW5 OW2 O16 103.5(3) 1_554 1_455 ? O5 OW2 O16 116.8(2) 1_554 1_455 ? O1 OW2 O16 145.2(3) . 1_455 ? O2 OW2 O16 67.07(15) 1_454 1_455 ? Ca1 OW2 O17 118.5(2) 1_455 . ? OW5 OW2 O17 108.7(2) 1_554 . ? O5 OW2 O17 141.7(2) 1_554 . ? O1 OW2 O17 49.48(16) . . ? O2 OW2 O17 164.6(3) 1_454 . ? O16 OW2 O17 97.9(2) 1_455 . ? Ca1 OW2 OW3 126.4(3) 1_455 . ? OW5 OW2 OW3 44.0(2) 1_554 . ? O5 OW2 OW3 93.7(2) 1_554 . ? O1 OW2 OW3 81.5(2) . . ? O2 OW2 OW3 102.1(2) 1_454 . ? O16 OW2 OW3 78.5(2) 1_455 . ? O17 OW2 OW3 77.0(2) . . ? Ca1 OW2 OW1 46.50(13) 1_455 1_554 ? OW5 OW2 OW1 155.0(3) 1_554 1_554 ? O5 OW2 OW1 104.9(2) 1_554 1_554 ? O1 OW2 OW1 102.90(19) . 1_554 ? O2 OW2 OW1 84.92(17) 1_454 1_554 ? O16 OW2 OW1 87.8(2) 1_455 1_554 ? O17 OW2 OW1 91.36(18) . 1_554 ? OW3 OW2 OW1 160.6(3) . 1_554 ? Ca1 OW2 Be6 67.6(2) 1_455 . ? OW5 OW2 Be6 112.3(3) 1_554 . ? O5 OW2 Be6 143.8(2) 1_554 . ? O1 OW2 Be6 117.5(3) . . ? O2 OW2 Be6 95.6(2) 1_454 . ? O16 OW2 Be6 28.60(18) 1_455 . ? O17 OW2 Be6 69.3(2) . . ? OW3 OW2 Be6 73.0(3) . . ? OW1 OW2 Be6 88.4(2) 1_554 . ? Ca1 OW2 OH27 58.76(14) 1_455 1_554 ? OW5 OW2 OH27 98.1(2) 1_554 1_554 ? O5 OW2 OH27 48.51(14) 1_554 1_554 ? O1 OW2 OH27 110.1(2) . 1_554 ? O2 OW2 OH27 46.84(13) 1_454 1_554 ? O16 OW2 OH27 103.62(18) 1_455 1_554 ? O17 OW2 OH27 140.4(2) . 1_554 ? OW3 OW2 OH27 139.5(2) . 1_554 ? OW1 OW2 OH27 57.20(16) 1_554 1_554 ? Be6 OW2 OH27 126.3(2) . 1_554 ? Ca1 OW2 Be3 68.43(19) 1_455 1_554 ? OW5 OW2 Be3 72.2(2) 1_554 1_554 ? O5 OW2 Be3 28.65(18) 1_554 1_554 ? O1 OW2 Be3 117.2(3) . 1_554 ? O2 OW2 Be3 29.55(18) 1_454 1_554 ? O16 OW2 Be3 96.6(2) 1_455 1_554 ? O17 OW2 Be3 164.7(3) . 1_554 ? OW3 OW2 Be3 110.6(2) . 1_554 ? OW1 OW2 Be3 84.5(2) 1_554 1_554 ? Be6 OW2 Be3 125.1(2) . 1_554 ? OH27 OW2 Be3 29.16(16) 1_554 1_554 ? OW5 OW3 Ca3 157.5(5) 1_554 . ? OW5 OW3 OW4 41.9(3) 1_554 1_454 ? Ca3 OW3 OW4 119.9(4) . 1_454 ? OW5 OW3 O23 103.5(5) 1_554 2_656 ? Ca3 OW3 O23 96.5(3) . 2_656 ? OW4 OW3 O23 113.9(4) 1_454 2_656 ? OW5 OW3 O19 128.6(4) 1_554 . ? Ca3 OW3 O19 55.7(2) . . ? OW4 OW3 O19 146.0(4) 1_454 . ? O23 OW3 O19 99.9(3) 2_656 . ? OW5 OW3 OW2 64.4(3) 1_554 . ? Ca3 OW3 OW2 116.5(3) . . ? OW4 OW3 OW2 97.9(3) 1_454 . ? O23 OW3 OW2 113.3(3) 2_656 . ? O19 OW3 OW2 64.4(2) . . ? OW5 OW3 Be1 120.0(5) 1_554 2_656 ? Ca3 OW3 Be1 82.5(2) . 2_656 ? OW4 OW3 Be1 140.8(4) 1_454 2_656 ? O23 OW3 Be1 27.1(2) 2_656 2_656 ? O19 OW3 Be1 72.9(3) . 2_656 ? OW2 OW3 Be1 99.5(3) . 2_656 ? OW5 OW3 Si7 98.5(4) 1_554 2_656 ? Ca3 OW3 Si7 95.3(2) . 2_656 ? OW4 OW3 Si7 93.4(3) 1_454 2_656 ? O23 OW3 Si7 25.32(13) 2_656 2_656 ? O19 OW3 Si7 120.0(3) . 2_656 ? OW2 OW3 Si7 133.9(3) . 2_656 ? Be1 OW3 Si7 50.2(2) 2_656 2_656 ? OW5 OW3 Si6 128.1(4) 1_554 . ? Ca3 OW3 Si6 66.71(17) . . ? OW4 OW3 Si6 166.4(3) 1_454 . ? O23 OW3 Si6 75.4(2) 2_656 . ? O19 OW3 Si6 25.68(15) . . ? OW2 OW3 Si6 68.77(18) . . ? Be1 OW3 Si6 48.40(19) 2_656 . ? Si7 OW3 Si6 97.98(19) 2_656 . ? OW5 OW3 Na1 75.0(4) 1_554 2 ? Ca3 OW3 Na1 82.7(2) . 2 ? OW4 OW3 Na1 43.5(2) 1_454 2 ? O23 OW3 Na1 146.2(3) 2_656 2 ? O19 OW3 Na1 107.0(3) . 2 ? OW2 OW3 Na1 96.8(2) . 2 ? Be1 OW3 Na1 161.7(3) 2_656 2 ? Si7 OW3 Na1 120.9(2) 2_656 2 ? Si6 OW3 Na1 132.6(3) . 2 ? OW5 OW3 Na1 72.2(4) 1_554 2_655 ? Ca3 OW3 Na1 129.8(3) . 2_655 ? OW4 OW3 Na1 99.2(3) 1_454 2_655 ? O23 OW3 Na1 35.45(16) 2_656 2_655 ? O19 OW3 Na1 107.1(3) . 2_655 ? OW2 OW3 Na1 84.8(2) . 2_655 ? Be1 OW3 Na1 48.17(18) 2_656 2_655 ? Si7 OW3 Na1 49.19(12) 2_656 2_655 ? Si6 OW3 Na1 82.72(17) . 2_655 ? Na1 OW3 Na1 142.7(2) 2 2_655 ? OW5 OW3 OW1 81.1(3) 1_554 2_556 ? Ca3 OW3 OW1 88.5(2) . 2_556 ? OW4 OW3 OW1 43.2(2) 1_454 2_556 ? O23 OW3 OW1 91.5(2) 2_656 2_556 ? O19 OW3 OW1 143.2(3) . 2_556 ? OW2 OW3 OW1 140.9(2) . 2_556 ? Be1 OW3 OW1 114.1(3) 2_656 2_556 ? Si7 OW3 OW1 66.15(14) 2_656 2_556 ? Si6 OW3 OW1 149.8(2) . 2_556 ? Na1 OW3 OW1 54.76(13) 2 2_556 ? Na1 OW3 OW1 102.39(19) 2_655 2_556 ? OW5 OW4 Na1 123.8(5) 1_655 2_656 ? OW5 OW4 Ca4 63.9(4) 1_655 . ? Na1 OW4 Ca4 111.9(3) 2_656 . ? OW5 OW4 OW3 62.0(4) 1_655 1_656 ? Na1 OW4 OW3 92.0(3) 2_656 1_656 ? Ca4 OW4 OW3 125.3(3) . 1_656 ? OW5 OW4 O13 109.0(5) 1_655 2_656 ? Na1 OW4 O13 111.0(3) 2_656 2_656 ? Ca4 OW4 O13 55.66(17) . 2_656 ? OW3 OW4 O13 155.1(4) 1_656 2_656 ? OW5 OW4 O4 90.0(4) 1_655 . ? Na1 OW4 O4 54.45(18) 2_656 . ? Ca4 OW4 O4 58.35(17) . . ? OW3 OW4 O4 114.1(3) 1_656 . ? O13 OW4 O4 87.9(2) 2_656 . ? OW5 OW4 OW1 146.1(5) 1_655 2_657 ? Na1 OW4 OW1 83.8(2) 2_656 2_657 ? Ca4 OW4 OW1 128.1(3) . 2_657 ? OW3 OW4 OW1 101.8(3) 1_656 2_657 ? O13 OW4 OW1 72.5(2) 2_656 2_657 ? O4 OW4 OW1 123.7(3) . 2_657 ? OW5 OW4 Be2 103.0(5) 1_655 2_656 ? Na1 OW4 Be2 129.4(3) 2_656 2_656 ? Ca4 OW4 Be2 70.1(2) . 2_656 ? OW3 OW4 Be2 129.6(3) 1_656 2_656 ? O13 OW4 Be2 26.05(17) 2_656 2_656 ? O4 OW4 Be2 113.5(2) . 2_656 ? OW1 OW4 Be2 62.9(2) 2_657 2_656 ? OW5 OW4 Si4 121.7(4) 1_655 2_656 ? Na1 OW4 Si4 87.66(19) 2_656 2_656 ? Ca4 OW4 Si4 58.74(14) . 2_656 ? OW3 OW4 Si4 175.6(3) 1_656 2_656 ? O13 OW4 Si4 23.90(13) 2_656 2_656 ? O4 OW4 Si4 69.13(15) . 2_656 ? OW1 OW4 Si4 73.77(19) 2_657 2_656 ? Be2 OW4 Si4 48.50(16) 2_656 2_656 ? OW5 OW4 Ca3 89.7(4) 1_655 1_656 ? Na1 OW4 Ca3 68.67(17) 2_656 1_656 ? Ca4 OW4 Ca3 149.3(3) . 1_656 ? OW3 OW4 Ca3 28.9(2) 1_656 1_656 ? O13 OW4 Ca3 154.7(3) 2_656 1_656 ? O4 OW4 Ca3 109.4(2) . 1_656 ? OW1 OW4 Ca3 82.47(19) 2_657 1_656 ? Be2 OW4 Ca3 134.9(2) 2_656 1_656 ? Si4 OW4 Ca3 148.1(2) 2_656 1_656 ? OW5 OW4 OW2 32.8(4) 1_655 1_656 ? Na1 OW4 OW2 92.5(2) 2_656 1_656 ? Ca4 OW4 OW2 82.6(2) . 1_656 ? OW3 OW4 OW2 46.5(2) 1_656 1_656 ? O13 OW4 OW2 137.0(3) 2_656 1_656 ? O4 OW4 OW2 77.01(18) . 1_656 ? OW1 OW4 OW2 148.1(2) 2_657 1_656 ? Be2 OW4 OW2 135.8(3) 2_656 1_656 ? Si4 OW4 OW2 138.0(2) 2_656 1_656 ? Ca3 OW4 OW2 66.79(14) 1_656 1_656 ? OW5 OW4 Ca1 118.4(4) 1_655 2_756 ? Na1 OW4 Ca1 112.6(2) 2_656 2_756 ? Ca4 OW4 Ca1 116.6(2) . 2_756 ? OW3 OW4 Ca1 95.5(3) 1_656 2_756 ? O13 OW4 Ca1 67.48(17) 2_656 2_756 ? O4 OW4 Ca1 146.7(2) . 2_756 ? OW1 OW4 Ca1 29.15(14) 2_657 2_756 ? Be2 OW4 Ca1 46.87(15) 2_656 2_756 ? Si4 OW4 Ca1 80.60(14) 2_656 2_756 ? Ca3 OW4 Ca1 88.95(13) 1_656 2_756 ? OW2 OW4 Ca1 136.26(17) 1_656 2_756 ? OW4 OW5 OW3 76.1(5) 1_455 1_556 ? OW4 OW5 Ca4 74.4(4) 1_455 1_455 ? OW3 OW5 Ca4 149.5(6) 1_556 1_455 ? OW4 OW5 O10 103.1(5) 1_455 2_656 ? OW3 OW5 O10 105.3(5) 1_556 2_656 ? Ca4 OW5 O10 89.1(3) 1_455 2_656 ? OW4 OW5 O5 125.7(5) 1_455 . ? OW3 OW5 O5 136.1(5) 1_556 . ? Ca4 OW5 O5 60.7(2) 1_455 . ? O10 OW5 O5 105.1(4) 2_656 . ? OW4 OW5 OW2 128.8(6) 1_455 1_556 ? OW3 OW5 OW2 71.6(3) 1_556 1_556 ? Ca4 OW5 OW2 122.7(4) 1_455 1_556 ? O10 OW5 OW2 123.1(4) 2_656 1_556 ? O5 OW5 OW2 65.4(3) . 1_556 ? OW4 OW5 Be4 127.6(5) 1_455 2_656 ? OW3 OW5 Be4 121.1(5) 1_556 2_656 ? Ca4 OW5 Be4 83.9(3) 1_455 2_656 ? O10 OW5 Be4 28.4(3) 2_656 2_656 ? O5 OW5 Be4 78.3(3) . 2_656 ? OW2 OW5 Be4 103.2(4) 1_556 2_656 ? OW4 OW5 Si2 143.5(5) 1_455 . ? OW3 OW5 Si2 139.2(4) 1_556 . ? Ca4 OW5 Si2 69.2(2) 1_455 . ? O10 OW5 Si2 79.2(3) 2_656 . ? O5 OW5 Si2 27.62(16) . . ? OW2 OW5 Si2 72.4(2) 1_556 . ? Be4 OW5 Si2 51.3(2) 2_656 . ? OW4 OW5 Si3 82.7(4) 1_455 2_656 ? OW3 OW5 Si3 93.3(4) 1_556 2_656 ? Ca4 OW5 Si3 90.9(3) 1_455 2_656 ? O10 OW5 Si3 21.71(16) 2_656 2_656 ? O5 OW5 Si3 124.2(4) . 2_656 ? OW2 OW5 Si3 136.9(3) 1_556 2_656 ? Be4 OW5 Si3 50.0(2) 2_656 2_656 ? Si2 OW5 Si3 100.0(3) . 2_656 ? OW4 OW5 Na1 33.5(3) 1_455 2_556 ? OW3 OW5 Na1 68.6(4) 1_556 2_556 ? Ca4 OW5 Na1 82.3(3) 1_455 2_556 ? O10 OW5 Na1 136.4(4) 2_656 2_556 ? O5 OW5 Na1 107.5(3) . 2_556 ? OW2 OW5 Na1 96.8(3) 1_556 2_556 ? Be4 OW5 Na1 159.7(3) 2_656 2_556 ? Si2 OW5 Na1 134.7(3) . 2_556 ? Si3 OW5 Na1 115.3(3) 2_656 2_556 ? OW4 OW5 Na1 120.0(4) 1_455 2_656 ? OW3 OW5 Na1 73.5(4) 1_556 2_656 ? Ca4 OW5 Na1 129.4(4) 1_455 2_656 ? O10 OW5 Na1 41.82(19) 2_656 2_656 ? O5 OW5 Na1 112.0(4) . 2_656 ? OW2 OW5 Na1 87.4(3) 1_556 2_656 ? Be4 OW5 Na1 47.6(2) 2_656 2_656 ? Si2 OW5 Na1 86.2(2) . 2_656 ? Si3 OW5 Na1 49.48(14) 2_656 2_656 ? Na1 OW5 Na1 138.2(3) 2_556 2_656 ? _diffrn_measured_fraction_theta_max 1.000 _diffrn_reflns_theta_full 22.53 _diffrn_measured_fraction_theta_full 1.000 _refine_diff_density_max 0.918 _refine_diff_density_min -0.684 _refine_diff_density_rms 0.162