data_esquireite _audit_creation_method SHELXL-2013 _chemical_name_mineral 'esquireite' _chemical_compound_source 'Trumbull Peak, California' _chemical_formula_sum 'H14 Ba O20 Si6' _chemical_formula_weight 639.99 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'Ba' 'Ba' -0.3244 2.2819 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 5 _space_group_name_H-M_alt 'C 2' _space_group_name_Hall 'C 2y' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' _cell_length_a 13.601(4) _cell_length_b 4.9222(10) _cell_length_c 15.092(5) _cell_angle_alpha 90 _cell_angle_beta 111.578(19) _cell_angle_gamma 90 _cell_volume 939.6(4) _cell_formula_units_Z 2 _cell_measurement_temperature 293(2) _exptl_crystal_density_diffrn 2.262 _exptl_crystal_F_000 628 _exptl_crystal_size_max 0.080 _exptl_crystal_size_mid 0.060 _exptl_crystal_size_min 0.010 _exptl_absorpt_coefficient_mu 2.590 _shelx_estimated_absorpt_T_min 0.820 _shelx_estimated_absorpt_T_max 0.975 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details Higashi2001 _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71075 _diffrn_radiation_type MoK\a _diffrn_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_reflns_number 3253 _diffrn_reflns_av_unetI/netI 0.0844 _diffrn_reflns_av_R_equivalents 0.1725 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -3 _diffrn_reflns_limit_k_max 3 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_theta_min 3.007 _diffrn_reflns_theta_max 14.961 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measured_fraction_theta_full 0.241 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_Laue_measured_fraction_full 0.241 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_point_group_measured_fraction_full 0.229 _reflns_number_total 387 _reflns_number_gt 323 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.683 _reflns_Friedel_fraction_max 1.000 _reflns_Friedel_fraction_full 0.213 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1503P)^2^+102.6008P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 110 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons and Flack (2004), Acta Cryst. A60, s61). ; _refine_ls_abs_structure_Flack 0.50(10) _chemical_absolute_configuration ? _refine_ls_number_reflns 387 _refine_ls_number_parameters 72 _refine_ls_number_restraints 13 _refine_ls_R_factor_all 0.1227 _refine_ls_R_factor_gt 0.1083 _refine_ls_wR_factor_ref 0.2706 _refine_ls_wR_factor_gt 0.2522 _refine_ls_goodness_of_fit_ref 1.113 _refine_ls_restrained_S_all 1.126 _refine_ls_shift/su_max 0.007 _refine_ls_shift/su_mean 0.001 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ba Ba 0.5000 0.373(3) 0.0000 0.094(5) Uani 1 2 d S T P . . Si1 Si 0.2151(19) 0.549(5) 0.4371(17) 0.055(9) Uiso 1 1 d D . . . . Si2 Si 0.4821(15) 0.876(6) 0.3936(14) 0.053(8) Uiso 1 1 d D . . . . Si3 Si 0.3450(18) 0.396(6) 0.3071(16) 0.065(9) Uiso 1 1 d D . . . . O1 O 0.268(4) 0.529(10) 0.357(3) 0.07(2) Uiso 1 1 d D . . . . O2 O 0.278(3) 0.372(8) 0.531(3) 0.061(15) Uiso 1 1 d D . . . . O3 O 0.092(2) 0.465(10) 0.381(3) 0.06(2) Uiso 1 1 d D . . . . O4 O 0.401(5) 0.115(9) 0.348(4) 0.09(2) Uiso 1 1 d D . . . . O5 O 0.446(5) 0.599(11) 0.333(6) 0.15(4) Uiso 1 1 d D . . . . O6 O 0.5000 0.783(15) 0.5000 0.09(3) Uiso 1 2 d DS . P . . O7 O 0.278(3) 0.428(13) 0.195(2) 0.046(17) Uiso 1 1 d D . . . . O8 O 0.136(7) 0.33(3) 0.022(6) 0.05(3) Uiso 0.5 1 d . . P . . O9 O 0.240(7) 0.90(3) 0.104(6) 0.05(3) Uiso 0.5 1 d . . P . . O10 O 0.359(8) 1.21(2) 0.080(7) 0.04(3) Uiso 0.5 1 d . . P . . O11 O 0.555(11) 0.99(3) 0.162(10) 0.11(6) Uiso 0.5 1 d . . P . . O12 O 0.558(14) 0.53(3) 0.189(12) 0.14(6) Uiso 0.5 1 d . . P . . O13 O 0.179(8) 0.95(2) 0.155(8) 0.07(4) Uiso 0.5 1 d . . P . . O14 O 0.419(15) 0.62(4) 0.109(13) 0.15(7) Uiso 0.5 1 d . . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ba 0.079(7) 0.067(7) 0.150(10) 0.000 0.058(6) 0.000 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ba O14 2.59(18) 2_655 ? Ba O14 2.59(18) . ? Ba O13 2.72(10) 3_545 ? Ba O13 2.72(10) 4_545 ? Ba O10 2.73(10) 1_545 ? Ba O10 2.73(10) 2_645 ? Ba O12 2.78(16) 2_655 ? Ba O12 2.78(16) . ? Ba O8 2.86(11) 3 ? Ba O8 2.86(11) 4 ? Ba O11 2.97(14) 2_645 ? Ba O11 2.97(14) 1_545 ? Ba O9 3.06(8) 3_545 ? Ba O9 3.06(8) 4_545 ? Ba O8 3.19(12) 4_545 ? Ba O8 3.19(12) 3_545 ? Si1 O2 1.61(2) . ? Si1 O1 1.62(3) . ? Si1 O3 1.63(3) . ? Si1 O2 1.65(3) 4_556 ? Si2 O4 1.58(3) 1_565 ? Si2 O6 1.60(2) . ? Si2 O5 1.61(3) . ? Si2 O3 1.64(3) 3 ? Si3 O4 1.59(3) . ? Si3 O7 1.61(3) . ? Si3 O5 1.62(3) . ? Si3 O1 1.64(3) . ? O2 Si1 1.65(3) 4_546 ? O3 Si2 1.64(3) 3_445 ? O4 Si2 1.58(3) 1_545 ? O6 Si2 1.60(2) 2_656 ? O8 Ba 2.86(11) 3_445 ? O8 Ba 3.19(12) 3_455 ? O9 O13 1.36(12) . ? O9 Ba 3.06(8) 3_455 ? O10 Ba 2.73(10) 1_565 ? O11 Ba 2.97(14) 1_565 ? O13 Ba 2.72(10) 3_455 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O14 Ba O14 125(8) 2_655 . ? O14 Ba O13 92(5) 2_655 3_545 ? O14 Ba O13 81(5) . 3_545 ? O14 Ba O13 81(5) 2_655 4_545 ? O14 Ba O13 92(5) . 4_545 ? O13 Ba O13 164(5) 3_545 4_545 ? O14 Ba O10 162(4) 2_655 1_545 ? O14 Ba O10 47(5) . 1_545 ? O13 Ba O10 102(3) 3_545 1_545 ? O13 Ba O10 83(3) 4_545 1_545 ? O14 Ba O10 47(5) 2_655 2_645 ? O14 Ba O10 162(4) . 2_645 ? O13 Ba O10 83(3) 3_545 2_645 ? O13 Ba O10 102(3) 4_545 2_645 ? O10 Ba O10 146(4) 1_545 2_645 ? O14 Ba O12 41(5) 2_655 2_655 ? O14 Ba O12 120(5) . 2_655 ? O13 Ba O12 132(4) 3_545 2_655 ? O13 Ba O12 41(4) 4_545 2_655 ? O10 Ba O12 124(4) 1_545 2_655 ? O10 Ba O12 67(4) 2_645 2_655 ? O14 Ba O12 120(5) 2_655 . ? O14 Ba O12 41(5) . . ? O13 Ba O12 41(4) 3_545 . ? O13 Ba O12 132(4) 4_545 . ? O10 Ba O12 67(4) 1_545 . ? O10 Ba O12 124(4) 2_645 . ? O12 Ba O12 148(7) 2_655 . ? O14 Ba O8 46(4) 2_655 3 ? O14 Ba O8 88(4) . 3 ? O13 Ba O8 57(3) 3_545 3 ? O13 Ba O8 109(3) 4_545 3 ? O10 Ba O8 135(3) 1_545 3 ? O10 Ba O8 76(3) 2_645 3 ? O12 Ba O8 80(4) 2_655 3 ? O12 Ba O8 75(4) . 3 ? O14 Ba O8 88(4) 2_655 4 ? O14 Ba O8 46(4) . 4 ? O13 Ba O8 109(3) 3_545 4 ? O13 Ba O8 57(3) 4_545 4 ? O10 Ba O8 76(3) 1_545 4 ? O10 Ba O8 135(3) 2_645 4 ? O12 Ba O8 75(4) 2_655 4 ? O12 Ba O8 80(4) . 4 ? O8 Ba O8 76(4) 3 4 ? O14 Ba O11 79(5) 2_655 2_645 ? O14 Ba O11 141(5) . 2_645 ? O13 Ba O11 133(4) 3_545 2_645 ? O13 Ba O11 60(3) 4_545 2_645 ? O10 Ba O11 100(3) 1_545 2_645 ? O10 Ba O11 57(3) 2_645 2_645 ? O12 Ba O11 56(4) 2_655 2_645 ? O12 Ba O11 156(4) . 2_645 ? O8 Ba O11 124(3) 3 2_645 ? O8 Ba O11 117(3) 4 2_645 ? O14 Ba O11 141(5) 2_655 1_545 ? O14 Ba O11 79(5) . 1_545 ? O13 Ba O11 60(3) 3_545 1_545 ? O13 Ba O11 133(4) 4_545 1_545 ? O10 Ba O11 57(3) 1_545 1_545 ? O10 Ba O11 100(3) 2_645 1_545 ? O12 Ba O11 156(4) 2_655 1_545 ? O12 Ba O11 56(4) . 1_545 ? O8 Ba O11 117(3) 3 1_545 ? O8 Ba O11 124(3) 4 1_545 ? O11 Ba O11 100(5) 2_645 1_545 ? O14 Ba O9 72(5) 2_655 3_545 ? O14 Ba O9 106(4) . 3_545 ? O13 Ba O9 26(2) 3_545 3_545 ? O13 Ba O9 152(3) 4_545 3_545 ? O10 Ba O9 125(3) 1_545 3_545 ? O10 Ba O9 57(3) 2_645 3_545 ? O12 Ba O9 111(4) 2_655 3_545 ? O12 Ba O9 68(4) . 3_545 ? O8 Ba O9 52(3) 3 3_545 ? O8 Ba O9 124(4) 4 3_545 ? O11 Ba O9 110(3) 2_645 3_545 ? O11 Ba O9 73(4) 1_545 3_545 ? O14 Ba O9 106(4) 2_655 4_545 ? O14 Ba O9 72(5) . 4_545 ? O13 Ba O9 152(3) 3_545 4_545 ? O13 Ba O9 26(2) 4_545 4_545 ? O10 Ba O9 57(3) 1_545 4_545 ? O10 Ba O9 125(3) 2_645 4_545 ? O12 Ba O9 68(4) 2_655 4_545 ? O12 Ba O9 111(4) . 4_545 ? O8 Ba O9 124(4) 3 4_545 ? O8 Ba O9 52(3) 4 4_545 ? O11 Ba O9 73(4) 2_645 4_545 ? O11 Ba O9 110(3) 1_545 4_545 ? O9 Ba O9 176(6) 3_545 4_545 ? O14 Ba O8 133(4) 2_655 4_545 ? O14 Ba O8 95(5) . 4_545 ? O13 Ba O8 121(3) 3_545 4_545 ? O13 Ba O8 74(3) 4_545 4_545 ? O10 Ba O8 48(3) 1_545 4_545 ? O10 Ba O8 100(3) 2_645 4_545 ? O12 Ba O8 101(4) 2_655 4_545 ? O12 Ba O8 106(4) . 4_545 ? O8 Ba O8 176(3) 3 4_545 ? O8 Ba O8 109(3) 4 4_545 ? O11 Ba O8 54(3) 2_645 4_545 ? O11 Ba O8 61(3) 1_545 4_545 ? O9 Ba O8 124(3) 3_545 4_545 ? O9 Ba O8 61(3) 4_545 4_545 ? O14 Ba O8 95(5) 2_655 3_545 ? O14 Ba O8 133(4) . 3_545 ? O13 Ba O8 74(3) 3_545 3_545 ? O13 Ba O8 121(3) 4_545 3_545 ? O10 Ba O8 100(3) 1_545 3_545 ? O10 Ba O8 48(3) 2_645 3_545 ? O12 Ba O8 106(4) 2_655 3_545 ? O12 Ba O8 101(4) . 3_545 ? O8 Ba O8 109(3) 3 3_545 ? O8 Ba O8 176(3) 4 3_545 ? O11 Ba O8 61(3) 2_645 3_545 ? O11 Ba O8 54(3) 1_545 3_545 ? O9 Ba O8 61(3) 3_545 3_545 ? O9 Ba O8 124(3) 4_545 3_545 ? O8 Ba O8 67(4) 4_545 3_545 ? O2 Si1 O1 112(3) . . ? O2 Si1 O3 116(3) . . ? O1 Si1 O3 104(3) . . ? O2 Si1 O2 108.0(15) . 4_556 ? O1 Si1 O2 107(3) . 4_556 ? O3 Si1 O2 109(3) . 4_556 ? O4 Si2 O6 118(3) 1_565 . ? O4 Si2 O5 111(4) 1_565 . ? O6 Si2 O5 103(4) . . ? O4 Si2 O3 106(4) 1_565 3 ? O6 Si2 O3 113(2) . 3 ? O5 Si2 O3 105(3) . 3 ? O4 Si3 O7 120(4) . . ? O4 Si3 O5 102(4) . . ? O7 Si3 O5 107(4) . . ? O4 Si3 O1 118(3) . . ? O7 Si3 O1 103(3) . . ? O5 Si3 O1 106(4) . . ? Si1 O1 Si3 155(4) . . ? Si1 O2 Si1 137(3) . 4_546 ? Si1 O3 Si2 145(3) . 3_445 ? Si2 O4 Si3 166(5) 1_545 . ? Si2 O5 Si3 135(5) . . ? Si2 O6 Si2 147(5) . 2_656 ? Ba O8 Ba 109(3) 3_445 3_455 ? O13 O9 Ba 62(6) . 3_455 ? Ba O11 Ba 93(3) 1_565 . ? O9 O13 Ba 91(6) . 3_455 ? _refine_diff_density_max 0.929 _refine_diff_density_min -0.746 _refine_diff_density_rms 0.201 _shelxl_version_number 2013-4 _shelx_res_file ; TITL Mineral 21 CELL 0.71075 13.60090 4.92220 15.09220 90.000 111.578 90.000 ZERR 2 0.00350 0.00100 0.00450 0.000 0.019 0.000 LATT -7 SYMM -X, +Y, -Z SFAC BA SI O H UNIT 2 12 40 28 L.S. 8 CONN 16 3 BA OMIT -4 0 1 EQIV $1 x, y+1, z EQIV $2 x+1/2, y+1/2, z EQIV $3 -x+1/2, y+1/2, -z+1 FMAP 2 PLAN 8 ACTA DFIX 1.64 0.02 SI1 O3 SI1 O2 SI1 O2_$3 SI1 O1 DFIX 1.64 0.02 SI2 O4_$1 SI2 O6 SI2 O3_$2 SI2 O5 DFIX 1.64 0.02 SI3 O4 SI3 O5 SI3 O1 SI3 O7 SIZE 0.080 0.060 0.010 WGHT 0.150300 102.600800 FVAR 0.29669 BA 1 0.500000 0.372880 0.000000 10.50000 0.07894 0.06663 = 0.15023 0.00000 0.05808 0.00000 SI1 2 0.215140 0.549247 0.437075 11.00000 0.05541 SI2 2 0.482114 0.875697 0.393616 11.00000 0.05295 SI3 2 0.344985 0.395626 0.307091 11.00000 0.06451 O1 3 0.267706 0.528838 0.357059 11.00000 0.06955 O2 3 0.278298 0.371792 0.530776 11.00000 0.06101 O3 3 0.091911 0.465169 0.380739 11.00000 0.05911 O4 3 0.401058 0.114586 0.348359 11.00000 0.09210 O5 3 0.445594 0.598960 0.332880 11.00000 0.15203 O6 3 0.500000 0.782747 0.500000 10.50000 0.09031 O7 3 0.277642 0.428386 0.194755 11.00000 0.04606 O8 3 0.136165 0.332495 0.022409 10.50000 0.04564 O9 3 0.240173 0.896568 0.104003 10.50000 0.04586 O10 3 0.359245 1.209538 0.080099 10.50000 0.03567 O11 3 0.555170 0.986122 0.161916 10.50000 0.11220 O12 3 0.557530 0.529713 0.189375 10.50000 0.13663 O13 3 0.178932 0.950500 0.155416 10.50000 0.07160 O14 3 0.418625 0.615202 0.109140 10.50000 0.14872 HKLF 4 REM Mineral 21 REM R1 = 0.1083 for 323 Fo > 4sig(Fo) and 0.1227 for all 387 data REM 72 parameters refined using 13 restraints END WGHT 0.1487 96.0849 REM Highest difference peak 0.929, deepest hole -0.746, 1-sigma level 0.201 Q1 1 0.1201 0.3707 0.0894 11.00000 0.05 0.93 Q2 1 0.4053 0.5602 0.3826 11.00000 0.05 0.80 Q3 1 0.5000 0.7310 0.0000 10.50000 0.05 0.66 Q4 1 0.4229 -0.0184 0.3129 11.00000 0.05 0.65 Q5 1 0.2040 0.2040 0.4259 11.00000 0.05 0.64 Q6 1 0.0571 0.4934 0.3016 11.00000 0.05 0.61 Q7 1 0.3078 1.3435 0.0301 11.00000 0.05 0.61 Q8 1 0.5449 0.3789 0.0982 11.00000 0.05 0.61 ; _shelx_res_checksum 59408 _shelx_hkl_file ; 2 0 -1 244.06 39.93 2 0 -1 192.24 29.80 2 0 -1 204.92 35.10 -2 0 1 210.66 14.60 -2 0 1 193.25 33.14 -2 0 1 218.95 37.17 -2 0 1 219.57 31.56 2 0 0 361.77 38.38 2 0 0 278.61 51.37 -2 0 0 347.08 51.46 -2 0 0 245.85 24.15 -2 0 0 455.76 71.30 -2 0 0 338.77 28.61 -2 0 0 374.09 31.50 -2 0 2 1490.22 104.28 -2 0 2 1367.92 78.30 -2 0 2 1480.12 84.41 2 0 -2 1470.68 73.61 2 0 -2 1397.21 85.14 2 0 -2 1484.46 115.32 -2 0 2 1620.34 109.32 -2 0 2 1461.45 89.88 2 0 -2 1546.66 86.11 -2 0 -1 2163.73 138.44 -2 0 -1 2248.04 137.39 -2 0 -1 2247.62 183.44 -2 0 -1 2133.53 130.70 2 0 1 2167.59 136.01 2 0 1 2280.61 175.26 0 0 -3 1907.58 203.08 0 0 -3 1956.17 186.57 0 0 -3 1835.71 152.45 0 0 -3 2039.86 159.02 0 0 3 2046.78 161.51 0 0 3 1952.04 145.71 0 0 3 1820.02 181.22 0 0 3 1930.28 146.42 0 0 3 1910.77 114.90 0 0 -3 1863.38 137.54 2 0 -3 2404.17 184.65 2 0 -3 2596.01 158.34 2 0 -3 2501.80 124.82 -2 0 3 2605.18 206.93 -2 0 3 2313.42 106.48 -2 0 3 2777.50 208.89 2 0 -3 2351.19 145.74 -2 0 3 2532.28 157.90 -2 0 3 2601.19 173.53 -1 -1 0 180.27 28.48 1 -1 0 134.65 49.37 -1 -1 0 217.48 53.62 -1 -1 0 226.97 39.50 -1 -1 0 179.99 59.04 -1 -1 0 311.00 49.77 -1 1 0 199.75 47.72 1 1 0 208.00 37.37 -1 1 0 246.01 53.78 -1 1 0 314.95 54.37 1 -1 0 202.56 35.99 1 -1 0 186.31 49.61 1 -1 0 210.48 39.11 1 1 0 208.65 28.90 1 -1 0 308.01 49.57 1 1 0 127.23 55.60 -1 -1 0 339.63 47.87 -1 1 0 220.13 35.50 -1 1 0 227.43 66.33 1 1 -1 439.26 60.47 1 1 -1 426.36 55.55 -1 -1 1 356.78 53.05 -1 -1 1 381.30 48.19 -1 1 1 339.58 29.45 -1 1 1 509.70 74.77 -1 1 1 423.53 52.42 -1 -1 1 340.50 62.94 1 -1 -1 403.63 40.36 -1 1 1 343.91 48.79 1 -1 -1 455.36 77.31 1 1 -1 328.74 61.82 1 -1 -1 346.63 60.37 1 -1 -1 344.96 71.14 1 1 -1 343.21 51.10 -1 -1 1 396.44 54.85 -1 1 1 488.72 73.03 1 -1 1 3356.53 171.54 1 1 1 3380.81 211.04 1 -1 1 3373.05 178.27 1 -1 1 3331.14 184.56 1 1 1 3430.08 267.35 1 1 1 3577.26 211.54 -1 1 -1 3354.05 178.80 -1 1 -1 3267.06 229.81 -1 -1 -1 3470.89 252.79 -1 -1 -1 3320.28 199.89 -1 -1 -1 3394.77 237.07 -1 1 -1 3363.26 174.99 -1 -1 -1 3324.87 208.65 -1 1 -1 3370.59 180.45 1 1 1 3387.77 120.11 1 1 1 3337.08 122.53 1 -1 1 3155.54 174.09 1 1 1 3420.53 232.11 -1 1 -1 3433.48 226.80 1 -1 1 3456.30 241.93 1 -1 -2 1137.35 143.23 -1 -1 2 1302.27 124.56 -1 1 2 748.03 77.29 -1 1 2 1185.73 131.63 -1 -1 2 1096.25 110.97 1 -1 -2 767.79 87.23 1 -1 -2 1045.21 68.88 -1 1 2 974.95 129.70 1 -1 -2 753.93 90.23 -1 1 2 808.50 60.61 1 -1 -2 1300.42 149.12 -1 1 2 1215.28 85.47 -1 -1 2 873.78 77.58 -1 -1 2 920.71 79.62 1 1 -2 811.84 82.21 1 1 -2 1306.56 86.62 1 1 -2 1307.57 124.82 1 1 -2 1055.09 105.56 -2 0 -2 96.90 36.13 2 0 2 95.89 19.04 -2 0 -2 50.53 47.22 2 0 2 55.98 36.85 -2 0 -2 55.50 72.17 -2 0 -2 30.77 59.86 -2 0 -2 122.42 23.13 -2 0 -2 23.17 26.73 2 0 2 36.03 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