data_shelxl _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'As1.80 Pb3.20 S34 Sb17.60, 3.4(Tl)' _chemical_formula_sum 'As1.80 Pb3.20 S34 Sb17.60 Tl3.40' _chemical_formula_weight 4726.14 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'As' 'As' -0.9300 1.0051 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pb' 'Pb' -4.0753 8.5060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Sb' 'Sb' -0.0562 5.8946 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Tl' 'Tl' -4.1627 8.0900 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting ? _symmetry_space_group_name_H-M P-1 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.150(2) _cell_length_b 8.716(2) _cell_length_c 21.579(4) _cell_angle_alpha 85.183(10) _cell_angle_beta 96.935(10) _cell_angle_gamma 88.595(10) _cell_volume 1515.4(6) _cell_formula_units_Z 1 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.20 _exptl_crystal_size_min 0.15 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 5.179 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 2038.8 _exptl_absorpt_coefficient_mu 35.456 _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 1.00000 _diffrn_radiation_type synchrotron _diffrn_radiation_source 'XRD1 beamline, Elettra, Trieste Italy' _diffrn_radiation_monochromator Si _diffrn_measurement_device_type 'Single axis rotation and Mar CCD plate' _diffrn_measurement_method 'integration of the spots (Denzo program)' _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 12478 _diffrn_reflns_av_R_equivalents 0.0443 _diffrn_reflns_av_sigmaI/netI 0.0309 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_theta_min 2.69 _diffrn_reflns_theta_max 32.18 _diffrn_special_details ; The resolution of the collected data is approximately 0.95 Å depending on the area of the detector. The data were collected by rotation around a spindle axis only (standard on some image-plate systems). ; _reflns_number_total 3401 _reflns_number_gt 3392 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction 'Scalepack (Otwinowski & Minor, 1997)' _computing_structure_solution 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0712P)^2^+31.1933P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens '' _refine_ls_hydrogen_treatment none _refine_ls_extinction_method SHELXL _refine_ls_extinction_coef 0.0090(3) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_number_reflns 3401 _refine_ls_number_parameters 276 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0438 _refine_ls_R_factor_gt 0.0437 _refine_ls_wR_factor_ref 0.1229 _refine_ls_wR_factor_gt 0.1228 _refine_ls_goodness_of_fit_ref 1.076 _refine_ls_restrained_S_all 1.076 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Tl1 Tl 0.46572(12) 0.59783(10) 0.18388(4) 0.0702(3) Uani 1 1 d . . . Tl2 Tl 0.45170(13) 0.09914(10) 0.18031(4) 0.0700(3) Uani 0.70 1 d P . . Pb2 Pb 0.45170(13) 0.09914(10) 0.18031(4) 0.0700(3) Uani 0.30 1 d P . . Pb Pb 0.01006(10) 0.09270(9) 0.27277(3) 0.0584(3) Uani 1 1 d . . . Sb1 Sb 0.03574(13) 0.77903(12) 0.47663(6) 0.0406(4) Uani 0.90 1 d P . . As1 As 0.03574(13) 0.77903(12) 0.47663(6) 0.0406(4) Uani 0.10 1 d P . . Sb2 Sb 0.30066(12) 0.48033(11) 0.43880(5) 0.0367(3) Uani 1 1 d . . . Sb3 Sb 0.63563(13) 0.77765(12) 0.37853(5) 0.0388(3) Uani 1 1 d . . . Sb4 Sb 0.68517(13) 0.10849(11) 0.02106(5) 0.0381(3) Uani 1 1 d . . . Sb5 Sb 0.34253(13) 0.05073(11) 0.42918(5) 0.0408(4) Uani 1 1 d . . . Sb6 Sb 0.66208(13) 0.30672(11) 0.36511(5) 0.0404(3) Uani 1 1 d . . . Sb7 Sb 0.01040(12) 0.36166(12) 0.11215(5) 0.0395(3) Uani 1 1 d . . . Sb8 Sb 0.9473(6) 0.5906(9) 0.2696(3) 0.0465(8) Uani 0.70 1 d P . . Pb8 Pb 0.9909(11) 0.5962(14) 0.2798(5) 0.0465(8) Uani 0.30 1 d P . . Sb9 Sb 0.02634(16) 0.86168(13) 0.12617(6) 0.0395(4) Uani 0.55 1 d P . . As9 As 0.02634(16) 0.86168(13) 0.12617(6) 0.0395(4) Uani 0.45 1 d P . . Sb10 Sb 0.29518(15) 0.37041(13) -0.00011(5) 0.0380(4) Uani 0.65 1 d P . . As10 As 0.29518(15) 0.37041(13) -0.00011(5) 0.0380(4) Uani 0.35 1 d P . . S1 S -0.1443(5) 0.5812(4) 0.42578(18) 0.0370(9) Uani 1 1 d . . . S2 S 0.1300(5) 0.2526(4) 0.39841(18) 0.0345(9) Uani 1 1 d . . . S3 S -0.1328(5) 0.6411(4) 0.15706(18) 0.0404(10) Uani 1 1 d . . . S4 S 0.1755(5) 0.8441(4) 0.38057(18) 0.0385(9) Uani 1 1 d . . . S5 S -0.1791(5) 0.9754(4) 0.4451(2) 0.0429(10) Uani 1 1 d . . . S6 S 0.5576(5) 0.3328(4) 0.06632(18) 0.0390(9) Uani 1 1 d . . . S7 S 0.4723(5) 0.1027(4) 0.32964(18) 0.0388(9) Uani 1 1 d . . . S8 S 0.7524(5) 0.3587(5) 0.25899(19) 0.0428(10) Uani 1 1 d . . . S9 S 0.1651(5) 0.1638(4) 0.0567(2) 0.0437(10) Uani 1 1 d . . . S10 S 0.4475(5) 0.5197(4) 0.34106(17) 0.0350(9) Uani 1 1 d . . . S11 S -0.1501(5) 0.0649(4) 0.15148(18) 0.0379(9) Uani 1 1 d . . . S12 S 0.1895(5) 0.5615(4) 0.06063(19) 0.0415(10) Uani 1 1 d . . . S13 S 0.5401(5) 0.8907(4) 0.07004(18) 0.0388(9) Uani 1 1 d . . . S14 S 0.5125(4) 0.3016(4) 0.49138(17) 0.0356(9) Uani 1 1 d . . . S15 S 0.7414(5) 0.8113(5) 0.27697(18) 0.0413(10) Uani 1 1 d . . . S16 S 0.1832(5) 0.3322(4) 0.21197(19) 0.0406(10) Uani 1 1 d . . . S17 S 0.2029(6) 0.8470(5) 0.2215(2) 0.0539(12) Uani 1 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Tl1 0.0778(7) 0.0684(6) 0.0625(6) -0.0098(4) 0.0008(5) 0.0114(5) Tl2 0.0904(7) 0.0647(6) 0.0601(6) -0.0156(4) 0.0213(5) -0.0112(5) Pb2 0.0904(7) 0.0647(6) 0.0601(6) -0.0156(4) 0.0213(5) -0.0112(5) Pb 0.0658(6) 0.0637(5) 0.0449(5) -0.0166(4) -0.0023(4) 0.0074(4) Sb1 0.0379(6) 0.0319(6) 0.0512(7) -0.0065(5) 0.0002(5) -0.0004(5) As1 0.0379(6) 0.0319(6) 0.0512(7) -0.0065(5) 0.0002(5) -0.0004(5) Sb2 0.0371(6) 0.0323(6) 0.0400(6) -0.0069(4) -0.0001(5) 0.0023(5) Sb3 0.0386(6) 0.0408(6) 0.0371(6) -0.0100(5) 0.0018(5) 0.0037(5) Sb4 0.0402(6) 0.0373(6) 0.0370(6) -0.0103(4) 0.0018(5) -0.0001(5) Sb5 0.0426(6) 0.0353(6) 0.0446(6) -0.0091(5) 0.0014(5) -0.0016(5) Sb6 0.0415(6) 0.0339(6) 0.0466(7) -0.0081(5) 0.0056(5) -0.0022(5) Sb7 0.0365(6) 0.0445(6) 0.0372(6) -0.0089(5) 0.0000(5) 0.0000(5) Sb8 0.045(3) 0.0560(9) 0.035(2) -0.0096(13) -0.0106(18) -0.004(2) Pb8 0.045(3) 0.0560(9) 0.035(2) -0.0096(13) -0.0106(18) -0.004(2) Sb9 0.0497(8) 0.0314(6) 0.0375(7) -0.0086(5) 0.0019(6) 0.0001(6) As9 0.0497(8) 0.0314(6) 0.0375(7) -0.0086(5) 0.0019(6) 0.0001(6) Sb10 0.0439(7) 0.0356(6) 0.0349(7) -0.0093(5) 0.0022(6) 0.0000(5) As10 0.0439(7) 0.0356(6) 0.0349(7) -0.0093(5) 0.0022(6) 0.0000(5) S1 0.035(2) 0.0309(18) 0.044(2) -0.0079(16) -0.0039(18) -0.0013(16) S2 0.036(2) 0.0294(18) 0.038(2) -0.0087(16) -0.0001(17) -0.0030(16) S3 0.050(2) 0.0349(19) 0.035(2) -0.0090(16) -0.0020(19) 0.0038(18) S4 0.043(2) 0.037(2) 0.034(2) -0.0061(16) -0.0028(18) -0.0012(17) S5 0.040(2) 0.0287(19) 0.057(3) -0.0080(18) -0.008(2) 0.0006(17) S6 0.042(2) 0.038(2) 0.037(2) -0.0121(17) 0.0006(18) 0.0014(17) S7 0.043(2) 0.035(2) 0.039(2) -0.0097(17) 0.0033(18) -0.0021(17) S8 0.043(2) 0.042(2) 0.043(2) -0.0062(18) 0.0051(19) 0.0032(18) S9 0.047(2) 0.034(2) 0.053(2) -0.0131(18) 0.010(2) -0.0006(18) S10 0.039(2) 0.0329(18) 0.0332(19) -0.0060(15) 0.0013(17) -0.0017(16) S11 0.040(2) 0.040(2) 0.034(2) -0.0088(16) -0.0019(18) -0.0033(17) S12 0.049(2) 0.0349(19) 0.042(2) -0.0088(17) 0.0058(19) -0.0031(18) S13 0.047(2) 0.0363(19) 0.033(2) -0.0062(16) -0.0014(18) -0.0016(17) S14 0.036(2) 0.0317(18) 0.039(2) -0.0085(16) -0.0019(18) 0.0008(16) S15 0.044(2) 0.044(2) 0.035(2) -0.0075(17) 0.0019(18) 0.0069(18) S16 0.042(2) 0.040(2) 0.038(2) -0.0080(17) -0.0047(19) -0.0006(18) S17 0.053(3) 0.053(2) 0.053(3) -0.020(2) -0.010(2) 0.014(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Tl1 S17 3.234(4) . ? Tl1 S8 3.273(4) . ? Tl1 S12 3.312(4) . ? Tl1 S16 3.375(4) . ? Tl1 S3 3.415(5) 1_655 ? Tl1 S10 3.425(4) . ? Tl1 S15 3.506(4) . ? Tl1 S13 3.507(4) . ? Tl1 S6 3.700(4) . ? Tl1 S3 4.844(4) . ? Tl1 S7 5.117(4) . ? Tl1 S11 5.248(4) 1_665 ? Tl2 S16 3.124(4) . ? Tl2 S17 3.172(5) 1_545 ? Tl2 S7 3.209(4) . ? Tl2 S13 3.249(4) 1_545 ? Tl2 S6 3.271(4) . ? Tl2 S9 3.327(4) . ? Tl2 S11 3.388(4) 1_655 ? Tl2 S15 3.723(4) 1_545 ? Tl2 S8 3.731(4) . ? Tl2 S11 4.888(4) . ? Tl2 S12 4.896(4) . ? Tl2 S10 5.256(4) . ? Pb S11 2.812(4) . ? Pb S16 2.864(4) . ? Pb S17 2.988(4) 1_545 ? Pb S8 3.061(4) 1_455 ? Pb S4 3.190(4) 1_545 ? Pb S2 3.211(4) . ? Pb S15 3.330(5) 1_445 ? Pb S7 3.824(4) . ? Pb S5 4.250(5) 1_545 ? Pb S7 4.692(4) 1_455 ? Pb S3 4.925(4) 1_545 ? Pb S9 4.970(5) . ? Sb1 S5 2.414(4) . ? Sb1 S4 2.514(4) . ? Sb1 S1 2.526(4) . ? Sb1 S5 3.009(4) 2_576 ? Sb1 S2 3.153(4) 2_566 ? Sb1 S1 3.658(4) 2_566 ? Sb1 S14 3.702(4) 2_666 ? Sb1 S2 4.447(4) 1_565 ? Sb1 S15 4.654(4) 1_455 ? Sb1 S14 4.664(4) 2_566 ? Sb1 S2 5.092(4) . ? Sb1 S4 5.094(4) 2_576 ? Sb2 S14 2.407(4) . ? Sb2 S10 2.551(4) . ? Sb2 S2 2.601(4) . ? Sb2 S14 2.876(4) 2_666 ? Sb2 S1 3.335(4) 2_566 ? Sb2 S4 3.397(4) . ? Sb2 S1 3.682(4) . ? Sb2 S7 4.496(4) . ? Sb2 S1 4.667(4) 1_655 ? Sb2 S5 4.708(4) 2_566 ? Sb2 S10 4.942(4) 2_666 ? Sb2 S16 5.151(4) . ? Sb3 S15 2.448(4) . ? Sb3 S1 2.511(4) 1_655 ? Sb3 S5 2.708(4) 1_655 ? Sb3 S10 2.870(4) . ? Sb3 S7 3.144(4) 1_565 ? Sb3 S14 3.217(4) 2_666 ? Sb3 S4 3.787(4) . ? Sb3 S4 4.448(4) 1_655 ? Sb3 S17 4.577(4) . ? Sb3 S8 4.785(4) . ? Sb3 S14 4.822(4) . ? Sb3 S2 4.943(4) 2_666 ? Sb4 S13 2.488(4) 1_545 ? Sb4 S6 2.515(4) . ? Sb4 S13 2.522(4) 2_665 ? Sb4 S11 2.958(4) 1_655 ? Sb4 S9 3.310(4) 2_655 ? Sb4 S12 3.486(4) 2_665 ? Sb4 S9 3.944(4) 1_655 ? Sb4 S9 4.420(4) . ? Sb4 S6 4.791(4) 2_655 ? Sb4 S3 4.904(4) 1_645 ? Sb4 S6 5.317(4) 2_665 ? Sb4 S17 5.406(5) 2_665 ? Sb5 S2 2.432(4) . ? Sb5 S4 2.508(4) 1_545 ? Sb5 S7 2.519(4) . ? Sb5 S14 2.948(4) . ? Sb5 S5 3.158(5) 2_566 ? Sb5 S14 3.495(4) 2_656 ? Sb5 S5 3.907(4) 1_645 ? Sb5 S5 4.367(5) 1_545 ? Sb5 S10 4.507(4) . ? Sb5 S17 4.973(4) 1_545 ? Sb5 S1 5.035(4) 2_566 ? Sb5 S16 5.111(4) . ? Sb6 S7 2.493(4) . ? Sb6 S10 2.496(4) . ? Sb6 S8 2.498(5) . ? Sb6 S14 3.114(4) . ? Sb6 S1 3.184(4) 1_655 ? Sb6 S5 3.381(4) 1_645 ? Sb6 S2 3.804(4) 1_655 ? Sb6 S2 4.510(4) . ? Sb6 S15 4.734(5) . ? Sb6 S16 4.788(4) . ? Sb6 S15 4.921(4) 1_545 ? Sb6 S14 5.086(4) 2_666 ? Sb7 S16 2.418(4) . ? Sb7 S12 2.567(5) . ? Sb7 S9 2.569(4) . ? Sb7 S3 2.961(4) . ? Sb7 S11 3.031(4) . ? Sb7 S6 3.724(4) 1_455 ? Sb7 S12 3.881(4) 2_565 ? Sb7 S8 4.008(4) 1_455 ? Sb7 S6 4.688(4) . ? Sb7 S17 5.014(5) 1_545 ? Sb7 S17 5.200(4) . ? Sb7 S9 5.324(4) 2_565 ? Sb8 S3 2.437(8) 1_655 ? Sb8 S15 2.549(8) . ? Sb8 S8 2.610(8) . ? Sb8 S17 3.281(9) 1_655 ? Sb8 S16 3.339(9) 1_655 ? Sb8 S1 3.534(9) 1_655 ? Sb8 S4 3.754(6) 1_655 ? Sb8 S2 4.005(8) 1_655 ? Sb8 S10 4.193(6) 1_655 ? Sb8 S10 4.565(8) . ? Sb8 S11 4.668(9) 1_665 ? Sb8 S12 5.158(9) 1_655 ? Pb8 S3 2.710(10) 1_655 ? Pb8 S15 2.723(12) . ? Pb8 S8 2.900(11) . ? Pb8 S17 3.097(14) 1_655 ? Pb8 S16 3.292(13) 1_655 ? Pb8 S4 3.438(10) 1_655 ? Pb8 S1 3.454(13) 1_655 ? Pb8 S10 3.819(8) 1_655 ? Pb8 S2 3.828(13) 1_655 ? Pb8 S11 4.772(13) 1_665 ? Pb8 S10 4.818(12) . ? Pb8 S12 5.210(13) 1_655 ? Sb9 S17 2.357(4) . ? Sb9 S11 2.394(4) 1_565 ? Sb9 S3 2.437(5) . ? Sb9 S9 3.218(5) 1_565 ? Sb9 S12 3.394(4) . ? Sb9 S13 3.997(4) 1_455 ? Sb9 S9 4.090(4) 2_565 ? Sb9 S15 4.220(5) 1_455 ? Sb9 S13 4.505(5) . ? Sb9 S16 4.780(4) 1_565 ? Sb9 S16 4.905(4) . ? Sb9 S4 5.466(4) . ? Sb10 S12 2.409(4) . ? Sb10 S6 2.425(4) . ? Sb10 S9 2.430(5) . ? Sb10 S6 3.181(4) 2_665 ? Sb10 S13 3.190(4) 2_665 ? Sb10 S3 3.495(4) 2_565 ? Sb10 S12 4.021(4) 2_565 ? Sb10 S12 4.584(5) 2_665 ? Sb10 S13 4.643(4) 1_545 ? Sb10 S16 4.760(4) . ? Sb10 S13 5.264(4) . ? Sb10 S11 5.276(4) 2 ? S1 Sb3 2.511(4) 1_455 ? S1 Sb6 3.184(4) 1_455 ? S1 Sb2 3.335(4) 2_566 ? S1 Pb8 3.454(13) 1_455 ? S1 S5 3.504(5) . ? S1 Sb8 3.534(9) 1_455 ? S1 S15 3.648(6) 1_455 ? S1 As1 3.658(4) 2_566 ? S1 Sb1 3.658(4) 2_566 ? S1 S10 3.672(5) 1_455 ? S2 As1 3.153(4) 2_566 ? S2 Sb1 3.153(4) 2_566 ? S2 S14 3.553(5) . ? S2 S7 3.584(6) . ? S2 S4 3.628(5) 1_545 ? S2 S5 3.701(6) 1_545 ? S2 S5 3.745(6) 2_566 ? S2 S10 3.772(6) . ? S3 Sb8 2.437(8) 1_455 ? S3 Pb8 2.710(10) 1_455 ? S3 S15 3.340(5) 1_455 ? S3 S8 3.387(6) 1_455 ? S3 Tl1 3.415(5) 1_455 ? S3 As10 3.495(4) 2_565 ? S3 Sb10 3.495(4) 2_565 ? S3 S17 3.519(6) . ? S3 S13 3.631(5) 1_455 ? S4 Sb5 2.508(4) 1_565 ? S4 Pb 3.190(4) 1_565 ? S4 Pb8 3.438(10) 1_455 ? S4 S17 3.464(6) . ? S4 S7 3.554(6) 1_565 ? S4 S5 3.560(6) . ? S4 S2 3.628(5) 1_565 ? S4 S14 3.643(5) 2_666 ? S5 Sb3 2.708(4) 1_455 ? S5 As1 3.009(4) 2_576 ? S5 Sb1 3.009(4) 2_576 ? S5 Sb5 3.158(5) 2_566 ? S5 Sb6 3.381(4) 1_465 ? S5 S5 3.591(7) 2_576 ? S5 S7 3.630(5) 1_465 ? S5 S2 3.701(6) 1_565 ? S6 As10 3.181(4) 2_665 ? S6 Sb10 3.181(4) 2_665 ? S6 S11 3.529(5) 1_655 ? S6 S12 3.545(5) . ? S6 S9 3.545(6) . ? S6 S13 3.683(5) 2_665 ? S6 S12 3.693(6) 2_665 ? S7 Sb3 3.144(4) 1_545 ? S7 S4 3.554(6) 1_545 ? S7 S8 3.610(6) . ? S7 S5 3.630(5) 1_645 ? S7 S15 3.656(5) 1_545 ? S7 S10 3.665(5) . ? S7 S16 3.671(5) . ? S8 Pb 3.061(4) 1_655 ? S8 S3 3.387(6) 1_655 ? S8 S10 3.548(6) . ? S8 S11 3.730(5) 1_655 ? S8 S16 3.777(6) 1_655 ? S9 As9 3.218(5) 1_545 ? S9 Sb9 3.218(5) 1_545 ? S9 Sb4 3.310(4) 2_655 ? S9 S12 3.484(6) . ? S9 S11 3.550(6) . ? S9 S16 3.758(6) . ? S10 S14 3.594(5) . ? S10 S1 3.672(5) 1_655 ? S10 S16 3.815(5) . ? S10 Pb8 3.819(8) 1_455 ? S11 As9 2.394(4) 1_545 ? S11 Sb9 2.394(4) 1_545 ? S11 Sb4 2.958(4) 1_455 ? S11 S13 3.367(5) 1_445 ? S11 Pb2 3.388(4) 1_455 ? S11 Tl2 3.388(4) 1_455 ? S11 S17 3.517(5) 1_545 ? S11 S6 3.529(5) 1_455 ? S11 S15 3.560(6) 1_445 ? S12 Sb4 3.486(4) 2_665 ? S12 S16 3.689(6) . ? S12 S6 3.693(6) 2_665 ? S13 Sb4 2.488(4) 1_565 ? S13 Sb4 2.522(4) 2_665 ? S13 As10 3.190(4) 2_665 ? S13 Sb10 3.190(4) 2_665 ? S13 Pb2 3.249(4) 1_565 ? S13 Tl2 3.249(4) 1_565 ? S13 S11 3.367(5) 1_665 ? S13 S13 3.419(8) 2_675 ? S13 S3 3.631(5) 1_655 ? S13 S6 3.683(5) 2_665 ? S13 S9 3.796(5) 1_565 ? S14 Sb2 2.876(4) 2_666 ? S14 Sb3 3.217(4) 2_666 ? S14 Sb5 3.495(4) 2_656 ? S14 S14 3.513(7) 2_666 ? S14 S4 3.643(5) 2_666 ? S14 As1 3.702(4) 2_666 ? S14 Sb1 3.702(4) 2_666 ? S15 Pb 3.330(5) 1_665 ? S15 S3 3.340(5) 1_655 ? S15 S11 3.560(6) 1_665 ? S15 S1 3.648(6) 1_655 ? S15 S7 3.656(5) 1_565 ? S15 Pb2 3.723(4) 1_565 ? S15 Tl2 3.723(4) 1_565 ? S16 Pb8 3.292(13) 1_455 ? S16 Sb8 3.339(9) 1_455 ? S16 S8 3.777(6) 1_455 ? S17 Pb 2.988(4) 1_565 ? S17 Pb8 3.097(14) 1_455 ? S17 Pb2 3.172(5) 1_565 ? S17 Tl2 3.172(5) 1_565 ? S17 Sb8 3.281(9) 1_455 ? S17 S11 3.517(5) 1_565 ? S17 S7 3.887(6) 1_565 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag S17 Tl1 S8 136.20(11) . . ? S17 Tl1 S12 85.20(10) . . ? S8 Tl1 S12 131.62(10) . . ? S17 Tl1 S16 86.15(12) . . ? S8 Tl1 S16 88.59(10) . . ? S12 Tl1 S16 66.95(10) . . ? S17 Tl1 S3 129.71(11) . 1_655 ? S8 Tl1 S3 60.82(10) . 1_655 ? S12 Tl1 S3 117.19(10) . 1_655 ? S16 Tl1 S3 143.24(9) . 1_655 ? S17 Tl1 S10 73.81(10) . . ? S8 Tl1 S10 63.93(10) . . ? S12 Tl1 S10 131.35(11) . . ? S16 Tl1 S10 68.25(9) . . ? S3 Tl1 S10 109.85(9) 1_655 . ? S17 Tl1 S15 81.50(10) . . ? S8 Tl1 S15 72.16(10) . . ? S12 Tl1 S15 152.63(10) . . ? S16 Tl1 S15 135.22(10) . . ? S3 Tl1 S15 57.70(9) 1_655 . ? S10 Tl1 S15 66.96(9) . . ? S17 Tl1 S13 84.03(12) . . ? S8 Tl1 S13 124.00(11) . . ? S12 Tl1 S13 73.83(10) . . ? S16 Tl1 S13 140.19(9) . . ? S3 Tl1 S13 63.26(9) 1_655 . ? S10 Tl1 S13 143.10(9) . . ? S15 Tl1 S13 81.05(9) . . ? S17 Tl1 S6 145.60(10) . . ? S8 Tl1 S6 75.75(9) . . ? S12 Tl1 S6 60.43(9) . . ? S16 Tl1 S6 81.76(10) . . ? S3 Tl1 S6 71.77(9) 1_655 . ? S10 Tl1 S6 129.21(9) . . ? S15 Tl1 S6 128.56(9) . . ? S13 Tl1 S6 84.95(9) . . ? S17 Tl1 S3 46.57(9) . . ? S8 Tl1 S3 136.92(10) . . ? S12 Tl1 S3 48.53(9) . . ? S16 Tl1 S3 49.62(8) . . ? S3 Tl1 S3 161.06(11) 1_655 . ? S10 Tl1 S3 87.54(8) . . ? S15 Tl1 S3 127.38(8) . . ? S13 Tl1 S3 98.39(8) . . ? S6 Tl1 S3 103.49(8) . . ? S17 Tl1 S7 109.84(11) . . ? S8 Tl1 S7 44.55(9) . . ? S12 Tl1 S7 107.62(9) . . ? S16 Tl1 S7 45.75(8) . . ? S3 Tl1 S7 105.08(8) 1_655 . ? S10 Tl1 S7 45.70(7) . . ? S15 Tl1 S7 99.39(8) . . ? S13 Tl1 S7 166.08(8) . . ? S6 Tl1 S7 83.97(8) . . ? S3 Tl1 S7 92.38(7) . . ? S17 Tl1 S11 86.01(10) . 1_665 ? S8 Tl1 S11 96.58(9) . 1_665 ? S12 Tl1 S11 113.04(9) . 1_665 ? S16 Tl1 S11 172.13(8) . 1_665 ? S3 Tl1 S11 44.35(8) 1_655 1_665 ? S10 Tl1 S11 108.73(8) . 1_665 ? S15 Tl1 S11 42.42(8) . 1_665 ? S13 Tl1 S11 39.24(7) . 1_665 ? S6 Tl1 S11 105.22(8) . 1_665 ? S3 Tl1 S11 123.97(6) . 1_665 ? S7 Tl1 S11 137.43(6) . 1_665 ? S16 Tl2 S17 84.05(11) . 1_545 ? S16 Tl2 S7 70.83(10) . . ? S17 Tl2 S7 75.05(11) 1_545 . ? S16 Tl2 S13 141.63(10) . 1_545 ? S17 Tl2 S13 89.40(11) 1_545 1_545 ? S7 Tl2 S13 143.11(10) . 1_545 ? S16 Tl2 S6 92.93(11) . . ? S17 Tl2 S6 146.49(10) 1_545 . ? S7 Tl2 S6 135.21(10) . . ? S13 Tl2 S6 72.46(10) 1_545 . ? S16 Tl2 S9 71.18(10) . . ? S17 Tl2 S9 82.63(11) 1_545 . ? S7 Tl2 S9 137.43(11) . . ? S13 Tl2 S9 70.50(9) 1_545 . ? S6 Tl2 S9 64.99(10) . . ? S16 Tl2 S11 143.52(10) . 1_655 ? S17 Tl2 S11 130.99(10) 1_545 1_655 ? S7 Tl2 S11 104.91(10) . 1_655 ? S13 Tl2 S11 60.91(9) 1_545 1_655 ? S6 Tl2 S11 63.98(10) . 1_655 ? S9 Tl2 S11 117.02(10) . 1_655 ? S16 Tl2 S15 133.58(10) . 1_545 ? S17 Tl2 S15 78.95(10) 1_545 1_545 ? S7 Tl2 S15 63.14(9) . 1_545 ? S13 Tl2 S15 81.32(9) 1_545 1_545 ? S6 Tl2 S15 123.83(10) . 1_545 ? S9 Tl2 S15 146.33(9) . 1_545 ? S11 Tl2 S15 59.85(10) 1_655 1_545 ? S16 Tl2 S8 84.79(9) . . ? S17 Tl2 S8 137.09(11) 1_545 . ? S7 Tl2 S8 62.15(10) . . ? S13 Tl2 S8 123.03(10) 1_545 . ? S6 Tl2 S8 75.34(9) . . ? S9 Tl2 S8 131.55(10) . . ? S11 Tl2 S8 62.98(9) 1_655 . ? S15 Tl2 S8 79.33(9) 1_545 . ? S16 Tl2 S11 51.09(8) . . ? S17 Tl2 S11 45.88(9) 1_545 . ? S7 Tl2 S11 93.67(9) . . ? S13 Tl2 S11 99.06(8) 1_545 . ? S6 Tl2 S11 108.21(8) . . ? S9 Tl2 S11 46.58(9) . . ? S11 Tl2 S11 159.59(10) 1_655 . ? S15 Tl2 S11 124.67(9) 1_545 . ? S8 Tl2 S11 135.52(8) . . ? S16 Tl2 S12 48.87(9) . . ? S17 Tl2 S12 114.87(9) 1_545 . ? S7 Tl2 S12 114.73(8) . . ? S13 Tl2 S12 102.16(8) 1_545 . ? S6 Tl2 S12 46.35(8) . . ? S9 Tl2 S12 45.33(8) . . ? S11 Tl2 S12 109.33(9) 1_655 . ? S15 Tl2 S12 165.56(9) 1_545 . ? S8 Tl2 S12 87.16(8) . . ? S11 Tl2 S12 68.99(7) . . ? S16 Tl2 S10 45.96(8) . . ? S17 Tl2 S10 105.99(9) 1_545 . ? S7 Tl2 S10 43.45(8) . . ? S13 Tl2 S10 164.34(9) 1_545 . ? S6 Tl2 S10 95.20(8) . . ? S9 Tl2 S10 113.62(8) . . ? S11 Tl2 S10 105.34(8) 1_655 . ? S15 Tl2 S10 98.51(7) 1_545 . ? S8 Tl2 S10 42.41(8) . . ? S11 Tl2 S10 93.90(6) . . ? S12 Tl2 S10 74.32(6) . . ? S11 Pb S16 84.16(11) . . ? S11 Pb S17 74.57(11) . 1_545 ? S16 Pb S17 92.13(13) . 1_545 ? S11 Pb S8 78.73(11) . 1_455 ? S16 Pb S8 79.14(12) . 1_455 ? S17 Pb S8 152.63(11) 1_545 1_455 ? S11 Pb S4 132.33(10) . 1_545 ? S16 Pb S4 124.81(11) . 1_545 ? S17 Pb S4 68.11(11) 1_545 1_545 ? S8 Pb S4 137.62(11) 1_455 1_545 ? S11 Pb S2 158.21(10) . . ? S16 Pb S2 84.73(11) . . ? S17 Pb S2 124.57(10) 1_545 . ? S8 Pb S2 80.80(10) 1_455 . ? S4 Pb S2 69.05(9) 1_545 . ? S11 Pb S15 70.25(11) . 1_445 ? S16 Pb S15 154.40(10) . 1_445 ? S17 Pb S15 80.56(12) 1_545 1_445 ? S8 Pb S15 96.14(11) 1_455 1_445 ? S4 Pb S15 75.21(10) 1_545 1_445 ? S2 Pb S15 119.63(10) . 1_445 ? S11 Pb S7 129.46(11) . . ? S16 Pb S7 64.72(10) . . ? S17 Pb S7 68.31(10) 1_545 . ? S8 Pb S7 127.85(10) 1_455 . ? S4 Pb S7 60.08(10) 1_545 . ? S2 Pb S7 60.50(9) . . ? S15 Pb S7 132.18(9) 1_445 . ? S11 Pb S5 126.93(10) . 1_545 ? S16 Pb S5 140.66(9) . 1_545 ? S17 Pb S5 117.10(11) 1_545 1_545 ? S8 Pb S5 83.98(10) 1_455 1_545 ? S4 Pb S5 54.97(9) 1_545 1_545 ? S2 Pb S5 57.47(9) . 1_545 ? S15 Pb S5 62.24(9) 1_445 1_545 ? S7 Pb S5 100.54(8) . 1_545 ? S11 Pb S7 84.46(10) . 1_455 ? S16 Pb S7 129.40(9) . 1_455 ? S17 Pb S7 131.24(11) 1_545 1_455 ? S8 Pb S7 50.28(10) 1_455 1_455 ? S4 Pb S7 98.39(9) 1_545 1_455 ? S2 Pb S7 88.21(8) . 1_455 ? S15 Pb S7 50.82(8) 1_445 1_455 ? S7 Pb S7 146.07(10) . 1_455 ? S5 Pb S7 47.58(7) 1_545 1_455 ? S11 Pb S3 47.85(9) . 1_545 ? S16 Pb S3 117.64(9) . 1_545 ? S17 Pb S3 45.03(10) 1_545 1_545 ? S8 Pb S3 117.08(9) 1_455 1_545 ? S4 Pb S3 84.52(8) 1_545 1_545 ? S2 Pb S3 152.60(8) . 1_545 ? S15 Pb S3 42.49(9) 1_445 1_545 ? S7 Pb S3 112.73(7) . 1_545 ? S5 Pb S3 101.69(7) 1_545 1_545 ? S7 Pb S3 88.65(7) 1_455 1_545 ? S11 Pb S9 44.31(10) . . ? S16 Pb S9 48.72(9) . . ? S17 Pb S9 59.20(11) 1_545 . ? S8 Pb S9 96.99(9) 1_455 . ? S4 Pb S9 125.29(9) 1_545 . ? S2 Pb S9 132.37(9) . . ? S15 Pb S9 107.95(8) 1_445 . ? S7 Pb S9 86.63(8) . . ? S5 Pb S9 170.16(7) 1_545 . ? S7 Pb S9 126.57(7) 1_455 . ? S3 Pb S9 69.11(7) 1_545 . ? S5 Sb1 S4 92.48(15) . . ? S5 Sb1 S1 90.32(13) . . ? S4 Sb1 S1 93.72(13) . . ? S5 Sb1 S5 82.12(12) . 2_576 ? S4 Sb1 S5 98.46(13) . 2_576 ? S1 Sb1 S5 165.90(13) . 2_576 ? S5 Sb1 S2 83.41(13) . 2_566 ? S4 Sb1 S2 171.61(11) . 2_566 ? S1 Sb1 S2 93.61(12) . 2_566 ? S5 Sb1 S2 73.78(11) 2_576 2_566 ? S5 Sb1 S1 144.45(13) . 2_566 ? S4 Sb1 S1 120.28(11) . 2_566 ? S1 Sb1 S1 75.23(11) . 2_566 ? S5 Sb1 S1 104.28(10) 2_576 2_566 ? S2 Sb1 S1 65.72(9) 2_566 2_566 ? S5 Sb1 S14 145.29(12) . 2_666 ? S4 Sb1 S14 68.72(11) . 2_666 ? S1 Sb1 S14 118.78(10) . 2_666 ? S5 Sb1 S14 72.69(10) 2_576 2_666 ? S2 Sb1 S14 110.98(9) 2_566 2_666 ? S1 Sb1 S14 66.95(9) 2_566 2_666 ? S5 Sb1 S2 56.33(11) . 1_565 ? S4 Sb1 S2 54.65(10) . 1_565 ? S1 Sb1 S2 127.94(10) . 1_565 ? S5 Sb1 S2 56.42(10) 2_576 1_565 ? S2 Sb1 S2 117.25(7) 2_566 1_565 ? S1 Sb1 S2 154.20(8) 2_566 1_565 ? S14 Sb1 S2 89.49(8) 2_666 1_565 ? S5 Sb1 S15 59.16(11) . 1_455 ? S4 Sb1 S15 58.75(10) . 1_455 ? S1 Sb1 S15 51.19(10) . 1_455 ? S5 Sb1 S15 131.26(9) 2_576 1_455 ? S2 Sb1 S15 124.00(9) 2_566 1_455 ? S1 Sb1 S15 124.46(8) 2_566 1_455 ? S14 Sb1 S15 123.67(8) 2_666 1_455 ? S2 Sb1 S15 76.79(7) 1_565 1_455 ? S5 Sb1 S14 58.34(12) . 2_566 ? S4 Sb1 S14 133.42(10) . 2_566 ? S1 Sb1 S14 55.24(10) . 2_566 ? S5 Sb1 S14 110.76(10) 2_576 2_566 ? S2 Sb1 S14 49.58(8) 2_566 2_566 ? S1 Sb1 S14 87.33(8) 2_566 2_566 ? S14 Sb1 S14 153.73(11) 2_666 2_566 ? S2 Sb1 S14 114.49(7) 1_565 2_566 ? S15 Sb1 S14 74.77(7) 1_455 2_566 ? S5 Sb1 S2 131.17(10) . . ? S4 Sb1 S2 77.39(10) . . ? S1 Sb1 S2 44.09(9) . . ? S5 Sb1 S2 146.23(8) 2_576 . ? S2 Sb1 S2 110.80(7) 2_566 . ? S1 Sb1 S2 53.84(7) 2_566 . ? S14 Sb1 S2 74.69(7) 2_666 . ? S2 Sb1 S2 131.93(9) 1_565 . ? S15 Sb1 S2 75.48(6) 1_455 . ? S14 Sb1 S2 94.89(6) 2_566 . ? S5 Sb1 S4 54.81(11) . 2_576 ? S4 Sb1 S4 126.94(8) . 2_576 ? S1 Sb1 S4 122.93(10) . 2_576 ? S5 Sb1 S4 43.25(10) 2_576 2_576 ? S2 Sb1 S4 44.96(8) 2_566 2_576 ? S1 Sb1 S4 106.41(8) 2_566 2_576 ? S14 Sb1 S4 113.14(7) 2_666 2_576 ? S2 Sb1 S4 72.30(7) 1_565 2_576 ? S15 Sb1 S4 113.74(6) 1_455 2_576 ? S14 Sb1 S4 67.75(6) 2_566 2_576 ? S2 Sb1 S4 155.61(7) . 2_576 ? S14 Sb2 S10 92.88(13) . . ? S14 Sb2 S2 90.29(12) . . ? S10 Sb2 S2 94.14(12) . . ? S14 Sb2 S14 82.85(12) . 2_666 ? S10 Sb2 S14 95.93(12) . 2_666 ? S2 Sb2 S14 168.07(13) . 2_666 ? S14 Sb2 S1 82.06(12) . 2_566 ? S10 Sb2 S1 174.46(10) . 2_566 ? S2 Sb2 S1 88.15(11) . 2_566 ? S14 Sb2 S1 81.27(10) 2_666 2_566 ? S14 Sb2 S4 150.08(12) . . ? S10 Sb2 S4 77.16(11) . . ? S2 Sb2 S4 118.23(11) . . ? S14 Sb2 S4 70.45(10) 2_666 . ? S1 Sb2 S4 106.18(9) 2_566 . ? S14 Sb2 S1 143.20(13) . . ? S10 Sb2 S1 118.61(11) . . ? S2 Sb2 S1 70.20(10) . . ? S14 Sb2 S1 110.07(9) 2_666 . ? S1 Sb2 S1 66.91(10) 2_566 . ? S4 Sb2 S1 62.46(9) . . ? S14 Sb2 S7 62.65(10) . . ? S10 Sb2 S7 54.61(10) . . ? S2 Sb2 S7 52.82(10) . . ? S14 Sb2 S7 130.20(9) 2_666 . ? S1 Sb2 S7 123.96(8) 2_566 . ? S4 Sb2 S7 126.44(9) . . ? S1 Sb2 S7 119.15(8) . . ? S14 Sb2 S1 60.42(11) . 1_655 ? S10 Sb2 S1 51.56(9) . 1_655 ? S2 Sb2 S1 128.95(10) . 1_655 ? S14 Sb2 S1 55.11(9) 2_666 1_655 ? S1 Sb2 S1 123.35(6) 2_566 1_655 ? S4 Sb2 S1 92.39(9) . 1_655 ? S1 Sb2 S1 154.78(10) . 1_655 ? S7 Sb2 S1 76.21(7) . 1_655 ? S14 Sb2 S5 57.43(11) . 2_566 ? S10 Sb2 S5 130.49(10) . 2_566 ? S2 Sb2 S5 52.52(10) . 2_566 ? S14 Sb2 S5 115.65(10) 2_666 2_566 ? S1 Sb2 S5 48.02(8) 2_566 2_566 ? S4 Sb2 S5 147.38(9) . 2_566 ? S1 Sb2 S5 86.46(8) . 2_566 ? S7 Sb2 S5 76.01(8) . 2_566 ? S1 Sb2 S5 117.85(7) 1_655 2_566 ? S14 Sb2 S10 54.18(9) . 2_666 ? S10 Sb2 S10 126.92(7) . 2_666 ? S2 Sb2 S10 122.32(10) . 2_666 ? S14 Sb2 S10 45.90(9) 2_666 2_666 ? S1 Sb2 S10 47.99(8) 2_566 2_666 ? S4 Sb2 S10 110.00(8) . 2_666 ? S1 Sb2 S10 110.03(8) . 2_666 ? S7 Sb2 S10 116.79(7) . 2_666 ? S1 Sb2 S10 75.38(7) 1_655 2_666 ? S5 Sb2 S10 69.80(7) 2_566 2_666 ? S14 Sb2 S16 106.62(10) . . ? S10 Sb2 S16 45.31(10) . . ? S2 Sb2 S16 52.06(10) . . ? S14 Sb2 S16 139.41(10) 2_666 . ? S1 Sb2 S16 138.42(8) 2_566 . ? S4 Sb2 S16 86.47(8) . . ? S1 Sb2 S16 86.07(8) . . ? S7 Sb2 S16 44.09(6) . . ? S1 Sb2 S16 94.64(7) 1_655 . ? S5 Sb2 S16 101.91(7) 2_566 . ? S10 Sb2 S16 160.77(6) 2_666 . ? S15 Sb3 S1 94.71(13) . 1_655 ? S15 Sb3 S5 101.51(15) . 1_655 ? S1 Sb3 S5 84.28(12) 1_655 1_655 ? S15 Sb3 S10 91.60(13) . . ? S1 Sb3 S10 85.79(11) 1_655 . ? S5 Sb3 S10 164.14(13) 1_655 . ? S15 Sb3 S7 80.60(12) . 1_565 ? S1 Sb3 S7 158.54(12) 1_655 1_565 ? S5 Sb3 S7 76.27(11) 1_655 1_565 ? S10 Sb3 S7 115.11(11) . 1_565 ? S15 Sb3 S14 174.16(12) . 2_666 ? S1 Sb3 S14 83.04(12) 1_655 2_666 ? S5 Sb3 S14 83.66(12) 1_655 2_666 ? S10 Sb3 S14 82.88(11) . 2_666 ? S7 Sb3 S14 103.42(10) 1_565 2_666 ? S15 Sb3 S4 117.48(11) . . ? S1 Sb3 S4 137.38(12) 1_655 . ? S5 Sb3 S4 113.08(11) 1_655 . ? S10 Sb3 S4 67.32(10) . . ? S7 Sb3 S4 60.87(10) 1_565 . ? S14 Sb3 S4 62.06(9) 2_666 . ? S15 Sb3 S4 62.87(11) . 1_655 ? S1 Sb3 S4 55.79(11) 1_655 1_655 ? S5 Sb3 S4 53.17(11) 1_655 1_655 ? S10 Sb3 S4 128.58(9) . 1_655 ? S7 Sb3 S4 104.27(10) 1_565 1_655 ? S14 Sb3 S4 119.43(8) 2_666 1_655 ? S4 Sb3 S4 163.56(11) . 1_655 ? S15 Sb3 S17 70.32(12) . . ? S1 Sb3 S17 141.04(10) 1_655 . ? S5 Sb3 S17 133.06(10) 1_655 . ? S10 Sb3 S17 59.91(9) . . ? S7 Sb3 S17 56.88(9) 1_565 . ? S14 Sb3 S17 108.16(9) 2_666 . ? S4 Sb3 S17 47.79(8) . . ? S4 Sb3 S17 132.10(9) 1_655 . ? S15 Sb3 S8 56.53(11) . . ? S1 Sb3 S8 62.06(10) 1_655 . ? S5 Sb3 S8 135.01(11) 1_655 . ? S10 Sb3 S8 47.53(10) . . ? S7 Sb3 S8 128.13(9) 1_565 . ? S14 Sb3 S8 117.83(9) 2_666 . ? S4 Sb3 S8 111.91(8) . . ? S4 Sb3 S8 82.43(7) 1_655 . ? S17 Sb3 S8 80.27(7) . . ? S15 Sb3 S14 127.65(11) . . ? S1 Sb3 S14 57.32(11) 1_655 . ? S5 Sb3 S14 116.31(10) 1_655 . ? S10 Sb3 S14 47.85(9) . . ? S7 Sb3 S14 140.59(10) 1_565 . ? S14 Sb3 S14 46.75(9) 2_666 . ? S4 Sb3 S14 80.40(8) . . ? S4 Sb3 S14 112.95(7) 1_655 . ? S17 Sb3 S14 102.94(8) . . ? S8 Sb3 S14 71.12(7) . . ? S15 Sb3 S2 136.65(11) . 2_666 ? S1 Sb3 S2 57.31(10) 1_655 2_666 ? S5 Sb3 S2 48.51(10) 1_655 2_666 ? S10 Sb3 S2 115.64(9) . 2_666 ? S7 Sb3 S2 112.87(8) 1_565 2_666 ? S14 Sb3 S2 45.84(8) 2_666 2_666 ? S4 Sb3 S2 104.39(8) . 2_666 ? S4 Sb3 S2 73.81(7) 1_655 2_666 ? S17 Sb3 S2 152.15(8) . 2_666 ? S8 Sb3 S2 118.24(6) . 2_666 ? S14 Sb3 S2 67.81(6) . 2_666 ? S13 Sb4 S6 100.76(14) 1_545 . ? S13 Sb4 S13 86.05(13) 1_545 2_665 ? S6 Sb4 S13 93.96(12) . 2_665 ? S13 Sb4 S11 75.81(12) 1_545 1_655 ? S6 Sb4 S11 79.86(11) . 1_655 ? S13 Sb4 S11 159.24(14) 2_665 1_655 ? S13 Sb4 S9 83.29(12) 1_545 2_655 ? S6 Sb4 S9 172.50(12) . 2_655 ? S13 Sb4 S9 79.95(11) 2_665 2_655 ? S11 Sb4 S9 107.36(11) 1_655 2_655 ? S13 Sb4 S12 168.73(12) 1_545 2_665 ? S6 Sb4 S12 73.98(12) . 2_665 ? S13 Sb4 S12 84.41(12) 2_665 2_665 ? S11 Sb4 S12 112.35(11) 1_655 2_665 ? S9 Sb4 S12 100.90(10) 2_655 2_665 ? S13 Sb4 S9 123.33(11) 1_545 1_655 ? S6 Sb4 S9 103.99(11) . 1_655 ? S13 Sb4 S9 140.65(12) 2_665 1_655 ? S11 Sb4 S9 59.91(11) 1_655 1_655 ? S9 Sb4 S9 78.59(10) 2_655 1_655 ? S12 Sb4 S9 67.92(9) 2_665 1_655 ? S13 Sb4 S9 59.02(10) 1_545 . ? S6 Sb4 S9 53.27(11) . . ? S13 Sb4 S9 61.40(11) 2_665 . ? S11 Sb4 S9 99.91(10) 1_655 . ? S9 Sb4 S9 125.70(7) 2_655 . ? S12 Sb4 S9 110.79(9) 2_665 . ? S9 Sb4 S9 154.00(11) 1_655 . ? S13 Sb4 S6 49.19(10) 1_545 2_655 ? S6 Sb4 S6 131.16(7) . 2_655 ? S13 Sb4 S6 53.24(10) 2_665 2_655 ? S11 Sb4 S6 117.22(9) 1_655 2_655 ? S9 Sb4 S6 47.70(9) 2_655 2_655 ? S12 Sb4 S6 127.08(8) 2_665 2_655 ? S9 Sb4 S6 124.44(7) 1_655 2_655 ? S9 Sb4 S6 78.15(7) . 2_655 ? S13 Sb4 S3 45.65(10) 1_545 1_645 ? S6 Sb4 S3 119.78(11) . 1_645 ? S13 Sb4 S3 122.57(10) 2_665 1_645 ? S11 Sb4 S3 48.50(9) 1_655 1_645 ? S9 Sb4 S3 67.54(9) 2_655 1_645 ? S12 Sb4 S3 145.60(9) 2_665 1_645 ? S9 Sb4 S3 77.91(8) 1_655 1_645 ? S9 Sb4 S3 101.53(8) . 1_645 ? S6 Sb4 S3 70.11(7) 2_655 1_645 ? S13 Sb4 S6 128.47(10) 1_545 2_665 ? S6 Sb4 S6 44.08(13) . 2_665 ? S13 Sb4 S6 65.97(9) 2_665 2_665 ? S11 Sb4 S6 118.25(8) 1_655 2_665 ? S9 Sb4 S6 128.60(9) 2_655 2_665 ? S12 Sb4 S6 41.28(8) 2_665 2_665 ? S9 Sb4 S6 104.03(8) 1_655 2_665 ? S9 Sb4 S6 69.55(7) . 2_665 ? S6 Sb4 S6 119.06(7) 2_655 2_665 ? S3 Sb4 S6 163.86(6) 1_645 2_665 ? S13 Sb4 S17 123.36(10) 1_545 2_665 ? S6 Sb4 S17 120.32(11) . 2_665 ? S13 Sb4 S17 56.17(11) 2_665 2_665 ? S11 Sb4 S17 143.50(10) 1_655 2_665 ? S9 Sb4 S17 52.55(9) 2_655 2_665 ? S12 Sb4 S17 54.78(8) 2_665 2_665 ? S9 Sb4 S17 84.67(8) 1_655 2_665 ? S9 Sb4 S17 116.56(7) . 2_665 ? S6 Sb4 S17 74.19(7) 2_655 2_665 ? S3 Sb4 S17 119.78(7) 1_645 2_665 ? S6 Sb4 S17 76.31(6) 2_665 2_665 ? S2 Sb5 S4 94.50(12) . 1_545 ? S2 Sb5 S7 92.72(13) . . ? S4 Sb5 S7 89.99(13) 1_545 . ? S2 Sb5 S14 82.05(11) . . ? S4 Sb5 S14 174.88(13) 1_545 . ? S7 Sb5 S14 93.94(12) . . ? S2 Sb5 S5 83.04(12) . 2_566 ? S4 Sb5 S5 94.85(12) 1_545 2_566 ? S7 Sb5 S5 173.78(11) . 2_566 ? S14 Sb5 S5 81.01(11) . 2_566 ? S2 Sb5 S14 152.36(13) . 2_656 ? S4 Sb5 S14 72.64(10) 1_545 2_656 ? S7 Sb5 S14 111.19(11) . 2_656 ? S14 Sb5 S14 108.84(8) . 2_656 ? S5 Sb5 S14 74.08(9) 2_566 2_656 ? S2 Sb5 S5 141.83(12) . 1_645 ? S4 Sb5 S5 114.60(11) 1_545 1_645 ? S7 Sb5 S5 64.63(11) . 1_645 ? S14 Sb5 S5 70.16(9) . 1_645 ? S5 Sb5 S5 116.43(8) 2_566 1_645 ? S14 Sb5 S5 64.59(9) 2_656 1_645 ? S2 Sb5 S5 57.89(11) . 1_545 ? S4 Sb5 S5 54.60(11) 1_545 1_545 ? S7 Sb5 S5 126.93(11) . 1_545 ? S14 Sb5 S5 120.28(9) . 1_545 ? S5 Sb5 S5 54.15(11) 2_566 1_545 ? S14 Sb5 S5 95.53(9) 2_656 1_545 ? S5 Sb5 S5 160.11(11) 1_645 1_545 ? S2 Sb5 S10 56.83(11) . . ? S4 Sb5 S10 128.14(11) 1_545 . ? S7 Sb5 S10 54.39(10) . . ? S14 Sb5 S10 52.74(9) . . ? S5 Sb5 S10 119.40(8) 2_566 . ? S14 Sb5 S10 149.51(9) 2_656 . ? S5 Sb5 S10 85.25(8) 1_645 . ? S5 Sb5 S10 114.62(7) 1_545 . ? S2 Sb5 S17 88.78(10) . 1_545 ? S4 Sb5 S17 40.31(11) 1_545 1_545 ? S7 Sb5 S17 50.41(11) . 1_545 ? S14 Sb5 S17 142.83(11) . 1_545 ? S5 Sb5 S17 133.66(10) 2_566 1_545 ? S14 Sb5 S17 95.83(8) 2_656 1_545 ? S5 Sb5 S17 97.71(8) 1_645 1_545 ? S5 Sb5 S17 83.08(8) 1_545 1_545 ? S10 Sb5 S17 92.34(8) . 1_545 ? S2 Sb5 S1 55.31(10) . 2_566 ? S4 Sb5 S1 125.55(11) 1_545 2_566 ? S7 Sb5 S1 130.22(10) . 2_566 ? S14 Sb5 S1 49.33(9) . 2_566 ? S5 Sb5 S1 43.56(8) 2_566 2_566 ? S14 Sb5 S1 112.16(8) 2_656 2_566 ? S5 Sb5 S1 115.56(7) 1_645 2_566 ? S5 Sb5 S1 71.11(7) 1_545 2_566 ? S10 Sb5 S1 75.84(7) . 2_566 ? S17 Sb5 S1 143.08(6) 1_545 2_566 ? S2 Sb5 S16 52.27(11) . . ? S4 Sb5 S16 81.93(10) 1_545 . ? S7 Sb5 S16 42.49(10) . . ? S14 Sb5 S16 98.78(9) . . ? S5 Sb5 S16 134.44(8) 2_566 . ? S14 Sb5 S16 143.93(8) 2_656 . ? S5 Sb5 S16 105.80(9) 1_645 . ? S5 Sb5 S16 89.88(7) 1_545 . ? S10 Sb5 S16 46.22(6) . . ? S17 Sb5 S16 49.40(7) 1_545 . ? S1 Sb5 S16 103.35(6) 2_566 . ? S7 Sb6 S10 94.54(13) . . ? S7 Sb6 S8 92.63(14) . . ? S10 Sb6 S8 90.53(13) . . ? S7 Sb6 S14 90.54(12) . . ? S10 Sb6 S14 78.82(11) . . ? S8 Sb6 S14 169.10(11) . . ? S7 Sb6 S1 169.84(13) . 1_655 ? S10 Sb6 S1 79.53(11) . 1_655 ? S8 Sb6 S1 95.64(13) . 1_655 ? S14 Sb6 S1 80.26(10) . 1_655 ? S7 Sb6 S5 74.62(11) . 1_645 ? S10 Sb6 S5 152.63(13) . 1_645 ? S8 Sb6 S5 114.61(12) . 1_645 ? S14 Sb6 S5 76.28(10) . 1_645 ? S1 Sb6 S5 107.00(10) 1_655 1_645 ? S7 Sb6 S2 124.31(11) . 1_655 ? S10 Sb6 S2 139.30(11) . 1_655 ? S8 Sb6 S2 77.30(11) . 1_655 ? S14 Sb6 S2 109.33(9) . 1_655 ? S1 Sb6 S2 63.59(8) 1_655 1_655 ? S5 Sb6 S2 61.68(9) 1_645 1_655 ? S7 Sb6 S2 52.42(10) . . ? S10 Sb6 S2 56.76(11) . . ? S8 Sb6 S2 123.71(11) . . ? S14 Sb6 S2 51.68(8) . . ? S1 Sb6 S2 117.65(9) 1_655 . ? S5 Sb6 S2 98.18(9) 1_645 . ? S2 Sb6 S2 157.08(11) 1_655 . ? S7 Sb6 S15 131.71(11) . . ? S10 Sb6 S15 53.62(11) . . ? S8 Sb6 S15 57.58(10) . . ? S14 Sb6 S15 113.08(9) . . ? S1 Sb6 S15 50.34(8) 1_655 . ? S5 Sb6 S15 149.50(9) 1_645 . ? S2 Sb6 S15 88.13(8) 1_655 . ? S2 Sb6 S15 110.37(7) . . ? S7 Sb6 S16 48.99(10) . . ? S10 Sb6 S16 52.36(9) . . ? S8 Sb6 S16 71.46(11) . . ? S14 Sb6 S16 103.16(9) . . ? S1 Sb6 S16 128.87(8) 1_655 . ? S5 Sb6 S16 123.56(8) 1_645 . ? S2 Sb6 S16 147.10(8) 1_655 . ? S2 Sb6 S16 52.25(7) . . ? S15 Sb6 S16 83.85(7) . . ? S7 Sb6 S15 45.92(10) . 1_545 ? S10 Sb6 S15 133.21(10) . 1_545 ? S8 Sb6 S15 71.45(11) . 1_545 ? S14 Sb6 S15 117.70(9) . 1_545 ? S1 Sb6 S15 143.05(9) 1_655 1_545 ? S5 Sb6 S15 53.74(8) 1_645 1_545 ? S2 Sb6 S15 79.66(7) 1_655 1_545 ? S2 Sb6 S15 97.56(7) . 1_545 ? S15 Sb6 S15 129.02(9) . 1_545 ? S16 Sb6 S15 80.86(6) . 1_545 ? S7 Sb6 S14 121.07(11) . 2_666 ? S10 Sb6 S14 51.50(9) . 2_666 ? S8 Sb6 S14 127.61(11) . 2_666 ? S14 Sb6 S14 42.85(11) . 2_666 ? S1 Sb6 S14 48.85(9) 1_655 2_666 ? S5 Sb6 S14 112.54(9) 1_645 2_666 ? S2 Sb6 S14 107.11(7) 1_655 2_666 ? S2 Sb6 S14 68.88(6) . 2_666 ? S15 Sb6 S14 70.25(7) . 2_666 ? S16 Sb6 S14 100.06(6) . 2_666 ? S15 Sb6 S14 160.42(7) 1_545 2_666 ? S16 Sb7 S12 95.43(14) . . ? S16 Sb7 S9 97.76(13) . . ? S12 Sb7 S9 85.43(14) . . ? S16 Sb7 S3 86.24(12) . . ? S12 Sb7 S3 81.79(12) . . ? S9 Sb7 S3 166.92(14) . . ? S16 Sb7 S11 87.82(12) . . ? S12 Sb7 S11 163.62(12) . . ? S9 Sb7 S11 78.22(13) . . ? S3 Sb7 S11 114.48(12) . . ? S16 Sb7 S6 133.03(13) . 1_455 ? S12 Sb7 S6 123.91(11) . 1_455 ? S9 Sb7 S6 108.92(11) . 1_455 ? S3 Sb7 S6 76.39(10) . 1_455 ? S11 Sb7 S6 62.00(9) . 1_455 ? S16 Sb7 S12 168.78(13) . 2_565 ? S12 Sb7 S12 74.16(12) . 2_565 ? S9 Sb7 S12 77.56(11) . 2_565 ? S3 Sb7 S12 96.20(10) . 2_565 ? S11 Sb7 S12 101.02(9) . 2_565 ? S6 Sb7 S12 58.06(9) 1_455 2_565 ? S16 Sb7 S8 66.79(12) . 1_455 ? S12 Sb7 S8 133.65(11) . 1_455 ? S9 Sb7 S8 137.19(12) . 1_455 ? S3 Sb7 S8 55.76(10) . 1_455 ? S11 Sb7 S8 62.19(9) . 1_455 ? S6 Sb7 S8 67.36(9) 1_455 1_455 ? S12 Sb7 S8 123.46(9) 2_565 1_455 ? S16 Sb7 S6 73.81(12) . . ? S12 Sb7 S6 48.33(10) . . ? S9 Sb7 S6 48.33(11) . . ? S3 Sb7 S6 122.16(10) . . ? S11 Sb7 S6 118.19(9) . . ? S6 Sb7 S6 151.12(10) 1_455 . ? S12 Sb7 S6 95.76(8) 2_565 . ? S8 Sb7 S6 140.59(8) 1_455 . ? S16 Sb7 S17 56.97(10) . 1_545 ? S12 Sb7 S17 126.65(11) . 1_545 ? S9 Sb7 S17 58.87(11) . 1_545 ? S3 Sb7 S17 132.25(10) . 1_545 ? S11 Sb7 S17 43.74(9) . 1_545 ? S6 Sb7 S17 105.65(9) 1_455 1_545 ? S12 Sb7 S17 126.04(8) 2_565 1_545 ? S8 Sb7 S17 80.46(8) 1_455 1_545 ? S6 Sb7 S17 78.89(8) . 1_545 ? S16 Sb7 S17 60.19(10) . . ? S12 Sb7 S17 58.39(10) . . ? S9 Sb7 S17 132.22(11) . . ? S3 Sb7 S17 40.48(9) . . ? S11 Sb7 S17 135.42(10) . . ? S6 Sb7 S17 116.84(8) 1_455 . ? S12 Sb7 S17 115.50(8) 2_565 . ? S8 Sb7 S17 76.20(8) 1_455 . ? S6 Sb7 S17 83.96(7) . . ? S17 Sb7 S17 117.15(8) 1_545 . ? S16 Sb7 S9 134.07(11) . 2_565 ? S12 Sb7 S9 50.01(10) . 2_565 ? S9 Sb7 S9 106.68(9) . 2_565 ? S3 Sb7 S9 62.60(9) . 2_565 ? S11 Sb7 S9 134.47(9) . 2_565 ? S6 Sb7 S9 74.15(8) 1_455 2_565 ? S12 Sb7 S9 40.83(7) 2_565 2_565 ? S8 Sb7 S9 112.39(7) 1_455 2_565 ? S6 Sb7 S9 94.20(7) . 2_565 ? S17 Sb7 S9 165.05(7) 1_545 2_565 ? S17 Sb7 S9 74.74(7) . 2_565 ? S3 Sb8 S15 84.1(2) 1_655 . ? S3 Sb8 S8 84.25(19) 1_655 . ? S15 Sb8 S8 101.5(2) . . ? S3 Sb8 S17 74.3(2) 1_655 1_655 ? S15 Sb8 S17 88.2(3) . 1_655 ? S8 Sb8 S17 155.5(3) . 1_655 ? S3 Sb8 S16 77.9(2) 1_655 1_655 ? S15 Sb8 S16 162.0(3) . 1_655 ? S8 Sb8 S16 77.8(2) . 1_655 ? S17 Sb8 S16 86.0(2) 1_655 1_655 ? S3 Sb8 S1 151.3(3) 1_655 1_655 ? S15 Sb8 S1 71.6(2) . 1_655 ? S8 Sb8 S1 85.8(2) . 1_655 ? S17 Sb8 S1 118.75(19) 1_655 1_655 ? S16 Sb8 S1 125.9(2) 1_655 1_655 ? S3 Sb8 S4 128.6(3) 1_655 1_655 ? S15 Sb8 S4 75.63(19) . 1_655 ? S8 Sb8 S4 145.6(3) . 1_655 ? S17 Sb8 S4 58.53(13) 1_655 1_655 ? S16 Sb8 S4 115.20(15) 1_655 1_655 ? S1 Sb8 S4 60.52(13) 1_655 1_655 ? S3 Sb8 S2 141.1(3) 1_655 1_655 ? S15 Sb8 S2 130.2(3) . 1_655 ? S8 Sb8 S2 72.4(2) . 1_655 ? S17 Sb8 S2 117.99(14) 1_655 1_655 ? S16 Sb8 S2 67.20(16) 1_655 1_655 ? S1 Sb8 S2 58.73(14) 1_655 1_655 ? S4 Sb8 S2 83.38(12) 1_655 1_655 ? S3 Sb8 S10 120.1(3) 1_655 1_655 ? S15 Sb8 S10 131.6(2) . 1_655 ? S8 Sb8 S10 120.8(3) . 1_655 ? S17 Sb8 S10 63.37(12) 1_655 1_655 ? S16 Sb8 S10 59.60(12) 1_655 1_655 ? S1 Sb8 S10 88.04(13) 1_655 1_655 ? S4 Sb8 S10 56.27(9) 1_655 1_655 ? S2 Sb8 S10 54.74(10) 1_655 1_655 ? S3 Sb8 S10 101.83(16) 1_655 . ? S15 Sb8 S10 56.89(17) . . ? S8 Sb8 S10 50.80(16) . . ? S17 Sb8 S10 145.0(2) 1_655 . ? S16 Sb8 S10 127.9(2) 1_655 . ? S1 Sb8 S10 52.05(13) 1_655 . ? S4 Sb8 S10 105.2(2) 1_655 . ? S2 Sb8 S10 87.23(17) 1_655 . ? S10 Sb8 S10 137.0(2) 1_655 . ? S3 Sb8 S11 51.53(18) 1_655 1_665 ? S15 Sb8 S11 48.98(18) . 1_665 ? S8 Sb8 S11 123.90(16) . 1_665 ? S17 Sb8 S11 48.77(14) 1_655 1_665 ? S16 Sb8 S11 116.3(2) 1_655 1_665 ? S1 Sb8 S11 115.6(2) 1_655 1_665 ? S4 Sb8 S11 80.61(16) 1_655 1_665 ? S2 Sb8 S11 163.42(13) 1_655 1_665 ? S10 Sb8 S11 111.67(17) 1_655 1_665 ? S10 Sb8 S11 101.08(14) . 1_665 ? S3 Sb8 S12 39.64(17) 1_655 1_655 ? S15 Sb8 S12 117.6(2) . 1_655 ? S8 Sb8 S12 97.3(2) . 1_655 ? S17 Sb8 S12 58.40(15) 1_655 1_655 ? S16 Sb8 S12 45.50(13) 1_655 1_655 ? S1 Sb8 S12 169.09(15) 1_655 1_655 ? S4 Sb8 S12 114.54(18) 1_655 1_655 ? S2 Sb8 S12 112.18(18) 1_655 1_655 ? S10 Sb8 S12 81.37(14) 1_655 1_655 ? S10 Sb8 S12 137.03(10) . 1_655 ? S11 Sb8 S12 71.25(13) 1_665 1_655 ? S3 Pb8 S15 75.9(3) 1_655 . ? S3 Pb8 S8 74.2(2) 1_655 . ? S15 Pb8 S8 90.5(3) . . ? S3 Pb8 S17 74.3(3) 1_655 1_655 ? S15 Pb8 S17 89.1(4) . 1_655 ? S8 Pb8 S17 147.5(4) . 1_655 ? S3 Pb8 S16 75.4(3) 1_655 1_655 ? S15 Pb8 S16 150.3(3) . 1_655 ? S8 Pb8 S16 74.9(3) . 1_655 ? S17 Pb8 S16 89.9(3) 1_655 1_655 ? S3 Pb8 S4 131.2(5) 1_655 1_655 ? S15 Pb8 S4 79.6(3) . 1_655 ? S8 Pb8 S4 147.6(5) . 1_655 ? S17 Pb8 S4 63.8(2) 1_655 1_655 ? S16 Pb8 S4 125.9(3) 1_655 1_655 ? S3 Pb8 S1 139.6(3) 1_655 1_655 ? S15 Pb8 S1 71.3(3) . 1_655 ? S8 Pb8 S1 83.1(3) . 1_655 ? S17 Pb8 S1 127.1(3) 1_655 1_655 ? S16 Pb8 S1 130.3(4) 1_655 1_655 ? S4 Pb8 S1 64.5(2) 1_655 1_655 ? S3 Pb8 S10 124.9(4) 1_655 1_655 ? S15 Pb8 S10 141.4(3) . 1_655 ? S8 Pb8 S10 124.6(4) . 1_655 ? S17 Pb8 S10 69.81(19) 1_655 1_655 ? S16 Pb8 S10 64.4(2) 1_655 1_655 ? S4 Pb8 S10 62.29(13) 1_655 1_655 ? S1 Pb8 S10 95.5(2) 1_655 1_655 ? S3 Pb8 S2 137.0(4) 1_655 1_655 ? S15 Pb8 S2 130.9(4) . 1_655 ? S8 Pb8 S2 72.9(3) . 1_655 ? S17 Pb8 S2 128.9(2) 1_655 1_655 ? S16 Pb8 S2 69.9(2) 1_655 1_655 ? S4 Pb8 S2 90.4(2) 1_655 1_655 ? S1 Pb8 S2 61.2(2) 1_655 1_655 ? S10 Pb8 S2 59.12(16) 1_655 1_655 ? S3 Pb8 S11 50.2(2) 1_655 1_665 ? S15 Pb8 S11 47.6(2) . 1_665 ? S8 Pb8 S11 113.4(2) . 1_665 ? S17 Pb8 S11 47.42(19) 1_655 1_665 ? S16 Pb8 S11 114.7(3) 1_655 1_665 ? S4 Pb8 S11 82.2(3) 1_655 1_665 ? S1 Pb8 S11 114.8(3) 1_655 1_665 ? S10 Pb8 S11 116.9(3) 1_655 1_665 ? S2 Pb8 S11 172.7(2) 1_655 1_665 ? S3 Pb8 S10 91.7(2) 1_655 . ? S15 Pb8 S10 52.4(2) . . ? S8 Pb8 S10 47.06(19) . . ? S17 Pb8 S10 141.5(3) 1_655 . ? S16 Pb8 S10 121.6(3) 1_655 . ? S4 Pb8 S10 105.6(3) 1_655 . ? S1 Pb8 S10 49.40(16) 1_655 . ? S10 Pb8 S10 141.1(3) 1_655 . ? S2 Pb8 S10 85.7(3) 1_655 . ? S11 Pb8 S10 96.03(19) 1_665 . ? S3 Pb8 S12 41.0(2) 1_655 1_655 ? S15 Pb8 S12 112.3(3) . 1_655 ? S8 Pb8 S12 92.5(3) . 1_655 ? S17 Pb8 S12 58.0(2) 1_655 1_655 ? S16 Pb8 S12 44.73(18) 1_655 1_655 ? S4 Pb8 S12 119.8(3) 1_655 1_655 ? S1 Pb8 S12 174.5(3) 1_655 1_655 ? S10 Pb8 S12 84.2(2) 1_655 1_655 ? S2 Pb8 S12 114.3(3) 1_655 1_655 ? S11 Pb8 S12 70.00(18) 1_665 1_655 ? S10 Pb8 S12 128.91(15) . 1_655 ? S17 Sb9 S11 95.50(13) . 1_565 ? S17 Sb9 S3 94.45(16) . . ? S11 Sb9 S3 99.40(15) 1_565 . ? S17 Sb9 S9 99.53(15) . 1_565 ? S11 Sb9 S9 76.95(13) 1_565 1_565 ? S3 Sb9 S9 165.81(12) . 1_565 ? S17 Sb9 S12 99.22(12) . . ? S11 Sb9 S12 164.59(12) 1_565 . ? S3 Sb9 S12 75.03(12) . . ? S9 Sb9 S12 104.87(11) 1_565 . ? S17 Sb9 S13 137.58(14) . 1_455 ? S11 Sb9 S13 57.18(10) 1_565 1_455 ? S3 Sb9 S13 63.38(11) . 1_455 ? S9 Sb9 S13 103.94(10) 1_565 1_455 ? S12 Sb9 S13 108.04(9) . 1_455 ? S17 Sb9 S9 163.93(13) . 2_565 ? S11 Sb9 S9 99.08(11) 1_565 2_565 ? S3 Sb9 S9 89.81(11) . 2_565 ? S9 Sb9 S9 77.40(10) 1_565 2_565 ? S12 Sb9 S9 66.93(9) . 2_565 ? S13 Sb9 S9 57.68(8) 1_455 2_565 ? S17 Sb9 S15 70.59(14) . 1_455 ? S11 Sb9 S15 57.45(12) 1_565 1_455 ? S3 Sb9 S15 52.25(11) . 1_455 ? S9 Sb9 S15 131.02(9) 1_565 1_455 ? S12 Sb9 S15 123.90(10) . 1_455 ? S13 Sb9 S15 67.30(8) 1_455 1_455 ? S9 Sb9 S15 123.39(9) 2_565 1_455 ? S17 Sb9 S13 75.14(14) . . ? S11 Sb9 S13 128.52(12) 1_565 . ? S3 Sb9 S13 131.33(11) . . ? S9 Sb9 S13 55.93(9) 1_565 . ? S12 Sb9 S13 60.61(9) . . ? S13 Sb9 S13 146.89(11) 1_455 . ? S9 Sb9 S13 90.43(8) 2_565 . ? S15 Sb9 S13 145.72(8) 1_455 . ? S17 Sb9 S16 61.84(12) . 1_565 ? S11 Sb9 S16 51.95(11) 1_565 1_565 ? S3 Sb9 S16 136.02(11) . 1_565 ? S9 Sb9 S16 51.67(9) 1_565 1_565 ? S12 Sb9 S16 140.81(10) . 1_565 ? S13 Sb9 S16 108.19(7) 1_455 1_565 ? S9 Sb9 S16 123.57(8) 2_565 1_565 ? S15 Sb9 S16 84.08(8) 1_455 1_565 ? S13 Sb9 S16 80.78(7) . 1_565 ? S17 Sb9 S16 66.47(12) . . ? S11 Sb9 S16 136.25(12) 1_565 . ? S3 Sb9 S16 46.92(10) . . ? S9 Sb9 S16 142.72(9) 1_565 . ? S12 Sb9 S16 48.71(9) . . ? S13 Sb9 S16 109.17(8) 1_455 . ? S9 Sb9 S16 106.36(7) 2_565 . ? S15 Sb9 S16 78.80(8) 1_455 . ? S13 Sb9 S16 86.80(7) . . ? S16 Sb9 S16 128.31(8) 1_565 . ? S17 Sb9 S4 24.55(13) . . ? S11 Sb9 S4 78.00(10) 1_565 . ? S3 Sb9 S4 80.53(10) . . ? S9 Sb9 S4 111.62(9) 1_565 . ? S12 Sb9 S4 114.50(8) . . ? S13 Sb9 S4 113.03(8) 1_455 . ? S9 Sb9 S4 169.23(8) 2_565 . ? S15 Sb9 S4 46.35(7) 1_455 . ? S13 Sb9 S4 99.52(7) . . ? S16 Sb9 S4 62.76(7) 1_565 . ? S16 Sb9 S4 70.36(6) . . ? S12 Sb10 S6 94.32(13) . . ? S12 Sb10 S9 92.11(14) . . ? S6 Sb10 S9 93.79(15) . . ? S12 Sb10 S6 81.43(13) . 2_665 ? S6 Sb10 S6 87.71(12) . 2_665 ? S9 Sb10 S6 173.47(12) . 2_665 ? S12 Sb10 S13 174.84(12) . 2_665 ? S6 Sb10 S13 80.72(11) . 2_665 ? S9 Sb10 S13 86.84(12) . 2_665 ? S6 Sb10 S13 99.68(11) 2_665 2_665 ? S12 Sb10 S3 119.51(12) . 2_565 ? S6 Sb10 S3 139.67(13) . 2_565 ? S9 Sb10 S3 105.31(12) . 2_565 ? S6 Sb10 S3 77.30(10) 2_665 2_565 ? S13 Sb10 S3 65.62(9) 2_665 2_565 ? S12 Sb10 S12 72.72(12) . 2_565 ? S6 Sb10 S12 162.93(12) . 2_565 ? S9 Sb10 S12 76.07(12) . 2_565 ? S6 Sb10 S12 100.90(9) 2_665 2_565 ? S13 Sb10 S12 111.85(9) 2_665 2_565 ? S3 Sb10 S12 57.27(9) 2_565 2_565 ? S12 Sb10 S12 117.51(10) . 2_665 ? S6 Sb10 S12 53.39(12) . 2_665 ? S9 Sb10 S12 134.83(11) . 2_665 ? S6 Sb10 S12 50.45(8) 2_665 2_665 ? S13 Sb10 S12 60.53(9) 2_665 2_665 ? S3 Sb10 S12 89.54(9) 2_565 2_665 ? S12 Sb10 S12 142.47(11) 2_565 2_665 ? S12 Sb10 S13 128.33(11) . 1_545 ? S6 Sb10 S13 56.02(10) . 1_545 ? S9 Sb10 S13 54.65(11) . 1_545 ? S6 Sb10 S13 130.66(9) 2_665 1_545 ? S13 Sb10 S13 47.42(11) 2_665 1_545 ? S3 Sb10 S13 107.89(8) 2_565 1_545 ? S12 Sb10 S13 123.63(8) 2_565 1_545 ? S12 Sb10 S13 80.24(8) 2_665 1_545 ? S12 Sb10 S16 49.65(11) . . ? S6 Sb10 S16 72.26(11) . . ? S9 Sb10 S16 51.38(10) . . ? S6 Sb10 S16 123.47(8) 2_665 . ? S13 Sb10 S16 126.71(9) 2_665 . ? S3 Sb10 S16 146.25(9) 2_565 . ? S12 Sb10 S16 90.74(8) 2_565 . ? S12 Sb10 S16 124.18(7) 2_665 . ? S13 Sb10 S16 79.60(7) 1_545 . ? S12 Sb10 S13 48.78(12) . . ? S6 Sb10 S13 67.22(10) . . ? S9 Sb10 S13 131.62(11) . . ? S6 Sb10 S13 43.56(8) 2_665 . ? S13 Sb10 S13 129.30(6) 2_665 . ? S3 Sb10 S13 117.94(8) 2_565 . ? S12 Sb10 S13 109.22(7) 2_565 . ? S12 Sb10 S13 68.82(7) 2_665 . ? S13 Sb10 S13 123.11(8) 1_545 . ? S16 Sb10 S13 80.25(7) . . ? S12 Sb10 S11 146.33(12) . 2 ? S6 Sb10 S11 115.34(10) . 2 ? S9 Sb10 S11 71.38(11) . 2 ? S6 Sb10 S11 113.68(8) 2_665 2 ? S13 Sb10 S11 37.57(8) 2_665 2 ? S3 Sb10 S11 44.12(8) 2_565 2 ? S12 Sb10 S11 74.85(7) 2_565 2 ? S12 Sb10 S11 93.88(7) 2_665 2 ? S13 Sb10 S11 65.49(6) 1_545 2 ? S16 Sb10 S11 122.75(7) . 2 ? S13 Sb10 S11 156.94(7) . 2 ? Sb3 S1 Sb1 93.47(12) 1_455 . ? Sb3 S1 Sb6 92.53(11) 1_455 1_455 ? Sb1 S1 Sb6 173.87(14) . 1_455 ? Sb3 S1 Sb2 94.79(12) 1_455 2_566 ? Sb1 S1 Sb2 87.53(11) . 2_566 ? Sb6 S1 Sb2 93.28(11) 1_455 2_566 ? Sb3 S1 Pb8 86.8(2) 1_455 1_455 ? Sb1 S1 Pb8 100.5(2) . 1_455 ? Sb6 S1 Pb8 78.49(18) 1_455 1_455 ? Sb2 S1 Pb8 171.7(2) 2_566 1_455 ? Sb3 S1 S5 50.24(9) 1_455 . ? Sb1 S1 S5 43.55(8) . . ? Sb6 S1 S5 142.55(13) 1_455 . ? Sb2 S1 S5 86.96(12) 2_566 . ? Pb8 S1 S5 100.2(2) 1_455 . ? Sb3 S1 Sb8 82.64(15) 1_455 1_455 ? Sb1 S1 Sb8 105.66(17) . 1_455 ? Sb6 S1 Sb8 73.83(13) 1_455 1_455 ? Sb2 S1 Sb8 166.67(15) 2_566 1_455 ? Pb8 S1 Sb8 6.45(17) 1_455 1_455 ? S5 S1 Sb8 101.13(18) . 1_455 ? Sb3 S1 S15 41.98(9) 1_455 1_455 ? Sb1 S1 S15 96.15(13) . 1_455 ? Sb6 S1 S15 87.44(11) 1_455 1_455 ? Sb2 S1 S15 136.68(13) 2_566 1_455 ? Pb8 S1 S15 45.0(2) 1_455 1_455 ? S5 S1 S15 67.90(11) . 1_455 ? Sb8 S1 S15 41.54(14) 1_455 1_455 ? Sb3 S1 As1 148.12(16) 1_455 2_566 ? Sb1 S1 As1 104.77(11) . 2_566 ? Sb6 S1 As1 70.49(8) 1_455 2_566 ? Sb2 S1 As1 60.84(7) 2_566 2_566 ? Pb8 S1 As1 114.5(2) 1_455 2_566 ? S5 S1 As1 138.11(13) . 2_566 ? Sb8 S1 As1 116.07(16) 1_455 2_566 ? S15 S1 As1 153.96(12) 1_455 2_566 ? Sb3 S1 Sb1 148.12(16) 1_455 2_566 ? Sb1 S1 Sb1 104.77(11) . 2_566 ? Sb6 S1 Sb1 70.49(8) 1_455 2_566 ? Sb2 S1 Sb1 60.84(7) 2_566 2_566 ? Pb8 S1 Sb1 114.5(2) 1_455 2_566 ? S5 S1 Sb1 138.11(13) . 2_566 ? Sb8 S1 Sb1 116.07(16) 1_455 2_566 ? S15 S1 Sb1 153.96(12) 1_455 2_566 ? As1 S1 Sb1 0.000(19) 2_566 2_566 ? Sb3 S1 S10 51.21(9) 1_455 1_455 ? Sb1 S1 S10 144.17(14) . 1_455 ? Sb6 S1 S10 41.95(7) 1_455 1_455 ? Sb2 S1 S10 89.58(12) 2_566 1_455 ? Pb8 S1 S10 85.03(15) 1_455 1_455 ? S5 S1 S10 100.64(12) . 1_455 ? Sb8 S1 S10 78.58(12) 1_455 1_455 ? S15 S1 S10 62.98(11) 1_455 1_455 ? As1 S1 S10 104.82(11) 2_566 1_455 ? Sb1 S1 S10 104.82(11) 2_566 1_455 ? Sb5 S2 Sb2 97.19(13) . . ? Sb5 S2 As1 96.65(12) . 2_566 ? Sb2 S2 As1 90.23(11) . 2_566 ? Sb5 S2 Sb1 96.65(12) . 2_566 ? Sb2 S2 Sb1 90.23(11) . 2_566 ? As1 S2 Sb1 0.00(5) 2_566 2_566 ? Sb5 S2 Pb 90.66(10) . . ? Sb2 S2 Pb 141.97(16) . . ? As1 S2 Pb 125.85(12) 2_566 . ? Sb1 S2 Pb 125.85(12) 2_566 . ? Sb5 S2 S14 55.27(9) . . ? Sb2 S2 S14 42.64(8) . . ? As1 S2 S14 87.91(11) 2_566 . ? Sb1 S2 S14 87.91(11) 2_566 . ? Pb S2 S14 136.48(13) . . ? Sb5 S2 S7 44.61(9) . . ? Sb2 S2 S7 91.85(12) . . ? As1 S2 S7 141.13(13) 2_566 . ? Sb1 S2 S7 141.13(13) 2_566 . ? Pb S2 S7 68.26(9) . . ? S14 S2 S7 68.33(11) . . ? Sb5 S2 S4 43.56(8) . 1_545 ? Sb2 S2 S4 140.56(14) . 1_545 ? As1 S2 S4 97.15(12) 2_566 1_545 ? Sb1 S2 S4 97.15(12) 2_566 1_545 ? Pb S2 S4 55.20(8) . 1_545 ? S14 S2 S4 98.76(11) . 1_545 ? S7 S2 S4 59.06(10) . 1_545 ? Sb5 S2 S5 88.29(12) . 1_545 ? Sb2 S2 S5 141.55(15) . 1_545 ? As1 S2 S5 51.33(9) 2_566 1_545 ? Sb1 S2 S5 51.33(9) 2_566 1_545 ? Pb S2 S5 75.52(10) . 1_545 ? S14 S2 S5 123.28(14) . 1_545 ? S7 S2 S5 117.14(12) . 1_545 ? S4 S2 S5 58.12(11) 1_545 1_545 ? Sb5 S2 S1 154.62(15) . . ? Sb2 S2 S1 68.65(10) . . ? As1 S2 S1 63.68(9) 2_566 . ? Sb1 S2 S1 63.68(9) 2_566 . ? Pb S2 S1 113.61(11) . . ? S14 S2 S1 105.54(11) . . ? S7 S2 S1 150.56(15) . . ? S4 S2 S1 147.90(15) 1_545 . ? S5 S2 S1 90.69(12) 1_545 . ? Sb5 S2 S5 56.83(10) . 2_566 ? Sb2 S2 S5 94.03(12) . 2_566 ? As1 S2 S5 39.82(8) 2_566 2_566 ? Sb1 S2 S5 39.82(8) 2_566 2_566 ? Pb S2 S5 120.81(12) . 2_566 ? S14 S2 S5 65.84(11) . 2_566 ? S7 S2 S5 101.33(12) . 2_566 ? S4 S2 S5 69.35(11) 1_545 2_566 ? S5 S2 S5 57.65(12) 1_545 2_566 ? S1 S2 S5 101.84(13) . 2_566 ? Sb5 S2 S10 90.52(12) . . ? Sb2 S2 S10 42.41(8) . . ? As1 S2 S10 132.63(11) 2_566 . ? Sb1 S2 S10 132.63(11) 2_566 . ? Pb S2 S10 100.69(12) . . ? S14 S2 S10 58.67(10) . . ? S7 S2 S10 59.71(10) . . ? S4 S2 S10 118.76(13) 1_545 . ? S5 S2 S10 176.01(13) 1_545 . ? S1 S2 S10 92.02(11) . . ? S5 S2 S10 124.50(12) 2_566 . ? Sb8 S3 Sb9 104.7(2) 1_455 . ? Sb8 S3 Pb8 6.5(4) 1_455 1_455 ? Sb9 S3 Pb8 99.2(3) . 1_455 ? Sb8 S3 Sb7 100.4(2) 1_455 . ? Sb9 S3 Sb7 108.74(16) . . ? Pb8 S3 Sb7 99.1(3) 1_455 . ? Sb8 S3 S15 49.4(2) 1_455 1_455 ? Sb9 S3 S15 92.51(14) . 1_455 ? Pb8 S3 S15 52.2(3) 1_455 1_455 ? Sb7 S3 S15 147.59(16) . 1_455 ? Sb8 S3 S8 50.05(19) 1_455 1_455 ? Sb9 S3 S8 154.68(16) . 1_455 ? Pb8 S3 S8 55.5(3) 1_455 1_455 ? Sb7 S3 S8 77.98(11) . 1_455 ? S15 S3 S8 72.89(13) 1_455 1_455 ? Sb8 S3 Tl1 88.1(2) 1_455 1_455 ? Sb9 S3 Tl1 133.81(14) . 1_455 ? Pb8 S3 Tl1 94.5(3) 1_455 1_455 ? Sb7 S3 Tl1 112.25(12) . 1_455 ? S15 S3 Tl1 62.51(11) 1_455 1_455 ? S8 S3 Tl1 57.51(10) 1_455 1_455 ? Sb8 S3 As10 166.2(2) 1_455 2_565 ? Sb9 S3 As10 88.88(12) . 2_565 ? Pb8 S3 As10 170.1(3) 1_455 2_565 ? Sb7 S3 As10 72.67(8) . 2_565 ? S15 S3 As10 133.61(13) 1_455 2_565 ? S8 S3 As10 116.23(13) 1_455 2_565 ? Tl1 S3 As10 83.82(9) 1_455 2_565 ? Sb8 S3 Sb10 166.2(2) 1_455 2_565 ? Sb9 S3 Sb10 88.88(12) . 2_565 ? Pb8 S3 Sb10 170.1(3) 1_455 2_565 ? Sb7 S3 Sb10 72.67(8) . 2_565 ? S15 S3 Sb10 133.61(13) 1_455 2_565 ? S8 S3 Sb10 116.23(13) 1_455 2_565 ? Tl1 S3 Sb10 83.82(9) 1_455 2_565 ? As10 S3 Sb10 0.00(6) 2_565 2_565 ? Sb8 S3 S17 63.86(19) 1_455 . ? Sb9 S3 S17 41.89(10) . . ? Pb8 S3 S17 57.9(3) 1_455 . ? Sb7 S3 S17 106.41(14) . . ? S15 S3 S17 73.22(13) 1_455 . ? S8 S3 S17 112.96(15) 1_455 . ? Tl1 S3 S17 135.63(14) 1_455 . ? As10 S3 S17 129.11(16) 2_565 . ? Sb10 S3 S17 129.11(16) 2_565 . ? Sb8 S3 S13 130.5(2) 1_455 1_455 ? Sb9 S3 S13 79.75(12) . 1_455 ? Pb8 S3 S13 133.8(3) 1_455 1_455 ? Sb7 S3 S13 125.29(13) . 1_455 ? S15 S3 S13 81.52(12) 1_455 1_455 ? S8 S3 S13 117.07(16) 1_455 1_455 ? Tl1 S3 S13 59.61(10) 1_455 1_455 ? As10 S3 S13 53.15(8) 2_565 1_455 ? Sb10 S3 S13 53.15(8) 2_565 1_455 ? S17 S3 S13 112.71(14) . 1_455 ? Sb5 S4 Sb1 93.64(13) 1_565 . ? Sb5 S4 Pb 89.78(12) 1_565 1_565 ? Sb1 S4 Pb 120.35(14) . 1_565 ? Sb5 S4 Sb2 114.18(12) 1_565 . ? Sb1 S4 Sb2 72.11(10) . . ? Pb S4 Sb2 153.18(12) 1_565 . ? Sb5 S4 Pb8 165.1(3) 1_565 1_455 ? Sb1 S4 Pb8 101.2(3) . 1_455 ? Pb S4 Pb8 81.4(2) 1_565 1_455 ? Sb2 S4 Pb8 72.6(2) . 1_455 ? Sb5 S4 S17 111.77(16) 1_565 . ? Sb1 S4 S17 152.80(17) . . ? Pb S4 S17 53.18(9) 1_565 . ? Sb2 S4 S17 104.15(12) . . ? Pb8 S4 S17 53.3(2) 1_455 . ? Sb5 S4 S7 45.14(9) 1_565 1_565 ? Sb1 S4 S7 138.78(14) . 1_565 ? Pb S4 S7 68.85(10) 1_565 1_565 ? Sb2 S4 S7 119.21(13) . 1_565 ? Pb8 S4 S7 120.0(3) 1_455 1_565 ? S17 S4 S7 67.25(13) . 1_565 ? Sb5 S4 S5 90.36(12) 1_565 . ? Sb1 S4 S5 42.65(9) . . ? Pb S4 S5 77.84(10) 1_565 . ? Sb2 S4 S5 112.14(14) . . ? Pb8 S4 S5 99.4(2) 1_455 . ? S17 S4 S5 124.30(14) . . ? S7 S4 S5 121.80(13) 1_565 . ? Sb5 S4 S2 41.94(8) 1_565 1_565 ? Sb1 S4 S2 90.92(12) . 1_565 ? Pb S4 S2 55.75(8) 1_565 1_565 ? Sb2 S4 S2 151.06(12) . 1_565 ? Pb8 S4 S2 135.1(2) 1_455 1_565 ? S17 S4 S2 101.41(14) . 1_565 ? S7 S4 S2 59.85(11) 1_565 1_565 ? S5 S4 S2 61.98(10) . 1_565 ? Sb5 S4 S14 66.29(10) 1_565 2_666 ? Sb1 S4 S14 71.26(11) . 2_666 ? Pb S4 S14 154.82(15) 1_565 2_666 ? Sb2 S4 S14 48.07(8) . 2_666 ? Pb8 S4 S14 120.1(2) 1_455 2_666 ? S17 S4 S14 127.04(15) . 2_666 ? S7 S4 S14 87.84(12) 1_565 2_666 ? S5 S4 S14 108.63(14) . 2_666 ? S2 S4 S14 104.81(12) 1_565 2_666 ? Sb5 S4 S1 136.84(16) 1_565 . ? Sb1 S4 S1 43.27(9) . . ? Pb S4 S1 108.55(12) 1_565 . ? Sb2 S4 S1 62.57(9) . . ? Pb8 S4 S1 58.0(2) 1_455 . ? S17 S4 S1 110.42(14) . . ? S7 S4 S1 177.17(14) 1_565 . ? S5 S4 S1 57.89(11) . . ? S2 S4 S1 119.85(13) 1_565 . ? S14 S4 S1 94.91(13) 2_666 . ? Sb1 S5 Sb3 91.28(12) . 1_455 ? Sb1 S5 As1 97.88(12) . 2_576 ? Sb3 S5 As1 169.07(17) 1_455 2_576 ? Sb1 S5 Sb1 97.88(12) . 2_576 ? Sb3 S5 Sb1 169.07(17) 1_455 2_576 ? As1 S5 Sb1 0.00(4) 2_576 2_576 ? Sb1 S5 Sb5 96.88(14) . 2_566 ? Sb3 S5 Sb5 100.30(14) 1_455 2_566 ? As1 S5 Sb5 72.80(10) 2_576 2_566 ? Sb1 S5 Sb5 72.80(10) 2_576 2_566 ? Sb1 S5 Sb6 153.76(19) . 1_465 ? Sb3 S5 Sb6 97.77(11) 1_455 1_465 ? As1 S5 Sb6 76.50(8) 2_576 1_465 ? Sb1 S5 Sb6 76.50(8) 2_576 1_465 ? Sb5 S5 Sb6 105.57(11) 2_566 1_465 ? Sb1 S5 S1 46.13(9) . . ? Sb3 S5 S1 45.47(8) 1_455 . ? As1 S5 S1 142.53(13) 2_576 . ? Sb1 S5 S1 142.53(13) 2_576 . ? Sb5 S5 S1 98.04(13) 2_566 . ? Sb6 S5 S1 139.82(13) 1_465 . ? Sb1 S5 S4 44.87(10) . . ? Sb3 S5 S4 89.33(12) 1_455 . ? As1 S5 S4 101.36(13) 2_576 . ? Sb1 S5 S4 101.36(13) 2_576 . ? Sb5 S5 S4 141.08(13) 2_566 . ? Sb6 S5 S4 110.37(14) 1_465 . ? S1 S5 S4 62.74(11) . . ? Sb1 S5 S5 56.12(10) . 2_576 ? Sb3 S5 S5 146.93(18) 1_455 2_576 ? As1 S5 S5 41.77(8) 2_576 2_576 ? Sb1 S5 S5 41.77(8) 2_576 2_576 ? Sb5 S5 S5 80.37(15) 2_566 2_576 ? Sb6 S5 S5 114.05(16) 1_465 2_576 ? S1 S5 S5 101.49(15) . 2_576 ? S4 S5 S5 71.85(14) . 2_576 ? Sb1 S5 S7 145.49(15) . 1_465 ? Sb3 S5 S7 57.29(9) 1_455 1_465 ? As1 S5 S7 115.08(12) 2_576 1_465 ? Sb1 S5 S7 115.08(12) 2_576 1_465 ? Sb5 S5 S7 102.18(13) 2_566 1_465 ? Sb6 S5 S7 41.48(8) 1_465 1_465 ? S1 S5 S7 102.32(12) . 1_465 ? S4 S5 S7 114.47(15) . 1_465 ? S5 S5 S7 155.42(18) 2_576 1_465 ? Sb1 S5 S2 90.79(14) . 1_565 ? Sb3 S5 S2 131.28(17) 1_455 1_565 ? As1 S5 S2 54.89(9) 2_576 1_565 ? Sb1 S5 S2 54.89(9) 2_576 1_565 ? Sb5 S5 S2 127.69(12) 2_566 1_565 ? Sb6 S5 S2 64.80(9) 1_465 1_565 ? S1 S5 S2 122.64(15) . 1_565 ? S4 S5 S2 59.91(11) . 1_565 ? S5 S5 S2 61.79(13) 2_576 1_565 ? S7 S5 S2 99.66(13) 1_465 1_565 ? Sb10 S6 Sb4 101.52(13) . . ? Sb10 S6 As10 92.29(12) . 2_665 ? Sb4 S6 As10 104.94(14) . 2_665 ? Sb10 S6 Sb10 92.29(12) . 2_665 ? Sb4 S6 Sb10 104.94(14) . 2_665 ? As10 S6 Sb10 0.00(5) 2_665 2_665 ? Sb10 S6 Tl2 100.53(14) . . ? Sb4 S6 Tl2 89.83(11) . . ? As10 S6 Tl2 158.17(12) 2_665 . ? Sb10 S6 Tl2 158.17(12) 2_665 . ? Sb10 S6 S11 146.47(16) . 1_655 ? Sb4 S6 S11 55.60(9) . 1_655 ? As10 S6 S11 115.87(14) 2_665 1_655 ? Sb10 S6 S11 115.87(14) 2_665 1_655 ? Tl2 S6 S11 59.63(10) . 1_655 ? Sb10 S6 S12 42.66(9) . . ? Sb4 S6 S12 143.70(15) . . ? As10 S6 S12 85.76(11) 2_665 . ? Sb10 S6 S12 85.76(11) 2_665 . ? Tl2 S6 S12 91.75(12) . . ? S11 S6 S12 148.86(16) 1_655 . ? Sb10 S6 S9 43.16(10) . . ? Sb4 S6 S9 92.08(13) . . ? As10 S6 S9 135.11(14) 2_665 . ? Sb10 S6 S9 135.11(14) 2_665 . ? Tl2 S6 S9 58.27(10) . . ? S11 S6 S9 108.09(14) 1_655 . ? S12 S6 S9 58.88(11) . . ? Sb10 S6 S13 58.75(10) . 2_665 ? Sb4 S6 S13 43.10(8) . 2_665 ? As10 S6 S13 99.91(13) 2_665 2_665 ? Sb10 S6 S13 99.91(13) 2_665 2_665 ? Tl2 S6 S13 101.84(12) . 2_665 ? S11 S6 S13 96.74(12) 1_655 2_665 ? S12 S6 S13 101.40(13) . 2_665 ? S9 S6 S13 65.32(12) . 2_665 ? Sb10 S6 S12 94.79(14) . 2_665 ? Sb4 S6 S12 65.14(11) . 2_665 ? As10 S6 S12 40.17(8) 2_665 2_665 ? Sb10 S6 S12 40.17(8) 2_665 2_665 ? Tl2 S6 S12 152.91(13) . 2_665 ? S11 S6 S12 95.84(13) 1_655 2_665 ? S12 S6 S12 114.41(13) . 2_665 ? S9 S6 S12 128.86(14) . 2_665 ? S13 S6 S12 67.53(11) 2_665 2_665 ? Sb6 S7 Sb5 97.98(13) . . ? Sb6 S7 Sb3 109.11(13) . 1_545 ? Sb5 S7 Sb3 79.53(11) . 1_545 ? Sb6 S7 Tl2 109.39(15) . . ? Sb5 S7 Tl2 149.66(15) . . ? Sb3 S7 Tl2 102.72(10) 1_545 . ? Sb6 S7 S4 142.82(16) . 1_545 ? Sb5 S7 S4 44.87(9) . 1_545 ? Sb3 S7 S4 68.53(10) 1_545 1_545 ? Tl2 S7 S4 107.16(12) . 1_545 ? Sb6 S7 S2 94.12(12) . . ? Sb5 S7 S2 42.68(9) . . ? Sb3 S7 S2 120.59(14) 1_545 . ? Tl2 S7 S2 120.11(12) . . ? S4 S7 S2 61.09(11) 1_545 . ? Sb6 S7 S8 43.73(10) . . ? Sb5 S7 S8 141.43(15) . . ? Sb3 S7 S8 113.16(13) 1_545 . ? Tl2 S7 S8 66.03(10) . . ? S4 S7 S8 173.11(14) 1_545 . ? S2 S7 S8 120.72(13) . . ? Sb6 S7 S5 63.91(10) . 1_645 ? Sb5 S7 S5 76.53(12) . 1_645 ? Sb3 S7 S5 46.44(8) 1_545 1_645 ? Tl2 S7 S5 127.04(14) . 1_645 ? S4 S7 S5 98.69(13) 1_545 1_645 ? S2 S7 S5 112.83(14) . 1_645 ? S8 S7 S5 86.72(13) . 1_645 ? Sb6 S7 S15 104.74(14) . 1_545 ? Sb5 S7 S15 120.67(15) . 1_545 ? Sb3 S7 S15 41.35(8) 1_545 1_545 ? Tl2 S7 S15 65.31(9) . 1_545 ? S4 S7 S15 96.38(13) 1_545 1_545 ? S2 S7 S15 157.42(15) . 1_545 ? S8 S7 S15 81.82(13) . 1_545 ? S5 S7 S15 66.53(11) 1_645 1_545 ? Sb6 S7 S10 42.76(8) . . ? Sb5 S7 S10 91.64(12) . . ? Sb3 S7 S10 149.44(13) 1_545 . ? Tl2 S7 S10 99.52(12) . . ? S4 S7 S10 123.79(14) 1_545 . ? S2 S7 S10 62.71(10) . . ? S8 S7 S10 58.37(11) . . ? S5 S7 S10 103.13(12) 1_645 . ? S15 S7 S10 139.83(16) 1_545 . ? Sb6 S7 S16 100.17(13) . . ? Sb5 S7 S16 109.90(14) . . ? Sb3 S7 S16 147.79(13) 1_545 . ? Tl2 S7 S16 53.50(9) . . ? S4 S7 S16 95.93(13) 1_545 . ? S2 S7 S16 68.85(11) . . ? S8 S7 S16 79.25(12) . . ? S5 S7 S16 163.88(15) 1_645 . ? S15 S7 S16 118.53(13) 1_545 . ? S10 S7 S16 62.67(10) . . ? Sb6 S8 Sb8 104.7(2) . . ? Sb6 S8 Pb8 102.1(3) . . ? Sb8 S8 Pb8 5.8(3) . . ? Sb6 S8 Pb 96.07(13) . 1_655 ? Sb8 S8 Pb 99.9(2) . 1_655 ? Pb8 S8 Pb 95.2(2) . 1_655 ? Sb6 S8 Tl1 104.04(13) . . ? Sb8 S8 Tl1 88.40(18) . . ? Pb8 S8 Tl1 94.0(2) . . ? Pb S8 Tl1 155.55(14) 1_655 . ? Sb6 S8 S3 143.39(16) . 1_655 ? Sb8 S8 S3 45.70(18) . 1_655 ? Pb8 S8 S3 50.3(2) . 1_655 ? Pb S8 S3 108.62(14) 1_655 1_655 ? Tl1 S8 S3 61.67(10) . 1_655 ? Sb6 S8 S10 44.71(9) . . ? Sb8 S8 S10 94.5(2) . . ? Pb8 S8 S10 96.2(3) . . ? Pb S8 S10 140.68(15) 1_655 . ? Tl1 S8 S10 60.12(9) . . ? S3 S8 S10 107.61(13) 1_655 . ? Sb6 S8 S7 43.63(9) . . ? Sb8 S8 S7 148.2(2) . . ? Pb8 S8 S7 145.7(3) . . ? Pb S8 S7 89.01(12) 1_655 . ? Tl1 S8 S7 95.95(12) . . ? S3 S8 S7 156.59(15) 1_655 . ? S10 S8 S7 61.60(11) . . ? Sb6 S8 S11 126.41(16) . 1_655 ? Sb8 S8 S11 117.7(2) . 1_655 ? Pb8 S8 S11 116.8(3) . 1_655 ? Pb S8 S11 47.68(8) 1_655 1_655 ? Tl1 S8 S11 108.15(12) . 1_655 ? S3 S8 S11 90.00(13) 1_655 1_655 ? S10 S8 S11 146.32(15) . 1_655 ? S7 S8 S11 90.93(13) . 1_655 ? Sb6 S8 Tl2 95.15(13) . . ? Sb8 S8 Tl2 157.6(2) . . ? Pb8 S8 Tl2 162.0(3) . . ? Pb S8 Tl2 87.95(10) 1_655 . ? Tl1 S8 Tl2 76.65(9) . . ? S3 S8 Tl2 111.92(12) 1_655 . ? S10 S8 Tl2 92.42(12) . . ? S7 S8 Tl2 51.82(9) . . ? S11 S8 Tl2 54.02(8) 1_655 . ? Sb6 S8 S16 128.74(15) . 1_655 ? Sb8 S8 S16 59.8(2) . 1_655 ? Pb8 S8 S16 57.3(3) . 1_655 ? Pb S8 S16 48.13(9) 1_655 1_655 ? Tl1 S8 S16 122.22(14) . 1_655 ? S3 S8 S16 61.86(12) 1_655 1_655 ? S10 S8 S16 152.78(14) . 1_655 ? S7 S8 S16 137.11(14) . 1_655 ? S11 S8 S16 60.89(10) 1_655 1_655 ? Tl2 S8 S16 114.73(11) . 1_655 ? Sb10 S9 Sb7 90.42(13) . . ? Sb10 S9 As9 172.83(16) . 1_545 ? Sb7 S9 As9 96.55(14) . 1_545 ? Sb10 S9 Sb9 172.83(16) . 1_545 ? Sb7 S9 Sb9 96.55(14) . 1_545 ? As9 S9 Sb9 0.00(7) 1_545 1_545 ? Sb10 S9 Sb4 93.89(14) . 2_655 ? Sb7 S9 Sb4 172.29(17) . 2_655 ? As9 S9 Sb4 79.37(9) 1_545 2_655 ? Sb9 S9 Sb4 79.37(9) 1_545 2_655 ? Sb10 S9 Tl2 98.92(13) . . ? Sb7 S9 Tl2 91.41(12) . . ? As9 S9 Tl2 79.30(10) 1_545 . ? Sb9 S9 Tl2 79.30(10) 1_545 . ? Sb4 S9 Tl2 94.23(10) 2_655 . ? Sb10 S9 S12 43.70(10) . . ? Sb7 S9 S12 47.26(10) . . ? As9 S9 S12 142.89(16) 1_545 . ? Sb9 S9 S12 142.89(16) 1_545 . ? Sb4 S9 S12 137.56(17) 2_655 . ? Tl2 S9 S12 91.89(11) . . ? Sb10 S9 S6 43.05(10) . . ? Sb7 S9 S6 98.89(13) . . ? As9 S9 S6 133.44(15) 1_545 . ? Sb9 S9 S6 133.44(15) 1_545 . ? Sb4 S9 S6 88.61(12) 2_655 . ? Tl2 S9 S6 56.75(9) . . ? S12 S9 S6 60.56(11) . . ? Sb10 S9 S11 146.11(15) . . ? Sb7 S9 S11 56.68(11) . . ? As9 S9 S11 41.06(9) 1_545 . ? Sb9 S9 S11 41.06(9) 1_545 . ? Sb4 S9 S11 117.93(13) 2_655 . ? Tl2 S9 S11 90.54(12) . . ? S12 S9 S11 103.94(14) . . ? S6 S9 S11 140.48(15) . . ? Sb10 S9 S16 98.28(13) . . ? Sb7 S9 S16 39.60(8) . . ? As9 S9 S16 86.13(12) 1_545 . ? Sb9 S9 S16 86.13(12) 1_545 . ? Sb4 S9 S16 145.32(14) 2_655 . ? Tl2 S9 S16 51.90(8) . . ? S12 S9 S16 61.11(11) . . ? S6 S9 S16 78.78(12) . . ? S11 S9 S16 62.66(11) . . ? Sb6 S10 Sb2 99.37(13) . . ? Sb6 S10 Sb3 100.78(13) . . ? Sb2 S10 Sb3 96.89(11) . . ? Sb6 S10 Tl1 99.95(12) . . ? Sb2 S10 Tl1 154.67(14) . . ? Sb3 S10 Tl1 95.43(12) . . ? Sb6 S10 S8 44.75(9) . . ? Sb2 S10 S8 143.70(15) . . ? Sb3 S10 S8 95.84(13) . . ? Tl1 S10 S8 55.95(9) . . ? Sb6 S10 S14 58.22(10) . . ? Sb2 S10 S14 41.98(8) . . ? Sb3 S10 S14 95.85(11) . . ? Tl1 S10 S14 157.02(12) . . ? S8 S10 S14 102.94(12) . . ? Sb6 S10 S7 42.70(8) . . ? Sb2 S10 S7 90.83(13) . . ? Sb3 S10 S7 143.48(13) . . ? Tl1 S10 S7 92.34(10) . . ? S8 S10 S7 60.03(11) . . ? S14 S10 S7 67.01(10) . . ? Sb6 S10 S1 58.51(9) . 1_655 ? Sb2 S10 S1 95.48(12) . 1_655 ? Sb3 S10 S1 43.00(8) . 1_655 ? Tl1 S10 S1 108.55(13) . 1_655 ? S8 S10 S1 71.83(11) . 1_655 ? S14 S10 S1 67.93(11) . 1_655 ? S7 S10 S1 100.85(11) . 1_655 ? Sb6 S10 S4 154.83(14) . . ? Sb2 S10 S4 61.53(10) . . ? Sb3 S10 S4 68.02(9) . . ? Tl1 S10 S4 103.45(11) . . ? S8 S10 S4 153.75(15) . . ? S14 S10 S4 99.33(12) . . ? S7 S10 S4 143.72(15) . . ? S1 S10 S4 104.57(11) 1_655 . ? Sb6 S10 S2 89.63(12) . . ? Sb2 S10 S2 43.46(9) . . ? Sb3 S10 S2 140.32(14) . . ? Tl1 S10 S2 120.56(11) . . ? S8 S10 S2 117.27(13) . . ? S14 S10 S2 57.61(10) . . ? S7 S10 S2 57.59(10) . . ? S1 S10 S2 125.52(13) 1_655 . ? S4 S10 S2 86.45(12) . . ? Sb6 S10 S16 96.44(12) . . ? Sb2 S10 S16 106.32(14) . . ? Sb3 S10 S16 148.34(15) . . ? Tl1 S10 S16 55.26(9) . . ? S8 S10 S16 78.09(11) . . ? S14 S10 S16 115.82(14) . . ? S7 S10 S16 58.73(9) . . ? S1 S10 S16 149.57(14) 1_655 . ? S4 S10 S16 104.43(12) . . ? S2 S10 S16 65.44(11) . . ? Sb6 S10 Pb8 141.8(2) . 1_455 ? Sb2 S10 Pb8 76.0(2) . 1_455 ? Sb3 S10 Pb8 117.4(2) . 1_455 ? Tl1 S10 Pb8 78.7(2) . 1_455 ? S8 S10 Pb8 126.3(2) . 1_455 ? S14 S10 Pb8 113.2(2) . 1_455 ? S7 S10 Pb8 99.1(2) . 1_455 ? S1 S10 Pb8 158.4(2) 1_655 1_455 ? S4 S10 Pb8 53.89(19) . 1_455 ? S2 S10 Pb8 60.6(2) . 1_455 ? S16 S10 Pb8 51.08(19) . 1_455 ? As9 S11 Sb9 0.00(6) 1_545 1_545 ? As9 S11 Pb 96.82(12) 1_545 . ? Sb9 S11 Pb 96.82(12) 1_545 . ? As9 S11 Sb4 91.56(12) 1_545 1_455 ? Sb9 S11 Sb4 91.56(12) 1_545 1_455 ? Pb S11 Sb4 167.70(15) . 1_455 ? As9 S11 Sb7 105.69(15) 1_545 . ? Sb9 S11 Sb7 105.69(15) 1_545 . ? Pb S11 Sb7 86.82(10) . . ? Sb4 S11 Sb7 82.24(11) 1_455 . ? As9 S11 S13 86.12(12) 1_545 1_445 ? Sb9 S11 S13 86.12(12) 1_545 1_445 ? Pb S11 S13 143.60(17) . 1_445 ? Sb4 S11 S13 45.77(9) 1_455 1_445 ? Sb7 S11 S13 127.43(14) . 1_445 ? As9 S11 Pb2 135.76(15) 1_545 1_455 ? Sb9 S11 Pb2 135.76(15) 1_545 1_455 ? Pb S11 Pb2 99.29(12) . 1_455 ? Sb4 S11 Pb2 80.65(9) 1_455 1_455 ? Sb7 S11 Pb2 116.08(11) . 1_455 ? S13 S11 Pb2 57.50(10) 1_445 1_455 ? As9 S11 Tl2 135.76(15) 1_545 1_455 ? Sb9 S11 Tl2 135.76(15) 1_545 1_455 ? Pb S11 Tl2 99.29(12) . 1_455 ? Sb4 S11 Tl2 80.65(9) 1_455 1_455 ? Sb7 S11 Tl2 116.08(11) . 1_455 ? S13 S11 Tl2 57.50(10) 1_445 1_455 ? Pb2 S11 Tl2 0.00(3) 1_455 1_455 ? As9 S11 S17 41.84(9) 1_545 1_545 ? Sb9 S11 S17 41.84(9) 1_545 1_545 ? Pb S11 S17 54.99(9) . 1_545 ? Sb4 S11 S17 132.52(14) 1_455 1_545 ? Sb7 S11 S17 99.68(14) . 1_545 ? S13 S11 S17 119.71(14) 1_445 1_545 ? Pb2 S11 S17 135.34(16) 1_455 1_545 ? Tl2 S11 S17 135.34(16) 1_455 1_545 ? As9 S11 S6 135.68(15) 1_545 1_455 ? Sb9 S11 S6 135.68(15) 1_545 1_455 ? Pb S11 S6 125.58(13) . 1_455 ? Sb4 S11 S6 44.54(8) 1_455 1_455 ? Sb7 S11 S6 68.69(10) . 1_455 ? S13 S11 S6 67.90(11) 1_445 1_455 ? Pb2 S11 S6 56.39(9) 1_455 1_455 ? Tl2 S11 S6 56.39(9) 1_455 1_455 ? S17 S11 S6 167.75(18) 1_545 1_455 ? As9 S11 S9 61.99(11) 1_545 . ? Sb9 S11 S9 61.99(11) 1_545 . ? Pb S11 S9 102.09(13) . . ? Sb4 S11 S9 73.96(11) 1_455 . ? Sb7 S11 S9 45.10(9) . . ? S13 S11 S9 111.05(14) 1_445 . ? Pb2 S11 S9 149.84(14) 1_455 . ? Tl2 S11 S9 149.84(14) 1_455 . ? S17 S11 S9 74.78(14) 1_545 . ? S6 S11 S9 93.68(14) 1_455 . ? As9 S11 S15 88.01(13) 1_545 1_445 ? Sb9 S11 S15 88.01(13) 1_545 1_445 ? Pb S11 S15 61.71(10) . 1_445 ? Sb4 S11 S15 127.85(14) 1_455 1_445 ? Sb7 S11 S15 147.24(13) . 1_445 ? S13 S11 S15 82.23(13) 1_445 1_445 ? Pb2 S11 S15 64.75(10) 1_455 1_445 ? Tl2 S11 S15 64.75(10) 1_455 1_445 ? S17 S11 S15 70.68(13) 1_545 1_445 ? S6 S11 S15 121.14(15) 1_455 1_445 ? S9 S11 S15 145.04(14) . 1_445 ? Sb10 S12 Sb7 90.94(13) . . ? Sb10 S12 Tl1 108.15(14) . . ? Sb7 S12 Tl1 97.98(13) . . ? Sb10 S12 Sb9 171.72(17) . . ? Sb7 S12 Sb9 94.06(13) . . ? Tl1 S12 Sb9 77.70(8) . . ? Sb10 S12 S9 44.18(10) . . ? Sb7 S12 S9 47.30(10) . . ? Tl1 S12 S9 103.29(12) . . ? Sb9 S12 S9 141.35(17) . . ? Sb10 S12 Sb4 98.94(14) . 2_665 ? Sb7 S12 Sb4 162.36(15) . 2_665 ? Tl1 S12 Sb4 92.80(10) . 2_665 ? Sb9 S12 Sb4 74.60(8) . 2_665 ? S9 S12 Sb4 142.70(15) . 2_665 ? Sb10 S12 S6 43.02(9) . . ? Sb7 S12 S6 98.92(13) . . ? Tl1 S12 S6 65.21(9) . . ? Sb9 S12 S6 141.96(13) . . ? S9 S12 S6 60.56(11) . . ? Sb4 S12 S6 98.26(13) 2_665 . ? Sb10 S12 S3 143.42(17) . . ? Sb7 S12 S3 53.80(10) . . ? Tl1 S12 S3 88.35(11) . . ? Sb9 S12 S3 40.42(8) . . ? S9 S12 S3 101.07(15) . . ? Sb4 S12 S3 112.97(12) 2_665 . ? S6 S12 S3 140.17(15) . . ? Sb10 S12 S16 100.51(14) . . ? Sb7 S12 S16 40.72(9) . . ? Tl1 S12 S16 57.34(9) . . ? Sb9 S12 S16 87.56(11) . . ? S9 S12 S16 63.11(12) . . ? Sb4 S12 S16 148.29(13) 2_665 . ? S6 S12 S16 79.71(12) . . ? S3 S12 S16 60.67(11) . . ? Sb10 S12 S6 58.40(11) . 2_665 ? Sb7 S12 S6 148.15(15) . 2_665 ? Tl1 S12 S6 99.74(13) . 2_665 ? Sb9 S12 S6 115.46(13) . 2_665 ? S9 S12 S6 102.58(14) . 2_665 ? Sb4 S12 S6 40.88(8) 2_665 2_665 ? S6 S12 S6 65.59(13) . 2_665 ? S3 S12 S6 152.43(15) . 2_665 ? S16 S12 S6 144.66(14) . 2_665 ? Sb4 S13 Sb4 93.95(13) 1_565 2_665 ? Sb4 S13 As10 95.74(13) 1_565 2_665 ? Sb4 S13 As10 83.23(10) 2_665 2_665 ? Sb4 S13 Sb10 95.74(13) 1_565 2_665 ? Sb4 S13 Sb10 83.23(10) 2_665 2_665 ? As10 S13 Sb10 0.00(4) 2_665 2_665 ? Sb4 S13 Pb2 90.80(11) 1_565 1_565 ? Sb4 S13 Pb2 114.25(14) 2_665 1_565 ? As10 S13 Pb2 160.91(13) 2_665 1_565 ? Sb10 S13 Pb2 160.91(13) 2_665 1_565 ? Sb4 S13 Tl2 90.80(11) 1_565 1_565 ? Sb4 S13 Tl2 114.25(14) 2_665 1_565 ? As10 S13 Tl2 160.91(13) 2_665 1_565 ? Sb10 S13 Tl2 160.91(13) 2_665 1_565 ? Pb2 S13 Tl2 0.00(4) 1_565 1_565 ? Sb4 S13 S11 58.42(11) 1_565 1_665 ? Sb4 S13 S11 150.76(17) 2_665 1_665 ? As10 S13 S11 107.13(13) 2_665 1_665 ? Sb10 S13 S11 107.13(13) 2_665 1_665 ? Pb2 S13 S11 61.59(9) 1_565 1_665 ? Tl2 S13 S11 61.59(9) 1_565 1_665 ? Sb4 S13 S13 47.39(11) 1_565 2_675 ? Sb4 S13 S13 46.56(9) 2_665 2_675 ? As10 S13 S13 89.19(15) 2_665 2_675 ? Sb10 S13 S13 89.19(15) 2_665 2_675 ? Pb2 S13 S13 108.25(15) 1_565 2_675 ? Tl2 S13 S13 108.25(15) 1_565 2_675 ? S11 S13 S13 105.23(18) 1_665 2_675 ? Sb4 S13 Tl1 157.63(14) 1_565 . ? Sb4 S13 Tl1 108.41(13) 2_665 . ? As10 S13 Tl1 87.00(9) 2_665 . ? Sb10 S13 Tl1 87.00(9) 2_665 . ? Pb2 S13 Tl1 80.32(9) 1_565 . ? Tl2 S13 Tl1 80.32(9) 1_565 . ? S11 S13 Tl1 99.53(12) 1_665 . ? S13 S13 Tl1 154.97(19) 2_675 . ? Sb4 S13 S3 105.00(15) 1_565 1_655 ? Sb4 S13 S3 140.75(14) 2_665 1_655 ? As10 S13 S3 61.24(9) 2_665 1_655 ? Sb10 S13 S3 61.24(9) 2_665 1_655 ? Pb2 S13 S3 99.75(11) 1_565 1_655 ? Tl2 S13 S3 99.75(11) 1_565 1_655 ? S11 S13 S3 63.41(11) 1_665 1_655 ? S13 S13 S3 139.4(2) 2_675 1_655 ? Tl1 S13 S3 57.13(9) . 1_655 ? Sb4 S13 S6 100.06(14) 1_565 2_665 ? Sb4 S13 S6 42.94(8) 2_665 2_665 ? As10 S13 S6 40.53(7) 2_665 2_665 ? Sb10 S13 S6 40.53(7) 2_665 2_665 ? Pb2 S13 S6 154.88(15) 1_565 2_665 ? Tl2 S13 S6 154.88(15) 1_565 2_665 ? S11 S13 S6 142.89(16) 1_665 2_665 ? S13 S13 S6 65.61(13) 2_675 2_665 ? Tl1 S13 S6 96.41(11) . 2_665 ? S3 S13 S6 99.19(12) 1_655 2_665 ? Sb4 S13 S9 86.78(12) 1_565 1_565 ? Sb4 S13 S9 59.18(10) 2_665 1_565 ? As10 S13 S9 142.40(13) 2_665 1_565 ? Sb10 S13 S9 142.40(13) 2_665 1_565 ? Pb2 S13 S9 55.71(9) 1_565 1_565 ? Tl2 S13 S9 55.71(9) 1_565 1_565 ? S11 S13 S9 106.02(13) 1_665 1_565 ? S13 S13 S9 65.24(13) 2_675 1_565 ? Tl1 S13 S9 104.51(13) . 1_565 ? S3 S13 S9 153.50(15) 1_655 1_565 ? S6 S13 S9 102.02(12) 2_665 1_565 ? Sb2 S14 Sb2 97.15(12) . 2_666 ? Sb2 S14 Sb5 89.11(11) . . ? Sb2 S14 Sb5 173.55(14) 2_666 . ? Sb2 S14 Sb6 87.41(12) . . ? Sb2 S14 Sb6 104.58(13) 2_666 . ? Sb5 S14 Sb6 77.16(9) . . ? Sb2 S14 Sb3 99.98(13) . 2_666 ? Sb2 S14 Sb3 83.42(9) 2_666 2_666 ? Sb5 S14 Sb3 94.00(11) . 2_666 ? Sb6 S14 Sb3 168.47(13) . 2_666 ? Sb2 S14 Sb5 153.97(16) . 2_656 ? Sb2 S14 Sb5 102.40(10) 2_666 2_656 ? Sb5 S14 Sb5 71.16(8) . 2_656 ? Sb6 S14 Sb5 103.89(10) . 2_656 ? Sb3 S14 Sb5 65.82(8) 2_666 2_656 ? Sb2 S14 S14 54.32(10) . 2_666 ? Sb2 S14 S14 42.82(8) 2_666 2_666 ? Sb5 S14 S14 143.41(17) . 2_666 ? Sb6 S14 S14 100.08(17) . 2_666 ? Sb3 S14 S14 91.43(14) 2_666 2_666 ? Sb5 S14 S14 142.31(16) 2_656 2_666 ? Sb2 S14 S2 47.07(9) . . ? Sb2 S14 S2 143.20(13) 2_666 . ? Sb5 S14 S2 42.68(7) . . ? Sb6 S14 S2 84.87(11) . . ? Sb3 S14 S2 93.66(12) 2_666 . ? Sb5 S14 S2 109.78(12) 2_656 . ? S14 S14 S2 100.89(14) 2_666 . ? Sb2 S14 S10 45.14(9) . . ? Sb2 S14 S10 99.01(13) 2_666 . ? Sb5 S14 S10 86.49(10) . . ? Sb6 S14 S10 42.96(8) . . ? Sb3 S14 S10 145.12(13) 2_666 . ? Sb5 S14 S10 144.66(12) 2_656 . ? S14 S14 S10 69.21(13) 2_666 . ? S2 S14 S10 63.72(11) . . ? Sb2 S14 S4 155.00(15) . 2_666 ? Sb2 S14 S4 61.48(9) 2_666 2_666 ? Sb5 S14 S4 112.07(12) . 2_666 ? Sb6 S14 S4 109.51(12) . 2_666 ? Sb3 S14 S4 66.67(10) 2_666 2_666 ? Sb5 S14 S4 41.07(7) 2_656 2_666 ? S14 S14 S4 103.29(14) 2_666 2_666 ? S2 S14 S4 148.94(15) . 2_666 ? S10 S14 S4 144.28(15) . 2_666 ? Sb2 S14 As1 144.55(16) . 2_666 ? Sb2 S14 As1 63.91(7) 2_666 2_666 ? Sb5 S14 As1 111.49(10) . 2_666 ? Sb6 S14 As1 70.58(8) . 2_666 ? Sb3 S14 As1 106.66(10) 2_666 2_666 ? Sb5 S14 As1 61.09(6) 2_656 2_666 ? S14 S14 As1 101.42(14) 2_666 2_666 ? S2 S14 As1 149.24(12) . 2_666 ? S10 S14 As1 105.50(12) . 2_666 ? S4 S14 As1 40.02(8) 2_666 2_666 ? Sb2 S14 Sb1 144.55(16) . 2_666 ? Sb2 S14 Sb1 63.91(7) 2_666 2_666 ? Sb5 S14 Sb1 111.49(10) . 2_666 ? Sb6 S14 Sb1 70.58(8) . 2_666 ? Sb3 S14 Sb1 106.66(10) 2_666 2_666 ? Sb5 S14 Sb1 61.09(6) 2_656 2_666 ? S14 S14 Sb1 101.42(14) 2_666 2_666 ? S2 S14 Sb1 149.24(12) . 2_666 ? S10 S14 Sb1 105.50(12) . 2_666 ? S4 S14 Sb1 40.02(8) 2_666 2_666 ? As1 S14 Sb1 0.00(4) 2_666 2_666 ? Sb3 S15 Sb8 108.8(2) . . ? Sb3 S15 Pb8 106.8(3) . . ? Sb8 S15 Pb8 7.9(2) . . ? Sb3 S15 Pb 111.66(13) . 1_665 ? Sb8 S15 Pb 96.69(19) . 1_665 ? Pb8 S15 Pb 90.6(3) . 1_665 ? Sb3 S15 S3 146.83(18) . 1_655 ? Sb8 S15 S3 46.52(18) . 1_655 ? Pb8 S15 S3 51.9(2) . 1_655 ? Pb S15 S3 95.18(14) 1_665 1_655 ? Sb3 S15 Tl1 101.91(15) . . ? Sb8 S15 Tl1 84.40(14) . . ? Pb8 S15 Tl1 92.3(2) . . ? Pb S15 Tl1 143.87(13) 1_665 . ? S3 S15 Tl1 59.79(10) 1_655 . ? Sb3 S15 S11 148.64(16) . 1_665 ? Sb8 S15 S11 98.3(2) . 1_665 ? Pb8 S15 S11 98.0(3) . 1_665 ? Pb S15 S11 48.04(8) 1_665 1_665 ? S3 S15 S11 64.46(12) 1_655 1_665 ? Tl1 S15 S11 95.95(11) . 1_665 ? Sb3 S15 S1 43.31(9) . 1_655 ? Sb8 S15 S1 66.8(2) . 1_655 ? Pb8 S15 S1 63.7(3) . 1_655 ? Pb S15 S1 106.18(12) 1_665 1_655 ? S3 S15 S1 111.84(13) 1_655 1_655 ? Tl1 S15 S1 107.34(13) . 1_655 ? S11 S15 S1 150.35(15) 1_665 1_655 ? Sb3 S15 S7 58.05(10) . 1_565 ? Sb8 S15 S7 165.7(2) . 1_565 ? Pb8 S15 S7 159.9(3) . 1_565 ? Pb S15 S7 84.25(11) 1_665 1_565 ? S3 S15 S7 147.79(15) 1_655 1_565 ? Tl1 S15 S7 103.31(12) . 1_565 ? S11 S15 S7 92.96(13) 1_665 1_565 ? S1 S15 S7 99.09(13) 1_655 1_565 ? Sb3 S15 Pb2 105.18(12) . 1_565 ? Sb8 S15 Pb2 142.8(2) . 1_565 ? Pb8 S15 Pb2 147.2(3) . 1_565 ? Pb S15 Pb2 84.25(9) 1_665 1_565 ? S3 S15 Pb2 96.28(11) 1_655 1_565 ? Tl1 S15 Pb2 74.16(8) . 1_565 ? S11 S15 Pb2 55.40(9) 1_665 1_565 ? S1 S15 Pb2 148.49(14) 1_655 1_565 ? S7 S15 Pb2 51.55(8) 1_565 1_565 ? Sb3 S15 Tl2 105.18(12) . 1_565 ? Sb8 S15 Tl2 142.8(2) . 1_565 ? Pb8 S15 Tl2 147.2(3) . 1_565 ? Pb S15 Tl2 84.25(9) 1_665 1_565 ? S3 S15 Tl2 96.28(11) 1_655 1_565 ? Tl1 S15 Tl2 74.16(8) . 1_565 ? S11 S15 Tl2 55.40(9) 1_665 1_565 ? S1 S15 Tl2 148.49(14) 1_655 1_565 ? S7 S15 Tl2 51.55(8) 1_565 1_565 ? Pb2 S15 Tl2 0.00(3) 1_565 1_565 ? Sb3 S15 S10 48.61(10) . . ? Sb8 S15 S10 89.2(2) . . ? Pb8 S15 S10 93.2(3) . . ? Pb S15 S10 160.09(13) 1_665 . ? S3 S15 S10 102.56(14) 1_655 . ? Tl1 S15 S10 55.51(9) . . ? S11 S15 S10 149.80(14) 1_665 . ? S1 S15 S10 58.82(10) 1_655 . ? S7 S15 S10 85.47(12) 1_565 . ? Pb2 S15 S10 102.49(11) 1_565 . ? Tl2 S15 S10 102.49(11) 1_565 . ? Sb7 S16 Pb 98.72(13) . . ? Sb7 S16 Tl2 99.45(13) . . ? Pb S16 Tl2 92.25(11) . . ? Sb7 S16 Pb8 97.14(18) . 1_455 ? Pb S16 Pb8 91.1(3) . 1_455 ? Tl2 S16 Pb8 162.37(17) . 1_455 ? Sb7 S16 Sb8 91.08(14) . 1_455 ? Pb S16 Sb8 88.76(18) . 1_455 ? Tl2 S16 Sb8 169.13(14) . 1_455 ? Pb8 S16 Sb8 6.89(16) 1_455 1_455 ? Sb7 S16 Tl1 99.48(14) . . ? Pb S16 Tl1 161.78(13) . . ? Tl2 S16 Tl1 84.11(11) . . ? Pb8 S16 Tl1 87.3(2) 1_455 . ? Sb8 S16 Tl1 91.56(15) 1_455 . ? Sb7 S16 S7 150.91(15) . . ? Pb S16 S7 70.41(11) . . ? Tl2 S16 S7 55.67(9) . . ? Pb8 S16 S7 109.6(2) 1_455 . ? Sb8 S16 S7 114.85(16) 1_455 . ? Tl1 S16 S7 93.05(11) . . ? Sb7 S16 S12 43.85(10) . . ? Pb S16 S12 142.42(14) . . ? Tl2 S16 S12 91.50(12) . . ? Pb8 S16 S12 96.4(2) 1_455 . ? Sb8 S16 S12 94.30(18) 1_455 . ? Tl1 S16 S12 55.71(9) . . ? S7 S16 S12 138.66(15) . . ? Sb7 S16 S3 53.03(9) . . ? Pb S16 S3 105.29(14) . . ? Tl2 S16 S3 148.75(15) . . ? Pb8 S16 S3 45.17(18) 1_455 . ? Sb8 S16 S3 40.11(13) 1_455 . ? Tl1 S16 S3 86.33(11) . . ? S7 S16 S3 154.81(15) . . ? S12 S16 S3 58.89(11) . . ? Sb7 S16 S9 42.64(9) . . ? Pb S16 S9 96.33(12) . . ? Tl2 S16 S9 56.92(9) . . ? Pb8 S16 S9 139.74(19) 1_455 . ? Sb8 S16 S9 133.71(15) 1_455 . ? Tl1 S16 S9 96.57(13) . . ? S7 S16 S9 110.13(13) . . ? S12 S16 S9 55.78(11) . . ? S3 S16 S9 94.93(12) . . ? Sb7 S16 S8 77.18(12) . 1_455 ? Pb S16 S8 52.73(10) . 1_455 ? Tl2 S16 S8 142.82(14) . 1_455 ? Pb8 S16 S8 47.83(19) 1_455 1_455 ? Sb8 S16 S8 42.47(13) 1_455 1_455 ? Tl1 S16 S8 133.07(13) . 1_455 ? S7 S16 S8 112.51(14) . 1_455 ? S12 S16 S8 108.79(13) . 1_455 ? S3 S16 S8 53.88(11) . 1_455 ? S9 S16 S8 109.29(12) . 1_455 ? Sb9 S17 Pb 93.07(13) . 1_565 ? Sb9 S17 Pb8 91.0(2) . 1_455 ? Pb S17 Pb8 90.6(3) 1_565 1_455 ? Sb9 S17 Pb2 97.05(17) . 1_565 ? Pb S17 Pb2 89.03(12) 1_565 1_565 ? Pb8 S17 Pb2 171.9(2) 1_455 1_565 ? Sb9 S17 Tl2 97.05(17) . 1_565 ? Pb S17 Tl2 89.03(12) 1_565 1_565 ? Pb8 S17 Tl2 171.9(2) 1_455 1_565 ? Pb2 S17 Tl2 0.00(4) 1_565 1_565 ? Sb9 S17 Tl1 96.37(13) . . ? Pb S17 Tl1 169.74(16) 1_565 . ? Pb8 S17 Tl1 93.3(2) 1_455 . ? Pb2 S17 Tl1 85.84(13) 1_565 . ? Tl2 S17 Tl1 85.84(13) 1_565 . ? Sb9 S17 Sb8 84.72(17) . 1_455 ? Pb S17 Sb8 89.62(19) 1_565 1_455 ? Pb8 S17 Sb8 6.4(2) 1_455 1_455 ? Pb2 S17 Sb8 177.83(19) 1_565 1_455 ? Tl2 S17 Sb8 177.83(19) 1_565 1_455 ? Tl1 S17 Sb8 95.22(18) . 1_455 ? Sb9 S17 S4 139.0(2) . . ? Pb S17 S4 58.71(10) 1_565 . ? Pb8 S17 S4 62.9(2) 1_455 . ? Pb2 S17 S4 110.26(14) 1_565 . ? Tl2 S17 S4 110.26(14) 1_565 . ? Tl1 S17 S4 115.02(14) . . ? Sb8 S17 S4 67.58(16) 1_455 . ? Sb9 S17 S11 42.66(9) . 1_565 ? Pb S17 S11 50.43(9) 1_565 1_565 ? Pb8 S17 S11 92.2(2) 1_455 1_565 ? Pb2 S17 S11 93.78(14) 1_565 1_565 ? Tl2 S17 S11 93.78(14) 1_565 1_565 ? Tl1 S17 S11 138.76(15) . 1_565 ? Sb8 S17 S11 86.67(17) 1_455 1_565 ? S4 S17 S11 103.78(14) . 1_565 ? Sb9 S17 S3 43.66(11) . . ? Pb S17 S3 98.04(14) 1_565 . ? Pb8 S17 S3 47.84(18) 1_455 . ? Pb2 S17 S3 140.13(16) 1_565 . ? Tl2 S17 S3 140.13(16) 1_565 . ? Tl1 S17 S3 91.58(12) . . ? Sb8 S17 S3 41.81(13) 1_455 . ? S4 S17 S3 106.81(17) . . ? S11 S17 S3 63.16(11) 1_565 . ? Sb9 S17 S7 141.38(19) . 1_565 ? Pb S17 S7 66.11(10) 1_565 1_565 ? Pb8 S17 S7 119.8(2) 1_455 1_565 ? Pb2 S17 S7 52.92(9) 1_565 1_565 ? Tl2 S17 S7 52.92(9) 1_565 1_565 ? Tl1 S17 S7 103.80(13) . 1_565 ? Sb8 S17 S7 124.94(18) 1_455 1_565 ? S4 S17 S7 57.49(11) . 1_565 ? S11 S17 S7 108.63(13) 1_565 1_565 ? S3 S17 S7 161.52(17) . 1_565 ? _diffrn_measured_fraction_theta_max 0.908 _diffrn_reflns_theta_full 32.18 _diffrn_measured_fraction_theta_full 0.908 _diffrn_measured_details ; the lower than ideal value is due to data collection by rotation around to the spindle axis only (standard on the image-plate system at the beamline XRD1) ; _refine_diff_density_max 1.560 _refine_diff_density_min -1.718 _refine_diff_density_rms 0.293