# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_billwiseite _shelx_title ' wsbtantm in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 1518.10 _exptl_crystal_F_000 2609.72 _reflns_d_resolution_high 0.7106 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 54.1160 _cell_length_b 4.9143 _cell_length_c 5.5482 _cell_angle_alpha 90.000 _cell_angle_beta 90.425 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2230.07 1.68 3.22 o 6 0 0 5288.86 5959.46 596.66 o 8 0 0 19828.24 18913.71 1109.39 o 10 0 0 51460.38 51476.53 2329.38 o 12 0 0 3021.66 3256.43 349.57 o 14 0 0 42.63 1920.34 501.91 o 16 0 0 9445.67 8093.81 587.08 o 18 0 0 2304635.00 1906241.50 62721.00 o 20 0 0 28098.63 26709.22 595.00 o 22 0 0 4221.78 5600.28 312.55 o 24 0 0 3447.87 3588.30 262.46 o 26 0 0 4254.86 3710.64 182.80 o 28 0 0 63041.91 67479.02 1699.52 o 30 0 0 668.43 957.61 149.62 o 32 0 0 2465.54 3012.02 261.16 o 34 0 0 25743.69 24112.78 1508.49 o 36 0 0 1237988.63 1292605.63 29975.91 o 38 0 0 48892.25 50419.70 1289.64 o 40 0 0 4708.44 5827.69 323.42 o 42 0 0 1978.20 3120.42 260.74 o 44 0 0 1325.35 1694.81 205.41 o 46 0 0 1895.78 2686.51 371.45 o 48 0 0 59.44 392.35 134.35 o 50 0 0 5909.76 6899.97 768.10 o 52 0 0 37105.55 36683.57 1093.68 o 54 0 0 650233.06 666214.50 13524.42 o 56 0 0 79297.48 80595.38 2688.70 o 58 0 0 4142.46 5873.97 569.81 o 60 0 0 658.55 1329.40 309.07 o 62 0 0 150.92 411.18 234.23 o 64 0 0 30644.29 29003.75 1660.75 o 66 0 0 2207.68 2647.92 418.83 o 68 0 0 6810.47 8733.08 589.31 o 70 0 0 27943.90 28397.15 1346.56 o 72 0 0 270863.16 260847.33 7451.27 o 74 0 0 61979.26 66576.16 3199.86 o 76 0 0 1478.82 4336.82 1833.66 o 1 1 0 58.40 616.89 33.47 o 3 1 0 1603.26 1573.62 344.53 o 5 1 0 131738.61 139851.22 10285.40 o 7 1 0 2720.33 2538.57 148.62 o 9 1 0 2919.24 1089.87 104.87 o 11 1 0 5829.94 4990.60 426.23 o 13 1 0 110654.80 114386.56 4258.85 o 15 1 0 14483.26 13139.47 1137.71 o 17 1 0 799.81 1106.28 83.31 o 19 1 0 130.92 759.95 60.03 o 21 1 0 60.83 483.85 56.30 o 23 1 0 12490.15 18301.12 4424.77 o 25 1 0 995.97 1393.78 116.64 o 27 1 0 1150.99 1093.65 123.69 o 29 1 0 2552.63 2568.67 386.62 o 31 1 0 32815.25 35588.17 1188.98 o 33 1 0 9965.40 9662.78 974.32 o 35 1 0 389.21 583.27 76.15 o 37 1 0 333.03 864.37 91.94 o 39 1 0 701.02 857.04 197.50 o 41 1 0 32784.38 32596.18 7525.00 o 43 1 0 429.55 498.24 87.55 o 45 1 0 363.53 810.20 109.37 o 47 1 0 1400.47 1691.72 332.66 o 49 1 0 13512.20 13166.87 387.17 o 51 1 0 8323.81 8287.01 615.28 o 53 1 0 467.71 618.26 108.16 o 55 1 0 305.20 818.14 124.26 o 57 1 0 1428.89 1595.58 218.35 o 59 1 0 16785.98 19146.46 3272.06 o 61 1 0 2444.19 2249.55 199.96 o 63 1 0 192.24 503.78 124.09 o 65 1 0 805.50 1357.89 317.95 o 67 1 0 7035.72 6764.84 390.55 o 69 1 0 1882.03 1908.77 287.59 o 71 1 0 914.25 874.87 174.18 o 73 1 0 120.44 752.62 194.80 o 75 1 0 299.37 675.60 181.31 o 0 2 0 1292563.88 1307949.75 23141.58 o 2 2 0 312.77 865.22 140.63 o 4 2 0 573.81 2171.64 269.50 o 6 2 0 2082.14 2389.09 102.69 o 8 2 0 11495.83 9525.13 297.51 o 10 2 0 15497.63 12681.75 334.28 o 12 2 0 538.96 622.97 79.84 o 14 2 0 533.64 1665.92 120.35 o 16 2 0 9899.32 8576.74 585.62 o 18 2 0 1626710.00 1606080.38 28426.80 o 20 2 0 22849.58 22056.56 1329.22 o 22 2 0 4169.20 6422.98 326.59 o 24 2 0 4214.84 4808.09 222.64 o 26 2 0 9513.57 8890.35 519.22 o 28 2 0 44808.82 44389.30 706.06 o 30 2 0 41.46 178.38 48.14 o 32 2 0 3250.16 4716.39 307.66 o 34 2 0 28944.00 26090.11 725.42 o 36 2 0 1021804.63 1069102.50 15104.18 o 38 2 0 71830.56 72465.38 1919.57 o 40 2 0 6139.58 8491.46 464.04 o 42 2 0 3083.42 3673.78 211.09 o 44 2 0 1313.89 2631.64 316.51 o 46 2 0 103904.56 111571.13 1841.99 o 48 2 0 1292.10 1499.75 153.16 o 50 2 0 4702.67 7188.14 376.06 o 52 2 0 27165.54 27609.38 775.97 o 54 2 0 471232.59 493664.25 10693.08 o 56 2 0 79167.24 80839.29 3114.64 o 58 2 0 4491.29 7086.38 467.57 o 60 2 0 1576.76 2221.22 237.88 o 62 2 0 178.80 780.95 194.51 o 64 2 0 35820.62 35858.98 953.20 o 66 2 0 1329.46 2134.24 249.70 o 68 2 0 5216.79 6770.69 404.59 o 70 2 0 21499.18 21451.99 708.72 o 72 2 0 209277.97 205042.89 6112.34 o 1 3 0 124.04 362.21 65.14 o 3 3 0 1402.41 1011.36 73.51 o 5 3 0 273674.84 302001.91 10272.52 o 7 3 0 984.70 1136.06 181.52 o 9 3 0 1960.17 1809.44 122.36 o 11 3 0 2562.70 3035.63 300.44 o 13 3 0 155252.81 157655.11 6770.64 o 15 3 0 521.78 580.40 77.55 o 17 3 0 110.52 481.43 75.04 o 19 3 0 10.42 443.65 64.37 o 21 3 0 392.60 621.58 71.99 o 23 3 0 256122.94 277256.91 14942.27 o 25 3 0 268.95 513.12 74.15 o 27 3 0 1652.21 1793.60 119.59 o 29 3 0 4979.15 5701.45 350.33 o 31 3 0 111744.27 117222.07 6084.72 o 33 3 0 2016.61 2109.66 210.69 o 35 3 0 349.68 774.88 105.09 o 37 3 0 340.85 790.55 104.04 o 39 3 0 1895.03 2349.74 162.57 o 41 3 0 111260.32 127227.39 9677.39 o 43 3 0 1246.01 1110.22 131.99 o 45 3 0 1273.56 1902.25 178.11 o 47 3 0 5905.99 6881.39 680.67 o 49 3 0 68678.58 68157.93 2806.47 o 51 3 0 15324.33 15575.82 612.65 o 53 3 0 424.27 1000.47 191.96 o 55 3 0 396.14 969.40 187.21 o 57 3 0 1766.19 2718.87 287.70 o 59 3 0 39928.09 43587.79 6983.47 o 61 3 0 420.29 622.71 175.19 o 63 3 0 1027.84 1662.85 254.37 o 65 3 0 4185.76 4814.99 511.63 o 67 3 0 27748.30 28659.88 1593.19 o 0 4 0 554002.88 589798.50 12057.55 o 2 4 0 1332.44 2119.83 471.16 o 4 4 0 3094.24 4285.40 353.25 o 6 4 0 9283.35 8896.45 409.93 o 8 4 0 90825.38 91788.62 1529.12 o 10 4 0 143209.94 144446.42 2278.80 o 12 4 0 5861.12 5302.05 255.36 o 14 4 0 492.45 1679.55 332.42 o 16 4 0 1149.10 1428.31 226.31 o 18 4 0 530907.00 563837.94 8149.74 o 20 4 0 10953.50 11295.32 1143.89 o 22 4 0 5309.76 6477.17 459.48 o 24 4 0 6301.85 7173.86 356.82 o 26 4 0 28021.01 29905.97 994.78 o 28 4 0 80124.59 85781.73 1794.79 o 30 4 0 1332.21 1491.38 138.62 o 32 4 0 24.66 1173.87 125.77 o 34 4 0 4399.44 4995.00 390.09 o 36 4 0 286628.59 304542.63 8591.81 o 38 4 0 12660.41 15212.37 1305.10 o 40 4 0 4578.61 6686.40 291.70 o 42 4 0 4128.62 6245.33 287.74 o 44 4 0 9411.10 11326.63 388.13 o 46 4 0 93199.28 98049.22 2105.84 o 48 4 0 56.95 337.62 141.36 o 50 4 0 761.90 2148.72 364.21 o 52 4 0 6931.04 7038.71 417.60 o 54 4 0 164426.19 167288.72 10507.48 o 56 4 0 15780.31 16496.84 2063.35 o 58 4 0 3352.76 4189.25 483.10 o 60 4 0 2206.89 3103.48 528.67 o 62 4 0 1337.78 2561.49 826.35 o 1 5 0 15.64 374.56 91.47 o 3 5 0 428.37 946.33 132.73 o 5 5 0 125093.36 130900.36 8624.93 o 7 5 0 652.09 723.00 190.32 o 9 5 0 1760.23 2019.19 174.80 o 11 5 0 3506.25 3805.72 313.28 o 13 5 0 192668.67 189474.91 12031.66 o 15 5 0 3212.49 3954.71 476.52 o 17 5 0 599.71 1246.78 168.18 o 19 5 0 364.16 709.42 107.53 o 21 5 0 2306.90 3339.45 337.19 o 23 5 0 150009.30 160468.64 10191.88 o 25 5 0 34.14 371.29 99.42 o 27 5 0 1794.71 2211.08 254.76 o 29 5 0 6331.53 6429.16 404.67 o 31 5 0 142815.09 146748.73 7018.28 o 33 5 0 9340.29 10108.75 1085.07 o 35 5 0 1133.64 1912.43 317.77 o 37 5 0 613.78 1347.07 217.89 o 39 5 0 3308.61 4472.53 407.16 o 41 5 0 65244.17 68206.91 5786.71 o 43 5 0 542.16 840.43 248.97 o 45 5 0 1630.77 2089.33 356.50 o 47 5 0 4807.00 4622.70 555.86 o 49 5 0 72777.09 83047.32 2693.37 o 51 5 0 579.75 1722.75 463.44 o 0 6 0 98431.91 97113.77 2767.92 o 2 6 0 531.84 864.16 156.75 o 4 6 0 2598.27 2895.14 230.67 o 6 6 0 6623.08 7077.76 373.27 o 8 6 0 72447.16 72364.23 2552.34 o 10 6 0 105482.31 104417.00 2845.45 o 12 6 0 4906.53 4803.94 385.87 o 14 6 0 1468.29 2191.33 360.03 o 16 6 0 13.33 325.45 130.67 o 18 6 0 53969.31 53664.49 1246.14 o 20 6 0 2761.91 3383.68 303.38 o 22 6 0 3486.96 4866.13 466.20 o 24 6 0 8339.92 9076.50 427.45 o 26 6 0 45427.12 49100.55 1186.68 o 28 6 0 173780.48 178849.53 6376.32 o 30 6 0 1621.11 1915.14 269.77 o 32 6 0 319.18 1262.34 288.19 o 34 6 0 338.84 453.48 203.90 o 36 6 0 64204.50 69589.55 2080.50 o -73 1 1 1572.24 2367.96 254.67 o -71 1 1 1336.46 1259.92 171.38 o -69 1 1 21810.85 21879.06 613.86 o -67 1 1 44022.07 43098.63 945.19 o -65 1 1 100258.92 90970.52 1645.37 o -63 1 1 204646.06 213990.63 6684.58 o -61 1 1 6078.67 13540.19 766.97 o -59 1 1 157429.89 144714.08 3518.73 o -57 1 1 8866.92 8233.77 361.91 o -55 1 1 3706.83 5336.10 315.30 o -53 1 1 2858.41 2466.99 236.03 o -51 1 1 23221.42 24363.89 591.53 o -49 1 1 102307.33 97149.48 1644.94 o -47 1 1 96847.16 82723.18 1435.29 o -45 1 1 489290.31 508733.75 15020.99 o -43 1 1 9210.96 12589.19 411.07 o -41 1 1 204219.19 195155.38 3880.79 o -39 1 1 2765.91 2833.35 170.90 o -37 1 1 3087.39 3315.04 202.16 o -35 1 1 4513.28 4105.15 250.12 o -33 1 1 37551.81 37293.00 654.87 o -31 1 1 237245.16 234381.72 3686.20 o -29 1 1 96184.16 83198.53 2512.52 o -27 1 1 1124112.50 1155877.13 16261.25 o -25 1 1 8353.07 10481.44 239.05 o -23 1 1 376107.59 382271.16 4838.91 o -21 1 1 1038.66 1500.67 107.11 o -19 1 1 1839.42 3330.93 199.31 o -17 1 1 2409.70 3191.79 240.99 o -15 1 1 6659.25 5641.75 150.66 o -13 1 1 279961.44 273774.16 3718.19 o -11 1 1 29190.38 24477.67 1411.86 o -9 1 1 1718431.50 1507396.25 24099.81 o -7 1 1 5154.65 3823.40 144.29 o -5 1 1 508912.44 506826.22 6691.52 o -3 1 1 6084.28 5198.20 122.86 o -1 1 1 3116.78 2592.11 160.03 o 1 1 1 1768.06 2129.51 299.31 o 3 1 1 3323.87 2736.92 164.55 o 5 1 1 507920.72 512601.13 7036.75 o 7 1 1 2715.85 2317.72 393.83 o 9 1 1 1763961.50 1577547.00 20705.61 o 11 1 1 3174.77 8297.72 508.68 o 13 1 1 239259.52 243739.89 3265.05 o 15 1 1 8158.25 7147.24 345.66 o 17 1 1 768.42 1495.18 68.76 o 19 1 1 2887.13 4365.23 413.95 o 21 1 1 365.13 985.94 87.44 o 23 1 1 292893.25 326102.38 4142.76 o 25 1 1 19616.07 19454.20 800.47 o 27 1 1 1346846.25 1342416.25 16965.97 o 29 1 1 12138.49 24217.39 551.20 o 31 1 1 168229.88 182792.75 2427.56 o 33 1 1 45298.29 45262.90 1309.27 o 35 1 1 1077.06 2221.67 112.84 o 37 1 1 1946.27 2510.07 219.15 o 39 1 1 1131.32 1775.13 125.18 o 41 1 1 134871.13 158010.81 2968.03 o 43 1 1 34201.79 31204.95 1507.53 o 45 1 1 643989.25 617077.00 16383.82 o 47 1 1 17881.10 28545.29 1940.01 o 49 1 1 67324.13 69292.49 1235.31 o 51 1 1 26995.51 25876.06 912.63 o 53 1 1 489.09 971.72 159.47 o 55 1 1 7042.42 6406.34 408.41 o 57 1 1 2379.09 3054.76 256.86 o 59 1 1 90288.25 99091.38 3030.83 o 61 1 1 52590.28 45597.70 2627.80 o 63 1 1 319996.09 292133.66 6350.54 o 65 1 1 28163.89 38065.33 2798.44 o 67 1 1 25307.57 25625.50 1118.16 o 69 1 1 25340.72 24252.22 876.20 o 71 1 1 240.18 422.66 163.97 o 73 1 1 4209.45 4115.81 394.07 o -72 2 1 546.24 1194.53 259.46 o -70 2 1 2268.67 2658.07 339.79 o -68 2 1 19610.08 20584.83 3064.78 o -66 2 1 294.89 1233.83 167.04 o -64 2 1 5706.52 6539.54 597.21 o -62 2 1 5965.87 6649.00 335.23 o -60 2 1 15023.74 14881.19 509.68 o -58 2 1 16587.14 17982.60 673.32 o -56 2 1 902.78 2190.29 192.72 o -54 2 1 1811.99 2014.36 468.91 o -52 2 1 409.78 637.18 113.38 o -50 2 1 28952.85 32095.53 4424.94 o -48 2 1 352.49 837.13 124.78 o -46 2 1 2044.89 3163.28 548.94 o -44 2 1 7391.09 7555.23 413.40 o -42 2 1 9065.45 7808.35 307.51 o -40 2 1 51171.53 51750.29 900.62 o -38 2 1 5596.15 6158.52 629.81 o -36 2 1 1446.21 3287.28 327.86 o -34 2 1 1483.82 1510.30 149.41 o -32 2 1 98854.58 103996.29 7484.58 o -30 2 1 210.43 637.39 73.69 o -28 2 1 2352.18 3473.91 604.81 o -26 2 1 18571.45 17001.02 901.37 o -24 2 1 28361.39 25109.24 451.59 o -22 2 1 98404.09 106266.20 2603.72 o -20 2 1 2308.91 3419.69 332.00 o -18 2 1 13947.85 11172.12 1637.73 o -16 2 1 2149.55 2268.45 125.82 o -14 2 1 174705.39 176903.53 6834.55 o -12 2 1 815.41 1128.39 157.59 o -10 2 1 44987.64 47679.50 2603.81 o -8 2 1 6788.68 6521.04 760.12 o -6 2 1 7867.46 6323.00 256.66 o -4 2 1 80139.63 75953.90 4552.96 o -2 2 1 3287.31 2922.20 390.51 o 0 2 1 808.77 1668.60 314.33 o 2 2 1 878.30 1053.41 121.96 o 4 2 1 88339.74 84613.98 4515.93 o 6 2 1 6324.17 5450.66 260.95 o 8 2 1 5441.04 5984.36 810.66 o 10 2 1 50228.64 52270.84 3313.88 o 12 2 1 6229.95 5586.37 182.86 o 14 2 1 139221.34 146909.27 6877.39 o 16 2 1 342.61 561.94 69.06 o 18 2 1 2565.49 5358.81 664.85 o 20 2 1 9678.66 8824.35 211.70 o 22 2 1 135913.58 134851.33 3749.13 o 24 2 1 9844.55 11192.03 383.28 o 26 2 1 7947.17 9900.14 711.77 o 28 2 1 981.35 2822.26 492.72 o 30 2 1 442.48 834.80 85.78 o 32 2 1 103439.25 104253.84 7218.22 o 34 2 1 241.08 585.75 73.53 o 36 2 1 7149.06 6844.24 1029.42 o 38 2 1 1929.71 3003.55 241.42 o 40 2 1 58457.68 57840.21 987.31 o 42 2 1 2032.80 3292.19 206.68 o 44 2 1 3302.07 4233.56 273.26 o 46 2 1 1449.71 2692.63 808.10 o 48 2 1 245.85 493.07 123.55 o 50 2 1 25548.00 28199.09 3722.26 o 52 2 1 784.96 915.22 162.30 o 54 2 1 352.27 1087.38 170.89 o 56 2 1 8427.72 8130.62 562.14 o 58 2 1 27597.38 26991.62 768.21 o 60 2 1 4906.23 6402.65 521.86 o 62 2 1 2915.72 3532.53 291.50 o 64 2 1 2857.70 4118.33 574.89 o 66 2 1 2707.54 3103.21 490.15 o 68 2 1 21254.98 23062.80 3009.71 o 70 2 1 2193.09 1751.26 272.62 o 72 2 1 81.09 522.11 184.58 o -67 3 1 28874.32 28939.63 1172.63 o -65 3 1 42457.40 39823.75 1630.21 o -63 3 1 122332.43 118132.30 6765.82 o -61 3 1 3767.31 5698.47 398.67 o -59 3 1 76090.20 74969.26 1739.88 o -57 3 1 1632.72 1785.46 249.41 o -55 3 1 18280.46 17998.84 656.17 o -53 3 1 385.84 1116.88 196.53 o -51 3 1 29183.78 30766.75 890.54 o -49 3 1 71841.78 71490.41 1459.31 o -47 3 1 62328.67 60438.88 3683.96 o -45 3 1 243048.41 255079.30 9187.95 o -43 3 1 3393.17 5754.43 272.65 o -41 3 1 191959.67 191860.70 2970.76 o -39 3 1 1564.00 1720.76 180.24 o -37 3 1 22911.98 22787.39 629.81 o -35 3 1 613.91 1611.27 140.09 o -33 3 1 7096.02 8606.45 283.24 o -31 3 1 115752.22 111927.72 2277.31 o -29 3 1 38024.67 35617.43 2820.94 o -27 3 1 360748.47 386942.72 7417.98 o -25 3 1 5670.13 5341.51 193.17 o -23 3 1 188246.28 193325.02 2734.12 o -21 3 1 3283.42 2838.61 177.29 o -19 3 1 61730.73 56165.88 1001.52 o -17 3 1 2192.75 4439.03 455.77 o -15 3 1 20286.14 20567.19 534.76 o -13 3 1 285967.81 291765.78 4224.72 o -11 3 1 28208.79 26335.76 2558.91 o -9 3 1 671794.75 717263.13 10153.13 o -7 3 1 3688.52 3404.45 198.61 o -5 3 1 158250.00 164381.33 2324.71 o -3 3 1 8358.51 7062.00 405.77 o -1 3 1 18560.16 15597.88 490.13 o 1 3 1 4103.33 4408.93 485.70 o 3 3 1 3782.90 3664.49 177.81 o 5 3 1 161247.89 170612.20 5053.87 o 7 3 1 418.86 2206.28 148.71 o 9 3 1 749865.06 764184.25 9577.72 o 11 3 1 3302.27 5743.86 663.84 o 13 3 1 231468.63 239530.44 3333.92 o 15 3 1 43038.32 38925.66 1341.85 o 17 3 1 18415.88 15508.06 614.85 o 19 3 1 30336.06 31203.58 908.96 o 21 3 1 1634.68 1874.67 117.21 o 23 3 1 178707.00 183408.34 7871.10 o 25 3 1 2623.83 4050.94 524.45 o 27 3 1 426296.59 445809.91 5713.80 o 29 3 1 5518.24 10515.11 839.82 o 31 3 1 78731.31 83000.42 1787.19 o 33 3 1 18664.74 18704.50 1043.67 o 35 3 1 5269.33 5916.29 586.13 o 37 3 1 17217.02 19340.79 539.11 o 39 3 1 334.15 615.38 124.61 o 41 3 1 145719.78 163530.03 4806.03 o 43 3 1 21405.90 18928.62 778.66 o 45 3 1 339773.31 335701.59 7329.69 o 47 3 1 12057.37 18853.58 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