data_kol _publ_requested_journal 'Canadian Mineralogist' _publ_contact_author_name 'Fernando Camara' _publ_contact_author_address 'Dipartimento di Scienze della Terra - Via Valperga Caluso, 35 - 10125 Torino' _publ_contact_author_email feranando.camaraartigas@unito.it _publ_contact_author_phone '+390116705132 ' _publ_contact_author_fax '+390112365132 ' loop_ _publ_author_name _publ_author_address 'Fernando Camara' 'Dipartimento di Scienze della Terra - Via Valperga Caluso, 35 - 10125 Torino' 'Elena Sokolova' 'Department of Geological Sciences, University of Manitoba, Winnipeg, Manitoba R3T 2N2, Canada' 'Yassir A. Abdu' 'Department of Geological Sciences, University of Manitoba, Winnipeg, Manitoba R3T 2N2, Canada' 'Frank C. Hawthorne' 'Department of Geological Sciences, University of Manitoba, Winnipeg, Manitoba R3T 2N2, Canada' 'Alexander P. Khomyakov' 'Institute of Mineralogy, Geochemistry and Crystal Chemistry of Rare Elements, Veresaev Street 15, Moscow 121357, Russia' _audit_creation_method SHELXL-97 _chemical_name_systematic kolskyite _chemical_name_common kolskyite _chemical_formula_moiety ? _chemical_formula_sum 'H6.80 Ba0.09 Ca0.35 F0.17 Fe0.05 K0.08 Mg0.09 Mn0.19 Na0.96 Nb0.23 O12.34 Si2 ' _chemical_melting_point ? _exptl_crystal_description 'flake' _exptl_crystal_colour 'pinkish yellow' _diffrn_ambient_temperature 293(2) _chemical_formula_weight 442.46 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ti Ti 0.2776 0.4457 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Nb Nb -2.0727 0.6215 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sr Sr -1.5307 3.2498 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ba Ba -0.3244 2.2819 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zr Zr -2.9673 0.5597 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting triclinic _symmetry_space_group_name_H-M 'P -1' _symmetry_int_tables_number 2 _symmetry_space_group_name_Hall 'P 1' _chemical_absolute_configuration ? loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 5.3874(11) _cell_length_b 7.0906(14) _cell_length_c 15.473(3) _cell_angle_alpha 96.580(4) _cell_angle_beta 93.948(4) _cell_angle_gamma 89.818(4) _cell_volume 585.8(2) _cell_formula_units_Z 2 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 3802 _cell_measurement_theta_min 5.313 _cell_measurement_theta_max 59.994 _exptl_crystal_size_max 0.30 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.02 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 2.509 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 433 _exptl_absorpt_coefficient_mu 3.303 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.581 _exptl_absorpt_correction_T_max 0.936 _exptl_absorpt_process_details ; SADABS - Bruker Nonius area detector scaling and absorption correction - V2.10) Settings for parameter refinement: Maximum resolution = 0.1000 A (Intensity/sigma) threshold = 3.000 Restraint esd for equal adjacent scale factors = 0.0050 Maximum odd and even orders for spherical harmonics = 3 6 6050 Reflections employed for parameter determination Effective data to parameter ratio = 1.06 R(int) = 0.0364 (selected reflections only, after parameter refinement) Ratio of minimum to maximum apparent transmission: 0.325441 ; _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker AXS SMART-APEX diifractometer' _diffrn_measurement_method 'area scan' _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 7038 _diffrn_reflns_av_R_equivalents 0.0396 _diffrn_reflns_av_sigmaI/netI 0.0478 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_theta_min 2.66 _diffrn_reflns_theta_max 27.50 _reflns_number_total 2667 _reflns_number_gt 2424 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0545P)^2^+12.1266P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens none _refine_ls_hydrogen_treatment none _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 2667 _refine_ls_number_parameters 214 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0952 _refine_ls_R_factor_gt 0.0880 _refine_ls_wR_factor_ref 0.2083 _refine_ls_wR_factor_gt 0.2051 _refine_ls_goodness_of_fit_ref 1.284 _refine_ls_restrained_S_all 1.284 _refine_ls_shift/su_max 0.069 _refine_ls_shift/su_mean 0.010 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group M1 Nb 0.2267(3) 0.38225(19) 0.49412(10) 0.0188(5) Uani 0.599(6) 1 d P . . M2 Na 0.2412(7) 0.8823(5) 0.4941(3) 0.0240(13) Uani 1.08(2) 1 d P . . MH Nb 0.0568(2) 0.09422(18) 0.29925(15) 0.0143(6) Uani 0.628(8) 1 d P . . Si1 Si 0.5703(4) 0.8111(3) 0.33161(16) 0.0113(6) Uani 1 1 d . . . Si2 Si 0.5537(4) 0.3788(3) 0.32064(16) 0.0100(5) Uani 1 1 d . . . AP Sr 0.0384(4) 0.5778(3) 0.2204(2) 0.0347(10) Uani 0.531(7) 1 d P . . BPW O 0.5321(14) 0.0508(12) 0.1609(6) 0.0202(16) Uani 0.55 1 d P . . BPCA Ca 0.5321(14) 0.0508(12) 0.1609(6) 0.0202(16) Uani 0.10 1 d P . . W3 O 0.528(4) 0.042(3) 0.1190(17) 0.022(5) Uiso 0.35 1 d P . . O1 O 0.6028(14) 0.8164(10) 0.4354(5) 0.0249(16) Uani 1 1 d . . . O2 O 0.5558(13) 0.5904(9) 0.2885(5) 0.0209(15) Uani 1 1 d . . . O3 O 0.3130(14) 0.9019(11) 0.2994(5) 0.0300(18) Uani 1 1 d . . . O4 O 0.2996(12) 0.2830(9) 0.2760(5) 0.0208(15) Uani 1 1 d . . . O5 O 0.8099(14) 0.8977(11) 0.2937(5) 0.0292(17) Uani 1 1 d . . . O6 O 0.5547(12) 0.3991(9) 0.4261(4) 0.0152(13) Uani 1 1 d . . . O7 O 0.7949(13) 0.2764(10) 0.2810(5) 0.0225(15) Uani 1 1 d . . . XOM O 0.0840(13) 0.1614(11) 0.4179(4) 0.0240(15) Uani 1 1 d . . . XOA O 0.0542(12) 0.5825(8) 0.4329(4) 0.0147(13) Uani 1 1 d . . . XPM O 0.0323(17) 0.0338(12) 0.1600(6) 0.037(2) Uani 1 1 d . . . XPA1 O 0.832(11) 0.336(8) 0.091(4) 0.043(13) Uiso 0.16 1 d P . . XPA2 O 0.250(12) 0.692(9) 0.088(4) 0.048(15) Uiso 0.16 1 d P . . XPA3 O 0.754(13) 0.711(9) 0.093(4) 0.049(15) Uiso 0.16 1 d P . . XPA4 O 0.236(12) 0.340(9) 0.086(4) 0.050(15) Uiso 0.16 1 d P . . XPB O 0.568(15) 0.717(11) 0.094(5) 0.063(18) Uiso 0.16 1 d P . . W1 O 0.153(6) 0.993(5) 0.001(2) 0.047(8) Uiso 0.30 1 d P . . W2 O 0.714(3) 0.500(2) -0.0023(11) 0.039(4) Uiso 0.50 1 d P . . MHA Nb 0.031(9) 0.081(7) 0.254(5) 0.020 Uiso 0.021(4) 1 d P . . 1 Ba 0.817(5) 0.114(3) 0.0964(16) 0.020 Uiso 0.0236(17) 1 d P . . 2 Ba 0.220(5) 0.116(4) 0.0961(17) 0.020 Uiso 0.0219(17) 1 d P . . 3 Ba 0.222(5) 0.940(3) 0.0951(16) 0.020 Uiso 0.0235(17) 1 d P . . 4 Ba 0.815(4) 0.942(3) 0.0978(14) 0.020 Uiso 0.0265(17) 1 d P . . 5 Ba 0.0495(17) 0.5882(13) 0.2747(8) 0.020 Uiso 0.068(2) 1 d P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 M1 0.0203(8) 0.0140(7) 0.0222(8) 0.0022(5) 0.0016(6) -0.0029(5) M2 0.018(2) 0.0154(19) 0.038(3) -0.0040(15) 0.0110(16) -0.0056(14) MH 0.0075(6) 0.0103(6) 0.0249(14) 0.0015(5) 0.0007(5) 0.0004(4) Si1 0.0093(11) 0.0071(10) 0.0177(12) 0.0024(8) 0.0014(9) -0.0008(8) Si2 0.0081(11) 0.0046(10) 0.0170(12) -0.0014(8) 0.0024(8) 0.0000(8) AP 0.0178(10) 0.0196(10) 0.066(2) 0.0000(10) 0.0046(10) 0.0010(7) BPW 0.012(4) 0.027(4) 0.021(4) 0.000(3) 0.003(3) -0.002(3) BPCA 0.012(4) 0.027(4) 0.021(4) 0.000(3) 0.003(3) -0.002(3) O1 0.024(4) 0.028(4) 0.022(4) 0.001(3) 0.002(3) 0.002(3) O2 0.026(4) 0.009(3) 0.027(4) 0.001(3) -0.003(3) -0.001(3) O3 0.020(4) 0.028(4) 0.040(5) 0.000(3) -0.005(3) 0.016(3) O4 0.017(3) 0.020(3) 0.025(4) 0.003(3) -0.006(3) -0.012(3) O5 0.024(4) 0.026(4) 0.040(4) 0.008(3) 0.006(3) -0.016(3) O6 0.014(3) 0.017(3) 0.014(3) -0.001(2) -0.001(2) 0.002(2) O7 0.016(3) 0.026(4) 0.025(4) 0.003(3) 0.001(3) 0.011(3) XOM 0.019(3) 0.036(4) 0.016(3) 0.001(3) 0.000(3) 0.007(3) XOA 0.015(3) 0.009(3) 0.020(3) 0.002(2) 0.001(2) -0.001(2) XPM 0.042(5) 0.033(4) 0.036(5) 0.000(4) 0.003(4) -0.005(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag M1 XOA 1.948(6) 2_566 ? M1 XOM 1.973(8) . ? M1 XOA 1.989(6) . ? M1 O1 2.055(8) 2_666 ? M1 O6 2.128(6) . ? M1 O6 2.165(6) 2_666 ? M1 M1 2.959(3) 2_566 ? M1 M2 3.174(4) 2_566 ? M1 M2 3.426(4) 2_666 ? M1 M2 3.546(4) 1_545 ? M1 M2 3.547(4) . ? M1 5 3.905(12) . ? M2 O1 2.232(8) . ? M2 XOM 2.334(8) 2_566 ? M2 O1 2.410(8) 2_676 ? M2 XOA 2.419(7) . ? M2 XOM 2.532(8) 1_565 ? M2 O6 2.660(7) 2_666 ? M2 M2 3.089(7) 2_576 ? M2 Si1 3.168(4) . ? M2 M1 3.174(4) 2_566 ? M2 M2 3.238(7) 2_676 ? M2 Si1 3.365(4) 2_676 ? M2 M1 3.426(4) 2_666 ? MH MHA 0.69(8) . ? MH XOM 1.839(7) . ? MH O5 1.920(7) 1_445 ? MH O3 1.937(7) 1_545 ? MH O7 1.938(7) 1_455 ? MH O4 1.954(6) . ? MH XPM 2.142(9) . ? MH 1 3.33(2) 1_455 ? MH 2 3.34(3) . ? MH 4 3.36(2) 1_445 ? MH 3 3.40(2) 1_545 ? MH BPCA 3.419(9) 1_455 ? Si1 O3 1.599(7) . ? Si1 O1 1.600(7) . ? Si1 O5 1.606(7) . ? Si1 O2 1.629(7) . ? Si1 5 3.147(10) 1_655 ? Si1 5 3.243(10) . ? Si1 BPCA 3.295(10) 1_565 ? Si1 BPW 3.295(10) 1_565 ? Si1 M2 3.365(4) 2_676 ? Si1 AP 3.460(3) 1_655 ? Si1 AP 3.551(3) . ? Si2 O4 1.606(7) . ? Si2 O7 1.610(7) . ? Si2 O6 1.622(7) . ? Si2 O2 1.634(7) . ? Si2 5 3.168(9) . ? Si2 BPW 3.190(9) . ? Si2 5 3.221(9) 1_655 ? Si2 AP 3.462(3) . ? Si2 AP 3.507(3) 1_655 ? AP 5 0.833(11) . ? AP XPA2 2.62(6) . ? AP XPA1 2.66(6) 1_455 ? AP XPA3 2.67(7) 1_455 ? AP O4 2.706(7) . ? AP O5 2.744(8) 1_455 ? AP XPA4 2.79(6) . ? AP O7 2.796(8) 1_455 ? AP O3 2.844(8) . ? AP O2 2.869(8) 1_455 ? AP O2 2.909(7) . ? AP XOA 3.280(7) . ? BPW W3 0.64(2) . ? BPW 1 1.97(3) . ? BPW 4 1.97(2) 1_545 ? BPW 2 1.98(3) . ? BPW 3 2.01(3) 1_545 ? BPW XPB 2.49(8) 1_545 ? BPW O7 2.643(11) . ? BPW O4 2.660(11) . ? BPW XPM 2.695(12) . ? BPW XPM 2.698(12) 1_655 ? BPW O5 2.778(12) 1_545 ? BPW XPA3 2.81(7) 1_545 ? BPW O3 2.824(12) 1_545 ? BPW XPA4 2.89(7) . ? BPW XPA1 2.94(6) . ? BPW MHA 2.96(6) 1_655 ? BPW XPA2 3.03(6) 1_545 ? BPW W1 3.09(3) 1_545 ? BPW W1 3.11(3) 2_665 ? BPW MHA 3.15(5) . ? W3 1 1.71(3) . ? W3 4 1.73(3) 1_545 ? W3 2 1.76(3) . ? W3 3 1.80(3) 1_545 ? W3 XPB 2.31(8) 1_545 ? W3 W1 2.61(4) 2_665 ? W3 W1 2.63(4) 1_545 ? W3 XPA3 2.65(7) 1_545 ? W3 XPA4 2.70(7) . ? W3 XPA1 2.75(6) . ? W3 XPM 2.75(3) 1_655 ? W3 XPM 2.79(2) . ? W3 XPA2 2.88(7) 1_545 ? W3 O7 3.11(3) . ? W3 O4 3.13(3) . ? W3 MHA 3.30(7) 1_655 ? W3 MHA 3.50(6) . ? W3 W3 3.65(5) 2_655 ? O1 M1 2.055(8) 2_666 ? O1 M2 2.410(8) 2_676 ? O2 5 2.683(12) 1_655 ? O2 5 2.721(11) . ? O2 AP 2.869(8) 1_655 ? O3 MH 1.937(7) 1_565 ? O3 MHA 2.11(6) 1_565 ? O3 5 2.619(12) . ? O3 XPM 2.795(12) 1_565 ? O3 BPCA 2.824(12) 1_565 ? O3 BPW 2.824(12) 1_565 ? O3 3 3.21(3) . ? O4 MHA 2.03(5) . ? O4 5 2.547(11) . ? O4 XPM 2.711(11) . ? O4 2 2.90(3) . ? O4 XPA4 3.00(6) . ? O5 MH 1.920(7) 1_665 ? O5 MHA 1.94(5) 1_665 ? O5 5 2.541(12) 1_655 ? O5 XPM 2.728(11) 1_665 ? O5 AP 2.744(8) 1_655 ? O5 BPCA 2.778(12) 1_565 ? O5 BPW 2.778(12) 1_565 ? O5 4 3.08(2) . ? O6 M1 2.165(6) 2_666 ? O6 M2 2.660(7) 2_666 ? O7 MHA 1.91(5) 1_655 ? O7 MH 1.938(7) 1_655 ? O7 5 2.621(12) 1_655 ? O7 XPM 2.771(11) 1_655 ? O7 AP 2.796(8) 1_655 ? O7 1 2.96(3) . ? O7 XPA1 3.04(6) . ? XOM M2 2.333(8) 2_566 ? XOM MHA 2.53(8) . ? XOM M2 2.532(8) 1_545 ? XOA M1 1.948(6) 2_566 ? XOA 5 2.452(14) . ? XPM MHA 1.46(8) . ? XPM 4 1.56(2) 1_445 ? XPM 3 1.58(3) 1_545 ? XPM 1 1.61(3) 1_455 ? XPM 2 1.62(3) . ? XPM W1 2.58(3) 1_545 ? XPM W1 2.60(3) 2_565 ? XPM XPA1 2.69(6) 1_455 ? XPM BPCA 2.698(12) 1_455 ? XPM BPW 2.698(12) 1_455 ? XPM O5 2.728(11) 1_445 ? XPM W3 2.75(3) 1_455 ? XPM O7 2.771(11) 1_455 ? XPM O3 2.795(12) 1_545 ? XPM XPA3 2.80(7) 1_445 ? XPA1 1 1.59(6) . ? XPA1 W2 2.02(6) . ? XPA1 XPA4 2.18(9) 1_655 ? XPA1 W1 2.59(7) 2_665 ? XPA1 2 2.61(7) 1_655 ? XPA1 AP 2.66(6) 1_655 ? XPA1 XPA3 2.69(9) . ? XPA1 XPM 2.69(6) 1_655 ? XPA1 XPA2 2.76(9) 2_665 ? XPA1 4 2.81(6) 1_545 ? XPA1 XPB 3.04(10) . ? XPA1 W2 3.17(6) 2_765 ? XPA1 XPA4 3.21(9) . ? XPA1 W1 3.22(7) 1_645 ? XPA1 3 3.29(6) 2_665 ? XPA1 5 3.32(6) 1_655 ? XPA2 XPB 1.71(10) . ? XPA2 3 1.75(7) . ? XPA2 W2 1.81(7) 2_665 ? XPA2 XPA4 2.49(9) . ? XPA2 W1 2.69(7) . ? XPA2 XPA3 2.69(9) 1_455 ? XPA2 XPA3 2.71(9) . ? XPA2 XPA1 2.76(9) 2_665 ? XPA2 XPM 2.84(6) 1_565 ? XPA2 W3 2.88(7) 1_565 ? XPA2 4 2.94(7) 1_455 ? XPA2 2 3.00(7) 1_565 ? XPA2 BPW 3.03(6) 1_565 ? XPA2 BPCA 3.03(6) 1_565 ? XPA2 W2 3.17(7) . ? XPA2 1 3.30(7) 2_665 ? XPA2 5 3.31(6) . ? XPA2 W2 3.35(7) 1_455 ? XPA2 XPA1 3.40(9) 1_455 ? XPA3 XPB 1.00(9) . ? XPA3 4 1.67(7) . ? XPA3 W2 1.98(7) . ? XPA3 W3 2.65(7) 1_565 ? XPA3 AP 2.67(7) 1_655 ? XPA3 XPA2 2.69(9) 1_655 ? XPA3 W1 2.75(7) 2_675 ? XPA3 XPA4 2.76(9) 2_665 ? XPA3 XPM 2.80(7) 1_665 ? XPA3 BPCA 2.81(7) 1_565 ? XPA3 BPW 2.81(7) 1_565 ? XPA3 1 2.88(7) 1_565 ? XPA3 3 3.00(7) 1_655 ? XPA3 W2 3.10(7) 2_665 ? XPA3 3 3.29(7) . ? XPA3 2 3.31(7) 2_665 ? XPA3 5 3.34(7) 1_655 ? XPA3 W1 3.43(7) 1_655 ? XPA4 2 1.61(7) . ? XPA4 W2 1.86(7) 2_665 ? XPA4 XPA1 2.18(9) 1_455 ? XPA4 W1 2.68(7) 1_545 ? XPA4 XPA3 2.76(9) 2_665 ? XPA4 1 2.79(7) 1_455 ? XPA4 3 2.86(7) 1_545 ? XPA4 XPB 3.04(10) 2_665 ? XPA4 XPB 3.20(10) . ? XPA4 W2 3.27(7) . ? XPA4 W1 3.27(7) 2_565 ? XPA4 4 3.29(7) 2_665 ? XPB 4 2.08(8) . ? XPB W2 2.20(8) . ? XPB W3 2.31(8) 1_565 ? XPB W2 2.43(8) 2_665 ? XPB 3 2.44(8) . ? XPB BPCA 2.49(8) 1_565 ? XPB BPW 2.49(8) 1_565 ? XPB XPA4 3.04(10) 2_665 ? XPB W1 3.11(8) 2_675 ? XPB 1 3.12(8) 1_565 ? XPB AP 3.31(8) 1_655 ? XPB W1 3.34(8) . ? XPB XPM 3.39(8) 1_665 ? XPB 2 3.39(8) 1_565 ? XPB XPA1 3.45(10) 2_665 ? XPB 2 3.56(8) 2_665 ? W1 3 1.57(4) . ? W1 1 1.62(4) 2_665 ? W1 2 1.64(4) 1_565 ? W1 W1 1.65(7) 2_575 ? W1 4 1.66(4) 2_675 ? W1 4 2.49(4) 1_455 ? W1 2 2.49(4) 2_565 ? W1 3 2.50(4) 2_575 ? W1 1 2.50(4) 1_465 ? W1 XPM 2.58(3) 1_565 ? W1 XPA1 2.59(7) 2_665 ? W1 XPM 2.60(3) 2_565 ? W1 W3 2.61(4) 2_665 ? W1 W3 2.63(4) 1_565 ? W1 XPA4 2.68(7) 1_565 ? W1 XPA3 2.75(7) 2_675 ? W1 BPW 3.09(3) 1_565 ? W1 BPCA 3.09(3) 1_565 ? W1 BPW 3.11(3) 2_665 ? W2 XPA2 1.81(7) 2_665 ? W2 XPA4 1.86(7) 2_665 ? W2 W2 2.31(4) 2_665 ? W2 XPB 2.43(8) 2_665 ? W2 W2 3.08(4) 2_765 ? W2 XPA3 3.10(7) 2_665 ? W2 XPA1 3.17(6) 2_765 ? W2 2 3.26(3) 2_665 ? W2 XPA4 3.30(7) 1_655 ? W2 3 3.30(3) 2_665 ? W2 1 3.31(3) . ? W2 XPA2 3.35(7) 1_655 ? W2 4 3.36(3) . ? W2 XPA1 3.42(6) 2_665 ? W2 XPA3 3.53(7) 2_765 ? MHA O7 1.91(5) 1_455 ? MHA O5 1.94(5) 1_445 ? MHA O3 2.11(6) 1_545 ? MHA 1 2.66(8) 1_455 ? MHA 4 2.70(8) 1_445 ? MHA 2 2.76(8) . ? MHA 3 2.81(8) 1_545 ? MHA BPCA 2.96(6) 1_455 ? 1 4 1.22(3) 1_545 ? 1 XPM 1.61(3) 1_655 ? 1 W1 1.62(4) 2_665 ? 1 2 2.17(4) 1_655 ? 1 W1 2.50(4) 1_645 ? 1 3 2.50(3) 1_645 ? 1 MHA 2.66(8) 1_655 ? 1 XPA4 2.79(7) 1_655 ? 2 3 1.25(4) 1_545 ? 2 W1 1.64(4) 1_545 ? 2 1 2.17(4) 1_455 ? 2 W1 2.49(4) 2_565 ? 2 4 2.52(3) 1_445 ? 2 XPA1 2.61(7) 1_455 ? 3 2 1.25(4) 1_565 ? 3 XPM 1.58(3) 1_565 ? 3 W3 1.80(3) 1_565 ? 3 BPCA 2.01(3) 1_565 ? 3 BPW 2.01(3) 1_565 ? 3 4 2.20(3) 1_455 ? 3 W1 2.50(4) 2_575 ? 3 1 2.50(3) 1_465 ? 3 MHA 2.81(8) 1_565 ? 4 1 1.22(3) 1_565 ? 4 XPM 1.56(2) 1_665 ? 4 W1 1.66(4) 2_675 ? 4 W3 1.73(3) 1_565 ? 4 BPCA 1.97(2) 1_565 ? 4 BPW 1.97(2) 1_565 ? 4 3 2.20(3) 1_655 ? 4 W1 2.49(4) 1_655 ? 4 2 2.52(3) 1_665 ? 4 MHA 2.70(8) 1_665 ? 5 O5 2.541(12) 1_455 ? 5 O7 2.621(12) 1_455 ? 5 O2 2.683(11) 1_455 ? 5 Si1 3.147(10) 1_455 ? 5 Si2 3.221(9) 1_455 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag XOA M1 XOM 95.6(3) 2_566 . ? XOA M1 XOA 82.5(3) 2_566 . ? XOM M1 XOA 97.2(3) . . ? XOA M1 O1 94.5(3) 2_566 2_666 ? XOM M1 O1 85.0(3) . 2_666 ? XOA M1 O1 176.4(3) . 2_666 ? XOA M1 O6 168.5(3) 2_566 . ? XOM M1 O6 95.5(3) . . ? XOA M1 O6 93.2(3) . . ? O1 M1 O6 89.4(3) 2_666 . ? XOA M1 O6 92.8(2) 2_566 2_666 ? XOM M1 O6 170.0(3) . 2_666 ? XOA M1 O6 89.2(3) . 2_666 ? O1 M1 O6 89.0(3) 2_666 2_666 ? O6 M1 O6 76.4(3) . 2_666 ? XOA M1 M1 41.79(18) 2_566 2_566 ? XOM M1 M1 98.6(2) . 2_566 ? XOA M1 M1 40.76(18) . 2_566 ? O1 M1 M1 136.2(2) 2_666 2_566 ? O6 M1 M1 133.07(19) . 2_566 ? O6 M1 M1 91.30(18) 2_666 2_566 ? XOA M1 M2 49.57(19) 2_566 2_566 ? XOM M1 M2 47.1(2) . 2_566 ? XOA M1 M2 98.0(2) . 2_566 ? O1 M1 M2 81.4(2) 2_666 2_566 ? O6 M1 M2 141.87(19) . 2_566 ? O6 M1 M2 139.68(19) 2_666 2_566 ? M1 M1 M2 70.55(9) 2_566 2_566 ? XOA M1 M2 133.1(2) 2_566 2_666 ? XOM M1 M2 85.5(2) . 2_666 ? XOA M1 M2 144.0(2) . 2_666 ? O1 M1 M2 38.7(2) 2_666 2_666 ? O6 M1 M2 50.92(18) . 2_666 ? O6 M1 M2 84.78(18) 2_666 2_666 ? M1 M1 M2 173.48(11) 2_566 2_666 ? M2 M1 M2 109.35(11) 2_566 2_666 ? XOA M1 M2 94.44(19) 2_566 1_545 ? XOM M1 M2 44.1(2) . 1_545 ? XOA M1 M2 140.9(2) . 1_545 ? O1 M1 M2 41.1(2) 2_666 1_545 ? O6 M1 M2 95.54(18) . 1_545 ? O6 M1 M2 129.89(19) 2_666 1_545 ? M1 M1 M2 124.94(9) 2_566 1_545 ? M2 M1 M2 54.39(11) 2_566 1_545 ? M2 M1 M2 55.32(10) 2_666 1_545 ? XOA M1 M2 87.62(19) 2_566 . ? XOM M1 M2 137.2(2) . . ? XOA M1 M2 40.78(19) . . ? O1 M1 M2 137.4(2) 2_666 . ? O6 M1 M2 82.28(18) . . ? O6 M1 M2 48.43(18) 2_666 . ? M1 M1 M2 57.57(7) 2_566 . ? M2 M1 M2 128.12(7) 2_566 . ? M2 M1 M2 122.17(7) 2_666 . ? M2 M1 M2 177.48(12) 1_545 . ? XOA M1 5 108.4(2) 2_566 . ? XOM M1 5 76.6(3) . . ? XOA M1 5 31.8(2) . . ? O1 M1 5 151.8(3) 2_666 . ? O6 M1 5 71.5(2) . . ? O6 M1 5 105.8(2) 2_666 . ? M1 M1 5 68.71(15) 2_566 . ? M2 M1 5 100.66(16) 2_566 . ? M2 M1 5 117.37(16) 2_666 . ? M2 M1 5 118.47(17) 1_545 . ? M2 M1 5 62.06(16) . . ? O1 M2 XOM 156.0(3) . 2_566 ? O1 M2 O1 91.6(3) . 2_676 ? XOM M2 O1 99.2(3) 2_566 2_676 ? O1 M2 XOA 93.5(3) . . ? XOM M2 XOA 75.4(3) 2_566 . ? O1 M2 XOA 174.6(3) 2_676 . ? O1 M2 XOM 102.7(3) . 1_565 ? XOM M2 XOM 101.3(3) 2_566 1_565 ? O1 M2 XOM 66.8(3) 2_676 1_565 ? XOA M2 XOM 113.5(3) . 1_565 ? O1 M2 O6 73.3(3) . 2_666 ? XOM M2 O6 82.8(3) 2_566 2_666 ? O1 M2 O6 110.0(3) 2_676 2_666 ? XOA M2 O6 70.0(2) . 2_666 ? XOM M2 O6 175.1(3) 1_565 2_666 ? O1 M2 M2 150.5(3) . 2_576 ? XOM M2 M2 53.5(2) 2_566 2_576 ? O1 M2 M2 78.4(2) 2_676 2_576 ? XOA M2 M2 97.9(2) . 2_576 ? XOM M2 M2 47.80(19) 1_565 2_576 ? O6 M2 M2 136.2(2) 2_666 2_576 ? O1 M2 Si1 28.2(2) . . ? XOM M2 Si1 157.9(2) 2_566 . ? O1 M2 Si1 102.3(2) 2_676 . ? XOA M2 Si1 83.02(18) . . ? XOM M2 Si1 83.01(19) 1_565 . ? O6 M2 Si1 94.23(17) 2_666 . ? M2 M2 Si1 126.9(2) 2_576 . ? O1 M2 M1 130.2(2) . 2_566 ? XOM M2 M1 38.29(19) 2_566 2_566 ? O1 M2 M1 136.8(2) 2_676 2_566 ? XOA M2 M1 37.81(16) . 2_566 ? XOM M2 M1 106.6(2) 1_565 2_566 ? O6 M2 M1 78.31(17) 2_666 2_566 ? M2 M2 M1 68.94(12) 2_576 2_566 ? Si1 M2 M1 119.65(12) . 2_566 ? O1 M2 M2 48.1(2) . 2_676 ? XOM M2 M2 138.5(3) 2_566 2_676 ? O1 M2 M2 43.54(19) 2_676 2_676 ? XOA M2 M2 141.6(2) . 2_676 ? XOM M2 M2 81.9(2) 1_565 2_676 ? O6 M2 M2 93.3(2) 2_666 2_676 ? M2 M2 M2 116.7(2) 2_576 2_676 ? Si1 M2 M2 63.35(12) . 2_676 ? M1 M2 M2 171.1(2) 2_566 2_676 ? O1 M2 Si1 100.8(2) . 2_676 ? XOM M2 Si1 81.3(2) 2_566 2_676 ? O1 M2 Si1 26.06(18) 2_676 2_676 ? XOA M2 Si1 150.2(2) . 2_676 ? XOM M2 Si1 88.75(19) 1_565 2_676 ? O6 M2 Si1 89.20(18) 2_666 2_676 ? M2 M2 Si1 82.39(14) 2_576 2_676 ? Si1 M2 Si1 120.66(11) . 2_676 ? M1 M2 Si1 119.02(12) 2_566 2_676 ? M2 M2 Si1 57.31(12) 2_676 2_676 ? O1 M2 M1 35.2(2) . 2_666 ? XOM M2 M1 121.1(2) 2_566 2_666 ? O1 M2 M1 99.9(2) 2_676 2_666 ? XOA M2 M1 83.39(18) . 2_666 ? XOM M2 M1 137.4(2) 1_565 2_666 ? O6 M2 M1 38.39(15) 2_666 2_666 ? M2 M2 M1 173.5(2) 2_576 2_666 ? Si1 M2 M1 59.56(8) . 2_666 ? M1 M2 M1 109.35(11) 2_566 2_666 ? M2 M2 M1 64.21(12) 2_676 2_666 ? Si1 M2 M1 93.35(11) 2_676 2_666 ? MHA MH XOM 170(4) . . ? MHA MH O5 81(4) . 1_445 ? XOM MH O5 99.0(3) . 1_445 ? MHA MH O3 95(4) . 1_545 ? XOM MH O3 95.3(3) . 1_545 ? O5 MH O3 89.1(4) 1_445 1_545 ? MHA MH O7 77(4) . 1_455 ? XOM MH O7 93.0(3) . 1_455 ? O5 MH O7 89.4(3) 1_445 1_455 ? O3 MH O7 171.7(3) 1_545 1_455 ? MHA MH O4 86(4) . . ? XOM MH O4 94.0(3) . . ? O5 MH O4 166.9(3) 1_445 . ? O3 MH O4 90.7(3) 1_545 . ? O7 MH O4 88.9(3) 1_455 . ? MHA MH XPM 9(4) . . ? XOM MH XPM 176.4(3) . . ? O5 MH XPM 84.2(3) 1_445 . ? O3 MH XPM 86.3(3) 1_545 . ? O7 MH XPM 85.4(3) 1_455 . ? O4 MH XPM 82.8(3) . . ? MHA MH 1 15(4) . 1_455 ? XOM MH 1 155.0(5) . 1_455 ? O5 MH 1 81.0(5) 1_445 1_455 ? O3 MH 1 109.6(5) 1_545 1_455 ? O7 MH 1 62.1(5) 1_455 1_455 ? O4 MH 1 86.8(5) . 1_455 ? XPM MH 1 23.6(5) . 1_455 ? MHA MH 2 29(4) . . ? XOM MH 2 153.6(5) . . ? O5 MH 2 107.3(5) 1_445 . ? O3 MH 2 82.9(5) 1_545 . ? O7 MH 2 89.8(5) 1_455 . ? O4 MH 2 59.8(5) . . ? XPM MH 2 23.4(5) . . ? 1 MH 2 38.0(6) 1_455 . ? MHA MH 4 16(4) . 1_445 ? XOM MH 4 161.0(4) . 1_445 ? O5 MH 4 65.0(4) 1_445 1_445 ? O3 MH 4 94.6(4) 1_545 1_445 ? O7 MH 4 77.3(4) 1_455 1_445 ? O4 MH 4 102.0(4) . 1_445 ? XPM MH 4 21.1(4) . 1_445 ? 1 MH 4 21.1(6) 1_455 1_445 ? 2 MH 4 44.2(6) . 1_445 ? MHA MH 3 29(4) . 1_545 ? XOM MH 3 159.8(5) . 1_545 ? O5 MH 3 91.6(5) 1_445 1_545 ? O3 MH 3 67.6(5) 1_545 1_545 ? O7 MH 3 104.3(5) 1_455 1_545 ? O4 MH 3 76.3(5) . 1_545 ? XPM MH 3 20.3(5) . 1_545 ? 1 MH 3 43.7(6) 1_455 1_545 ? 2 MH 3 21.3(6) . 1_545 ? 4 MH 3 38.0(6) 1_445 1_545 ? MHA MH BPCA 44(4) . 1_455 ? XOM MH BPCA 128.7(3) . 1_455 ? O5 MH BPCA 54.3(3) 1_445 1_455 ? O3 MH BPCA 123.0(3) 1_545 1_455 ? O7 MH BPCA 50.3(3) 1_455 1_455 ? O4 MH BPCA 115.9(3) . 1_455 ? XPM MH BPCA 52.1(3) . 1_455 ? 1 MH BPCA 33.9(4) 1_455 1_455 ? 2 MH BPCA 71.5(5) . 1_455 ? 4 MH BPCA 33.8(4) 1_445 1_455 ? 3 MH BPCA 71.3(4) 1_545 1_455 ? O3 Si1 O1 112.4(4) . . ? O3 Si1 O5 113.8(4) . . ? O1 Si1 O5 111.4(4) . . ? O3 Si1 O2 104.8(4) . . ? O1 Si1 O2 108.8(4) . . ? O5 Si1 O2 105.0(4) . . ? O3 Si1 5 145.9(4) . 1_655 ? O1 Si1 5 101.5(4) . 1_655 ? O5 Si1 5 53.4(3) . 1_655 ? O2 Si1 5 58.5(3) . 1_655 ? O3 Si1 M2 72.2(3) . . ? O1 Si1 M2 41.3(3) . . ? O5 Si1 M2 139.9(3) . . ? O2 Si1 M2 111.6(3) . . ? 5 Si1 M2 139.9(2) 1_655 . ? O3 Si1 5 53.2(3) . . ? O1 Si1 5 105.1(4) . . ? O5 Si1 5 143.1(4) . . ? O2 Si1 5 56.9(3) . . ? 5 Si1 5 114.9(3) 1_655 . ? M2 Si1 5 73.9(2) . . ? O3 Si1 BPCA 58.9(3) . 1_565 ? O1 Si1 BPCA 147.8(3) . 1_565 ? O5 Si1 BPCA 57.3(3) . 1_565 ? O2 Si1 BPCA 103.4(3) . 1_565 ? 5 Si1 BPCA 94.0(3) 1_655 1_565 ? M2 Si1 BPCA 125.43(17) . 1_565 ? 5 Si1 BPCA 93.4(2) . 1_565 ? O3 Si1 BPW 58.9(3) . 1_565 ? O1 Si1 BPW 147.8(3) . 1_565 ? O5 Si1 BPW 57.3(3) . 1_565 ? O2 Si1 BPW 103.4(3) . 1_565 ? 5 Si1 BPW 94.0(3) 1_655 1_565 ? M2 Si1 BPW 125.43(17) . 1_565 ? 5 Si1 BPW 93.4(2) . 1_565 ? BPCA Si1 BPW 0.0(4) 1_565 1_565 ? O3 Si1 M2 102.3(3) . 2_676 ? O1 Si1 M2 41.4(3) . 2_676 ? O5 Si1 M2 81.1(3) . 2_676 ? O2 Si1 M2 146.6(3) . 2_676 ? 5 Si1 M2 105.8(2) 1_655 2_676 ? M2 Si1 M2 59.34(11) . 2_676 ? 5 Si1 M2 132.7(2) . 2_676 ? BPCA Si1 M2 107.19(17) 1_565 2_676 ? BPW Si1 M2 107.19(17) 1_565 2_676 ? O3 Si1 AP 132.5(3) . 1_655 ? O1 Si1 AP 114.9(3) . 1_655 ? O5 Si1 AP 50.8(3) . 1_655 ? O2 Si1 AP 55.4(3) . 1_655 ? 5 Si1 AP 13.4(2) 1_655 1_655 ? M2 Si1 AP 152.11(12) . 1_655 ? 5 Si1 AP 108.7(2) . 1_655 ? BPCA Si1 AP 82.45(15) 1_565 1_655 ? BPW Si1 AP 82.45(15) 1_565 1_655 ? M2 Si1 AP 115.82(10) 2_676 1_655 ? O3 Si1 AP 51.5(3) . . ? O1 Si1 AP 118.2(3) . . ? O5 Si1 AP 130.0(3) . . ? O2 Si1 AP 54.0(3) . . ? 5 Si1 AP 108.9(2) 1_655 . ? M2 Si1 AP 85.99(10) . . ? 5 Si1 AP 13.1(2) . . ? BPCA Si1 AP 82.14(15) 1_565 . ? BPW Si1 AP 82.14(15) 1_565 . ? M2 Si1 AP 143.30(10) 2_676 . ? AP Si1 AP 100.41(9) 1_655 . ? O4 Si2 O7 111.8(4) . . ? O4 Si2 O6 111.1(4) . . ? O7 Si2 O6 114.9(4) . . ? O4 Si2 O2 104.7(4) . . ? O7 Si2 O2 104.4(4) . . ? O6 Si2 O2 109.2(4) . . ? O4 Si2 5 53.0(3) . . ? O7 Si2 5 144.7(4) . . ? O6 Si2 5 100.3(3) . . ? O2 Si2 5 59.2(3) . . ? O4 Si2 BPW 56.3(3) . . ? O7 Si2 BPW 55.8(3) . . ? O6 Si2 BPW 138.6(3) . . ? O2 Si2 BPW 112.2(3) . . ? 5 Si2 BPW 99.1(3) . . ? O4 Si2 5 141.8(4) . 1_655 ? O7 Si2 5 54.0(3) . 1_655 ? O6 Si2 5 106.7(3) . 1_655 ? O2 Si2 5 56.3(3) . 1_655 ? 5 Si2 5 115.0(3) . 1_655 ? BPW Si2 5 97.5(3) . 1_655 ? O4 Si2 AP 49.3(3) . . ? O7 Si2 AP 131.3(3) . . ? O6 Si2 AP 113.9(2) . . ? O2 Si2 AP 56.8(3) . . ? 5 Si2 AP 13.5(2) . . ? BPW Si2 AP 87.95(16) . . ? 5 Si2 AP 109.3(2) 1_655 . ? O4 Si2 AP 128.5(3) . 1_655 ? O7 Si2 AP 51.2(3) . 1_655 ? O6 Si2 AP 120.0(2) . 1_655 ? O2 Si2 AP 54.0(3) . 1_655 ? 5 Si2 AP 109.3(2) . 1_655 ? BPW Si2 AP 86.69(16) . 1_655 ? 5 Si2 AP 13.4(2) 1_655 1_655 ? AP Si2 AP 101.25(9) . 1_655 ? 5 AP XPA2 141.6(16) . . ? 5 AP XPA1 136.8(15) . 1_455 ? XPA2 AP XPA1 80.0(19) . 1_455 ? 5 AP XPA3 138.2(15) . 1_455 ? XPA2 AP XPA3 61(2) . 1_455 ? XPA1 AP XPA3 60.5(19) 1_455 1_455 ? 5 AP O4 70.2(7) . . ? XPA2 AP O4 108.9(14) . . ? XPA1 AP O4 88.0(13) 1_455 . ? XPA3 AP O4 147.5(14) 1_455 . ? 5 AP O5 67.3(7) . 1_455 ? XPA2 AP O5 103.9(14) . 1_455 ? XPA1 AP O5 124.4(13) 1_455 1_455 ? XPA3 AP O5 73.3(14) 1_455 1_455 ? O4 AP O5 137.4(3) . 1_455 ? 5 AP XPA4 136.2(15) . . ? XPA2 AP XPA4 54.9(19) . . ? XPA1 AP XPA4 47.1(18) 1_455 . ? XPA3 AP XPA4 85.0(19) 1_455 . ? O4 AP XPA4 66.3(13) . . ? O5 AP XPA4 155.8(13) 1_455 . ? 5 AP O7 69.3(7) . 1_455 ? XPA2 AP O7 145.1(14) . 1_455 ? XPA1 AP O7 67.5(13) 1_455 1_455 ? XPA3 AP O7 109.6(14) 1_455 1_455 ? O4 AP O7 59.4(2) . 1_455 ? O5 AP O7 104.8(2) 1_455 1_455 ? XPA4 AP O7 92.3(13) . 1_455 ? 5 AP O3 66.0(7) . . ? XPA2 AP O3 77.6(14) . . ? XPA1 AP O3 157.1(13) 1_455 . ? XPA3 AP O3 103.8(14) 1_455 . ? O4 AP O3 103.6(2) . . ? O5 AP O3 57.9(2) 1_455 . ? XPA4 AP O3 119.7(14) . . ? O7 AP O3 135.3(3) 1_455 . ? 5 AP O2 68.8(7) . 1_455 ? XPA2 AP O2 138.0(14) . 1_455 ? XPA1 AP O2 85.5(13) 1_455 1_455 ? XPA3 AP O2 77.6(14) 1_455 1_455 ? O4 AP O2 109.8(2) . 1_455 ? O5 AP O2 54.39(19) 1_455 1_455 ? XPA4 AP O2 131.6(14) . 1_455 ? O7 AP O2 53.80(19) 1_455 1_455 ? O3 AP O2 108.2(2) . 1_455 ? 5 AP O2 68.8(7) . . ? XPA2 AP O2 79.9(14) . . ? XPA1 AP O2 127.2(13) 1_455 . ? XPA3 AP O2 139.0(15) 1_455 . ? O4 AP O2 54.22(19) . . ? O5 AP O2 107.7(2) 1_455 . ? XPA4 AP O2 81.7(14) . . ? O7 AP O2 109.5(2) 1_455 . ? O3 AP O2 52.78(19) . . ? O2 AP O2 137.6(3) 1_455 . ? 5 AP XOA 5.2(7) . . ? XPA2 AP XOA 146.4(14) . . ? XPA1 AP XOA 131.7(13) 1_455 . ? XPA3 AP XOA 138.7(14) 1_455 . ? O4 AP XOA 67.9(2) . . ? O5 AP XOA 69.8(2) 1_455 . ? XPA4 AP XOA 134.1(13) . . ? O7 AP XOA 64.17(19) 1_455 . ? O3 AP XOA 71.2(2) . . ? O2 AP XOA 66.25(19) 1_455 . ? O2 AP XOA 71.49(19) . . ? W3 BPW 1 58(2) . . ? W3 BPW 4 59(2) . 1_545 ? 1 BPW 4 36.2(10) . 1_545 ? W3 BPW 2 61(2) . . ? 1 BPW 2 109.1(11) . . ? 4 BPW 2 120.4(11) 1_545 . ? W3 BPW 3 62(2) . 1_545 ? 1 BPW 3 119.6(11) . 1_545 ? 4 BPW 3 106.5(10) 1_545 1_545 ? 2 BPW 3 36.5(11) . 1_545 ? W3 BPW XPB 67(3) . 1_545 ? 1 BPW XPB 88.3(19) . 1_545 ? 4 BPW XPB 54.1(19) 1_545 1_545 ? 2 BPW XPB 98(2) . 1_545 ? 3 BPW XPB 65(2) 1_545 1_545 ? W3 BPW O7 132(2) . . ? 1 BPW O7 78.5(8) . . ? 4 BPW O7 97.1(7) 1_545 . ? 2 BPW O7 126.5(8) . . ? 3 BPW O7 156.2(8) 1_545 . ? XPB BPW O7 135.3(18) 1_545 . ? W3 BPW O4 132(2) . . ? 1 BPW O4 126.7(8) . . ? 4 BPW O4 157.1(8) 1_545 . ? 2 BPW O4 75.9(8) . . ? 3 BPW O4 96.0(8) 1_545 . ? XPB BPW O4 144.8(18) 1_545 . ? O7 BPW O4 60.3(3) . . ? W3 BPW XPM 92(2) . . ? 1 BPW XPM 145.6(9) . . ? 4 BPW XPM 141.9(8) 1_545 . ? 2 BPW XPM 36.7(8) . . ? 3 BPW XPM 35.5(7) 1_545 . ? XPB BPW XPM 93.5(19) 1_545 . ? O7 BPW XPM 121.0(4) . . ? O4 BPW XPM 60.8(3) . . ? W3 BPW XPM 88(2) . 1_655 ? 1 BPW XPM 36.4(7) . 1_655 ? 4 BPW XPM 34.8(7) 1_545 1_655 ? 2 BPW XPM 145.4(9) . 1_655 ? 3 BPW XPM 141.2(8) 1_545 1_655 ? XPB BPW XPM 81.7(19) 1_545 1_655 ? O7 BPW XPM 62.5(3) . 1_655 ? O4 BPW XPM 122.8(4) . 1_655 ? XPM BPW XPM 174.9(5) . 1_655 ? W3 BPW O5 137(2) . 1_545 ? 1 BPW O5 96.1(8) . 1_545 ? 4 BPW O5 79.0(7) 1_545 1_545 ? 2 BPW O5 154.6(9) . 1_545 ? 3 BPW O5 126.7(8) 1_545 1_545 ? XPB BPW O5 79.6(18) 1_545 1_545 ? O7 BPW O5 60.0(3) . 1_545 ? O4 BPW O5 91.3(4) . 1_545 ? XPM BPW O5 118.0(4) . 1_545 ? XPM BPW O5 59.8(3) 1_655 1_545 ? W3 BPW XPA3 68(3) . 1_545 ? 1 BPW XPA3 71.4(15) . 1_545 ? 4 BPW XPA3 35.5(15) 1_545 1_545 ? 2 BPW XPA3 114.5(16) . 1_545 ? 3 BPW XPA3 84.1(16) 1_545 1_545 ? XPB BPW XPA3 21(2) 1_545 1_545 ? O7 BPW XPA3 117.9(14) . 1_545 ? O4 BPW XPA3 156.7(14) . 1_545 ? XPM BPW XPA3 114.1(14) . 1_545 ? XPM BPW XPA3 61.0(14) 1_655 1_545 ? O5 BPW XPA3 70.6(13) 1_545 1_545 ? W3 BPW O3 141(2) . 1_545 ? 1 BPW O3 153.4(8) . 1_545 ? 4 BPW O3 126.5(7) 1_545 1_545 ? 2 BPW O3 97.4(8) . 1_545 ? 3 BPW O3 81.2(8) 1_545 1_545 ? XPB BPW O3 86.5(18) 1_545 1_545 ? O7 BPW O3 87.0(4) . 1_545 ? O4 BPW O3 60.5(3) . 1_545 ? XPM BPW O3 60.8(3) . 1_545 ? XPM BPW O3 117.0(4) 1_655 1_545 ? O5 BPW O3 57.3(3) 1_545 1_545 ? XPA3 BPW O3 96.6(14) 1_545 1_545 ? W3 BPW XPA4 67(3) . . ? 1 BPW XPA4 90.7(15) . . ? 4 BPW XPA4 118.6(15) 1_545 . ? 2 BPW XPA4 32.3(15) . . ? 3 BPW XPA4 68.7(15) 1_545 . ? XPB BPW XPA4 125(2) 1_545 . ? O7 BPW XPA4 97.7(13) . . ? O4 BPW XPA4 65.4(13) . . ? XPM BPW XPA4 60.6(13) . . ? XPM BPW XPA4 123.6(13) 1_655 . ? O5 BPW XPA4 154.6(13) 1_545 . ? XPA3 BPW XPA4 134.5(19) 1_545 . ? O3 BPW XPA4 113.5(13) 1_545 . ? W3 BPW XPA1 67(3) . . ? 1 BPW XPA1 30.3(13) . . ? 4 BPW XPA1 66.5(13) 1_545 . ? 2 BPW XPA1 94.2(14) . . ? 3 BPW XPA1 121.5(14) 1_545 . ? XPB BPW XPA1 117(2) 1_545 . ? O7 BPW XPA1 65.6(12) . . ? O4 BPW XPA1 98.2(12) . . ? XPM BPW XPA1 127.4(12) . . ? XPM BPW XPA1 56.9(12) 1_655 . ? O5 BPW XPA1 109.4(12) 1_545 . ? XPA3 BPW XPA1 101.6(18) 1_545 . ? O3 BPW XPA1 152.0(12) 1_545 . ? XPA4 BPW XPA1 66.8(17) . . ? W3 BPW MHA 117(3) . 1_655 ? 1 BPW MHA 61.7(15) . 1_655 ? 4 BPW MHA 62.6(15) 1_545 1_655 ? 2 BPW MHA 161.9(12) . 1_655 ? 3 BPW MHA 161.1(12) 1_545 1_655 ? XPB BPW MHA 97(2) 1_545 1_655 ? O7 BPW MHA 39.3(11) . 1_655 ? O4 BPW MHA 96.9(13) . 1_655 ? XPM BPW MHA 151.2(14) . 1_655 ? XPM BPW MHA 29.5(14) 1_655 1_655 ? O5 BPW MHA 39.3(11) 1_545 1_655 ? XPA3 BPW MHA 78.6(17) 1_545 1_655 ? O3 BPW MHA 93.1(13) 1_545 1_655 ? XPA4 BPW MHA 129.6(16) . 1_655 ? XPA1 BPW MHA 70.1(16) . 1_655 ? W3 BPW XPA2 70(3) . 1_545 ? 1 BPW XPA2 115.7(14) . 1_545 ? 4 BPW XPA2 86.4(14) 1_545 1_545 ? 2 BPW XPA2 70.1(14) . 1_545 ? 3 BPW XPA2 33.6(14) 1_545 1_545 ? XPB BPW XPA2 34(2) 1_545 1_545 ? O7 BPW XPA2 155.4(13) . 1_545 ? O4 BPW XPA2 115.5(12) . 1_545 ? XPM BPW XPA2 59.0(12) . 1_545 ? XPM BPW XPA2 116.1(13) 1_655 1_545 ? O5 BPW XPA2 97.1(12) 1_545 1_545 ? XPA3 BPW XPA2 55.1(18) 1_545 1_545 ? O3 BPW XPA2 71.6(12) 1_545 1_545 ? XPA4 BPW XPA2 101.9(18) . 1_545 ? XPA1 BPW XPA2 136.4(17) . 1_545 ? MHA BPW XPA2 127.5(15) 1_655 1_545 ? W3 BPW W1 39(2) . 1_545 ? 1 BPW W1 96.2(10) . 1_545 ? 4 BPW W1 94.9(9) 1_545 1_545 ? 2 BPW W1 28.3(10) . 1_545 ? 3 BPW W1 26.4(9) 1_545 1_545 ? XPB BPW W1 72.5(19) 1_545 1_545 ? O7 BPW W1 150.6(7) . 1_545 ? O4 BPW W1 103.7(7) . 1_545 ? XPM BPW W1 52.3(7) . 1_545 ? XPM BPW W1 126.9(7) 1_655 1_545 ? O5 BPW W1 149.1(7) 1_545 1_545 ? XPA3 BPW W1 86.7(15) 1_545 1_545 ? O3 BPW W1 107.0(7) 1_545 1_545 ? XPA4 BPW W1 53.1(14) . 1_545 ? XPA1 BPW W1 95.2(13) . 1_545 ? MHA BPW W1 156.3(15) 1_655 1_545 ? XPA2 BPW W1 52.0(14) 1_545 1_545 ? W3 BPW W1 35(2) . 2_665 ? 1 BPW W1 27.1(9) . 2_665 ? 4 BPW W1 28.5(9) 1_545 2_665 ? 2 BPW W1 95.2(10) . 2_665 ? 3 BPW W1 94.4(10) 1_545 2_665 ? XPB BPW W1 66.6(19) 1_545 2_665 ? O7 BPW W1 105.4(7) . 2_665 ? O4 BPW W1 147.6(7) . 2_665 ? XPM BPW W1 126.7(7) . 2_665 ? XPM BPW W1 52.7(7) 1_655 2_665 ? O5 BPW W1 106.7(7) 1_545 2_665 ? XPA3 BPW W1 55.1(15) 1_545 2_665 ? O3 BPW W1 151.7(7) 1_545 2_665 ? XPA4 BPW W1 90.3(14) . 2_665 ? XPA1 BPW W1 50.7(13) . 2_665 ? MHA BPW W1 82.0(15) 1_655 2_665 ? XPA2 BPW W1 89.3(14) 1_545 2_665 ? W1 BPW W1 74.4(10) 1_545 2_665 ? W3 BPW MHA 119(3) . . ? 1 BPW MHA 162.0(12) . . ? 4 BPW MHA 160.9(12) 1_545 . ? 2 BPW MHA 60.1(16) . . ? 3 BPW MHA 61.6(16) 1_545 . ? XPB BPW MHA 107(2) 1_545 . ? O7 BPW MHA 96.3(14) . . ? O4 BPW MHA 39.8(11) . . ? XPM BPW MHA 27.6(15) . . ? XPM BPW MHA 153.1(15) 1_655 . ? O5 BPW MHA 96.1(14) 1_545 . ? XPA3 BPW MHA 125.4(16) 1_545 . ? O3 BPW MHA 40.9(12) 1_545 . ? XPA4 BPW MHA 72.8(17) . . ? XPA1 BPW MHA 132.0(15) . . ? MHA BPW MHA 124(3) 1_655 . ? XPA2 BPW MHA 75.8(17) 1_545 . ? W1 BPW MHA 79.8(16) 1_545 . ? W1 BPW MHA 154.1(16) 2_665 . ? BPW W3 1 104(3) . . ? BPW W3 4 102(3) . 1_545 ? 1 W3 4 41.5(12) . 1_545 ? BPW W3 2 100(3) . . ? 1 W3 2 135.5(18) . . ? 4 W3 2 157(2) 1_545 . ? BPW W3 3 100(3) . 1_545 ? 1 W3 3 156(2) . 1_545 ? 4 W3 3 128.9(17) 1_545 1_545 ? 2 W3 3 41.1(13) . 1_545 ? BPW W3 XPB 98(3) . 1_545 ? 1 W3 XPB 101(2) . 1_545 ? 4 W3 XPB 60(2) 1_545 1_545 ? 2 W3 XPB 112(2) . 1_545 ? 3 W3 XPB 72(2) 1_545 1_545 ? BPW W3 W1 137(3) . 2_665 ? 1 W3 W1 37.4(12) . 2_665 ? 4 W3 W1 38.9(11) 1_545 2_665 ? 2 W3 W1 121.4(17) . 2_665 ? 3 W3 W1 119.4(16) 1_545 2_665 ? XPB W3 W1 78(2) 1_545 2_665 ? BPW W3 W1 132(3) . 1_545 ? 1 W3 W1 123.0(16) . 1_545 ? 4 W3 W1 120.1(16) 1_545 1_545 ? 2 W3 W1 37.9(12) . 1_545 ? 3 W3 W1 35.8(12) 1_545 1_545 ? XPB W3 W1 85(2) 1_545 1_545 ? W1 W3 W1 91.4(13) 2_665 1_545 ? BPW W3 XPA3 99(3) . 1_545 ? 1 W3 XPA3 79.4(19) . 1_545 ? 4 W3 XPA3 38.0(17) 1_545 1_545 ? 2 W3 XPA3 133(2) . 1_545 ? 3 W3 XPA3 93.4(19) 1_545 1_545 ? XPB W3 XPA3 22(2) 1_545 1_545 ? W1 W3 XPA3 63.1(17) 2_665 1_545 ? W1 W3 XPA3 100.7(18) 1_545 1_545 ? BPW W3 XPA4 101(3) . . ? 1 W3 XPA4 103.3(19) . . ? 4 W3 XPA4 142(2) 1_545 . ? 2 W3 XPA4 35.0(17) . . ? 3 W3 XPA4 75.9(18) 1_545 . ? XPB W3 XPA4 145(3) 1_545 . ? W1 W3 XPA4 106.5(18) 2_665 . ? W1 W3 XPA4 60.4(16) 1_545 . ? XPA3 W3 XPA4 159(2) 1_545 . ? BPW W3 XPA1 101(3) . . ? 1 W3 XPA1 32.3(15) . . ? 4 W3 XPA1 73.8(16) 1_545 . ? 2 W3 XPA1 106.6(18) . . ? 3 W3 XPA1 144.6(19) 1_545 . ? XPB W3 XPA1 132(3) 1_545 . ? W1 W3 XPA1 57.9(15) 2_665 . ? W1 W3 XPA1 112.0(17) 1_545 . ? XPA3 W3 XPA1 112(2) 1_545 . ? XPA4 W3 XPA1 72.2(19) . . ? BPW W3 XPM 79(2) . 1_655 ? 1 W3 XPM 33.1(9) . 1_655 ? 4 W3 XPM 31.4(9) 1_545 1_655 ? 2 W3 XPM 164.0(15) . 1_655 ? 3 W3 XPM 154.8(14) 1_545 1_655 ? XPB W3 XPM 84(2) 1_545 1_655 ? W1 W3 XPM 58.0(9) 2_665 1_655 ? W1 W3 XPM 149.0(13) 1_545 1_655 ? XPA3 W3 XPM 62.5(16) 1_545 1_655 ? XPA4 W3 XPM 129.2(16) . 1_655 ? XPA1 W3 XPM 58.6(13) . 1_655 ? BPW W3 XPM 75(2) . . ? 1 W3 XPM 164.0(15) . . ? 4 W3 XPM 154.4(14) 1_545 . ? 2 W3 XPM 32.8(10) . . ? 3 W3 XPM 31.8(9) 1_545 . ? XPB W3 XPM 95(2) 1_545 . ? W1 W3 XPM 148.1(13) 2_665 . ? W1 W3 XPM 56.7(9) 1_545 . ? XPA3 W3 XPM 116.6(17) 1_545 . ? XPA4 W3 XPM 61.9(15) . . ? XPA1 W3 XPM 131.8(15) . . ? XPM W3 XPM 153.1(11) 1_655 . ? BPW W3 XPA2 97(3) . 1_545 ? 1 W3 XPA2 135.2(19) . 1_545 ? 4 W3 XPA2 95.9(17) 1_545 1_545 ? 2 W3 XPA2 76.4(17) . 1_545 ? 3 W3 XPA2 35.4(16) 1_545 1_545 ? XPB W3 XPA2 37(2) 1_545 1_545 ? W1 W3 XPA2 103.5(17) 2_665 1_545 ? W1 W3 XPA2 58.2(15) 1_545 1_545 ? XPA3 W3 XPA2 59(2) 1_545 1_545 ? XPA4 W3 XPA2 111(2) . 1_545 ? XPA1 W3 XPA2 160(2) . 1_545 ? XPM W3 XPA2 119.5(15) 1_655 1_545 ? XPM W3 XPA2 60.0(14) . 1_545 ? BPW W3 O7 39(2) . . ? 1 W3 O7 69.0(11) . . ? 4 W3 O7 87.2(12) 1_545 . ? 2 W3 O7 113.4(14) . . ? 3 W3 O7 134.4(14) 1_545 . ? XPB W3 O7 121(2) 1_545 . ? W1 W3 O7 106.2(10) 2_665 . ? W1 W3 O7 150.5(12) 1_545 . ? XPA3 W3 O7 108.4(16) 1_545 . ? XPA4 W3 O7 91.4(15) . . ? XPA1 W3 O7 62.1(13) . . ? XPM W3 O7 56.0(5) 1_655 . ? XPM W3 O7 103.8(8) . . ? XPA2 W3 O7 135.5(15) 1_545 . ? BPW W3 O4 39(2) . . ? 1 W3 O4 114.9(13) . . ? 4 W3 O4 136.3(14) 1_545 . ? 2 W3 O4 66.1(11) . . ? 3 W3 O4 86.0(12) 1_545 . ? XPB W3 O4 128(2) 1_545 . ? W1 W3 O4 149.9(12) 2_665 . ? W1 W3 O4 103.6(10) 1_545 . ? XPA3 W3 O4 136.3(17) 1_545 . ? XPA4 W3 O4 61.5(14) . . ? XPA1 W3 O4 92.1(14) . . ? XPM W3 O4 106.2(8) 1_655 . ? XPM W3 O4 54.2(5) . . ? XPA2 W3 O4 106.6(15) 1_545 . ? O7 W3 O4 50.6(4) . . ? BPW W3 MHA 53(2) . 1_655 ? 1 W3 MHA 53.5(15) . 1_655 ? 4 W3 MHA 54.5(15) 1_545 1_655 ? 2 W3 MHA 147.4(18) . 1_655 ? 3 W3 MHA 146.4(17) 1_545 1_655 ? XPB W3 MHA 92(2) 1_545 1_655 ? W1 W3 MHA 83.8(15) 2_665 1_655 ? W1 W3 MHA 174.6(16) 1_545 1_655 ? XPA3 W3 MHA 75.0(18) 1_545 1_655 ? XPA4 W3 MHA 123.3(18) . 1_655 ? XPA1 W3 MHA 67.4(16) . 1_655 ? XPM W3 MHA 26.0(12) 1_655 1_655 ? XPM W3 MHA 127.9(14) . 1_655 ? XPA2 W3 MHA 120.6(17) 1_545 1_655 ? O7 W3 MHA 34.5(10) . 1_655 ? O4 W3 MHA 81.8(12) . 1_655 ? BPW W3 MHA 52(2) . . ? 1 W3 MHA 149.6(18) . . ? 4 W3 MHA 147.3(17) 1_545 . ? 2 W3 MHA 50.9(16) . . ? 3 W3 MHA 53.0(16) 1_545 . ? XPB W3 MHA 101(2) 1_545 . ? W1 W3 MHA 171.5(17) 2_665 . ? W1 W3 MHA 80.1(16) 1_545 . ? XPA3 W3 MHA 118.4(18) 1_545 . ? XPA4 W3 MHA 69.3(17) . . ? XPA1 W3 MHA 125.2(17) . . ? XPM W3 MHA 130.4(15) 1_655 . ? XPM W3 MHA 23.5(13) . . ? XPA2 W3 MHA 72.2(16) 1_545 . ? O7 W3 MHA 81.5(13) . . ? O4 W3 MHA 35.0(11) . . ? MHA W3 MHA 105(2) 1_655 . ? BPW W3 W3 175(3) . 2_655 ? 1 W3 W3 80.0(13) . 2_655 ? 4 W3 W3 78.8(12) 1_545 2_655 ? 2 W3 W3 78.7(13) . 2_655 ? 3 W3 W3 76.5(12) 1_545 2_655 ? XPB W3 W3 78(2) 1_545 2_655 ? W1 W3 W3 45.9(9) 2_665 2_655 ? W1 W3 W3 45.5(9) 1_545 2_655 ? XPA3 W3 W3 79.1(16) 1_545 2_655 ? XPA4 W3 W3 81.2(16) . 2_655 ? XPA1 W3 W3 83.7(15) . 2_655 ? XPM W3 W3 103.8(10) 1_655 2_655 ? XPM W3 W3 102.2(10) . 2_655 ? XPA2 W3 W3 77.7(15) 1_545 2_655 ? O7 W3 W3 145.5(11) . 2_655 ? O4 W3 W3 141.8(11) . 2_655 ? MHA W3 W3 129.7(15) 1_655 2_655 ? MHA W3 W3 125.6(16) . 2_655 ? Si1 O1 M1 127.4(4) . 2_666 ? Si1 O1 M2 110.5(4) . . ? M1 O1 M2 106.1(3) 2_666 . ? Si1 O1 M2 112.5(4) . 2_676 ? M1 O1 M2 104.9(3) 2_666 2_676 ? M2 O1 M2 88.4(3) . 2_676 ? Si1 O2 Si2 138.5(5) . . ? Si1 O2 5 90.4(4) . 1_655 ? Si2 O2 5 93.3(4) . 1_655 ? Si1 O2 5 93.0(4) . . ? Si2 O2 5 89.7(4) . . ? 5 O2 5 171.0(6) 1_655 . ? Si1 O2 AP 96.7(3) . 1_655 ? Si2 O2 AP 98.6(3) . 1_655 ? 5 O2 AP 16.8(2) 1_655 1_655 ? 5 O2 AP 154.2(4) . 1_655 ? Si1 O2 AP 99.0(3) . . ? Si2 O2 AP 95.2(3) . . ? 5 O2 AP 154.4(4) 1_655 . ? 5 O2 AP 16.6(2) . . ? AP O2 AP 137.6(3) 1_655 . ? Si1 O3 MH 155.3(5) . 1_565 ? Si1 O3 MHA 165.7(14) . 1_565 ? MH O3 MHA 19(2) 1_565 1_565 ? Si1 O3 5 97.5(4) . . ? MH O3 5 101.9(4) 1_565 . ? MHA O3 5 96.4(15) 1_565 . ? Si1 O3 XPM 146.3(5) . 1_565 ? MH O3 XPM 49.9(3) 1_565 1_565 ? MHA O3 XPM 31(2) 1_565 1_565 ? 5 O3 XPM 88.9(4) . 1_565 ? Si1 O3 BPCA 92.1(4) . 1_565 ? MH O3 BPCA 90.5(3) 1_565 1_565 ? MHA O3 BPCA 77.8(17) 1_565 1_565 ? 5 O3 BPCA 121.8(4) . 1_565 ? XPM O3 BPCA 57.3(3) 1_565 1_565 ? Si1 O3 BPW 92.1(4) . 1_565 ? MH O3 BPW 90.5(3) 1_565 1_565 ? MHA O3 BPW 77.8(17) 1_565 1_565 ? 5 O3 BPW 121.8(4) . 1_565 ? XPM O3 BPW 57.3(3) 1_565 1_565 ? BPCA O3 BPW 0.0(4) 1_565 1_565 ? Si1 O3 AP 102.4(3) . . ? MH O3 AP 100.6(3) 1_565 . ? MHA O3 AP 90.1(17) 1_565 . ? 5 O3 AP 16.9(2) . . ? XPM O3 AP 75.8(3) 1_565 . ? BPCA O3 AP 105.2(3) 1_565 . ? BPW O3 AP 105.2(3) 1_565 . ? Si1 O3 3 117.3(6) . . ? MH O3 3 78.5(5) 1_565 . ? MHA O3 3 60(2) 1_565 . ? 5 O3 3 88.7(6) . . ? XPM O3 3 29.4(5) 1_565 . ? BPCA O3 3 38.3(5) 1_565 . ? BPW O3 3 38.3(5) 1_565 . ? AP O3 3 72.0(5) . . ? Si2 O4 MH 138.6(4) . . ? Si2 O4 MHA 155.4(19) . . ? MH O4 MHA 20(2) . . ? Si2 O4 5 96.8(4) . . ? MH O4 5 104.0(4) . . ? MHA O4 5 102.3(14) . . ? Si2 O4 BPW 93.5(4) . . ? MH O4 BPW 95.2(3) . . ? MHA O4 BPW 83.2(17) . . ? 5 O4 BPW 136.6(4) . . ? Si2 O4 AP 103.9(3) . . ? MH O4 AP 106.8(3) . . ? MHA O4 AP 99.0(16) . . ? 5 O4 AP 17.9(3) . . ? BPW O4 AP 119.0(3) . . ? Si2 O4 XPM 153.7(5) . . ? MH O4 XPM 51.6(2) . . ? MHA O4 XPM 32(2) . . ? 5 O4 XPM 103.2(4) . . ? BPW O4 XPM 60.2(3) . . ? AP O4 XPM 91.0(3) . . ? Si2 O4 2 125.7(6) . . ? MH O4 2 84.7(6) . . ? MHA O4 2 65(2) . . ? 5 O4 2 101.7(6) . . ? BPW O4 2 41.4(6) . . ? AP O4 2 84.3(5) . . ? XPM O4 2 33.3(6) . . ? Si2 O4 XPA4 111.0(13) . . ? MH O4 XPA4 108.6(13) . . ? MHA O4 XPA4 89(3) . . ? 5 O4 XPA4 76.0(13) . . ? BPW O4 XPA4 61.0(13) . . ? AP O4 XPA4 58.2(12) . . ? XPM O4 XPA4 58.9(13) . . ? 2 O4 XPA4 31.7(13) . . ? Si2 O4 W3 97.6(5) . . ? MH O4 W3 97.0(5) . . ? MHA O4 W3 82.7(19) . . ? 5 O4 W3 128.0(6) . . ? BPW O4 W3 8.8(5) . . ? AP O4 W3 110.3(5) . . ? XPM O4 W3 56.5(5) . . ? 2 O4 W3 33.7(7) . . ? XPA4 O4 W3 52.2(13) . . ? Si1 O5 MH 149.7(5) . 1_665 ? Si1 O5 MHA 160.1(15) . 1_665 ? MH O5 MHA 21(2) 1_665 1_665 ? Si1 O5 5 96.1(4) . 1_655 ? MH O5 5 105.2(4) 1_665 1_655 ? MHA O5 5 103.7(14) 1_665 1_655 ? Si1 O5 XPM 150.1(5) . 1_665 ? MH O5 XPM 51.4(3) 1_665 1_665 ? MHA O5 XPM 31(2) 1_665 1_665 ? 5 O5 XPM 92.1(4) 1_655 1_665 ? Si1 O5 AP 102.2(3) . 1_655 ? MH O5 AP 104.6(3) 1_665 1_655 ? MHA O5 AP 96.9(16) 1_665 1_655 ? 5 O5 AP 17.6(3) 1_655 1_655 ? XPM O5 AP 78.6(3) 1_665 1_655 ? Si1 O5 BPCA 93.6(4) . 1_565 ? MH O5 BPCA 91.6(3) 1_665 1_565 ? MHA O5 BPCA 75(2) 1_665 1_565 ? 5 O5 BPCA 124.8(5) 1_655 1_565 ? XPM O5 BPCA 58.7(3) 1_665 1_565 ? AP O5 BPCA 107.5(3) 1_655 1_565 ? Si1 O5 BPW 93.6(4) . 1_565 ? MH O5 BPW 91.6(3) 1_665 1_565 ? MHA O5 BPW 75(2) 1_665 1_565 ? 5 O5 BPW 124.8(5) 1_655 1_565 ? XPM O5 BPW 58.7(3) 1_665 1_565 ? AP O5 BPW 107.5(3) 1_655 1_565 ? BPCA O5 BPW 0.0(4) 1_565 1_565 ? Si1 O5 4 120.4(6) . . ? MH O5 4 80.6(5) 1_665 . ? MHA O5 4 60(2) 1_665 . ? 5 O5 4 91.8(5) 1_655 . ? XPM O5 4 30.3(5) 1_665 . ? AP O5 4 74.5(4) 1_655 . ? BPCA O5 4 38.9(5) 1_565 . ? BPW O5 4 38.9(5) 1_565 . ? Si2 O6 M1 123.3(3) . . ? Si2 O6 M1 120.9(4) . 2_666 ? M1 O6 M1 103.6(3) . 2_666 ? Si2 O6 M2 117.1(3) . 2_666 ? M1 O6 M2 90.7(2) . 2_666 ? M1 O6 M2 94.1(2) 2_666 2_666 ? Si2 O7 MHA 158.6(17) . 1_655 ? Si2 O7 MH 145.0(5) . 1_655 ? MHA O7 MH 21(2) 1_655 1_655 ? Si2 O7 5 96.2(4) . 1_655 ? MHA O7 5 103.3(15) 1_655 1_655 ? MH O7 5 101.9(3) 1_655 1_655 ? Si2 O7 BPW 94.0(4) . . ? MHA O7 BPW 79(2) 1_655 . ? MH O7 BPW 95.3(3) 1_655 . ? 5 O7 BPW 132.7(4) 1_655 . ? Si2 O7 XPM 153.5(4) . 1_655 ? MHA O7 XPM 30(2) 1_655 1_655 ? MH O7 XPM 50.4(2) 1_655 1_655 ? 5 O7 XPM 99.7(4) 1_655 1_655 ? BPW O7 XPM 59.7(3) . 1_655 ? Si2 O7 AP 102.1(3) . 1_655 ? MHA O7 AP 99.1(15) 1_655 1_655 ? MH O7 AP 104.0(3) 1_655 1_655 ? 5 O7 AP 17.3(2) 1_655 1_655 ? BPW O7 AP 115.6(3) . 1_655 ? XPM O7 AP 87.9(3) 1_655 1_655 ? Si2 O7 1 124.2(6) . . ? MHA O7 1 62(3) 1_655 . ? MH O7 1 82.7(5) 1_655 . ? 5 O7 1 98.3(6) 1_655 . ? BPW O7 1 40.6(5) . . ? XPM O7 1 32.5(5) 1_655 . ? AP O7 1 81.5(5) 1_655 . ? Si2 O7 XPA1 111.8(12) . . ? MHA O7 XPA1 83(3) 1_655 . ? MH O7 XPA1 102.3(12) 1_655 . ? 5 O7 XPA1 71.5(12) 1_655 . ? BPW O7 XPA1 61.8(11) . . ? XPM O7 XPA1 55.0(11) 1_655 . ? AP O7 XPA1 54.2(11) 1_655 . ? 1 O7 XPA1 30.6(12) . . ? Si2 O7 W3 98.1(5) . . ? MHA O7 W3 78(2) 1_655 . ? MH O7 W3 96.1(5) 1_655 . ? 5 O7 W3 124.1(6) 1_655 . ? BPW O7 W3 8.8(4) . . ? XPM O7 W3 55.4(5) 1_655 . ? AP O7 W3 106.9(5) 1_655 . ? 1 O7 W3 32.7(6) . . ? XPA1 O7 W3 53.1(12) . . ? MH XOM M1 134.0(4) . . ? MH XOM M2 122.3(4) . 2_566 ? M1 XOM M2 94.6(3) . 2_566 ? MH XOM MHA 2.7(11) . . ? M1 XOM MHA 133.3(11) . . ? M2 XOM MHA 121.0(11) 2_566 . ? MH XOM M2 109.8(3) . 1_545 ? M1 XOM M2 103.1(3) . 1_545 ? M2 XOM M2 78.7(3) 2_566 1_545 ? MHA XOM M2 112.2(11) . 1_545 ? M1 XOA M1 97.5(3) 2_566 . ? M1 XOA M2 92.6(3) 2_566 . ? M1 XOA M2 106.7(3) . . ? M1 XOA 5 127.4(4) 2_566 . ? M1 XOA 5 122.8(4) . . ? M2 XOA 5 104.6(3) . . ? M1 XOA AP 126.8(3) 2_566 . ? M1 XOA AP 122.0(3) . . ? M2 XOA AP 106.3(2) . . ? 5 XOA AP 1.7(2) . . ? MHA XPM 4 126(2) . 1_445 ? MHA XPM 3 136(2) . 1_545 ? 4 XPM 3 89.1(13) 1_445 1_545 ? MHA XPM 1 120(2) . 1_455 ? 4 XPM 1 45.3(12) 1_445 1_455 ? 3 XPM 1 103.5(13) 1_545 1_455 ? MHA XPM 2 127(2) . . ? 4 XPM 2 104.8(13) 1_445 . ? 3 XPM 2 46.0(13) 1_545 . ? 1 XPM 2 84.4(13) 1_455 . ? MHA XPM MH 4(2) . . ? 4 XPM MH 129.4(9) 1_445 . ? 3 XPM MH 131.6(10) 1_545 . ? 1 XPM MH 124.2(10) 1_455 . ? 2 XPM MH 124.8(11) . . ? MHA XPM W1 164(2) . 1_545 ? 4 XPM W1 69.2(11) 1_445 1_545 ? 3 XPM W1 35.0(12) 1_545 1_545 ? 1 XPM W1 69.0(12) 1_455 1_545 ? 2 XPM W1 38.2(12) . 1_545 ? MH XPM W1 161.3(9) . 1_545 ? MHA XPM W1 156(2) . 2_565 ? 4 XPM W1 37.6(11) 1_445 2_565 ? 3 XPM W1 68.5(12) 1_545 2_565 ? 1 XPM W1 36.6(11) 1_455 2_565 ? 2 XPM W1 67.8(12) . 2_565 ? MH XPM W1 159.9(8) . 2_565 ? W1 XPM W1 37.1(14) 1_545 2_565 ? MHA XPM XPA1 105(2) . 1_455 ? 4 XPM XPA1 77.7(15) 1_445 1_455 ? 3 XPM XPA1 107.7(16) 1_545 1_455 ? 1 XPM XPA1 32.5(15) 1_455 1_455 ? 2 XPM XPA1 69.4(16) . 1_455 ? MH XPM XPA1 108.5(13) . 1_455 ? W1 XPM XPA1 75.4(15) 1_545 1_455 ? W1 XPM XPA1 58.7(15) 2_565 1_455 ? MHA XPM BPW 94(2) . . ? 4 XPM BPW 136.8(9) 1_445 . ? 3 XPM BPW 47.8(10) 1_545 . ? 1 XPM BPW 131.2(10) 1_455 . ? 2 XPM BPW 46.8(10) . . ? MH XPM BPW 89.9(4) . . ? W1 XPM BPW 71.8(8) 1_545 . ? W1 XPM BPW 108.7(8) 2_565 . ? XPA1 XPM BPW 109.6(13) 1_455 . ? MHA XPM BPCA 85(2) . 1_455 ? 4 XPM BPCA 46.2(8) 1_445 1_455 ? 3 XPM BPCA 135.2(10) 1_545 1_455 ? 1 XPM BPCA 46.4(9) 1_455 1_455 ? 2 XPM BPCA 130.7(11) . 1_455 ? MH XPM BPCA 89.1(4) . 1_455 ? W1 XPM BPCA 108.8(8) 1_545 1_455 ? W1 XPM BPCA 71.7(8) 2_565 1_455 ? XPA1 XPM BPCA 66.1(13) 1_455 1_455 ? BPW XPM BPCA 174.9(5) . 1_455 ? MHA XPM BPW 85(2) . 1_455 ? 4 XPM BPW 46.2(8) 1_445 1_455 ? 3 XPM BPW 135.2(10) 1_545 1_455 ? 1 XPM BPW 46.4(9) 1_455 1_455 ? 2 XPM BPW 130.7(11) . 1_455 ? MH XPM BPW 89.1(4) . 1_455 ? W1 XPM BPW 108.8(8) 1_545 1_455 ? W1 XPM BPW 71.7(8) 2_565 1_455 ? XPA1 XPM BPW 66.1(13) 1_455 1_455 ? BPW XPM BPW 174.9(5) . 1_455 ? BPCA XPM BPW 0.0(6) 1_455 1_455 ? MHA XPM O4 47.2(19) . . ? 4 XPM O4 161.4(10) 1_445 . ? 3 XPM O4 106.2(10) 1_545 . ? 1 XPM O4 118.8(10) 1_455 . ? 2 XPM O4 79.8(10) . . ? MH XPM O4 45.6(2) . . ? W1 XPM O4 118.0(8) 1_545 . ? W1 XPM O4 139.1(8) 2_565 . ? XPA1 XPM O4 87.3(13) 1_455 . ? BPW XPM O4 58.9(3) . . ? BPCA XPM O4 117.3(4) 1_455 . ? BPW XPM O4 117.3(4) 1_455 . ? MHA XPM O5 43.0(19) . 1_445 ? 4 XPM O5 87.5(9) 1_445 1_445 ? 3 XPM O5 131.3(10) 1_545 1_445 ? 1 XPM O5 108.0(10) 1_455 1_445 ? 2 XPM O5 166.8(11) . 1_445 ? MH XPM O5 44.4(2) . 1_445 ? W1 XPM O5 150.1(8) 1_545 1_445 ? W1 XPM O5 124.9(8) 2_565 1_445 ? XPA1 XPM O5 118.9(13) 1_455 1_445 ? BPW XPM O5 120.5(4) . 1_445 ? BPCA XPM O5 61.6(3) 1_455 1_445 ? BPW XPM O5 61.6(3) 1_455 1_445 ? O4 XPM O5 90.1(3) . 1_445 ? MHA XPM W3 99(2) . 1_455 ? 4 XPM W3 35.4(10) 1_445 1_455 ? 3 XPM W3 123.0(11) 1_545 1_455 ? 1 XPM W3 35.4(10) 1_455 1_455 ? 2 XPM W3 119.4(12) . 1_455 ? MH XPM W3 102.5(6) . 1_455 ? W1 XPM W3 95.3(10) 1_545 1_455 ? W1 XPM W3 58.2(9) 2_565 1_455 ? XPA1 XPM W3 60.6(14) 1_455 1_455 ? BPW XPM W3 166.0(7) . 1_455 ? BPCA XPM W3 13.5(4) 1_455 1_455 ? BPW XPM W3 13.5(4) 1_455 1_455 ? O4 XPM W3 126.6(6) . 1_455 ? O5 XPM W3 73.4(6) 1_445 1_455 ? MHA XPM O7 40.3(19) . 1_455 ? 4 XPM O7 103.8(9) 1_445 1_455 ? 3 XPM O7 164.5(10) 1_545 1_455 ? 1 XPM O7 80.4(9) 1_455 1_455 ? 2 XPM O7 120.7(10) . 1_455 ? MH XPM O7 44.2(2) . 1_455 ? W1 XPM O7 142.8(8) 1_545 1_455 ? W1 XPM O7 117.0(8) 2_565 1_455 ? XPA1 XPM O7 67.5(13) 1_455 1_455 ? BPW XPM O7 118.6(4) . 1_455 ? BPCA XPM O7 57.8(3) 1_455 1_455 ? BPW XPM O7 57.8(3) 1_455 1_455 ? O4 XPM O7 59.6(3) . 1_455 ? O5 XPM O7 59.2(3) 1_445 1_455 ? W3 XPM O7 68.6(6) 1_455 1_455 ? MHA XPM W3 107(2) . . ? 4 XPM W3 124.8(10) 1_445 . ? 3 XPM W3 37.0(11) 1_545 . ? 1 XPM W3 120.0(11) 1_455 . ? 2 XPM W3 36.1(11) . . ? MH XPM W3 103.1(6) . . ? W1 XPM W3 58.5(9) 1_545 . ? W1 XPM W3 95.3(9) 2_565 . ? XPA1 XPM W3 103.4(14) 1_455 . ? BPW XPM W3 13.3(4) . . ? BPCA XPM W3 166.2(7) 1_455 . ? BPW XPM W3 166.2(7) 1_455 . ? O4 XPM W3 69.3(6) . . ? O5 XPM W3 132.0(6) 1_445 . ? W3 XPM W3 153.1(11) 1_455 . ? O7 XPM W3 128.1(6) 1_455 . ? MHA XPM O3 48(2) . 1_545 ? 4 XPM O3 131.9(9) 1_445 1_545 ? 3 XPM O3 89.9(10) 1_545 1_545 ? 1 XPM O3 165.8(10) 1_455 1_545 ? 2 XPM O3 108.6(11) . 1_545 ? MH XPM O3 43.8(2) . 1_545 ? W1 XPM O3 124.7(8) 1_545 1_545 ? W1 XPM O3 153.4(8) 2_565 1_545 ? XPA1 XPM O3 146.8(13) 1_455 1_545 ? BPW XPM O3 61.9(3) . 1_545 ? BPCA XPM O3 120.1(4) 1_455 1_545 ? BPW XPM O3 120.1(4) 1_455 1_545 ? O4 XPM O3 60.3(3) . 1_545 ? O5 XPM O3 58.6(3) 1_445 1_545 ? W3 XPM O3 132.0(6) 1_455 1_545 ? O7 XPM O3 88.0(3) 1_455 1_545 ? W3 XPM O3 73.7(6) . 1_545 ? MHA XPM XPA3 115(2) . 1_445 ? 4 XPM XPA3 30.8(16) 1_445 1_445 ? 3 XPM XPA3 81.4(17) 1_545 1_445 ? 1 XPM XPA3 76.0(16) 1_455 1_445 ? 2 XPM XPA3 117.0(17) . 1_445 ? MH XPM XPA3 115.5(14) . 1_445 ? W1 XPM XPA3 79.1(15) 1_545 1_445 ? W1 XPM XPA3 61.0(15) 2_565 1_445 ? XPA1 XPM XPA3 108.5(19) 1_455 1_445 ? BPW XPM XPA3 123.3(14) . 1_445 ? BPCA XPM XPA3 61.5(14) 1_455 1_445 ? BPW XPM XPA3 61.5(14) 1_455 1_445 ? O4 XPM XPA3 159.8(14) . 1_445 ? O5 XPM XPA3 71.5(13) 1_445 1_445 ? W3 XPM XPA3 56.9(15) 1_455 1_445 ? O7 XPM XPA3 114.1(14) 1_455 1_445 ? W3 XPM XPA3 116.9(15) . 1_445 ? O3 XPM XPA3 101.8(14) 1_545 1_445 ? 1 XPA1 W2 132(4) . . ? 1 XPA1 XPA4 94(3) . 1_655 ? W2 XPA1 XPA4 103(3) . 1_655 ? 1 XPA1 W1 36.6(17) . 2_665 ? W2 XPA1 W1 100(2) . 2_665 ? XPA4 XPA1 W1 86(3) 1_655 2_665 ? 1 XPA1 2 56(2) . 1_655 ? W2 XPA1 2 129(3) . 1_655 ? XPA4 XPA1 2 38(2) 1_655 1_655 ? W1 XPA1 2 57.3(16) 2_665 1_655 ? 1 XPA1 AP 123(3) . 1_655 ? W2 XPA1 AP 105(2) . 1_655 ? XPA4 XPA1 AP 69(2) 1_655 1_655 ? W1 XPA1 AP 148(3) 2_665 1_655 ? 2 XPA1 AP 91.2(19) 1_655 1_655 ? 1 XPA1 XPA3 167(4) . . ? W2 XPA1 XPA3 47.0(19) . . ? XPA4 XPA1 XPA3 98(3) 1_655 . ? W1 XPA1 XPA3 147(3) 2_665 . ? 2 XPA1 XPA3 136(3) 1_655 . ? AP XPA1 XPA3 60.0(19) 1_655 . ? 1 XPA1 XPM 33.1(16) . 1_655 ? W2 XPA1 XPM 158(3) . 1_655 ? XPA4 XPA1 XPM 70(2) 1_655 1_655 ? W1 XPA1 XPM 59.0(15) 2_665 1_655 ? 2 XPA1 XPM 35.6(10) 1_655 1_655 ? AP XPA1 XPM 92.4(18) 1_655 1_655 ? XPA3 XPA1 XPM 152(3) . 1_655 ? 1 XPA1 W3 35.2(17) . . ? W2 XPA1 W3 117(3) . . ? XPA4 XPA1 W3 129(3) 1_655 . ? W1 XPA1 W3 58.4(15) 2_665 . ? 2 XPA1 W3 91(2) 1_655 . ? AP XPA1 W3 123(2) 1_655 . ? XPA3 XPA1 W3 132(3) . . ? XPM XPA1 W3 60.8(14) 1_655 . ? 1 XPA1 XPA2 95(3) . 2_665 ? W2 XPA1 XPA2 40.8(18) . 2_665 ? XPA4 XPA1 XPA2 93(3) 1_655 2_665 ? W1 XPA1 XPA2 60(2) 2_665 2_665 ? 2 XPA1 XPA2 97(2) 1_655 2_665 ? AP XPA1 XPA2 139(3) 1_655 2_665 ? XPA3 XPA1 XPA2 87(3) . 2_665 ? XPM XPA1 XPA2 117(2) 1_655 2_665 ? W3 XPA1 XPA2 98(2) . 2_665 ? 1 XPA1 4 1.3(14) . 1_545 ? W2 XPA1 4 132(3) . 1_545 ? XPA4 XPA1 4 93(3) 1_655 1_545 ? W1 XPA1 4 35.6(12) 2_665 1_545 ? 2 XPA1 4 55.3(14) 1_655 1_545 ? AP XPA1 4 123(2) 1_655 1_545 ? XPA3 XPA1 4 169(3) . 1_545 ? XPM XPA1 4 32.8(9) 1_655 1_545 ? W3 XPA1 4 36.4(10) . 1_545 ? XPA2 XPA1 4 94(2) 2_665 1_545 ? 1 XPA1 BPW 38.8(17) . . ? W2 XPA1 BPW 126(3) . . ? XPA4 XPA1 BPW 127(3) 1_655 . ? W1 XPA1 BPW 68.0(16) 2_665 . ? 2 XPA1 BPW 90.7(19) 1_655 . ? AP XPA1 BPW 110(2) 1_655 . ? XPA3 XPA1 BPW 129(3) . . ? XPM XPA1 BPW 57.1(12) 1_655 . ? W3 XPA1 BPW 12.4(5) . . ? XPA2 XPA1 BPW 110(2) 2_665 . ? 4 XPA1 BPW 40.0(9) 1_545 . ? 1 XPA1 O7 72(2) . . ? W2 XPA1 O7 144(3) . . ? XPA4 XPA1 O7 100(3) 1_655 . ? W1 XPA1 O7 109(2) 2_665 . ? 2 XPA1 O7 85.9(18) 1_655 . ? AP XPA1 O7 58.3(12) 1_655 . ? XPA3 XPA1 O7 103(2) . . ? XPM XPA1 O7 57.5(12) 1_655 . ? W3 XPA1 O7 64.9(14) . . ? XPA2 XPA1 O7 162(3) 2_665 . ? 4 XPA1 O7 73.2(15) 1_545 . ? BPW XPA1 O7 52.5(10) . . ? 1 XPA1 XPB 149(4) . . ? W2 XPA1 XPB 46.3(19) . . ? XPA4 XPA1 XPB 117(3) 1_655 . ? W1 XPA1 XPB 141(3) 2_665 . ? 2 XPA1 XPB 155(3) 1_655 . ? AP XPA1 XPB 70(2) 1_655 . ? XPA3 XPA1 XPB 18.9(19) . . ? XPM XPA1 XPB 156(3) 1_655 . ? W3 XPA1 XPB 114(3) . . ? XPA2 XPA1 XPB 86(3) 2_665 . ? 4 XPA1 XPB 150(3) 1_545 . ? BPW XPA1 XPB 112(2) . . ? O7 XPA1 XPB 98(2) . . ? 1 XPA1 W2 119(3) . 2_765 ? W2 XPA1 W2 68.5(18) . 2_765 ? XPA4 XPA1 W2 35(2) 1_655 2_765 ? W1 XPA1 W2 93.6(19) 2_665 2_765 ? 2 XPA1 W2 67.9(15) 1_655 2_765 ? AP XPA1 W2 78.0(15) 1_655 2_765 ? XPA3 XPA1 W2 74(2) . 2_765 ? XPM XPA1 W2 102.8(19) 1_655 2_765 ? W3 XPA1 W2 152(2) . 2_765 ? XPA2 XPA1 W2 68.2(19) 2_665 2_765 ? 4 XPA1 W2 118(2) 1_545 2_765 ? BPW XPA1 W2 157(2) . 2_765 ? O7 XPA1 W2 129(2) . 2_765 ? XPB XPA1 W2 91(2) . 2_765 ? 1 XPA1 XPA4 87(3) . . ? W2 XPA1 XPA4 73(2) . . ? XPA4 XPA1 XPA4 176(4) 1_655 . ? W1 XPA1 XPA4 94(2) 2_665 . ? 2 XPA1 XPA4 144(3) 1_655 . ? AP XPA1 XPA4 112(2) 1_655 . ? XPA3 XPA1 XPA4 80(2) . . ? XPM XPA1 XPA4 113(2) 1_655 . ? W3 XPA1 XPA4 53.2(16) . . ? XPA2 XPA1 XPA4 83(2) 2_665 . ? 4 XPA1 XPA4 88(2) 1_545 . ? BPW XPA1 XPA4 55.9(16) . . ? O7 XPA1 XPA4 83.8(18) . . ? XPB XPA1 XPA4 62(2) . . ? W2 XPA1 XPA4 142(2) 2_765 . ? 1 XPA1 W1 50(2) . 1_645 ? W2 XPA1 W1 108(2) . 1_645 ? XPA4 XPA1 W1 56(2) 1_655 1_645 ? W1 XPA1 W1 30.5(15) 2_665 1_645 ? 2 XPA1 W1 30.5(10) 1_655 1_645 ? AP XPA1 W1 120(2) 1_655 1_645 ? XPA3 XPA1 W1 142(3) . 1_645 ? XPM XPA1 W1 50.7(12) 1_655 1_645 ? W3 XPA1 W1 82.1(17) . 1_645 ? XPA2 XPA1 W1 69.8(19) 2_665 1_645 ? 4 XPA1 W1 48.2(12) 1_545 1_645 ? BPW XPA1 W1 88.1(17) . 1_645 ? O7 XPA1 W1 108.2(19) . 1_645 ? XPB XPA1 W1 153(3) . 1_645 ? W2 XPA1 W1 70.0(14) 2_765 1_645 ? XPA4 XPA1 W1 124(2) . 1_645 ? 1 XPA1 3 63(2) . 2_665 ? W2 XPA1 3 72.5(18) . 2_665 ? XPA4 XPA1 3 91(3) 1_655 2_665 ? W1 XPA1 3 27.9(11) 2_665 2_665 ? 2 XPA1 3 75.6(16) 1_655 2_665 ? AP XPA1 3 159(2) 1_655 2_665 ? XPA3 XPA1 3 119(2) . 2_665 ? XPM XPA1 3 86.3(16) 1_655 2_665 ? W3 XPA1 3 74.5(15) . 2_665 ? XPA2 XPA1 3 32.2(15) 2_665 2_665 ? 4 XPA1 3 62.4(13) 1_545 2_665 ? BPW XPA1 3 86.4(16) . 2_665 ? O7 XPA1 3 135(2) . 2_665 ? XPB XPA1 3 116(2) . 2_665 ? W2 XPA1 3 81.8(15) 2_765 2_665 ? XPA4 XPA1 3 87.5(19) . 2_665 ? W1 XPA1 3 45.1(11) 1_645 2_665 ? 1 XPA1 5 114(3) . 1_655 ? W2 XPA1 5 113(2) . 1_655 ? XPA4 XPA1 5 74(2) 1_655 1_655 ? W1 XPA1 5 144(2) 2_665 1_655 ? 2 XPA1 5 90.3(18) 1_655 1_655 ? AP XPA1 5 9.9(4) 1_655 1_655 ? XPA3 XPA1 5 66.6(19) . 1_655 ? XPM XPA1 5 85.9(16) 1_655 1_655 ? W3 XPA1 5 113(2) . 1_655 ? XPA2 XPA1 5 148(3) 2_665 1_655 ? 4 XPA1 5 114.9(19) 1_545 1_655 ? BPW XPA1 5 100.6(17) . 1_655 ? O7 XPA1 5 48.5(9) . 1_655 ? XPB XPA1 5 75(2) . 1_655 ? W2 XPA1 5 86.8(15) 2_765 1_655 ? XPA4 XPA1 5 108(2) . 1_655 ? W1 XPA1 5 120.6(19) 1_645 1_655 ? 3 XPA1 5 164(2) 2_665 1_655 ? XPB XPA2 3 89(4) . . ? XPB XPA2 W2 87(4) . 2_665 ? 3 XPA2 W2 136(4) . 2_665 ? XPB XPA2 XPA4 97(4) . . ? 3 XPA2 XPA4 172(4) . . ? W2 XPA2 XPA4 48(2) 2_665 . ? XPB XPA2 AP 119(4) . . ? 3 XPA2 AP 108(3) . . ? W2 XPA2 AP 112(3) 2_665 . ? XPA4 XPA2 AP 66(2) . . ? XPB XPA2 W1 96(4) . . ? 3 XPA2 W1 33.9(16) . . ? W2 XPA2 W1 103(3) 2_665 . ? XPA4 XPA2 W1 147(3) . . ? AP XPA2 W1 130(3) . . ? XPB XPA2 XPA3 171(4) . 1_455 ? 3 XPA2 XPA3 82(3) . 1_455 ? W2 XPA2 XPA3 102(3) 2_665 1_455 ? XPA4 XPA2 XPA3 91(3) . 1_455 ? AP XPA2 XPA3 61(2) . 1_455 ? W1 XPA2 XPA3 79(2) . 1_455 ? XPB XPA2 XPA3 3(3) . . ? 3 XPA2 XPA3 92(3) . . ? W2 XPA2 XPA3 84(3) 2_665 . ? XPA4 XPA2 XPA3 95(3) . . ? AP XPA2 XPA3 119(3) . . ? W1 XPA2 XPA3 98(3) . . ? XPA3 XPA2 XPA3 174(4) 1_455 . ? XPB XPA2 XPA1 98(4) . 2_665 ? 3 XPA2 XPA1 91(3) . 2_665 ? W2 XPA2 XPA1 47(2) 2_665 2_665 ? XPA4 XPA2 XPA1 92(3) . 2_665 ? AP XPA2 XPA1 138(3) . 2_665 ? W1 XPA2 XPA1 56.8(19) . 2_665 ? XPA3 XPA2 XPA1 86(3) 1_455 2_665 ? XPA3 XPA2 XPA1 97(3) . 2_665 ? XPB XPA2 XPM 110(4) . 1_565 ? 3 XPA2 XPM 29.8(14) . 1_565 ? W2 XPA2 XPM 153(3) 2_665 1_565 ? XPA4 XPA2 XPM 143(3) . 1_565 ? AP XPA2 XPM 78.8(17) . 1_565 ? W1 XPA2 XPM 55.5(14) . 1_565 ? XPA3 XPA2 XPM 60.9(19) 1_455 1_565 ? XPA3 XPA2 XPM 113(3) . 1_565 ? XPA1 XPA2 XPM 108(2) 2_665 1_565 ? XPB XPA2 W3 53(3) . 1_565 ? 3 XPA2 W3 36.5(16) . 1_565 ? W2 XPA2 W3 127(3) 2_665 1_565 ? XPA4 XPA2 W3 150(3) . 1_565 ? AP XPA2 W3 117(2) . 1_565 ? W1 XPA2 W3 56.2(15) . 1_565 ? XPA3 XPA2 W3 118(3) 1_455 1_565 ? XPA3 XPA2 W3 56.4(19) . 1_565 ? XPA1 XPA2 W3 100(2) 2_665 1_565 ? XPM XPA2 W3 58.4(13) 1_565 1_565 ? XPB XPA2 4 137(4) . 1_455 ? 3 XPA2 4 48.1(18) . 1_455 ? W2 XPA2 4 124(3) 2_665 1_455 ? XPA4 XPA2 4 125(3) . 1_455 ? AP XPA2 4 78.8(17) . 1_455 ? W1 XPA2 4 52.3(14) . 1_455 ? XPA3 XPA2 4 34.1(16) 1_455 1_455 ? XPA3 XPA2 4 140(3) . 1_455 ? XPA1 XPA2 4 87(2) 2_665 1_455 ? XPM XPA2 4 31.3(8) 1_565 1_455 ? W3 XPA2 4 84.0(18) 1_565 1_455 ? XPB XPA2 2 87(4) . 1_565 ? 3 XPA2 2 2.3(13) . 1_565 ? W2 XPA2 2 135(3) 2_665 1_565 ? XPA4 XPA2 2 175(3) . 1_565 ? AP XPA2 2 110(2) . 1_565 ? W1 XPA2 2 33.0(11) . 1_565 ? XPA3 XPA2 2 84(2) 1_455 1_565 ? XPA3 XPA2 2 90(2) . 1_565 ? XPA1 XPA2 2 90(2) 2_665 1_565 ? XPM XPA2 2 32.1(9) 1_565 1_565 ? W3 XPA2 2 34.7(10) 1_565 1_565 ? 4 XPA2 2 50.1(12) 1_455 1_565 ? XPB XPA2 BPW 55(3) . 1_565 ? 3 XPA2 BPW 39.3(16) . 1_565 ? W2 XPA2 BPW 137(3) 2_665 1_565 ? XPA4 XPA2 BPW 145(3) . 1_565 ? AP XPA2 BPW 105(2) . 1_565 ? W1 XPA2 BPW 65.2(16) . 1_565 ? XPA3 XPA2 BPW 115(3) 1_455 1_565 ? XPA3 XPA2 BPW 58.4(19) . 1_565 ? XPA1 XPA2 BPW 112(2) 2_665 1_565 ? XPM XPA2 BPW 54.6(12) 1_565 1_565 ? W3 XPA2 BPW 12.1(5) 1_565 1_565 ? 4 XPA2 BPW 83.5(17) 1_455 1_565 ? 2 XPA2 BPW 38.3(10) 1_565 1_565 ? XPB XPA2 BPCA 55(3) . 1_565 ? 3 XPA2 BPCA 39.3(16) . 1_565 ? W2 XPA2 BPCA 137(3) 2_665 1_565 ? XPA4 XPA2 BPCA 145(3) . 1_565 ? AP XPA2 BPCA 105(2) . 1_565 ? W1 XPA2 BPCA 65.2(16) . 1_565 ? XPA3 XPA2 BPCA 115(3) 1_455 1_565 ? XPA3 XPA2 BPCA 58.4(19) . 1_565 ? XPA1 XPA2 BPCA 112(2) 2_665 1_565 ? XPM XPA2 BPCA 54.6(12) 1_565 1_565 ? W3 XPA2 BPCA 12.1(5) 1_565 1_565 ? 4 XPA2 BPCA 83.5(17) 1_455 1_565 ? 2 XPA2 BPCA 38.3(10) 1_565 1_565 ? BPW XPA2 BPCA 0.0(2) 1_565 1_565 ? XPB XPA2 W2 41(3) . . ? 3 XPA2 W2 118(3) . . ? W2 XPA2 W2 45.8(17) 2_665 . ? XPA4 XPA2 W2 69(2) . . ? AP XPA2 W2 126(2) . . ? W1 XPA2 W2 104(2) . . ? XPA3 XPA2 W2 148(3) 1_455 . ? XPA3 XPA2 W2 38.2(16) . . ? XPA1 XPA2 W2 70.0(19) 2_665 . ? XPM XPA2 W2 147(2) 1_565 . ? W3 XPA2 W2 88.6(18) 1_565 . ? 4 XPA2 W2 154(2) 1_455 . ? 2 XPA2 W2 116(2) 1_565 . ? BPW XPA2 W2 94.2(18) 1_565 . ? BPCA XPA2 W2 94.2(18) 1_565 . ? XPB XPA2 1 93(4) . 2_665 ? 3 XPA2 1 62(2) . 2_665 ? W2 XPA2 1 74(2) 2_665 2_665 ? XPA4 XPA2 1 120(3) . 2_665 ? AP XPA2 1 148(2) . 2_665 ? W1 XPA2 1 29.2(10) . 2_665 ? XPA3 XPA2 1 87(2) 1_455 2_665 ? XPA3 XPA2 1 93(2) . 2_665 ? XPA1 XPA2 1 28.6(14) 2_665 2_665 ? XPM XPA2 1 84.0(17) 1_565 2_665 ? W3 XPA2 1 74.5(16) 1_565 2_665 ? 4 XPA2 1 72.3(15) 1_455 2_665 ? 2 XPA2 1 61.2(13) 1_565 2_665 ? BPW XPA2 1 85.9(16) 1_565 2_665 ? BPCA XPA2 1 85.9(16) 1_565 2_665 ? W2 XPA2 1 82.1(16) . 2_665 ? XPB XPA2 5 111(4) . . ? 3 XPA2 5 103(3) . . ? W2 XPA2 5 118(3) 2_665 . ? XPA4 XPA2 5 71(2) . . ? AP XPA2 5 9.0(4) . . ? W1 XPA2 5 130(2) . . ? XPA3 XPA2 5 66.8(19) 1_455 . ? XPA3 XPA2 5 112(2) . . ? XPA1 XPA2 5 147(3) 2_665 . ? XPM XPA2 5 75.8(15) 1_565 . ? W3 XPA2 5 109(2) 1_565 . ? 4 XPA2 5 80.7(16) 1_455 . ? 2 XPA2 5 105.4(19) 1_565 . ? BPW XPA2 5 97.1(17) 1_565 . ? BPCA XPA2 5 97.1(17) 1_565 . ? W2 XPA2 5 125(2) . . ? 1 XPA2 5 152(2) 2_665 . ? XPB XPA2 W2 153(4) . 1_455 ? 3 XPA2 W2 108(3) . 1_455 ? W2 XPA2 W2 66(2) 2_665 1_455 ? XPA4 XPA2 W2 67(2) . 1_455 ? AP XPA2 W2 76.5(16) . 1_455 ? W1 XPA2 W2 88.1(19) . 1_455 ? XPA3 XPA2 W2 36.2(16) 1_455 1_455 ? XPA3 XPA2 W2 150(3) . 1_455 ? XPA1 XPA2 W2 61.7(18) 2_665 1_455 ? XPM XPA2 W2 94.9(18) 1_565 1_455 ? W3 XPA2 W2 143(2) 1_565 1_455 ? 4 XPA2 W2 64.3(14) 1_455 1_455 ? 2 XPA2 W2 109(2) 1_565 1_455 ? BPW XPA2 W2 147(2) 1_565 1_455 ? BPCA XPA2 W2 147(2) 1_565 1_455 ? W2 XPA2 W2 111.4(19) . 1_455 ? 1 XPA2 W2 77.8(15) 2_665 1_455 ? 5 XPA2 W2 85.3(15) . 1_455 ? XPB XPA2 XPA1 137(4) . 1_455 ? 3 XPA2 XPA1 133(3) . 1_455 ? W2 XPA2 XPA1 67(2) 2_665 1_455 ? XPA4 XPA2 XPA1 40(2) . 1_455 ? AP XPA2 XPA1 50.6(15) . 1_455 ? W1 XPA2 XPA1 122(3) . 1_455 ? XPA3 XPA2 XPA1 51(2) 1_455 1_455 ? XPA3 XPA2 XPA1 134(3) . 1_455 ? XPA1 XPA2 XPA1 89(2) 2_665 1_455 ? XPM XPA2 XPA1 108(2) 1_565 1_455 ? W3 XPA2 XPA1 165(3) 1_565 1_455 ? 4 XPA2 XPA1 84.9(19) 1_455 1_455 ? 2 XPA2 XPA1 135(2) 1_565 1_455 ? BPW XPA2 XPA1 155(2) 1_565 1_455 ? BPCA XPA2 XPA1 155(2) 1_565 1_455 ? W2 XPA2 XPA1 106(2) . 1_455 ? 1 XPA2 XPA1 111(2) 2_665 1_455 ? 5 XPA2 XPA1 59.3(15) . 1_455 ? W2 XPA2 XPA1 34.9(12) 1_455 1_455 ? XPB XPA3 4 99(7) . . ? XPB XPA3 W2 89(6) . . ? 4 XPA3 W2 135(4) . . ? XPB XPA3 W3 60(6) . 1_565 ? 4 XPA3 W3 39.8(17) . 1_565 ? W2 XPA3 W3 132(3) . 1_565 ? XPB XPA3 AP 121(7) . 1_655 ? 4 XPA3 AP 107(3) . 1_655 ? W2 XPA3 AP 106(3) . 1_655 ? W3 XPA3 AP 121(2) 1_565 1_655 ? XPB XPA3 XPA2 179(7) . 1_655 ? 4 XPA3 XPA2 81(3) . 1_655 ? W2 XPA3 XPA2 90(3) . 1_655 ? W3 XPA3 XPA2 121(3) 1_565 1_655 ? AP XPA3 XPA2 59(2) 1_655 1_655 ? XPB XPA3 XPA1 101(7) . . ? 4 XPA3 XPA1 160(4) . . ? W2 XPA3 XPA1 49(2) . . ? W3 XPA3 XPA1 159(3) 1_565 . ? AP XPA3 XPA1 59.6(19) 1_655 . ? XPA2 XPA3 XPA1 78(3) 1_655 . ? XPB XPA3 XPA2 6(5) . . ? 4 XPA3 XPA2 104(3) . . ? W2 XPA3 XPA2 84(3) . . ? W3 XPA3 XPA2 65(2) 1_565 . ? AP XPA3 XPA2 121(3) 1_655 . ? XPA2 XPA3 XPA2 174(4) 1_655 . ? XPA1 XPA3 XPA2 96(3) . . ? XPB XPA3 W1 102(6) . 2_675 ? 4 XPA3 W1 34.3(17) . 2_675 ? W2 XPA3 W1 101(3) . 2_675 ? W3 XPA3 W1 57.7(16) 1_565 2_675 ? AP XPA3 W1 129(3) 1_655 2_675 ? XPA2 XPA3 W1 79(2) 1_655 2_675 ? XPA1 XPA3 W1 141(3) . 2_675 ? XPA2 XPA3 W1 104(3) . 2_675 ? XPB XPA3 XPA4 97(6) . 2_665 ? 4 XPA3 XPA4 93(3) . 2_665 ? W2 XPA3 XPA4 42.3(19) . 2_665 ? W3 XPA3 XPA4 102(3) 1_565 2_665 ? AP XPA3 XPA4 133(3) 1_655 2_665 ? XPA2 XPA3 XPA4 83(3) 1_655 2_665 ? XPA1 XPA3 XPA4 88(3) . 2_665 ? XPA2 XPA3 XPA4 94(3) . 2_665 ? W1 XPA3 XPA4 58(2) 2_675 2_665 ? XPB XPA3 XPM 118(7) . 1_665 ? 4 XPA3 XPM 28.6(15) . 1_665 ? W2 XPA3 XPM 145(3) . 1_665 ? W3 XPA3 XPM 60.6(15) 1_565 1_665 ? AP XPA3 XPM 78.5(18) 1_655 1_665 ? XPA2 XPA3 XPM 62(2) 1_655 1_665 ? XPA1 XPA3 XPM 134(3) . 1_665 ? XPA2 XPA3 XPM 124(3) . 1_665 ? W1 XPA3 XPM 55.9(15) 2_675 1_665 ? XPA4 XPA3 XPM 109(3) 2_665 1_665 ? XPB XPA3 BPCA 61(6) . 1_565 ? 4 XPA3 BPCA 43.4(17) . 1_565 ? W2 XPA3 BPCA 143(3) . 1_565 ? W3 XPA3 BPCA 13.1(6) 1_565 1_565 ? AP XPA3 BPCA 108(2) 1_655 1_565 ? XPA2 XPA3 BPCA 120(3) 1_655 1_565 ? XPA1 XPA3 BPCA 151(3) . 1_565 ? XPA2 XPA3 BPCA 66(2) . 1_565 ? W1 XPA3 BPCA 67.8(16) 2_675 1_565 ? XPA4 XPA3 BPCA 115(3) 2_665 1_565 ? XPM XPA3 BPCA 57.4(13) 1_665 1_565 ? XPB XPA3 BPW 61(6) . 1_565 ? 4 XPA3 BPW 43.4(17) . 1_565 ? W2 XPA3 BPW 143(3) . 1_565 ? W3 XPA3 BPW 13.1(6) 1_565 1_565 ? AP XPA3 BPW 108(2) 1_655 1_565 ? XPA2 XPA3 BPW 120(3) 1_655 1_565 ? XPA1 XPA3 BPW 151(3) . 1_565 ? XPA2 XPA3 BPW 66(2) . 1_565 ? W1 XPA3 BPW 67.8(16) 2_675 1_565 ? XPA4 XPA3 BPW 115(3) 2_665 1_565 ? XPM XPA3 BPW 57.4(13) 1_665 1_565 ? BPCA XPA3 BPW 0.0(5) 1_565 1_565 ? XPB XPA3 1 95(6) . 1_565 ? 4 XPA3 1 4.7(13) . 1_565 ? W2 XPA3 1 134(3) . 1_565 ? W3 XPA3 1 35.9(11) 1_565 1_565 ? AP XPA3 1 111(2) 1_655 1_565 ? XPA2 XPA3 1 86(2) 1_655 1_565 ? XPA1 XPA3 1 164(3) . 1_565 ? XPA2 XPA3 1 100(3) . 1_565 ? W1 XPA3 1 33.5(11) 2_675 1_565 ? XPA4 XPA3 1 91(2) 2_665 1_565 ? XPM XPA3 1 33.0(9) 1_665 1_565 ? BPCA XPA3 1 40.5(10) 1_565 1_565 ? BPW XPA3 1 40.5(10) 1_565 1_565 ? XPB XPA3 3 145(7) . 1_655 ? 4 XPA3 3 46.0(19) . 1_655 ? W2 XPA3 3 115(3) . 1_655 ? W3 XPA3 3 85.5(19) 1_565 1_655 ? AP XPA3 3 77.7(18) 1_655 1_655 ? XPA2 XPA3 3 35.4(17) 1_655 1_655 ? XPA1 XPA3 3 114(3) . 1_655 ? XPA2 XPA3 3 150(3) . 1_655 ? W1 XPA3 3 51.3(14) 2_675 1_655 ? XPA4 XPA3 3 87(2) 2_665 1_655 ? XPM XPA3 3 31.3(9) 1_665 1_655 ? BPCA XPA3 3 86.1(18) 1_565 1_655 ? BPW XPA3 3 86.1(18) 1_565 1_655 ? 1 XPA3 3 50.4(13) 1_565 1_655 ? XPB XPA3 W2 41(5) . 2_665 ? 4 XPA3 W2 127(3) . 2_665 ? W2 XPA3 W2 48.3(17) . 2_665 ? W3 XPA3 W2 94(2) 1_565 2_665 ? AP XPA3 W2 123(2) 1_655 2_665 ? XPA2 XPA3 W2 139(3) 1_655 2_665 ? XPA1 XPA3 W2 72(2) . 2_665 ? XPA2 XPA3 W2 35.5(16) . 2_665 ? W1 XPA3 W2 107(2) 2_675 2_665 ? XPA4 XPA3 W2 68(2) 2_665 2_665 ? XPM XPA3 W2 154(3) 1_665 2_665 ? BPCA XPA3 W2 100(2) 1_565 2_665 ? BPW XPA3 W2 100(2) 1_565 2_665 ? 1 XPA3 W2 122(2) 1_565 2_665 ? 3 XPA3 W2 154(2) 1_655 2_665 ? XPB XPA3 3 27(5) . . ? 4 XPA3 3 72(2) . . ? W2 XPA3 3 107(3) . . ? W3 XPA3 3 33.1(10) 1_565 . ? AP XPA3 3 131(2) 1_655 . ? XPA2 XPA3 3 153(3) 1_655 . ? XPA1 XPA3 3 128(3) . . ? XPA2 XPA3 3 32.2(16) . . ? W1 XPA3 3 78.1(18) 2_675 . ? XPA4 XPA3 3 96(2) 2_665 . ? XPM XPA3 3 93.5(18) 1_665 . ? BPCA XPA3 3 37.4(9) 1_565 . ? BPW XPA3 3 37.4(9) 1_565 . ? 1 XPA3 3 67.5(15) 1_565 . ? 3 XPA3 3 118(2) 1_655 . ? W2 XPA3 3 62.3(14) 2_665 . ? XPB XPA3 2 96(6) . 2_665 ? 4 XPA3 2 64(2) . 2_665 ? W2 XPA3 2 71(2) . 2_665 ? W3 XPA3 2 76.8(17) 1_565 2_665 ? AP XPA3 2 142(3) 1_655 2_665 ? XPA2 XPA3 2 84(2) 1_655 2_665 ? XPA1 XPA3 2 116(2) . 2_665 ? XPA2 XPA3 2 96(2) . 2_665 ? W1 XPA3 2 29.7(11) 2_675 2_665 ? XPA4 XPA3 2 29.1(15) 2_665 2_665 ? XPM XPA3 2 84.5(17) 1_665 2_665 ? BPCA XPA3 2 89.3(18) 1_565 2_665 ? BPW XPA3 2 89.3(18) 1_565 2_665 ? 1 XPA3 2 62.4(14) 1_565 2_665 ? 3 XPA3 2 70.7(15) 1_655 2_665 ? W2 XPA3 2 83.9(17) 2_665 2_665 ? 3 XPA3 2 82.4(16) . 2_665 ? XPB XPA3 5 114(6) . 1_655 ? 4 XPA3 5 103(3) . 1_655 ? W2 XPA3 5 114(3) . 1_655 ? W3 XPA3 5 112(2) 1_565 1_655 ? AP XPA3 5 9.6(4) 1_655 1_655 ? XPA2 XPA3 5 66(2) 1_655 1_655 ? XPA1 XPA3 5 65.8(19) . 1_655 ? XPA2 XPA3 5 115(2) . 1_655 ? W1 XPA3 5 129(2) 2_675 1_655 ? XPA4 XPA3 5 142(3) 2_665 1_655 ? XPM XPA3 5 75.7(15) 1_665 1_655 ? BPCA XPA3 5 99.6(19) 1_565 1_655 ? BPW XPA3 5 99.6(19) 1_565 1_655 ? 1 XPA3 5 107(2) 1_565 1_655 ? 3 XPA3 5 80.2(16) 1_655 1_655 ? W2 XPA3 5 123(2) 2_665 1_655 ? 3 XPA3 5 122(2) . 1_655 ? 2 XPA3 5 149(2) 2_665 1_655 ? XPB XPA3 W1 130(7) . 1_655 ? 4 XPA3 W1 43.3(19) . 1_655 ? W2 XPA3 W1 99(2) . 1_655 ? W3 XPA3 W1 79.7(18) 1_565 1_655 ? AP XPA3 W1 104(2) 1_655 1_655 ? XPA2 XPA3 W1 50.4(18) 1_655 1_655 ? XPA1 XPA3 W1 121(3) . 1_655 ? XPA2 XPA3 W1 132(3) . 1_655 ? W1 XPA3 W1 28.3(14) 2_675 1_655 ? XPA4 XPA3 W1 63(2) 2_665 1_655 ? XPM XPA3 W1 47.5(12) 1_665 1_655 ? BPCA XPA3 W1 86.2(18) 1_565 1_655 ? BPW XPA3 W1 86.2(18) 1_565 1_655 ? 1 XPA3 W1 45.7(12) 1_565 1_655 ? 3 XPA3 W1 27.3(9) 1_655 1_655 ? W2 XPA3 W1 127(2) 2_665 1_655 ? 3 XPA3 W1 105.4(19) . 1_655 ? 2 XPA3 W1 43.4(11) 2_665 1_655 ? 5 XPA3 W1 107.1(19) 1_655 1_655 ? 2 XPA4 W2 140(4) . 2_665 ? 2 XPA4 XPA1 85(3) . 1_455 ? W2 XPA4 XPA1 103(3) 2_665 1_455 ? 2 XPA4 XPA2 174(4) . . ? W2 XPA4 XPA2 46(2) 2_665 . ? XPA1 XPA4 XPA2 93(3) 1_455 . ? 2 XPA4 W1 35.0(18) . 1_545 ? W2 XPA4 W1 106(3) 2_665 1_545 ? XPA1 XPA4 W1 82(3) 1_455 1_545 ? XPA2 XPA4 W1 150(3) . 1_545 ? 2 XPA4 W3 38.7(18) . . ? W2 XPA4 W3 125(3) 2_665 . ? XPA1 XPA4 W3 123(3) 1_455 . ? XPA2 XPA4 W3 141(3) . . ? W1 XPA4 W3 58.4(16) 1_545 . ? 2 XPA4 XPA3 95(3) . 2_665 ? W2 XPA4 XPA3 46(2) 2_665 2_665 ? XPA1 XPA4 XPA3 97(3) 1_455 2_665 ? XPA2 XPA4 XPA3 91(3) . 2_665 ? W1 XPA4 XPA3 61(2) 1_545 2_665 ? W3 XPA4 XPA3 97(2) . 2_665 ? 2 XPA4 AP 115(3) . . ? W2 XPA4 AP 104(3) 2_665 . ? XPA1 XPA4 AP 63(2) 1_455 . ? XPA2 XPA4 AP 59(2) . . ? W1 XPA4 AP 139(3) 1_545 . ? W3 XPA4 AP 122(2) . . ? XPA3 XPA4 AP 141(3) 2_665 . ? 2 XPA4 1 51(2) . 1_455 ? W2 XPA4 1 127(3) 2_665 1_455 ? XPA1 XPA4 1 34.5(19) 1_455 1_455 ? XPA2 XPA4 1 127(3) . 1_455 ? W1 XPA4 1 54.3(15) 1_545 1_455 ? W3 XPA4 1 89(2) . 1_455 ? XPA3 XPA4 1 97(2) 2_665 1_455 ? AP XPA4 1 84.9(19) . 1_455 ? 2 XPA4 XPM 29.3(16) . . ? W2 XPA4 XPM 158(3) 2_665 . ? XPA1 XPA4 XPM 64(2) 1_455 . ? XPA2 XPA4 XPM 146(3) . . ? W1 XPA4 XPM 55.7(15) 1_545 . ? W3 XPA4 XPM 60.6(15) . . ? XPA3 XPA4 XPM 115(3) 2_665 . ? AP XPA4 XPM 87.1(18) . . ? 1 XPA4 XPM 33.4(9) 1_455 . ? 2 XPA4 3 3.1(14) . 1_545 ? W2 XPA4 3 137(3) 2_665 1_545 ? XPA1 XPA4 3 87(3) 1_455 1_545 ? XPA2 XPA4 3 177(3) . 1_545 ? W1 XPA4 3 32.7(12) 1_545 1_545 ? W3 XPA4 3 37.7(11) . 1_545 ? XPA3 XPA4 3 92(2) 2_665 1_545 ? AP XPA4 3 118(2) . 1_545 ? 1 XPA4 3 52.6(14) 1_455 1_545 ? XPM XPA4 3 32.2(9) . 1_545 ? 2 XPA4 BPW 41.0(18) . . ? W2 XPA4 BPW 134(3) 2_665 . ? XPA1 XPA4 BPW 120(3) 1_455 . ? XPA2 XPA4 BPW 137(3) . . ? W1 XPA4 BPW 67.3(17) 1_545 . ? W3 XPA4 BPW 12.6(6) . . ? XPA3 XPA4 BPW 110(3) 2_665 . ? AP XPA4 BPW 109(2) . . ? 1 XPA4 BPW 88.0(19) 1_455 . ? XPM XPA4 BPW 56.3(12) . . ? 3 XPA4 BPW 40.9(10) 1_545 . ? 2 XPA4 O4 71(2) . . ? W2 XPA4 O4 146(3) 2_665 . ? XPA1 XPA4 O4 91(3) 1_455 . ? XPA2 XPA4 O4 104(3) . . ? W1 XPA4 O4 106(2) 1_545 . ? W3 XPA4 O4 66.2(15) . . ? XPA3 XPA4 O4 163(3) 2_665 . ? AP XPA4 O4 55.6(12) . . ? 1 XPA4 O4 80.9(17) 1_455 . ? XPM XPA4 O4 55.4(12) . . ? 3 XPA4 O4 73.2(16) 1_545 . ? BPW XPA4 O4 53.6(12) . . ? 2 XPA4 XPB 95(3) . 2_665 ? W2 XPA4 XPB 46(2) 2_665 2_665 ? XPA1 XPA4 XPB 116(3) 1_455 2_665 ? XPA2 XPA4 XPB 91(3) . 2_665 ? W1 XPA4 XPB 66(2) 1_545 2_665 ? W3 XPA4 XPB 85(2) . 2_665 ? XPA3 XPA4 XPB 19.1(18) 2_665 2_665 ? AP XPA4 XPB 150(3) . 2_665 ? 1 XPA4 XPB 112(3) 1_455 2_665 ? XPM XPA4 XPB 121(3) . 2_665 ? 3 XPA4 XPB 92(2) 1_545 2_665 ? BPW XPA4 XPB 97(2) . 2_665 ? O4 XPA4 XPB 149(3) . 2_665 ? 2 XPA4 XPB 149(4) . . ? W2 XPA4 XPB 49(2) 2_665 . ? XPA1 XPA4 XPB 125(3) 1_455 . ? XPA2 XPA4 XPB 32(2) . . ? W1 XPA4 XPB 144(3) 1_545 . ? W3 XPA4 XPB 110(3) . . ? XPA3 XPA4 XPB 90(3) 2_665 . ? AP XPA4 XPB 77(2) . . ? 1 XPA4 XPB 159(3) 1_455 . ? XPM XPA4 XPB 153(3) . . ? 3 XPA4 XPB 148(3) 1_545 . ? BPW XPA4 XPB 109(2) . . ? O4 XPA4 XPB 98(2) . . ? XPB XPA4 XPB 80(3) 2_665 . ? 2 XPA4 XPA1 93(3) . . ? W2 XPA4 XPA1 80(2) 2_665 . ? XPA1 XPA4 XPA1 176(4) 1_455 . ? XPA2 XPA4 XPA1 89(3) . . ? W1 XPA4 XPA1 98(2) 1_545 . ? W3 XPA4 XPA1 54.6(17) . . ? XPA3 XPA4 XPA1 86(2) 2_665 . ? AP XPA4 XPA1 115(2) . . ? 1 XPA4 XPA1 144(3) 1_455 . ? XPM XPA4 XPA1 114(2) . . ? 3 XPA4 XPA1 91(2) 1_545 . ? BPW XPA4 XPA1 57.3(16) . . ? O4 XPA4 XPA1 86(2) . . ? XPB XPA4 XPA1 67(2) 2_665 . ? XPB XPA4 XPA1 57(2) . . ? 2 XPA4 W2 119(3) . . ? W2 XPA4 W2 43.7(16) 2_665 . ? XPA1 XPA4 W2 147(3) 1_455 . ? XPA2 XPA4 W2 65(2) . . ? W1 XPA4 W2 104(2) 1_545 . ? W3 XPA4 W2 86.0(18) . . ? XPA3 XPA4 W2 61.2(19) 2_665 . ? AP XPA4 W2 117(2) . . ? 1 XPA4 W2 157(2) 1_455 . ? XPM XPA4 W2 146(2) . . ? 3 XPA4 W2 116(2) 1_545 . ? BPW XPA4 W2 92.0(18) . . ? O4 XPA4 W2 118(2) . . ? XPB XPA4 W2 45.1(18) 2_665 . ? XPB XPA4 W2 39.8(16) . . ? XPA1 XPA4 W2 36.4(13) . . ? 2 XPA4 W1 48(2) . 2_565 ? W2 XPA4 W1 108(3) 2_665 2_565 ? XPA1 XPA4 W1 52(2) 1_455 2_565 ? XPA2 XPA4 W1 134(3) . 2_565 ? W1 XPA4 W1 30.1(14) 1_545 2_565 ? W3 XPA4 W1 83.2(18) . 2_565 ? XPA3 XPA4 W1 69(2) 2_665 2_565 ? AP XPA4 W1 113(2) . 2_565 ? 1 XPA4 W1 29.8(10) 1_455 2_565 ? XPM XPA4 W1 49.9(12) . 2_565 ? 3 XPA4 W1 47.6(13) 1_545 2_565 ? BPW XPA4 W1 88.4(18) . 2_565 ? O4 XPA4 W1 105(2) . 2_565 ? XPB XPA4 W1 82(2) 2_665 2_565 ? XPB XPA4 W1 157(3) . 2_565 ? XPA1 XPA4 W1 128(2) . 2_565 ? W2 XPA4 W1 127(2) . 2_565 ? 2 XPA4 4 65(2) . 2_665 ? W2 XPA4 4 76(2) 2_665 2_665 ? XPA1 XPA4 4 90(3) 1_455 2_665 ? XPA2 XPA4 4 121(3) . 2_665 ? W1 XPA4 4 30.3(11) 1_545 2_665 ? W3 XPA4 4 76.4(17) . 2_665 ? XPA3 XPA4 4 30.4(15) 2_665 2_665 ? AP XPA4 4 153(2) . 2_665 ? 1 XPA4 4 74.4(16) 1_455 2_665 ? XPM XPA4 4 85.3(17) . 2_665 ? 3 XPA4 4 62.0(14) 1_545 2_665 ? BPW XPA4 4 88.2(17) . 2_665 ? O4 XPA4 4 135(2) . 2_665 ? XPB XPA4 4 38.1(17) 2_665 2_665 ? XPB XPA4 4 118(2) . 2_665 ? XPA1 XPA4 4 92(2) . 2_665 ? W2 XPA4 4 82.1(16) . 2_665 ? W1 XPA4 4 44.7(11) 2_565 2_665 ? XPA3 XPB XPA2 171(8) . . ? XPA3 XPB 4 52(5) . . ? XPA2 XPB 4 135(5) . . ? XPA3 XPB W2 64(6) . . ? XPA2 XPB W2 108(4) . . ? 4 XPB W2 104(3) . . ? XPA3 XPB W3 98(7) . 1_565 ? XPA2 XPB W3 90(4) . 1_565 ? 4 XPB W3 46.2(18) . 1_565 ? W2 XPB W3 139(4) . 1_565 ? XPA3 XPB W2 123(7) . 2_665 ? XPA2 XPB W2 48(3) . 2_665 ? 4 XPB W2 145(4) . 2_665 ? W2 XPB W2 60(2) . 2_665 ? W3 XPB W2 126(3) 1_565 2_665 ? XPA3 XPB 3 142(7) . . ? XPA2 XPB 3 46(3) . . ? 4 XPB 3 89(3) . . ? W2 XPB 3 135(4) . . ? W3 XPB 3 44.4(16) 1_565 . ? W2 XPB 3 85(3) 2_665 . ? XPA3 XPB BPCA 98(7) . 1_565 ? XPA2 XPB BPCA 90(4) . 1_565 ? 4 XPB BPCA 50.2(18) . 1_565 ? W2 XPB BPCA 152(4) . 1_565 ? W3 XPB BPCA 14.8(7) 1_565 1_565 ? W2 XPB BPCA 134(3) 2_665 1_565 ? 3 XPB BPCA 48.1(16) . 1_565 ? XPA3 XPB BPW 98(7) . 1_565 ? XPA2 XPB BPW 90(4) . 1_565 ? 4 XPB BPW 50.2(18) . 1_565 ? W2 XPB BPW 152(4) . 1_565 ? W3 XPB BPW 14.8(7) 1_565 1_565 ? W2 XPB BPW 134(3) 2_665 1_565 ? 3 XPB BPW 48.1(16) . 1_565 ? BPCA XPB BPW 0.0(5) 1_565 1_565 ? XPA3 XPB XPA4 64(6) . 2_665 ? XPA2 XPB XPA4 111(4) . 2_665 ? 4 XPB XPA4 77(3) . 2_665 ? W2 XPB XPA4 37.3(18) . 2_665 ? W3 XPB XPA4 102(3) 1_565 2_665 ? W2 XPB XPA4 72(2) 2_665 2_665 ? 3 XPB XPA4 110(3) . 2_665 ? BPCA XPB XPA4 116(3) 1_565 2_665 ? BPW XPB XPA4 116(3) 1_565 2_665 ? XPA3 XPB XPA1 60(6) . . ? XPA2 XPB XPA1 112(4) . . ? 4 XPB XPA1 112(3) . . ? W2 XPB XPA1 41.6(18) . . ? W3 XPB XPA1 157(4) 1_565 . ? W2 XPB XPA1 76(2) 2_665 . ? 3 XPB XPA1 158(3) . . ? BPCA XPB XPA1 149(3) 1_565 . ? BPW XPB XPA1 149(3) 1_565 . ? XPA4 XPB XPA1 77(2) 2_665 . ? XPA3 XPB W1 60(6) . 2_675 ? XPA2 XPB W1 124(4) . 2_675 ? 4 XPB W1 29.6(14) . 2_675 ? W2 XPB W1 85(2) . 2_675 ? W3 XPB W1 55.1(18) 1_565 2_675 ? W2 XPB W1 116(3) 2_665 2_675 ? 3 XPB W1 86(2) . 2_675 ? BPCA XPB W1 66.2(19) 1_565 2_675 ? BPW XPB W1 66.2(19) 1_565 2_675 ? XPA4 XPB W1 51.6(18) 2_665 2_675 ? XPA1 XPB W1 113(3) . 2_675 ? XPA3 XPB 1 67(6) . 1_565 ? XPA2 XPB 1 121(4) . 1_565 ? 4 XPB 1 14.3(11) . 1_565 ? W2 XPB 1 113(3) . 1_565 ? W3 XPB 1 32.6(13) 1_565 1_565 ? W2 XPB 1 140(3) 2_665 1_565 ? 3 XPB 1 75(2) . 1_565 ? BPCA XPB 1 39.1(12) 1_565 1_565 ? BPW XPB 1 39.1(12) 1_565 1_565 ? XPA4 XPB 1 82(2) 2_665 1_565 ? XPA1 XPB 1 127(3) . 1_565 ? W1 XPB 1 30.2(11) 2_675 1_565 ? XPA3 XPB XPA4 122(7) . . ? XPA2 XPB XPA4 51(3) . . ? 4 XPB XPA4 174(4) . . ? W2 XPB XPA4 72(2) . . ? W3 XPB XPA4 140(3) 1_565 . ? W2 XPB XPA4 35.2(16) 2_665 . ? 3 XPB XPA4 96(3) . . ? BPCA XPB XPA4 135(3) 1_565 . ? BPW XPB XPA4 135(3) 1_565 . ? XPA4 XPB XPA4 100(3) 2_665 . ? XPA1 XPB XPA4 62(2) . . ? W1 XPB XPA4 150(3) 2_675 . ? 1 XPB XPA4 172(3) 1_565 . ? XPA3 XPB AP 44(5) . 1_655 ? XPA2 XPB AP 136(4) . 1_655 ? 4 XPB AP 78(2) . 1_655 ? W2 XPB AP 83(2) . 1_655 ? W3 XPB AP 110(3) 1_565 1_655 ? W2 XPB AP 124(3) 2_665 1_655 ? 3 XPB AP 142(3) . 1_655 ? BPCA XPB AP 100(2) 1_565 1_655 ? BPW XPB AP 100(2) 1_565 1_655 ? XPA4 XPB AP 103(3) 2_665 1_655 ? XPA1 XPB AP 49.4(16) . 1_655 ? W1 XPB AP 99(2) 2_675 1_655 ? 1 XPB AP 91(2) 1_565 1_655 ? XPA4 XPB AP 97(2) . 1_655 ? XPA3 XPB W1 131(7) . . ? XPA2 XPB W1 53(3) . . ? 4 XPB W1 86(3) . . ? W2 XPB W1 111(3) . . ? W3 XPB W1 51.7(17) 1_565 . ? W2 XPB W1 75(2) 2_665 . ? 3 XPB W1 26.1(12) . . ? BPCA XPB W1 62.2(17) 1_565 . ? BPW XPB W1 62.2(17) 1_565 . ? XPA4 XPB W1 83(2) 2_665 . ? XPA1 XPB W1 149(3) . . ? W1 XPB W1 70.9(18) 2_675 . ? 1 XPB W1 72.9(17) 1_565 . ? XPA4 XPB W1 99(2) . . ? AP XPB W1 161(3) 1_655 . ? XPA3 XPB XPM 47(5) . 1_665 ? XPA2 XPB XPM 142(4) . 1_665 ? 4 XPB XPM 18.1(12) . 1_665 ? W2 XPB XPM 107(3) . 1_665 ? W3 XPB XPM 53.7(17) 1_565 1_665 ? W2 XPB XPM 162(3) 2_665 1_665 ? 3 XPB XPM 98(2) . 1_665 ? BPCA XPB XPM 51.9(14) 1_565 1_665 ? BPW XPB XPM 51.9(14) 1_565 1_665 ? XPA4 XPB XPM 90(2) 2_665 1_665 ? XPA1 XPB XPM 103(3) . 1_665 ? W1 XPB XPM 46.9(13) 2_675 1_665 ? 1 XPB XPM 28.3(8) 1_565 1_665 ? XPA4 XPB XPM 159(3) . 1_665 ? AP XPB XPM 62.3(14) 1_655 1_665 ? W1 XPB XPM 101(2) . 1_665 ? XPA3 XPB 2 126(7) . 1_565 ? XPA2 XPB 2 62(3) . 1_565 ? 4 XPB 2 73(2) . 1_565 ? W2 XPB 2 138(3) . 1_565 ? W3 XPB 2 28.8(12) 1_565 1_565 ? W2 XPB 2 99(3) 2_665 1_565 ? 3 XPB 2 16.3(10) . 1_565 ? BPCA XPB 2 35.3(11) 1_565 1_565 ? BPW XPB 2 35.3(11) 1_565 1_565 ? XPA4 XPB 2 105(2) 2_665 1_565 ? XPA1 XPB 2 174(3) . 1_565 ? W1 XPB 2 72.0(18) 2_675 1_565 ? 1 XPB 2 59.0(15) 1_565 1_565 ? XPA4 XPB 2 113(3) . 1_565 ? AP XPB 2 134(2) 1_655 1_565 ? W1 XPB 2 28.3(10) . 1_565 ? XPM XPB 2 82.4(18) 1_665 1_565 ? XPA3 XPB XPA1 123(7) . 2_665 ? XPA2 XPB XPA1 52(3) . 2_665 ? 4 XPB XPA1 113(3) . 2_665 ? W2 XPB XPA1 70(2) . 2_665 ? W3 XPB XPA1 95(3) 1_565 2_665 ? W2 XPB XPA1 35.1(15) 2_665 2_665 ? 3 XPB XPA1 65(2) . 2_665 ? BPCA XPB XPA1 107(3) 1_565 2_665 ? BPW XPB XPA1 107(3) 1_565 2_665 ? XPA4 XPB XPA1 59(2) 2_665 2_665 ? XPA1 XPB XPA1 104(2) . 2_665 ? W1 XPB XPA1 85(2) 2_675 2_665 ? 1 XPB XPA1 105(2) 1_565 2_665 ? XPA4 XPB XPA1 69(2) . 2_665 ? AP XPB XPA1 153(3) 1_655 2_665 ? W1 XPB XPA1 44.9(15) . 2_665 ? XPM XPB XPA1 131(2) 1_665 2_665 ? 2 XPB XPA1 72.9(19) 1_565 2_665 ? XPA3 XPB 2 67(6) . 2_665 ? XPA2 XPB 2 112(4) . 2_665 ? 4 XPB 2 56.6(19) . 2_665 ? W2 XPB 2 63.9(19) . 2_665 ? W3 XPB 2 76(2) 1_565 2_665 ? W2 XPB 2 89(2) 2_665 2_665 ? 3 XPB 2 91(2) . 2_665 ? BPCA XPB 2 89(2) 1_565 2_665 ? BPW XPB 2 89(2) 1_565 2_665 ? XPA4 XPB 2 26.9(14) 2_665 2_665 ? XPA1 XPB 2 101(2) . 2_665 ? W1 XPB 2 27.5(10) 2_675 2_665 ? 1 XPB 2 57.2(14) 1_565 2_665 ? XPA4 XPB 2 122(3) . 2_665 ? AP XPB 2 111(2) 1_655 2_665 ? W1 XPB 2 67.4(16) . 2_665 ? XPM XPB 2 72.7(16) 1_665 2_665 ? 2 XPB 2 81.8(18) 1_565 2_665 ? XPA1 XPB 2 62.9(17) 2_665 2_665 ? 3 W1 1 134(3) . 2_665 ? 3 W1 2 45.7(16) . 1_565 ? 1 W1 2 161(3) 2_665 1_565 ? 3 W1 W1 102(3) . 2_575 ? 1 W1 W1 100(3) 2_665 2_575 ? 2 W1 W1 99(3) 1_565 2_575 ? 3 W1 4 160(3) . 2_675 ? 1 W1 4 43.7(14) 2_665 2_675 ? 2 W1 4 128(2) 1_565 2_675 ? W1 W1 4 98(3) 2_575 2_675 ? 3 W1 4 60.6(15) . 1_455 ? 1 W1 4 127(2) 2_665 1_455 ? 2 W1 4 71.7(16) 1_565 1_455 ? W1 W1 4 41.4(19) 2_575 1_455 ? 4 W1 4 139.1(19) 2_675 1_455 ? 3 W1 2 127(2) . 2_565 ? 1 W1 2 59.3(15) 2_665 2_565 ? 2 W1 2 139.2(19) 1_565 2_565 ? W1 W1 2 40.7(19) 2_575 2_565 ? 4 W1 2 71.4(15) 2_675 2_565 ? 4 W1 2 73.3(12) 1_455 2_565 ? 3 W1 3 139.9(19) . 2_575 ? 1 W1 3 71.2(16) 2_665 2_575 ? 2 W1 3 122(2) 1_565 2_575 ? W1 W1 3 37.9(19) 2_575 2_575 ? 4 W1 3 59.8(14) 2_675 2_575 ? 4 W1 3 79.3(12) 1_455 2_575 ? 2 W1 3 29.0(9) 2_565 2_575 ? 3 W1 1 71.8(16) . 1_465 ? 1 W1 1 139.6(19) 2_665 1_465 ? 2 W1 1 59.0(15) 1_565 1_465 ? W1 W1 1 39.7(19) 2_575 1_465 ? 4 W1 1 123.9(19) 2_675 1_465 ? 4 W1 1 28.4(9) 1_455 1_465 ? 2 W1 1 80.4(13) 2_565 1_465 ? 3 W1 1 71.9(12) 2_575 1_465 ? 3 W1 XPM 35.1(12) . 1_565 ? 1 W1 XPM 157(2) 2_665 1_565 ? 2 W1 XPM 37.6(12) 1_565 1_565 ? W1 W1 XPM 72(2) 2_575 1_565 ? 4 W1 XPM 156(2) 2_675 1_565 ? 4 W1 XPM 35.8(7) 1_455 1_565 ? 2 W1 XPM 108.8(14) 2_565 1_565 ? 3 W1 XPM 108.3(13) 2_575 1_565 ? 1 W1 XPM 37.0(8) 1_465 1_565 ? 3 W1 XPA1 101(2) . 2_665 ? 1 W1 XPA1 35.6(17) 2_665 2_665 ? 2 W1 XPA1 146(2) 1_565 2_665 ? W1 W1 XPA1 96(3) 2_575 2_665 ? 4 W1 XPA1 79(2) 2_675 2_665 ? 4 W1 XPA1 101.4(18) 1_455 2_665 ? 2 W1 XPA1 61.6(16) 2_565 2_665 ? 3 W1 XPA1 87.0(18) 2_575 2_665 ? 1 W1 XPA1 127(2) 1_465 2_665 ? XPM W1 XPA1 122.6(19) 1_565 2_665 ? 3 W1 XPM 160(2) . 2_565 ? 1 W1 XPM 36.4(11) 2_665 2_565 ? 2 W1 XPM 151(2) 1_565 2_565 ? W1 W1 XPM 71(2) 2_575 2_565 ? 4 W1 XPM 34.8(10) 2_675 2_565 ? 4 W1 XPM 109.2(13) 1_455 2_565 ? 2 W1 XPM 37.0(8) 2_565 2_565 ? 3 W1 XPM 35.9(8) 2_575 2_565 ? 1 W1 XPM 107.7(13) 1_465 2_565 ? XPM W1 XPM 142.9(14) 1_565 2_565 ? XPA1 W1 XPM 62.4(15) 2_665 2_565 ? 3 W1 W3 121(2) . 2_665 ? 1 W1 W3 39.9(13) 2_665 2_665 ? 2 W1 W3 121(2) 1_565 2_665 ? W1 W1 W3 134(3) 2_575 2_665 ? 4 W1 W3 40.9(12) 2_675 2_665 ? 4 W1 W3 165.0(16) 1_455 2_665 ? 2 W1 W3 96.9(14) 2_565 2_665 ? 3 W1 W3 97.6(14) 2_575 2_665 ? 1 W1 W3 163.3(17) 1_465 2_665 ? XPM W1 W3 153.3(15) 1_565 2_665 ? XPA1 W1 W3 63.7(16) 2_665 2_665 ? XPM W1 W3 63.8(10) 2_565 2_665 ? 3 W1 W3 42.0(13) . 1_565 ? 1 W1 W3 122.4(19) 2_665 1_565 ? 2 W1 W3 41.1(13) 1_565 1_565 ? W1 W1 W3 137(3) 2_575 1_565 ? 4 W1 W3 118.9(19) 2_675 1_565 ? 4 W1 W3 99.0(13) 1_455 1_565 ? 2 W1 W3 167.6(17) 2_565 1_565 ? 3 W1 W3 160.9(16) 2_575 1_565 ? 1 W1 W3 97.5(14) 1_465 1_565 ? XPM W1 W3 64.8(10) 1_565 1_565 ? XPA1 W1 W3 111.8(19) 2_665 1_565 ? XPM W1 W3 151.8(15) 2_565 1_565 ? W3 W1 W3 88.6(13) 2_665 1_565 ? 3 W1 XPA4 80(2) . 1_565 ? 1 W1 XPA4 138(2) 2_665 1_565 ? 2 W1 XPA4 34.2(18) 1_565 1_565 ? W1 W1 XPA4 95(3) 2_575 1_565 ? 4 W1 XPA4 95(2) 2_675 1_565 ? 4 W1 XPA4 89.8(18) 1_455 1_565 ? 2 W1 XPA4 127(2) 2_565 1_565 ? 3 W1 XPA4 99.8(19) 2_575 1_565 ? 1 W1 XPA4 65.1(17) 1_465 1_565 ? XPM W1 XPA4 64.9(16) 1_565 1_565 ? XPA1 W1 XPA4 168(2) 2_665 1_565 ? XPM W1 XPA4 118.5(19) 2_565 1_565 ? W3 W1 XPA4 105.2(19) 2_665 1_565 ? W3 W1 XPA4 61.1(16) 1_565 1_565 ? 3 W1 XPA2 38.5(18) . . ? 1 W1 XPA2 97(2) 2_665 . ? 2 W1 XPA2 84(2) 1_565 . ? W1 W1 XPA2 103(3) 2_575 . ? 4 W1 XPA2 139(2) 2_675 . ? 4 W1 XPA2 69.1(17) 1_455 . ? 2 W1 XPA2 102.3(19) 2_565 . ? 3 W1 XPA2 129(2) 2_575 . ? 1 W1 XPA2 93.7(18) 1_465 . ? XPM W1 XPA2 65.2(16) 1_565 . ? XPA1 W1 XPA2 63(2) 2_665 . ? XPM W1 XPA2 123.6(19) 2_565 . ? W3 W1 XPA2 103.0(18) 2_665 . ? W3 W1 XPA2 65.6(17) 1_565 . ? XPA4 W1 XPA2 118(2) 1_565 . ? 3 W1 XPA3 137(2) . 2_675 ? 1 W1 XPA3 78(2) 2_665 2_675 ? 2 W1 XPA3 94(2) 1_565 2_675 ? W1 W1 XPA3 99(3) 2_575 2_675 ? 4 W1 XPA3 34.4(17) 2_675 2_675 ? 4 W1 XPA3 131(2) 1_455 2_675 ? 2 W1 XPA3 93.4(19) 2_565 2_675 ? 3 W1 XPA3 69.6(17) 2_575 2_675 ? 1 W1 XPA3 104.3(19) 1_465 2_675 ? XPM W1 XPA3 124.2(18) 1_565 2_675 ? XPA1 W1 XPA3 113(2) 2_665 2_675 ? XPM W1 XPA3 63.1(16) 2_565 2_675 ? W3 W1 XPA3 59.2(16) 2_665 2_675 ? W3 W1 XPA3 98.9(19) 1_565 2_675 ? XPA4 W1 XPA3 61(2) 1_565 2_675 ? XPA2 W1 XPA3 158(2) . 2_675 ? 3 W1 BPW 34.6(12) . 1_565 ? 1 W1 BPW 130.2(19) 2_665 1_565 ? 2 W1 BPW 34.7(12) 1_565 1_565 ? W1 W1 BPW 128(3) 2_575 1_565 ? 4 W1 BPW 127.1(18) 2_675 1_565 ? 4 W1 BPW 90.2(11) 1_455 1_565 ? 2 W1 BPW 161.3(15) 2_565 1_565 ? 3 W1 BPW 157.1(15) 2_575 1_565 ? 1 W1 BPW 89.1(11) 1_465 1_565 ? XPM W1 BPW 55.9(7) 1_565 1_565 ? XPA1 W1 BPW 115.2(18) 2_665 1_565 ? XPM W1 BPW 160.6(13) 2_565 1_565 ? W3 W1 BPW 97.5(12) 2_665 1_565 ? W3 W1 BPW 8.9(5) 1_565 1_565 ? XPA4 W1 BPW 59.5(15) 1_565 1_565 ? XPA2 W1 BPW 62.8(15) . 1_565 ? XPA3 W1 BPW 104.2(18) 2_675 1_565 ? 3 W1 BPCA 34.6(12) . 1_565 ? 1 W1 BPCA 130.2(19) 2_665 1_565 ? 2 W1 BPCA 34.7(12) 1_565 1_565 ? W1 W1 BPCA 128(3) 2_575 1_565 ? 4 W1 BPCA 127.1(18) 2_675 1_565 ? 4 W1 BPCA 90.2(11) 1_455 1_565 ? 2 W1 BPCA 161.3(15) 2_565 1_565 ? 3 W1 BPCA 157.1(15) 2_575 1_565 ? 1 W1 BPCA 89.1(11) 1_465 1_565 ? XPM W1 BPCA 55.9(7) 1_565 1_565 ? XPA1 W1 BPCA 115.2(18) 2_665 1_565 ? XPM W1 BPCA 160.6(13) 2_565 1_565 ? W3 W1 BPCA 97.5(12) 2_665 1_565 ? W3 W1 BPCA 8.9(5) 1_565 1_565 ? XPA4 W1 BPCA 59.5(15) 1_565 1_565 ? XPA2 W1 BPCA 62.8(15) . 1_565 ? XPA3 W1 BPCA 104.2(18) 2_675 1_565 ? BPW W1 BPCA 0.0(4) 1_565 1_565 ? 3 W1 BPW 128.9(19) . 2_665 ? 1 W1 BPW 33.6(11) 2_665 2_665 ? 2 W1 BPW 128.0(19) 1_565 2_665 ? W1 W1 BPW 126(3) 2_575 2_665 ? 4 W1 BPW 34.4(10) 2_675 2_665 ? 4 W1 BPW 160.2(15) 1_455 2_665 ? 2 W1 BPW 89.1(12) 2_565 2_665 ? 3 W1 BPW 89.6(11) 2_575 2_665 ? 1 W1 BPW 158.3(15) 1_465 2_665 ? XPM W1 BPW 161.5(14) 1_565 2_665 ? XPA1 W1 BPW 61.3(15) 2_665 2_665 ? XPM W1 BPW 55.6(7) 2_565 2_665 ? W3 W1 BPW 8.2(6) 2_665 2_665 ? W3 W1 BPW 96.7(12) 1_565 2_665 ? XPA4 W1 BPW 108.4(18) 1_565 2_665 ? XPA2 W1 BPW 107.2(17) . 2_665 ? XPA3 W1 BPW 57.1(15) 2_675 2_665 ? BPW W1 BPW 105.6(10) 1_565 2_665 ? BPCA W1 BPW 105.6(10) 1_565 2_665 ? XPA2 W2 XPA4 86(3) 2_665 2_665 ? XPA2 W2 XPA3 168(3) 2_665 . ? XPA4 W2 XPA3 92(3) 2_665 . ? XPA2 W2 XPA1 92(3) 2_665 . ? XPA4 W2 XPA1 153(3) 2_665 . ? XPA3 W2 XPA1 84(3) . . ? XPA2 W2 XPB 165(3) 2_665 . ? XPA4 W2 XPB 97(3) 2_665 . ? XPA3 W2 XPB 27(2) . . ? XPA1 W2 XPB 92(3) . . ? XPA2 W2 W2 100(2) 2_665 2_665 ? XPA4 W2 W2 103(2) 2_665 2_665 ? XPA3 W2 W2 92(2) . 2_665 ? XPA1 W2 W2 104(2) . 2_665 ? XPB W2 W2 65(2) . 2_665 ? XPA2 W2 XPB 45(3) 2_665 2_665 ? XPA4 W2 XPB 96(3) 2_665 2_665 ? XPA3 W2 XPB 147(3) . 2_665 ? XPA1 W2 XPB 101(3) . 2_665 ? XPB W2 XPB 120(2) . 2_665 ? W2 W2 XPB 55(2) 2_665 2_665 ? XPA2 W2 W2 82(2) 2_665 2_765 ? XPA4 W2 W2 80(2) 2_665 2_765 ? XPA3 W2 W2 86(2) . 2_765 ? XPA1 W2 W2 73.7(18) . 2_765 ? XPB W2 W2 113(2) . 2_765 ? W2 W2 W2 176.9(15) 2_665 2_765 ? XPB W2 W2 127(2) 2_665 2_765 ? XPA2 W2 XPA3 61(2) 2_665 2_665 ? XPA4 W2 XPA3 98(2) 2_665 2_665 ? XPA3 W2 XPA3 131.7(17) . 2_665 ? XPA1 W2 XPA3 104(2) . 2_665 ? XPB W2 XPA3 105(2) . 2_665 ? W2 W2 XPA3 39.6(14) 2_665 2_665 ? XPB W2 XPA3 16(2) 2_665 2_665 ? W2 W2 XPA3 142.6(15) 2_765 2_665 ? XPA2 W2 XPA2 134.2(17) 2_665 . ? XPA4 W2 XPA2 102(2) 2_665 . ? XPA3 W2 XPA2 58(2) . . ? XPA1 W2 XPA2 99(2) . . ? XPB W2 XPA2 31(2) . . ? W2 W2 XPA2 34.1(13) 2_665 . ? XPB W2 XPA2 89(2) 2_665 . ? W2 W2 XPA2 143.7(15) 2_765 . ? XPA3 W2 XPA2 73.7(17) 2_665 . ? XPA2 W2 XPA1 81(2) 2_665 2_765 ? XPA4 W2 XPA1 42(2) 2_665 2_765 ? XPA3 W2 XPA1 89(2) . 2_765 ? XPA1 W2 XPA1 111.5(18) . 2_765 ? XPB W2 XPA1 111(2) . 2_765 ? W2 W2 XPA1 144.5(16) 2_665 2_765 ? XPB W2 XPA1 117(2) 2_665 2_765 ? W2 W2 XPA1 37.7(12) 2_765 2_765 ? XPA3 W2 XPA1 128.0(17) 2_665 2_765 ? XPA2 W2 XPA1 133.1(17) . 2_765 ? XPA2 W2 2 104(2) 2_665 2_665 ? XPA4 W2 2 19(2) 2_665 2_665 ? XPA3 W2 2 74(2) . 2_665 ? XPA1 W2 2 148.8(19) . 2_665 ? XPB W2 2 79(2) . 2_665 ? W2 W2 2 99.0(11) 2_665 2_665 ? XPB W2 2 109.0(19) 2_665 2_665 ? W2 W2 2 82.5(8) 2_765 2_665 ? XPA3 W2 2 107.2(14) 2_665 2_665 ? XPA2 W2 2 88.4(13) . 2_665 ? XPA1 W2 2 47.8(12) 2_765 2_665 ? XPA2 W2 XPA4 100(2) 2_665 . ? XPA4 W2 XPA4 136.3(16) 2_665 . ? XPA3 W2 XPA4 90(2) . . ? XPA1 W2 XPA4 70(2) . . ? XPB W2 XPA4 69(2) . . ? W2 W2 XPA4 33.7(13) 2_665 . ? XPB W2 XPA4 63(2) 2_665 . ? W2 W2 XPA4 144.0(15) 2_765 . ? XPA3 W2 XPA4 51.3(17) 2_665 . ? XPA2 W2 XPA4 45.6(16) . . ? XPA1 W2 XPA4 178.2(17) 2_765 . ? 2 W2 XPA4 130.5(14) 2_665 . ? XPA2 W2 XPA4 85(2) 2_665 1_655 ? XPA4 W2 XPA4 113(2) 2_665 1_655 ? XPA3 W2 XPA4 85(2) . 1_655 ? XPA1 W2 XPA4 40(2) . 1_655 ? XPB W2 XPA4 107(2) . 1_655 ? W2 W2 XPA4 144.0(16) 2_665 1_655 ? XPB W2 XPA4 120(2) 2_665 1_655 ? W2 W2 XPA4 33.7(12) 2_765 1_655 ? XPA3 W2 XPA4 131.4(18) 2_665 1_655 ? XPA2 W2 XPA4 129.7(17) . 1_655 ? XPA1 W2 XPA4 71.4(16) 2_765 1_655 ? 2 W2 XPA4 114.3(13) 2_665 1_655 ? XPA4 W2 XPA4 110.3(19) . 1_655 ? XPA2 W2 3 22(2) 2_665 2_665 ? XPA4 W2 3 107(2) 2_665 2_665 ? XPA3 W2 3 156(2) . 2_665 ? XPA1 W2 3 71.7(18) . 2_665 ? XPB W2 3 154(2) . 2_665 ? W2 W2 3 98.2(11) 2_665 2_665 ? XPB W2 3 47.4(19) 2_665 2_665 ? W2 W2 3 83.0(8) 2_765 2_665 ? XPA3 W2 3 61.7(13) 2_665 2_665 ? XPA2 W2 3 129.3(13) . 2_665 ? XPA1 W2 3 94.7(12) 2_765 2_665 ? 2 W2 3 125.7(8) 2_665 2_665 ? XPA4 W2 3 86.2(13) . 2_665 ? XPA4 W2 3 73.8(13) 1_655 2_665 ? XPA2 W2 1 74(2) 2_665 . ? XPA4 W2 1 154(2) 2_665 . ? XPA3 W2 1 104(2) . . ? XPA1 W2 1 20.8(17) . . ? XPB W2 1 107(2) . . ? W2 W2 1 96.8(11) 2_665 . ? XPB W2 1 81.3(19) 2_665 . ? W2 W2 1 81.7(8) 2_765 . ? XPA3 W2 1 86.1(13) 2_665 . ? XPA2 W2 1 104.0(13) . . ? XPA1 W2 1 117.1(13) 2_765 . ? 2 W2 1 164.1(9) 2_665 . ? XPA4 W2 1 64.6(13) . . ? XPA4 W2 1 50.0(12) 1_655 . ? 3 W2 1 52.8(7) 2_665 . ? XPA2 W2 XPA2 114(2) 2_665 1_655 ? XPA4 W2 XPA2 83(2) 2_665 1_655 ? XPA3 W2 XPA2 53(2) . 1_655 ? XPA1 W2 XPA2 74(2) . 1_655 ? XPB W2 XPA2 80(2) . 1_655 ? W2 W2 XPA2 145.4(15) 2_665 1_655 ? XPB W2 XPA2 159(2) 2_665 1_655 ? W2 W2 XPA2 32.3(12) 2_765 1_655 ? XPA3 W2 XPA2 174.6(17) 2_665 1_655 ? XPA2 W2 XPA2 111.4(19) . 1_655 ? XPA1 W2 XPA2 50.1(15) 2_765 1_655 ? 2 W2 XPA2 75.3(12) 2_665 1_655 ? XPA4 W2 XPA2 130.8(16) . 1_655 ? XPA4 W2 XPA2 44.1(16) 1_655 1_655 ? 3 W2 XPA2 113.0(13) 2_665 1_655 ? 1 W2 XPA2 90.9(12) . 1_655 ? XPA2 W2 4 154(2) 2_665 . ? XPA4 W2 4 71(2) 2_665 . ? XPA3 W2 4 20.5(19) . . ? XPA1 W2 4 102.6(18) . . ? XPB W2 4 37(2) . . ? W2 W2 4 96.8(10) 2_665 . ? XPB W2 4 147(2) 2_665 . ? W2 W2 4 81.8(8) 2_765 . ? XPA3 W2 4 133.3(14) 2_665 . ? XPA2 W2 4 64.8(13) . . ? XPA1 W2 4 73.9(12) 2_765 . ? 2 W2 4 53.3(7) 2_665 . ? XPA4 W2 4 105.4(13) . . ? XPA4 W2 4 92.7(13) 1_655 . ? 3 W2 4 164.8(8) 2_665 . ? 1 W2 4 123.1(8) . . ? XPA2 W2 4 52.0(12) 1_655 . ? XPA2 W2 XPA1 96(2) 2_665 2_665 ? XPA4 W2 XPA1 68(2) 2_665 2_665 ? XPA3 W2 XPA1 95(2) . 2_665 ? XPA1 W2 XPA1 139.0(14) . 2_665 ? XPB W2 XPA1 72(2) . 2_665 ? W2 W2 XPA1 35.1(12) 2_665 2_665 ? XPB W2 XPA1 60(2) 2_665 2_665 ? W2 W2 XPA1 147.2(13) 2_765 2_665 ? XPA3 W2 XPA1 48.4(16) 2_665 2_665 ? XPA2 W2 XPA1 49.4(15) . 2_665 ? XPA1 W2 XPA1 109.5(18) 2_765 2_665 ? 2 W2 XPA1 66.4(11) 2_665 2_665 ? XPA4 W2 XPA1 68.8(15) . 2_665 ? XPA4 W2 XPA1 179.0(16) 1_655 2_665 ? 3 W2 XPA1 106.4(12) 2_665 2_665 ? 1 W2 XPA1 129.3(12) . 2_665 ? XPA2 W2 XPA1 136.1(16) 1_655 2_665 ? 4 W2 XPA1 87.2(11) . 2_665 ? XPA2 W2 XPA3 48(2) 2_665 2_765 ? XPA4 W2 XPA3 80(2) 2_665 2_765 ? XPA3 W2 XPA3 119.6(18) . 2_765 ? XPA1 W2 XPA3 79(2) . 2_765 ? XPB W2 XPA3 147(2) . 2_765 ? W2 W2 XPA3 148.2(15) 2_665 2_765 ? XPB W2 XPA3 93(2) 2_665 2_765 ? W2 W2 XPA3 33.9(12) 2_765 2_765 ? XPA3 W2 XPA3 108.7(19) 2_665 2_765 ? XPA2 W2 XPA3 177.2(17) . 2_765 ? XPA1 W2 XPA3 46.9(15) 2_765 2_765 ? 2 W2 XPA3 92.5(12) 2_665 2_765 ? XPA4 W2 XPA3 134.5(17) . 2_765 ? XPA4 W2 XPA3 47.5(16) 1_655 2_765 ? 3 W2 XPA3 52.0(12) 2_665 2_765 ? 1 W2 XPA3 74.7(12) . 2_765 ? XPA2 W2 XPA3 66.2(15) 1_655 2_765 ? 4 W2 XPA3 113.6(12) . 2_765 ? XPA1 W2 XPA3 133.4(15) 2_665 2_765 ? MH MHA XPM 167(6) . . ? MH MHA O7 82(4) . 1_455 ? XPM MHA O7 110(4) . 1_455 ? MH MHA O5 78(4) . 1_445 ? XPM MHA O5 106(3) . 1_445 ? O7 MHA O5 90(2) 1_455 1_445 ? MH MHA O4 74(4) . . ? XPM MHA O4 101(3) . . ? O7 MHA O4 88(2) 1_455 . ? O5 MHA O4 152(5) 1_445 . ? MH MHA O3 66(4) . 1_545 ? XPM MHA O3 102(3) . 1_545 ? O7 MHA O3 148(5) 1_455 1_545 ? O5 MHA O3 84(2) 1_445 1_545 ? O4 MHA O3 84(2) . 1_545 ? MH MHA XOM 7(3) . . ? XPM MHA XOM 173(3) . . ? O7 MHA XOM 75(2) 1_455 . ? O5 MHA XOM 78(2) 1_445 . ? O4 MHA XOM 74(2) . . ? O3 MHA XOM 73(2) 1_545 . ? MH MHA 1 161(5) . 1_455 ? XPM MHA 1 31.6(17) . 1_455 ? O7 MHA 1 79(2) 1_455 1_455 ? O5 MHA 1 101(3) 1_445 1_455 ? O4 MHA 1 106(3) . 1_455 ? O3 MHA 1 133(3) 1_545 1_455 ? XOM MHA 1 154(2) . 1_455 ? MH MHA 4 160(5) . 1_445 ? XPM MHA 4 27.8(15) . 1_445 ? O7 MHA 4 97(3) 1_455 1_445 ? O5 MHA 4 82(2) 1_445 1_445 ? O4 MHA 4 126(3) . 1_445 ? O3 MHA 4 113(2) 1_545 1_445 ? XOM MHA 4 159(2) . 1_445 ? 1 MHA 4 26.4(11) 1_455 1_445 ? MH MHA 2 144(5) . . ? XPM MHA 2 28.0(13) . . ? O7 MHA 2 110(3) 1_455 . ? O5 MHA 2 133(3) 1_445 . ? O4 MHA 2 72.9(18) . . ? O3 MHA 2 96(2) 1_545 . ? XOM MHA 2 146(2) . . ? 1 MHA 2 47.2(15) 1_455 . ? 4 MHA 2 55.0(17) 1_445 . ? MH MHA 3 144(5) . 1_545 ? XPM MHA 3 23.0(12) . 1_545 ? O7 MHA 3 131(3) 1_455 1_545 ? O5 MHA 3 111(3) 1_445 1_545 ? O4 MHA 3 91(2) . 1_545 ? O3 MHA 3 79.9(18) 1_545 1_545 ? XOM MHA 3 151(2) . 1_545 ? 1 MHA 3 54.3(17) 1_455 1_545 ? 4 MHA 3 47.0(15) 1_445 1_545 ? 2 MHA 3 25.9(10) . 1_545 ? MH MHA BPCA 127(5) . 1_455 ? XPM MHA BPCA 65(2) . 1_455 ? O7 MHA BPCA 61.4(16) 1_455 1_455 ? O5 MHA BPCA 65.3(16) 1_445 1_455 ? O4 MHA BPCA 135(2) . 1_455 ? O3 MHA BPCA 139(2) 1_545 1_455 ? XOM MHA BPCA 121.5(19) . 1_455 ? 1 MHA BPCA 40.6(12) 1_455 1_455 ? 4 MHA BPCA 40.5(11) 1_445 1_455 ? 2 MHA BPCA 87(2) . 1_455 ? 3 MHA BPCA 87(2) 1_545 1_455 ? 4 1 XPA1 177(3) 1_545 . ? 4 1 XPM 65.0(15) 1_545 1_655 ? XPA1 1 XPM 114(3) . 1_655 ? 4 1 W1 69.9(19) 1_545 2_665 ? XPA1 1 W1 108(3) . 2_665 ? XPM 1 W1 107.0(18) 1_655 2_665 ? 4 1 W3 70.1(17) 1_545 . ? XPA1 1 W3 113(3) . . ? XPM 1 W3 111.5(16) 1_655 . ? W1 1 W3 102.7(19) 2_665 . ? 4 1 BPW 72.0(16) 1_545 . ? XPA1 1 BPW 111(3) . . ? XPM 1 BPW 97.2(13) 1_655 . ? W1 1 BPW 119.3(18) 2_665 . ? W3 1 BPW 18.5(8) . . ? 4 1 2 91.3(18) 1_545 1_655 ? XPA1 1 2 86(3) . 1_655 ? XPM 1 2 47.9(10) 1_655 1_655 ? W1 1 2 80.7(17) 2_665 1_655 ? W3 1 2 158.1(18) . 1_655 ? BPW 1 2 145.0(15) . 1_655 ? 4 1 W1 75.4(17) 1_545 1_645 ? XPA1 1 W1 102(3) . 1_645 ? XPM 1 W1 74.0(12) 1_655 1_645 ? W1 1 W1 40.4(19) 2_665 1_645 ? W3 1 W1 137.3(17) . 1_645 ? BPW 1 W1 146.8(15) . 1_645 ? 2 1 W1 40.4(11) 1_655 1_645 ? 4 1 3 61.4(15) 1_545 1_645 ? XPA1 1 3 116(3) . 1_645 ? XPM 1 3 37.7(8) 1_655 1_645 ? W1 1 3 70.9(16) 2_665 1_645 ? W3 1 3 130.4(16) . 1_645 ? BPW 1 3 124.9(13) . 1_645 ? 2 1 3 30.0(10) 1_655 1_645 ? W1 1 3 36.6(10) 1_645 1_645 ? 4 1 MHA 78.2(19) 1_545 1_655 ? XPA1 1 MHA 103(3) . 1_655 ? XPM 1 MHA 28.3(12) 1_655 1_655 ? W1 1 MHA 135(2) 2_665 1_655 ? W3 1 MHA 95.4(17) . 1_655 ? BPW 1 MHA 77.7(13) . 1_655 ? 2 1 MHA 68.6(14) 1_655 1_655 ? W1 1 MHA 101.5(16) 1_645 1_655 ? 3 1 MHA 65.9(14) 1_645 1_655 ? 4 1 XPA4 126(2) 1_545 1_655 ? XPA1 1 XPA4 51(3) . 1_655 ? XPM 1 XPA4 74.3(16) 1_655 1_655 ? W1 1 XPA4 92(2) 2_665 1_655 ? W3 1 XPA4 162(2) . 1_655 ? BPW 1 XPA4 149.0(18) . 1_655 ? 2 1 XPA4 35.2(15) 1_655 1_655 ? W1 1 XPA4 60.6(16) 1_645 1_655 ? 3 1 XPA4 65.1(16) 1_645 1_655 ? MHA 1 XPA4 82.1(18) 1_655 1_655 ? 3 2 XPA4 173(3) 1_545 . ? 3 2 XPM 65.1(16) 1_545 . ? XPA4 2 XPM 122(3) . . ? 3 2 W1 64(2) 1_545 1_545 ? XPA4 2 W1 111(3) . 1_545 ? XPM 2 W1 104.2(19) . 1_545 ? 3 2 W3 71.2(18) 1_545 . ? XPA4 2 W3 106(3) . . ? XPM 2 W3 111.1(17) . . ? W1 2 W3 101.0(19) 1_545 . ? 3 2 BPW 73.1(17) 1_545 . ? XPA4 2 BPW 107(3) . . ? XPM 2 BPW 96.5(13) . . ? W1 2 BPW 117.0(18) 1_545 . ? W3 2 BPW 18.7(8) . . ? 3 2 1 89.9(19) 1_545 1_455 ? XPA4 2 1 94(3) . 1_455 ? XPM 2 1 47.7(10) . 1_455 ? W1 2 1 80.6(17) 1_545 1_455 ? W3 2 1 157.4(18) . 1_455 ? BPW 2 1 144.1(15) . 1_455 ? 3 2 W1 75.8(18) 1_545 2_565 ? XPA4 2 W1 103(3) . 2_565 ? XPM 2 W1 75.2(13) . 2_565 ? W1 2 W1 40.8(19) 1_545 2_565 ? W3 2 W1 138.6(17) . 2_565 ? BPW 2 W1 148.4(15) . 2_565 ? 1 2 W1 40.0(11) 1_455 2_565 ? 3 2 4 60.8(16) 1_545 1_445 ? XPA4 2 4 123(3) . 1_445 ? XPM 2 4 36.8(8) . 1_445 ? W1 2 4 70.0(16) 1_545 1_445 ? W3 2 4 130.3(16) . 1_445 ? BPW 2 4 124.0(13) . 1_445 ? 1 2 4 29.1(9) 1_455 1_445 ? W1 2 4 38.8(10) 2_565 1_445 ? 3 2 XPA1 127(2) 1_545 1_455 ? XPA4 2 XPA1 57(3) . 1_455 ? XPM 2 XPA1 75.0(16) . 1_455 ? W1 2 XPA1 96(2) 1_545 1_455 ? W3 2 XPA1 160(2) . 1_455 ? BPW 2 XPA1 147.1(18) . 1_455 ? 1 2 XPA1 37.4(15) 1_455 1_455 ? W1 2 XPA1 61.1(16) 2_565 1_455 ? 4 2 XPA1 66.4(15) 1_445 1_455 ? 3 2 MHA 79.6(19) 1_545 . ? XPA4 2 MHA 107(3) . . ? XPM 2 MHA 25.1(14) . . ? W1 2 MHA 129(2) 1_545 . ? W3 2 MHA 99.4(18) . . ? BPW 2 MHA 81.5(15) . . ? 1 2 MHA 64.2(16) 1_455 . ? W1 2 MHA 98.4(18) 2_565 . ? 4 2 MHA 61.3(15) 1_445 . ? XPA1 2 MHA 78.2(18) 1_455 . ? 2 3 W1 70(2) 1_565 . ? 2 3 XPM 68.8(17) 1_565 1_565 ? W1 3 XPM 109.9(19) . 1_565 ? 2 3 XPA2 174(3) 1_565 . ? W1 3 XPA2 108(3) . . ? XPM 3 XPA2 117(3) 1_565 . ? 2 3 W3 67.7(18) 1_565 1_565 ? W1 3 W3 102.2(19) . 1_565 ? XPM 3 W3 111.2(16) 1_565 1_565 ? XPA2 3 W3 108(3) . 1_565 ? 2 3 BPCA 70.3(17) 1_565 1_565 ? W1 3 BPCA 119.0(19) . 1_565 ? XPM 3 BPCA 96.7(13) 1_565 1_565 ? XPA2 3 BPCA 107(2) . 1_565 ? W3 3 BPCA 18.4(8) 1_565 1_565 ? 2 3 BPW 70.3(17) 1_565 1_565 ? W1 3 BPW 119.0(19) . 1_565 ? XPM 3 BPW 96.7(13) 1_565 1_565 ? XPA2 3 BPW 107(2) . 1_565 ? W3 3 BPW 18.4(8) 1_565 1_565 ? BPCA 3 BPW 0.0(7) 1_565 1_565 ? 2 3 4 89.4(19) 1_565 1_455 ? W1 3 4 80.9(17) . 1_455 ? XPM 3 4 45.2(9) 1_565 1_455 ? XPA2 3 4 95(2) . 1_455 ? W3 3 4 153.6(17) 1_565 1_455 ? BPCA 3 4 141.8(14) 1_565 1_455 ? BPW 3 4 141.8(14) 1_565 1_455 ? 2 3 XPB 131(3) 1_565 . ? W1 3 XPB 111(2) . . ? XPM 3 XPB 139(2) 1_565 . ? XPA2 3 XPB 45(3) . . ? W3 3 XPB 64(2) 1_565 . ? BPCA 3 XPB 67(2) 1_565 . ? BPW 3 XPB 67(2) 1_565 . ? 4 3 XPB 140(2) 1_455 . ? 2 3 W1 75.2(18) 1_565 2_575 ? W1 3 W1 40(2) . 2_575 ? XPM 3 W1 75.6(12) 1_565 2_575 ? XPA2 3 W1 107(3) . 2_575 ? W3 3 W1 135.4(17) 1_565 2_575 ? BPCA 3 W1 145.1(14) 1_565 2_575 ? BPW 3 W1 145.1(14) 1_565 2_575 ? 4 3 W1 40.9(10) 1_455 2_575 ? XPB 3 W1 138(2) . 2_575 ? 2 3 1 60.2(17) 1_565 1_465 ? W1 3 1 71.6(16) . 1_465 ? XPM 3 1 38.8(9) 1_565 1_465 ? XPA2 3 1 125(3) . 1_465 ? W3 3 1 126.5(15) 1_565 1_465 ? BPCA 3 1 121.7(13) 1_565 1_465 ? BPW 3 1 121.7(13) 1_565 1_465 ? 4 3 1 29.2(9) 1_455 1_465 ? XPB 3 1 169(2) . 1_465 ? W1 3 1 37.9(10) 2_575 1_465 ? 2 3 MHA 74.5(19) 1_565 1_565 ? W1 3 MHA 130(2) . 1_565 ? XPM 3 MHA 21.2(14) 1_565 1_565 ? XPA2 3 MHA 110(3) . 1_565 ? W3 3 MHA 96.3(17) 1_565 1_565 ? BPCA 3 MHA 79.5(15) 1_565 1_565 ? BPW 3 MHA 79.5(15) 1_565 1_565 ? 4 3 MHA 63.7(15) 1_455 1_565 ? XPB 3 MHA 120(2) . 1_565 ? W1 3 MHA 96.8(17) 2_575 1_565 ? 1 3 MHA 59.8(15) 1_465 1_565 ? 1 4 XPM 69.7(16) 1_565 1_665 ? 1 4 W1 66.4(19) 1_565 2_675 ? XPM 4 W1 107.6(18) 1_665 2_675 ? 1 4 XPA3 169(3) 1_565 . ? XPM 4 XPA3 121(3) 1_665 . ? W1 4 XPA3 111(3) 2_675 . ? 1 4 W3 68.3(17) 1_565 1_565 ? XPM 4 W3 113.1(15) 1_665 1_565 ? W1 4 W3 100.1(18) 2_675 1_565 ? XPA3 4 W3 102(3) . 1_565 ? 1 4 BPCA 71.8(16) 1_565 1_565 ? XPM 4 BPCA 99.0(12) 1_665 1_565 ? W1 4 BPCA 117.1(17) 2_675 1_565 ? XPA3 4 BPCA 101(3) . 1_565 ? W3 4 BPCA 18.6(8) 1_565 1_565 ? 1 4 BPW 71.8(16) 1_565 1_565 ? XPM 4 BPW 99.0(12) 1_665 1_565 ? W1 4 BPW 117.1(17) 2_675 1_565 ? XPA3 4 BPW 101(3) . 1_565 ? W3 4 BPW 18.6(8) 1_565 1_565 ? BPCA 4 BPW 0.0(5) 1_565 1_565 ? 1 4 XPB 141(3) 1_565 . ? XPM 4 XPB 137(2) 1_665 . ? W1 4 XPB 112(3) 2_675 . ? XPA3 4 XPB 28(3) . . ? W3 4 XPB 74(2) 1_565 . ? BPCA 4 XPB 76(2) 1_565 . ? BPW 4 XPB 76(2) 1_565 . ? 1 4 3 89.3(18) 1_565 1_655 ? XPM 4 3 45.8(9) 1_665 1_655 ? W1 4 3 79.3(16) 2_675 1_655 ? XPA3 4 3 101(3) . 1_655 ? W3 4 3 155.2(16) 1_565 1_655 ? BPCA 4 3 144.7(13) 1_565 1_655 ? BPW 4 3 144.7(13) 1_565 1_655 ? XPB 4 3 129(2) . 1_655 ? 1 4 W1 76.3(17) 1_565 1_655 ? XPM 4 W1 75.0(12) 1_665 1_655 ? W1 4 W1 40.9(19) 2_675 1_655 ? XPA3 4 W1 109(3) . 1_655 ? W3 4 W1 136.6(16) 1_565 1_655 ? BPCA 4 W1 147.5(14) 1_565 1_655 ? BPW 4 W1 147.5(14) 1_565 1_655 ? XPB 4 W1 130(2) . 1_655 ? 3 4 W1 38.5(10) 1_655 1_655 ? 1 4 2 59.6(16) 1_565 1_665 ? XPM 4 2 38.5(9) 1_665 1_665 ? W1 4 2 69.8(15) 2_675 1_665 ? XPA3 4 2 131(3) . 1_665 ? W3 4 2 126.7(14) 1_565 1_665 ? BPCA 4 2 122.8(12) 1_565 1_665 ? BPW 4 2 122.8(12) 1_565 1_665 ? XPB 4 2 159(2) . 1_665 ? 3 4 2 29.8(9) 1_655 1_665 ? W1 4 2 38.3(10) 1_655 1_665 ? 1 4 MHA 75.4(19) 1_565 1_665 ? XPM 4 MHA 25.9(12) 1_665 1_665 ? W1 4 MHA 130(2) 2_675 1_665 ? XPA3 4 MHA 112(3) . 1_665 ? W3 4 MHA 93.8(16) 1_565 1_665 ? BPCA 4 MHA 77.0(12) 1_565 1_665 ? BPW 4 MHA 77.0(12) 1_565 1_665 ? XPB 4 MHA 117(3) . 1_665 ? 3 4 MHA 69.3(14) 1_655 1_665 ? W1 4 MHA 100.9(15) 1_655 1_665 ? 2 4 MHA 63.8(13) 1_665 1_665 ? AP 5 XOA 173.1(9) . . ? AP 5 O5 95.2(7) . 1_455 ? XOA 5 O5 88.2(4) . 1_455 ? AP 5 O4 91.9(7) . . ? XOA 5 O4 84.9(4) . . ? O5 5 O4 172.9(6) 1_455 . ? AP 5 O3 97.1(7) . . ? XOA 5 O3 89.8(4) . . ? O5 5 O3 63.2(3) 1_455 . ? O4 5 O3 115.2(4) . . ? AP 5 O7 93.4(7) . 1_455 ? XOA 5 O7 79.7(4) . 1_455 ? O5 5 O7 116.5(4) 1_455 1_455 ? O4 5 O7 63.7(3) . 1_455 ? O3 5 O7 169.5(6) . 1_455 ? AP 5 O2 94.4(7) . 1_455 ? XOA 5 O2 82.1(4) . 1_455 ? O5 5 O2 58.8(3) 1_455 1_455 ? O4 5 O2 121.4(4) . 1_455 ? O3 5 O2 121.6(4) . 1_455 ? O7 5 O2 57.8(3) 1_455 1_455 ? AP 5 O2 94.6(7) . . ? XOA 5 O2 88.9(4) . . ? O5 5 O2 120.4(4) 1_455 . ? O4 5 O2 58.2(3) . . ? O3 5 O2 57.2(3) . . ? O7 5 O2 121.4(4) 1_455 . ? O2 5 O2 171.0(6) 1_455 . ? AP 5 Si1 105.2(7) . 1_455 ? XOA 5 Si1 74.8(3) . 1_455 ? O5 5 Si1 30.50(19) 1_455 1_455 ? O4 5 Si1 147.0(4) . 1_455 ? O3 5 Si1 90.9(3) . 1_455 ? O7 5 Si1 86.9(3) 1_455 1_455 ? O2 5 Si1 31.17(17) 1_455 1_455 ? O2 5 Si1 144.6(4) . 1_455 ? AP 5 Si2 103.8(7) . . ? XOA 5 Si2 76.4(3) . . ? O5 5 Si2 145.7(4) 1_455 . ? O4 5 Si2 30.22(18) . . ? O3 5 Si2 86.0(3) . . ? O7 5 Si2 91.0(3) 1_455 . ? O2 5 Si2 145.0(4) 1_455 . ? O2 5 Si2 31.06(17) . . ? Si1 5 Si2 151.0(4) 1_455 . ? AP 5 Si2 103.3(7) . 1_455 ? XOA 5 Si2 70.8(3) . 1_455 ? O5 5 Si2 87.4(3) 1_455 1_455 ? O4 5 Si2 91.7(3) . 1_455 ? O3 5 Si2 145.6(4) . 1_455 ? O7 5 Si2 29.81(18) 1_455 1_455 ? O2 5 Si2 30.44(17) 1_455 1_455 ? O2 5 Si2 145.6(4) . 1_455 ? Si1 5 Si2 57.25(17) 1_455 1_455 ? Si2 5 Si2 115.0(3) . 1_455 ? AP 5 Si1 105.0(7) . . ? XOA 5 Si1 81.0(3) . . ? O5 5 Si1 90.9(3) 1_455 . ? O4 5 Si1 86.6(3) . . ? O3 5 Si1 29.27(18) . . ? O7 5 Si1 145.6(4) 1_455 . ? O2 5 Si1 145.7(4) 1_455 . ? O2 5 Si1 30.12(17) . . ? Si1 5 Si1 114.9(3) 1_455 . ? Si2 5 Si1 56.83(17) . . ? Si2 5 Si1 151.7(4) 1_455 . ? _diffrn_measured_fraction_theta_max 0.994 _diffrn_reflns_theta_full 27.50 _diffrn_measured_fraction_theta_full 0.994 _refine_diff_density_max 1.318 _refine_diff_density_min -1.384 _refine_diff_density_rms 0.254