data_CMN01 _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'Ca0.59 H Mn1.41 Na O9 Si3' _chemical_formula_weight 353.45 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Na' 'Na' 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Mn' 'Mn' 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ca' 'Ca' 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 7.7604(16) _cell_length_b 6.9259(14) _cell_length_c 6.8196(14) _cell_angle_alpha 90.60(3) _cell_angle_beta 94.23(3) _cell_angle_gamma 102.79(3) _cell_volume 356.33(13) _cell_formula_units_Z 2 _cell_measurement_temperature 298(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 3.294 _exptl_crystal_F_000 346 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_absorpt_coefficient_mu 3.574 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 298(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 4641 _diffrn_reflns_av_unetI/netI 0.0150 _diffrn_reflns_av_R_equivalents 0.0095 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_theta_min 2.700 _diffrn_reflns_theta_max 33.042 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.896 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.896 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.896 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 2415 _reflns_number_gt 2233 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0269P)^2^+0.1905P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens difmap _refine_ls_hydrogen_treatment refxyz _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 2415 _refine_ls_number_parameters 144 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0216 _refine_ls_R_factor_gt 0.0192 _refine_ls_wR_factor_ref 0.0518 _refine_ls_wR_factor_gt 0.0507 _refine_ls_goodness_of_fit_ref 1.095 _refine_ls_restrained_S_all 1.095 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Na1 Na 0.55606(8) 0.24932(9) 0.35087(9) 0.01874(13) Uani 1 1 d . . . . . M1MN Mn 0.85065(3) 0.59374(3) 0.14028(3) 0.01083(7) Uani 0.468(5) 1 d . . P . . M1CA Ca 0.85065(3) 0.59374(3) 0.14028(3) 0.01083(7) Uani 0.532(5) 1 d . . P . . M2MN Mn 0.85069(3) 0.08430(3) 0.13381(3) 0.01079(6) Uani 0.949(5) 1 d . . P . . M2CA Ca 0.85069(3) 0.08430(3) 0.13381(3) 0.01079(6) Uani 0.051(5) 1 d . . P . . Si1 Si 0.21782(5) 0.40483(5) 0.33851(5) 0.00906(8) Uani 1 1 d . . . . . Si2 Si 0.20592(5) 0.95593(5) 0.35073(5) 0.00870(8) Uani 1 1 d . . . . . Si3 Si 0.45254(5) 0.74280(5) 0.14291(5) 0.00886(8) Uani 1 1 d . . . . . O1 O 0.66057(13) 0.80150(15) 0.11762(15) 0.01366(19) Uani 1 1 d . . . . . O2 O 0.32406(14) 0.71685(15) 0.94365(14) 0.01345(19) Uani 1 1 d . . . . . O3 O 0.18618(15) 0.50264(16) 0.54580(15) 0.01441(19) Uani 1 1 d . . . . . O4 O 0.15625(14) 0.84928(14) 0.55372(14) 0.01301(19) Uani 1 1 d . . . . . O5 O 0.06087(13) 0.38794(14) 0.16948(14) 0.01186(18) Uani 1 1 d . . . . . O6 O 0.05451(13) 0.89859(14) 0.17270(14) 0.01192(18) Uani 1 1 d . . . . . O7 O 0.40590(13) 0.53313(14) 0.26444(15) 0.01423(19) Uani 1 1 d . . . . . O8 O 0.39388(13) 0.90473(14) 0.29146(15) 0.01278(18) Uani 1 1 d . . . . . O9 O 0.26298(13) 0.19348(13) 0.39321(14) 0.01182(18) Uani 1 1 d . . . . . H1 H 0.167(6) 0.591(7) 0.543(6) 0.015 Uiso 0.5 1 d . U P . . H2 H 0.154(5) 0.734(6) 0.533(6) 0.015 Uiso 0.5 1 d . U P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Na1 0.0137(3) 0.0211(3) 0.0207(3) 0.0005(2) 0.0030(2) 0.0018(2) M1MN 0.01214(12) 0.00905(11) 0.01119(11) 0.00105(7) 0.00108(8) 0.00205(8) M1CA 0.01214(12) 0.00905(11) 0.01119(11) 0.00105(7) 0.00108(8) 0.00205(8) M2MN 0.01144(11) 0.01041(10) 0.01083(10) 0.00069(7) 0.00074(7) 0.00314(7) M2CA 0.01144(11) 0.01041(10) 0.01083(10) 0.00069(7) 0.00074(7) 0.00314(7) Si1 0.01019(16) 0.00731(14) 0.00963(16) 0.00059(11) -0.00035(12) 0.00218(12) Si2 0.01012(16) 0.00730(15) 0.00859(15) 0.00052(11) 0.00006(12) 0.00198(12) Si3 0.00912(16) 0.00837(15) 0.00893(16) 0.00035(11) 0.00063(12) 0.00164(12) O1 0.0110(4) 0.0136(4) 0.0155(5) 0.0004(3) 0.0023(3) 0.0004(3) O2 0.0138(5) 0.0159(4) 0.0108(4) -0.0004(3) -0.0014(3) 0.0043(4) O3 0.0187(5) 0.0125(4) 0.0137(4) -0.0026(4) 0.0000(4) 0.0076(4) O4 0.0188(5) 0.0088(4) 0.0113(4) 0.0016(3) 0.0026(4) 0.0023(4) O5 0.0117(4) 0.0128(4) 0.0108(4) 0.0013(3) -0.0007(3) 0.0025(3) O6 0.0123(4) 0.0126(4) 0.0107(4) -0.0005(3) -0.0006(3) 0.0031(3) O7 0.0128(4) 0.0102(4) 0.0195(5) 0.0052(3) 0.0015(4) 0.0017(3) O8 0.0123(4) 0.0119(4) 0.0147(4) -0.0026(3) 0.0006(3) 0.0041(3) O9 0.0143(4) 0.0073(4) 0.0139(4) 0.0010(3) 0.0002(3) 0.0030(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Na1 O9 2.2618(13) . ? Na1 O2 2.2680(13) 2_666 ? Na1 O3 2.3862(15) 2_666 ? Na1 O8 2.4533(14) 1_545 ? Na1 O4 2.5188(14) 2_666 ? Na1 O7 2.5507(13) . ? Na1 O8 2.7087(14) 2_666 ? Na1 O7 2.9741(15) 2_666 ? Na1 Si2 3.0111(13) 1_545 ? Na1 Si1 3.0460(10) . ? Na1 Si2 3.2004(12) 2_666 ? M1MN O5 2.2652(12) 2_665 ? M1MN O3 2.2685(12) 2_666 ? M1MN O1 2.2762(12) . ? M1MN O2 2.3154(13) 2_666 ? M1MN O6 2.3386(13) 1_655 ? M1MN O5 2.3917(12) 1_655 ? M2MN O1 2.1719(13) 1_545 ? M2MN O2 2.1798(12) 2_666 ? M2MN O4 2.1823(11) 2_666 ? M2MN O6 2.2523(12) 1_645 ? M2MN O6 2.2623(11) 2_665 ? M2MN O5 2.3566(13) 1_655 ? Si1 O5 1.5978(12) . ? Si1 O3 1.6194(12) . ? Si1 O9 1.6198(10) . ? Si1 O7 1.6489(12) . ? Si2 O4 1.6076(11) . ? Si2 O6 1.6079(12) . ? Si2 O9 1.6234(11) 1_565 ? Si2 O8 1.6522(11) . ? Si3 O1 1.5979(11) . ? Si3 O2 1.6089(12) 1_554 ? Si3 O8 1.6618(11) . ? Si3 O7 1.6623(11) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O9 Na1 O2 125.17(5) . 2_666 ? O9 Na1 O3 136.28(5) . 2_666 ? O2 Na1 O3 82.86(5) 2_666 2_666 ? O9 Na1 O8 65.25(4) . 1_545 ? O2 Na1 O8 95.85(5) 2_666 1_545 ? O3 Na1 O8 153.03(5) 2_666 1_545 ? O9 Na1 O4 145.81(4) . 2_666 ? O2 Na1 O4 80.88(5) 2_666 2_666 ? O3 Na1 O4 60.21(4) 2_666 2_666 ? O8 Na1 O4 92.91(5) 1_545 2_666 ? O9 Na1 O7 64.02(4) . . ? O2 Na1 O7 88.75(5) 2_666 . ? O3 Na1 O7 86.73(4) 2_666 . ? O8 Na1 O7 120.22(4) 1_545 . ? O4 Na1 O7 146.22(4) 2_666 . ? O9 Na1 O8 88.66(5) . 2_666 ? O2 Na1 O8 140.30(4) 2_666 2_666 ? O3 Na1 O8 84.93(5) 2_666 2_666 ? O8 Na1 O8 78.97(5) 1_545 2_666 ? O4 Na1 O8 60.37(4) 2_666 2_666 ? O7 Na1 O8 128.09(5) . 2_666 ? O9 Na1 O7 83.79(5) . 2_666 ? O2 Na1 O7 138.84(4) 2_666 2_666 ? O3 Na1 O7 57.75(4) 2_666 2_666 ? O8 Na1 O7 124.48(5) 1_545 2_666 ? O4 Na1 O7 88.48(4) 2_666 2_666 ? O7 Na1 O7 78.40(4) . 2_666 ? O8 Na1 O7 54.23(3) 2_666 2_666 ? O9 Na1 Si2 32.03(3) . 1_545 ? O2 Na1 Si2 115.02(5) 2_666 1_545 ? O3 Na1 Si2 162.09(4) 2_666 1_545 ? O8 Na1 Si2 33.25(3) 1_545 1_545 ? O4 Na1 Si2 121.31(4) 2_666 1_545 ? O7 Na1 Si2 92.24(4) . 1_545 ? O8 Na1 Si2 81.66(4) 2_666 1_545 ? O7 Na1 Si2 104.52(4) 2_666 1_545 ? O9 Na1 Si1 31.33(3) . . ? O2 Na1 Si1 110.92(4) 2_666 . ? O3 Na1 Si1 112.62(4) 2_666 . ? O8 Na1 Si1 93.10(4) 1_545 . ? O4 Na1 Si1 166.11(4) 2_666 . ? O7 Na1 Si1 32.77(3) . . ? O8 Na1 Si1 108.67(4) 2_666 . ? O7 Na1 Si1 77.81(4) 2_666 . ? Si2 Na1 Si1 61.39(2) 1_545 . ? O9 Na1 Si2 117.18(4) . 2_666 ? O2 Na1 Si2 109.36(4) 2_666 2_666 ? O3 Na1 Si2 73.32(4) 2_666 2_666 ? O8 Na1 Si2 81.85(4) 1_545 2_666 ? O4 Na1 Si2 29.71(3) 2_666 2_666 ? O7 Na1 Si2 150.60(4) . 2_666 ? O8 Na1 Si2 31.08(3) 2_666 2_666 ? O7 Na1 Si2 72.74(3) 2_666 2_666 ? Si2 Na1 Si2 100.19(3) 1_545 2_666 ? Si1 Na1 Si2 139.72(3) . 2_666 ? O5 M1MN O3 161.20(4) 2_665 2_666 ? O5 M1MN O1 99.73(4) 2_665 . ? O3 M1MN O1 98.92(5) 2_666 . ? O5 M1MN O2 88.46(5) 2_665 2_666 ? O3 M1MN O2 84.45(5) 2_666 2_666 ? O1 M1MN O2 104.84(4) . 2_666 ? O5 M1MN O6 81.28(5) 2_665 1_655 ? O3 M1MN O6 104.31(5) 2_666 1_655 ? O1 M1MN O6 80.29(4) . 1_655 ? O2 M1MN O6 169.22(4) 2_666 1_655 ? O5 M1MN O5 80.42(5) 2_665 1_655 ? O3 M1MN O5 81.07(4) 2_666 1_655 ? O1 M1MN O5 177.39(4) . 1_655 ? O2 M1MN O5 77.76(4) 2_666 1_655 ? O6 M1MN O5 97.18(4) 1_655 1_655 ? O5 M1MN Na1 131.07(4) 2_665 . ? O3 M1MN Na1 45.67(4) 2_666 . ? O1 M1MN Na1 91.72(3) . . ? O2 M1MN Na1 42.76(3) 2_666 . ? O6 M1MN Na1 147.65(3) 1_655 . ? O5 M1MN Na1 90.12(3) 1_655 . ? O1 M2MN O2 100.40(4) 1_545 2_666 ? O1 M2MN O4 97.93(5) 1_545 2_666 ? O2 M2MN O4 90.98(5) 2_666 2_666 ? O1 M2MN O6 84.51(4) 1_545 1_645 ? O2 M2MN O6 170.91(4) 2_666 1_645 ? O4 M2MN O6 95.94(5) 2_666 1_645 ? O1 M2MN O6 101.66(5) 1_545 2_665 ? O2 M2MN O6 90.80(5) 2_666 2_665 ? O4 M2MN O6 159.66(4) 2_666 2_665 ? O6 M2MN O6 80.67(5) 1_645 2_665 ? O1 M2MN O5 176.88(4) 1_545 1_655 ? O2 M2MN O5 81.20(4) 2_666 1_655 ? O4 M2MN O5 79.32(5) 2_666 1_655 ? O6 M2MN O5 94.27(4) 1_645 1_655 ? O6 M2MN O5 80.94(5) 2_665 1_655 ? O1 M2MN Na1 85.67(4) 1_545 . ? O2 M2MN Na1 44.78(3) 2_666 . ? O4 M2MN Na1 51.37(4) 2_666 . ? O6 M2MN Na1 143.94(3) 1_645 . ? O6 M2MN Na1 135.35(3) 2_665 . ? O5 M2MN Na1 93.68(4) 1_655 . ? O5 Si1 O3 115.58(6) . . ? O5 Si1 O9 113.33(6) . . ? O3 Si1 O9 105.33(6) . . ? O5 Si1 O7 110.74(6) . . ? O3 Si1 O7 107.70(6) . . ? O9 Si1 O7 103.24(6) . . ? O5 Si1 Na1 130.69(5) . . ? O3 Si1 Na1 113.46(5) . . ? O9 Si1 Na1 46.55(4) . . ? O7 Si1 Na1 56.87(4) . . ? O5 Si1 Na1 136.34(4) . 2_666 ? O3 Si1 Na1 43.50(5) . 2_666 ? O9 Si1 Na1 109.75(5) . 2_666 ? O7 Si1 Na1 64.51(5) . 2_666 ? Na1 Si1 Na1 85.23(3) . 2_666 ? O4 Si2 O6 114.66(6) . . ? O4 Si2 O9 108.56(6) . 1_565 ? O6 Si2 O9 111.85(6) . 1_565 ? O4 Si2 O8 107.76(6) . . ? O6 Si2 O8 111.11(6) . . ? O9 Si2 O8 102.08(6) 1_565 . ? O4 Si2 Na1 117.51(5) . 1_565 ? O6 Si2 Na1 127.75(5) . 1_565 ? O9 Si2 Na1 47.65(4) 1_565 1_565 ? O8 Si2 Na1 54.50(4) . 1_565 ? O4 Si2 Na1 50.95(4) . 2_666 ? O6 Si2 Na1 140.17(4) . 2_666 ? O9 Si2 Na1 107.96(5) 1_565 2_666 ? O8 Si2 Na1 57.80(4) . 2_666 ? Na1 Si2 Na1 79.81(3) 1_565 2_666 ? O1 Si3 O2 116.32(6) . 1_554 ? O1 Si3 O8 110.79(6) . . ? O2 Si3 O8 108.49(6) 1_554 . ? O1 Si3 O7 109.24(6) . . ? O2 Si3 O7 108.16(6) 1_554 . ? O8 Si3 O7 102.97(6) . . ? O1 Si3 Na1 80.40(5) . 2_665 ? O2 Si3 Na1 35.95(4) 1_554 2_665 ? O8 Si3 Na1 127.03(4) . 2_665 ? O7 Si3 Na1 122.45(5) . 2_665 ? O1 Si3 Na1 101.71(5) . 2_666 ? O2 Si3 Na1 141.78(4) 1_554 2_666 ? O8 Si3 Na1 50.04(4) . 2_666 ? O7 Si3 Na1 59.27(5) . 2_666 ? Na1 Si3 Na1 176.81(2) 2_665 2_666 ? Si3 O1 M2MN 132.28(6) . 1_565 ? Si3 O1 M1MN 126.21(6) . . ? M2MN O1 M1MN 99.61(4) 1_565 . ? Si3 O2 M2MN 123.12(6) 1_556 2_666 ? Si3 O2 Na1 119.44(6) 1_556 2_666 ? M2MN O2 Na1 92.62(5) 2_666 2_666 ? Si3 O2 M1MN 118.50(6) 1_556 2_666 ? M2MN O2 M1MN 103.38(5) 2_666 2_666 ? Na1 O2 M1MN 93.36(5) 2_666 2_666 ? Si1 O3 M1MN 137.63(6) . 2_666 ? Si1 O3 Na1 108.65(6) . 2_666 ? M1MN O3 Na1 91.48(5) 2_666 2_666 ? Si2 O4 M2MN 141.28(6) . 2_666 ? Si2 O4 Na1 99.33(6) . 2_666 ? M2MN O4 Na1 86.03(5) 2_666 2_666 ? Si1 O5 M1MN 114.54(6) . 2_665 ? Si1 O5 M2MN 117.14(6) . 1_455 ? M1MN O5 M2MN 98.57(5) 2_665 1_455 ? Si1 O5 M1MN 126.11(6) . 1_455 ? M1MN O5 M1MN 99.58(5) 2_665 1_455 ? M2MN O5 M1MN 95.98(4) 1_455 1_455 ? Si2 O6 M2MN 118.28(6) . 1_465 ? Si2 O6 M2MN 116.08(6) . 2_665 ? M2MN O6 M2MN 99.33(5) 1_465 2_665 ? Si2 O6 M1MN 123.75(6) . 1_455 ? M2MN O6 M1MN 95.48(4) 1_465 1_455 ? M2MN O6 M1MN 99.18(5) 2_665 1_455 ? Si1 O7 Si3 131.46(7) . . ? Si1 O7 Na1 90.36(5) . . ? Si3 O7 Na1 137.15(6) . . ? Si1 O7 Na1 85.46(5) . 2_666 ? Si3 O7 Na1 92.02(5) . 2_666 ? Na1 O7 Na1 101.60(4) . 2_666 ? Si2 O8 Si3 136.25(7) . . ? Si2 O8 Na1 92.25(5) . 1_565 ? Si3 O8 Na1 124.89(6) . 1_565 ? Si2 O8 Na1 91.12(5) . 2_666 ? Si3 O8 Na1 101.91(5) . 2_666 ? Na1 O8 Na1 101.03(5) 1_565 2_666 ? Si1 O9 Si2 144.88(7) . 1_545 ? Si1 O9 Na1 102.12(6) . . ? Si2 O9 Na1 100.32(6) 1_545 . ? _refine_diff_density_max 0.493 _refine_diff_density_min -0.433 _refine_diff_density_rms 0.091 _shelx_res_file ; TITL al01-3 in P-1 CMN01.res created by SHELXL-2018/3 at 01:39:31 on 21-Aug-2020 CELL 0.71073 7.76040 6.92590 6.81960 90.5993 94.2303 102.7921 ZERR 2.00 0.00155 0.00139 0.00136 0.0300 0.0300 0.0300 LATT 1 SFAC O H NA SI MN CA UNIT 18 2 2 6 2.83 1.17 TEMP 25 ACTA L.S. 18 EXYZ M1MN M1CA EADP M1MN M1CA EXYZ M2MN M2CA EADP M2MN M2CA BOND FMAP 2 PLAN 20 WGHT 0.026900 0.190500 FVAR 0.66532 0.94889 0.46783 NA1 3 0.556057 0.249321 0.350874 11.00000 0.01367 0.02114 = 0.02068 0.00048 0.00296 0.00178 M1MN 5 0.850647 0.593738 0.140277 31.00000 0.01214 0.00905 = 0.01119 0.00105 0.00108 0.00205 M1CA 6 0.850647 0.593738 0.140277 -31.00000 0.01214 0.00905 = 0.01119 0.00105 0.00108 0.00205 M2MN 5 0.850690 0.084303 0.133815 21.00000 0.01144 0.01041 = 0.01083 0.00069 0.00074 0.00314 M2CA 6 0.850690 0.084303 0.133815 -21.00000 0.01144 0.01041 = 0.01083 0.00069 0.00074 0.00314 SI1 4 0.217820 0.404828 0.338509 11.00000 0.01019 0.00731 = 0.00963 0.00059 -0.00035 0.00218 SI2 4 0.205924 0.955932 0.350732 11.00000 0.01012 0.00730 = 0.00859 0.00052 0.00006 0.00198 SI3 4 0.452538 0.742797 0.142914 11.00000 0.00912 0.00837 = 0.00893 0.00035 0.00063 0.00164 O1 1 0.660568 0.801499 0.117619 11.00000 0.01098 0.01357 = 0.01551 0.00039 0.00227 0.00035 O2 1 0.324057 0.716846 0.943650 11.00000 0.01375 0.01585 = 0.01082 -0.00043 -0.00144 0.00427 O3 1 0.186179 0.502638 0.545796 11.00000 0.01870 0.01249 = 0.01370 -0.00264 0.00000 0.00756 O4 1 0.156249 0.849281 0.553717 11.00000 0.01884 0.00881 = 0.01125 0.00164 0.00260 0.00230 O5 1 0.060871 0.387936 0.169476 11.00000 0.01170 0.01278 = 0.01076 0.00127 -0.00074 0.00249 O6 1 0.054507 0.898585 0.172698 11.00000 0.01235 0.01259 = 0.01073 -0.00045 -0.00060 0.00312 O7 1 0.405902 0.533134 0.264444 11.00000 0.01277 0.01018 = 0.01946 0.00515 0.00153 0.00168 O8 1 0.393882 0.904727 0.291459 11.00000 0.01229 0.01188 = 0.01470 -0.00263 0.00058 0.00410 O9 1 0.262978 0.193482 0.393205 11.00000 0.01429 0.00735 = 0.01395 0.00105 0.00019 0.00298 H1 2 0.166726 0.591456 0.542578 10.50000 10.01500 H2 2 0.154424 0.733507 0.532741 10.50000 10.01500 HKLF 4 REM al01-3 in P-1 REM wR2 = 0.051805, GooF = S = 1.09510, Restrained GooF = 1.09510 for all data REM R1 = 0.019225 for 2233 Fo > 4sig(Fo) and 0.021618 for all 2415 data REM 144 parameters refined using 0 restraints END WGHT 0.0269 0.1905 REM Highest difference peak 0.493, deepest hole -0.433, 1-sigma level 0.091 Q1 1 0.4553 0.2414 0.1501 11.00000 0.05 0.46 Q2 1 0.5300 0.7523 0.0906 11.00000 0.05 0.44 Q3 1 0.5887 0.7814 0.1658 11.00000 0.05 0.42 Q4 1 0.9126 0.6003 0.0773 11.00000 0.05 0.42 Q5 1 0.2291 0.0830 0.3686 11.00000 0.05 0.40 Q6 1 0.4241 0.6184 0.2273 11.00000 0.05 0.36 Q7 1 0.3994 0.7221 1.0160 11.00000 0.05 0.35 Q8 1 0.3050 0.9112 0.2832 11.00000 0.05 0.34 Q9 1 0.3430 0.7176 0.9008 11.00000 0.05 0.34 Q10 1 0.3794 1.0070 0.2744 11.00000 0.05 0.33 Q11 1 0.0712 0.9032 0.3675 11.00000 0.05 0.31 Q12 1 0.3492 0.4613 0.3074 11.00000 0.05 0.31 Q13 1 0.1814 0.4514 0.4818 11.00000 0.05 0.30 Q14 1 0.8421 0.5031 0.1354 11.00000 0.05 0.30 Q15 1 0.1220 0.4035 0.2401 11.00000 0.05 0.29 Q16 1 0.4810 0.7577 0.9340 11.00000 0.05 0.29 Q17 1 0.4524 0.8438 0.2548 11.00000 0.05 0.29 Q18 1 0.7367 0.5833 0.1745 11.00000 0.05 0.28 Q19 1 0.0994 0.8837 0.2458 11.00000 0.05 0.28 Q20 1 0.2369 0.8837 0.4939 11.00000 0.05 0.28 ; _shelx_res_checksum 99247 _shelx_hkl_file ; 11 0 -1 73.20 2.70 11 0 -2 33.90 3.80 11 -1 0 2.20 1.60 11 -1 -1 9.60 1.50 11 -1 -2 5.80 1.60 11 -1 -3 86.40 4.70 11 -2 0 30.30 2.60 11 -2 -1 139.60 3.80 11 -2 -2 231.70 5.90 11 -3 0 19.40 2.50 11 -3 -1 13.30 2.00 11 -4 -1 148.60 7.90 10 2 1 10.20 2.30 10 2 0 87.80 6.00 10 2 -1 236.00 6.20 10 2 -2 95.70 4.00 10 1 2 136.20 4.50 10 1 1 3.20 1.50 10 1 0 0.70 1.40 10 1 -1 5.00 1.30 10 1 -2 143.10 4.70 10 1 -3 28.50 3.80 10 0 3 594.60 19.10 10 0 2 70.70 3.40 10 0 1 274.80 6.50 10 0 0 341.90 6.00 10 0 -1 262.70 5.00 10 0 -2 69.60 2.60 10 0 -3 505.50 14.10 10 0 -4 486.00 13.60 10 -1 3 12.50 1.90 10 -1 2 12.00 1.90 10 -1 1 1.90 1.50 10 -1 0 0.30 1.10 10 -1 -1 28.60 1.90 10 -1 -2 128.20 3.40 10 -1 -3 9.00 1.70 10 -1 -4 2.20 1.60 10 -2 3 88.70 3.70 10 -2 2 7.40 1.60 10 -2 1 476.80 9.40 10 -2 0 50.20 3.00 10 -2 -1 242.40 5.90 10 -2 -2 2.80 1.40 10 -2 -3 232.90 5.70 10 -2 -4 13.00 1.90 10 -2 -5 178.90 8.00 10 -3 3 49.70 3.00 10 -3 2 8.60 1.70 10 -3 1 171.90 5.00 10 -3 0 39.60 2.80 10 -3 -1 0.60 1.40 10 -3 -2 28.60 2.40 10 -3 -3 154.00 6.10 10 -3 -4 6.80 2.10 10 -3 -5 38.90 3.60 10 -4 3 248.60 6.40 10 -4 2 71.80 3.40 10 -4 1 37.40 2.70 10 -4 0 3.50 1.40 10 -4 -1 175.80 5.00 10 -4 -2 83.80 3.60 10 -4 -3 46.00 3.80 10 -4 -4 1.80 1.90 10 -5 3 1.50 1.60 10 -5 2 74.10 3.50 10 -5 1 13.10 1.90 10 -5 0 9.50 1.80 10 -5 -1 58.20 3.30 10 -5 -2 96.70 3.90 10 -5 -3 8.30 2.20 10 -6 1 202.90 7.00 10 -6 0 287.80 6.90 10 -6 -1 214.90 5.90 10 -6 -2 3.70 1.90 9 4 -1 205.20 5.70 9 4 -2 17.60 2.70 9 3 2 7.00 1.70 9 3 1 27.30 3.90 9 3 0 7.00 2.70 9 3 -1 1.20 1.40 9 3 -2 79.90 3.60 9 3 -3 1.20 2.10 9 2 3 60.90 3.20 9 2 2 26.30 2.30 9 2 1 333.10 7.30 9 2 0 9.20 1.30 9 2 -1 346.30 7.60 9 2 -2 7.10 1.70 9 2 -3 204.70 8.10 9 2 -4 19.10 3.20 9 1 4 28.70 2.50 9 1 3 5.20 1.60 9 1 2 44.40 2.70 9 1 1 12.60 1.80 9 1 0 6.90 1.20 9 1 -1 -0.60 0.90 9 1 -2 34.80 1.90 9 1 -3 209.70 7.80 9 1 -4 47.30 4.40 9 1 -5 17.30 3.20 9 0 5 179.70 7.80 9 0 4 7.00 1.60 9 0 3 387.80 8.10 9 0 2 52.60 2.80 9 0 1 91.10 3.40 9 0 0 1.20 1.00 9 0 -1 431.70 6.80 9 0 -2 62.00 2.40 9 0 -3 138.90 4.00 9 0 -4 34.10 3.90 9 0 -5 153.30 6.80 9 0 -6 172.90 7.30 9 -1 5 6.60 1.60 9 -1 4 97.50 3.80 9 -1 3 4.40 1.40 9 -1 2 99.90 3.60 9 -1 1 2.50 1.30 9 -1 0 5.80 1.10 9 -1 -1 7.90 1.20 9 -1 -2 182.20 3.90 9 -1 -3 2.50 1.30 9 -1 -4 55.00 2.80 9 -1 -5 13.60 2.90 9 -1 -6 60.80 4.90 9 -2 5 34.40 2.60 9 -2 4 102.50 3.70 9 -2 3 347.40 7.50 9 -2 2 34.10 2.40 9 -2 1 317.90 6.90 9 -2 0 497.20 9.30 9 -2 -1 559.00 10.30 9 -2 -2 10.50 1.50 9 -2 -3 939.60 21.30 9 -2 -4 231.40 7.30 9 -2 -5 119.80 3.90 9 -2 -6 32.40 3.80 9 -3 5 56.70 3.00 9 -3 4 6.50 1.60 9 -3 3 35.80 2.60 9 -3 2 14.30 1.80 9 -3 1 6.50 1.50 9 -3 0 78.80 3.20 9 -3 -1 262.50 6.00 9 -3 -2 7.50 1.50 9 -3 -3 15.50 2.40 9 -3 -4 2.40 1.70 9 -3 -5 102.40 4.80 9 -3 -6 62.90 2.90 9 -4 5 302.60 7.50 9 -4 4 1.00 1.30 9 -4 3 44.80 2.60 9 -4 2 150.10 4.50 9 -4 1 277.20 6.30 9 -4 0 65.80 3.10 9 -4 -1 233.30 5.70 9 -4 -2 100.50 3.70 9 -4 -3 161.00 6.00 9 -4 -4 44.00 3.70 9 -4 -5 236.90 7.90 9 -4 -6 31.90 3.40 9 -5 4 -1.80 2.80 9 -5 3 115.80 4.90 9 -5 2 99.20 3.70 9 -5 1 87.40 3.50 9 -5 0 72.30 3.20 9 -5 -1 77.90 3.30 9 -5 -2 0.20 1.30 9 -5 -3 135.30 5.50 9 -5 -4 1.80 1.70 9 -5 -5 80.60 4.60 9 -6 3 238.60 10.10 9 -6 2 64.30 5.50 9 -6 1 25.20 2.20 9 -6 0 15.60 1.90 9 -6 -1 440.60 8.90 9 -6 -2 29.90 2.30 9 -6 -3 12.70 2.30 9 -6 -4 81.90 4.70 9 -7 1 80.50 6.00 9 -7 0 169.90 4.90 9 -7 -1 71.40 3.30 9 -7 -2 76.30 3.50 8 5 0 3.20 2.50 8 5 -1 -1.00 1.40 8 5 -2 90.90 3.90 8 4 3 285.80 10.80 8 4 2 34.80 4.20 8 4 1 6.00 2.90 8 4 0 60.20 3.10 8 4 -1 401.00 8.70 8 4 -2 35.30 2.70 8 4 -3 49.80 4.60 8 4 -4 3.50 2.50 8 3 4 4.50 1.50 8 3 3 9.10 1.60 8 3 2 8.50 1.60 8 3 1 60.90 2.90 8 3 0 58.10 3.00 8 3 -1 45.00 2.70 8 3 -2 60.80 3.10 8 3 -3 3.10 2.10 8 3 -4 -0.10 2.10 8 3 -5 2.20 2.20 8 2 5 79.70 3.50 8 2 4 25.60 2.20 8 2 3 417.50 8.40 8 2 2 54.60 2.80 8 2 1 439.80 8.50 8 2 0 305.40 5.30 8 2 -1 568.80 8.30 8 2 -2 39.20 2.70 8 2 -3 792.00 19.70 8 2 -4 486.20 13.80 8 2 -5 48.50 4.50 8 2 -6 2.50 2.40 8 1 5 1.30 1.30 8 1 4 75.60 3.20 8 1 3 2.90 1.20 8 1 2 7.50 1.50 8 1 1 14.20 1.70 8 1 0 1.60 0.90 8 1 -1 1.40 0.90 8 1 -2 40.90 1.90 8 1 -3 4.00 2.10 8 1 -4 3.10 2.10 8 1 -5 112.50 5.80 8 1 -6 68.50 5.10 8 1 -7 11.20 2.90 8 0 6 283.80 9.20 8 0 5 651.70 11.80 8 0 4 0.00 1.20 8 0 3 137.50 4.10 8 0 2 124.40 3.70 8 0 1 460.30 6.90 8 0 0 123.30 3.00 8 0 -1 297.80 5.10 8 0 -2 97.60 2.70 8 0 -3 282.30 5.90 8 0 -4 69.30 4.50 8 0 -5 533.00 14.30 8 0 -6 27.20 3.40 8 0 -7 8.80 2.50 8 -1 6 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131.70 3.80 7 -4 6 1.50 1.80 7 -4 5 21.20 2.20 7 -4 4 162.10 7.10 7 -4 3 399.30 7.60 7 -4 2 8.40 1.00 7 -4 1 3.40 0.80 7 -4 0 140.60 2.90 7 -4 -1 1066.80 13.60 7 -4 -2 20.10 1.30 7 -4 -3 131.70 3.10 7 -4 -4 60.70 2.40 7 -4 -5 355.30 6.90 7 -4 -6 1.10 1.20 7 -4 -7 162.10 4.40 7 -5 6 18.20 2.90 7 -5 5 60.60 3.20 7 -5 4 255.90 9.20 7 -5 3 2.40 1.90 7 -5 2 1.80 1.00 7 -5 1 1.30 1.00 7 -5 0 342.30 5.40 7 -5 -1 64.60 2.10 7 -5 -2 71.00 2.20 7 -5 -3 77.60 3.30 7 -5 -4 173.80 4.20 7 -5 -5 471.00 8.50 7 -5 -6 277.40 6.00 7 -5 -7 22.90 2.10 7 -6 5 65.60 5.00 7 -6 4 114.00 6.10 7 -6 3 169.10 7.30 7 -6 2 1.80 1.70 7 -6 1 73.70 4.60 7 -6 0 157.60 4.10 7 -6 -1 57.50 2.50 7 -6 -2 85.90 3.10 7 -6 -3 55.10 3.40 7 -6 -4 250.40 7.60 7 -6 -5 9.40 1.50 7 -6 -6 26.90 2.10 7 -7 5 62.20 5.20 7 -7 4 12.50 2.80 7 -7 3 2.20 1.90 7 -7 2 11.70 2.60 7 -7 1 120.00 6.10 7 -7 0 10.60 2.60 7 -7 -1 21.20 1.80 7 -7 -2 10.50 1.40 7 -7 -3 111.40 4.80 7 -7 -4 19.30 2.50 7 -7 -5 92.60 4.70 7 -8 3 111.60 6.40 7 -8 2 535.40 15.80 7 -8 1 273.10 9.90 7 -8 0 6.60 1.60 7 -8 -1 295.90 6.90 7 -8 -2 619.90 11.00 7 -8 -3 55.70 3.70 7 -8 -4 101.90 5.60 7 -9 2 159.60 7.50 7 -9 1 19.90 3.40 7 -9 0 3.20 2.00 7 -9 -1 81.70 5.10 6 7 0 122.50 5.70 6 7 -1 21.30 3.00 6 6 3 270.00 10.00 6 6 2 13.40 2.80 6 6 1 91.60 5.70 6 6 0 1.80 1.30 6 6 -1 986.10 16.90 6 6 -2 1.40 1.40 6 6 -3 7.00 2.40 6 6 -4 0.30 2.20 6 5 5 27.60 2.30 6 5 4 16.60 1.90 6 5 3 7.10 2.50 6 5 2 30.50 4.00 6 5 1 83.60 5.30 6 5 0 27.20 2.20 6 5 -1 10.30 1.60 6 5 -2 0.20 1.20 6 5 -3 19.70 2.00 6 5 -4 53.00 4.40 6 5 -5 37.80 4.00 6 5 -6 8.70 2.90 6 4 5 21.80 2.00 6 4 4 9.10 1.50 6 4 3 283.90 6.20 6 4 2 0.60 1.00 6 4 1 242.90 4.70 6 4 0 49.00 2.50 6 4 -1 237.30 5.50 6 4 -2 7.20 1.50 6 4 -3 774.60 13.10 6 4 -4 290.30 9.50 6 4 -5 1.80 1.90 6 4 -6 53.60 4.40 6 4 -7 551.10 15.50 6 3 6 10.40 2.20 6 3 5 19.90 1.90 6 3 4 49.20 2.50 6 3 3 10.70 1.40 6 3 2 -0.70 0.90 6 3 1 9.80 1.00 6 3 0 135.50 2.90 6 3 -1 155.70 4.10 6 3 -2 228.80 5.30 6 3 -3 29.20 2.10 6 3 -4 8.70 2.10 6 3 -5 6.50 2.10 6 3 -6 5.40 2.20 6 3 -7 1.80 2.00 6 2 7 53.90 3.90 6 2 6 778.50 18.10 6 2 5 1119.80 17.90 6 2 4 3.10 1.10 6 2 3 0.90 0.70 6 2 2 802.20 13.10 6 2 1 2165.40 26.00 6 2 0 113.60 2.60 6 2 -1 428.10 6.20 6 2 -2 349.80 5.40 6 2 -3 504.00 9.20 6 2 -4 241.20 7.90 6 2 -5 675.50 16.80 6 2 -6 65.00 4.30 6 2 -7 30.50 3.40 6 1 7 12.80 2.40 6 1 6 2.50 1.60 6 1 5 22.20 1.80 6 1 4 58.30 1.80 6 1 3 0.20 0.60 6 1 2 25.80 1.30 6 1 1 5.60 0.80 6 1 0 89.70 2.20 6 1 -1 2.70 0.80 6 1 -2 3.70 0.70 6 1 -3 27.90 1.40 6 1 -4 35.10 3.20 6 1 -5 60.00 3.90 6 1 -6 102.60 5.10 6 1 -7 -3.50 1.70 6 0 7 18.10 2.40 6 0 6 0.60 1.40 6 0 5 141.20 3.90 6 0 4 520.90 9.10 6 0 3 730.30 9.60 6 0 2 308.00 4.60 6 0 1 175.80 3.20 6 0 0 215.40 3.60 6 0 -1 2487.00 29.30 6 0 -2 31.50 1.50 6 0 -3 322.50 4.90 6 0 -4 10.80 1.20 6 0 -5 983.30 15.60 6 0 -6 0.60 1.10 6 0 -7 340.80 7.00 6 0 -8 6.50 2.30 6 -1 8 49.70 2.80 6 -1 7 14.40 1.70 6 -1 6 26.00 1.90 6 -1 5 3.40 0.90 6 -1 4 133.70 2.50 6 -1 3 40.80 1.60 6 -1 2 5.80 0.80 6 -1 1 1.30 0.60 6 -1 0 458.70 6.30 6 -1 -1 157.40 3.60 6 -1 -2 160.10 3.70 6 -1 -3 12.70 1.00 6 -1 -4 226.20 4.50 6 -1 -5 265.60 4.40 6 -1 -6 75.30 2.90 6 -1 -7 2.00 1.50 6 -1 -8 -0.30 1.70 6 -2 8 196.10 9.00 6 -2 7 402.80 12.10 6 -2 6 60.00 2.50 6 -2 5 1.70 0.80 6 -2 4 396.80 5.20 6 -2 3 587.40 8.10 6 -2 2 171.10 3.10 6 -2 1 121.40 2.50 6 -2 0 18.60 1.10 6 -2 -1 160.70 2.40 6 -2 -2 4.60 0.60 6 -2 -3 885.00 11.20 6 -2 -4 83.40 2.50 6 -2 -5 34.20 1.90 6 -2 -6 36.30 2.10 6 -2 -7 178.80 6.40 6 -2 -8 150.30 6.20 6 -3 7 124.80 6.00 6 -3 6 134.20 5.90 6 -3 5 63.70 3.00 6 -3 4 8.30 0.90 6 -3 3 6.10 0.80 6 -3 2 15.20 1.00 6 -3 1 7.00 0.80 6 -3 0 181.20 3.20 6 -3 -1 6.70 0.80 6 -3 -2 13.00 0.80 6 -3 -3 195.80 2.90 6 -3 -4 79.90 2.10 6 -3 -5 31.20 1.90 6 -3 -6 2.20 1.10 6 -3 -7 7.70 1.40 6 -3 -8 18.90 2.90 6 -4 7 25.00 3.40 6 -4 6 756.00 19.00 6 -4 5 615.10 11.40 6 -4 4 13.80 2.50 6 -4 3 86.50 2.20 6 -4 2 1831.70 22.00 6 -4 1 1935.90 23.00 6 -4 0 87.80 2.10 6 -4 -1 633.20 8.40 6 -4 -2 953.80 10.40 6 -4 -3 873.80 9.60 6 -4 -4 316.80 4.90 6 -4 -5 749.70 10.10 6 -4 -6 260.30 5.50 6 -4 -7 11.20 1.60 6 -4 -8 236.30 5.80 6 -5 6 1.20 1.70 6 -5 5 3.50 1.30 6 -5 4 12.80 2.50 6 -5 3 195.70 7.20 6 -5 2 89.30 3.00 6 -5 1 127.00 2.70 6 -5 0 -0.30 0.60 6 -5 -1 168.40 3.20 6 -5 -2 426.10 6.30 6 -5 -3 80.70 1.90 6 -5 -4 7.90 1.20 6 -5 -5 106.00 3.20 6 -5 -6 27.30 2.00 6 -5 -7 337.50 6.80 6 -6 6 5.30 2.10 6 -6 5 36.70 3.90 6 -6 4 416.70 12.20 6 -6 3 81.90 4.70 6 -6 2 32.70 3.30 6 -6 1 55.90 3.90 6 -6 0 140.00 3.60 6 -6 -1 266.70 5.50 6 -6 -2 16.20 1.20 6 -6 -3 74.30 2.70 6 -6 -4 184.50 4.20 6 -6 -5 122.70 3.60 6 -6 -6 1.70 1.20 6 -6 -7 77.20 4.80 6 -7 5 -2.20 1.70 6 -7 4 212.40 8.20 6 -7 3 54.80 4.20 6 -7 2 76.70 4.70 6 -7 1 50.40 4.00 6 -7 0 336.10 10.20 6 -7 -1 1.70 0.80 6 -7 -2 1.50 0.80 6 -7 -3 3.70 1.20 6 -7 -4 254.20 5.40 6 -7 -5 91.20 3.10 6 -7 -6 66.60 4.20 6 -8 4 175.20 7.50 6 -8 3 125.20 6.30 6 -8 2 12.40 2.60 6 -8 1 420.60 8.80 6 -8 0 38.60 2.70 6 -8 -1 4.00 1.30 6 -8 -2 40.40 1.90 6 -8 -3 41.40 2.40 6 -8 -4 173.40 6.20 6 -8 -5 12.30 2.40 6 -9 3 3.50 2.10 6 -9 2 57.00 3.40 6 -9 1 86.00 3.80 6 -9 0 28.00 2.50 6 -9 -1 12.60 1.90 6 -9 -2 21.70 3.30 6 -9 -3 64.20 3.90 5 7 3 79.60 7.90 5 7 2 25.60 3.50 5 7 1 28.00 3.70 5 7 0 51.40 3.80 5 7 -1 111.30 5.40 5 7 -2 14.30 2.50 5 7 -3 14.80 2.80 5 6 5 619.90 16.80 5 6 4 23.60 2.20 5 6 3 1.90 1.30 5 6 2 696.00 18.60 5 6 1 495.40 9.40 5 6 0 4.80 1.30 5 6 -1 139.90 4.30 5 6 -2 211.40 7.40 5 6 -3 360.60 10.80 5 6 -4 86.90 5.10 5 6 -5 509.90 14.10 5 5 5 17.90 1.90 5 5 4 40.90 2.40 5 5 3 19.80 1.40 5 5 2 5.70 1.30 5 5 1 3.40 1.20 5 5 0 115.90 3.50 5 5 -1 24.50 1.90 5 5 -2 4.30 1.30 5 5 -3 31.60 2.30 5 5 -4 139.00 6.00 5 5 -5 7.10 2.30 5 5 -6 62.30 4.50 5 5 -7 14.80 2.80 5 4 6 9.10 2.10 5 4 5 36.70 2.30 5 4 4 230.40 5.30 5 4 3 330.80 6.60 5 4 2 12.20 1.30 5 4 1 2.00 0.70 5 4 0 116.90 3.40 5 4 -1 1723.30 25.70 5 4 -2 38.70 2.20 5 4 -3 7.10 1.20 5 4 -4 39.00 3.50 5 4 -5 1009.10 23.10 5 4 -6 1.30 1.90 5 4 -7 320.70 7.00 5 3 7 141.20 5.80 5 3 6 27.10 2.90 5 3 5 112.10 3.50 5 3 4 0.20 1.00 5 3 3 67.10 1.90 5 3 2 7.50 0.80 5 3 1 0.60 0.60 5 3 0 270.30 4.30 5 3 -1 58.90 2.40 5 3 -2 59.90 2.40 5 3 -3 62.90 2.50 5 3 -4 68.10 3.90 5 3 -5 13.80 2.40 5 3 -6 3.70 1.20 5 3 -7 13.30 1.70 5 3 -8 7.60 2.20 5 2 7 329.00 9.40 5 2 6 30.00 2.80 5 2 5 9.90 1.30 5 2 4 264.60 4.30 5 2 3 739.10 9.70 5 2 2 187.30 2.90 5 2 1 196.10 3.30 5 2 0 7.00 0.80 5 2 -1 319.60 4.80 5 2 -2 12.40 1.00 5 2 -3 677.60 11.10 5 2 -4 33.60 3.10 5 2 -5 19.90 1.70 5 2 -6 -0.40 1.00 5 2 -7 487.90 9.40 5 2 -8 98.50 4.80 5 1 8 79.90 4.50 5 1 7 27.10 2.70 5 1 6 165.60 5.60 5 1 5 7.10 0.90 5 1 4 101.90 2.30 5 1 3 62.20 1.70 5 1 2 127.00 2.00 5 1 1 110.60 2.30 5 1 0 36.50 1.40 5 1 -1 70.60 1.80 5 1 -2 41.40 1.40 5 1 -3 5.70 0.80 5 1 -4 352.50 9.50 5 1 -5 34.70 2.00 5 1 -6 51.00 2.30 5 1 -7 5.20 1.70 5 1 -8 10.70 2.10 5 1 -9 -0.10 1.80 5 0 8 133.70 4.10 5 0 7 31.30 2.20 5 0 6 974.50 15.70 5 0 5 509.70 6.20 5 0 4 186.50 2.80 5 0 3 87.80 1.70 5 0 2 3108.70 31.10 5 0 1 4743.10 46.70 5 0 0 503.70 6.60 5 0 -1 731.90 11.30 5 0 -2 1231.80 15.00 5 0 -3 2443.40 24.80 5 0 -4 444.50 6.10 5 0 -5 1247.30 18.90 5 0 -6 292.50 4.70 5 0 -7 36.00 2.10 5 0 -8 176.90 4.50 5 0 -9 619.00 17.50 5 -1 8 47.60 4.20 5 -1 7 2.00 1.10 5 -1 6 29.60 1.90 5 -1 5 0.60 0.70 5 -1 4 46.60 1.60 5 -1 3 52.20 1.30 5 -1 2 3.50 0.40 5 -1 1 58.50 1.50 5 -1 0 74.40 1.70 5 -1 -1 31.80 1.10 5 -1 -2 153.80 2.20 5 -1 -3 282.40 3.60 5 -1 -4 24.50 1.50 5 -1 -5 85.50 2.50 5 -1 -6 28.80 1.30 5 -1 -7 155.20 5.80 5 -1 -8 7.10 2.10 5 -1 -9 4.00 2.20 5 -2 8 443.30 13.30 5 -2 7 74.40 4.60 5 -2 6 2.30 0.90 5 -2 5 58.80 1.60 5 -2 4 944.50 10.50 5 -2 3 119.70 2.40 5 -2 2 414.10 5.80 5 -2 1 254.00 3.80 5 -2 0 2027.30 23.90 5 -2 -1 533.90 5.90 5 -2 -2 404.30 4.70 5 -2 -3 141.30 2.20 5 -2 -4 74.00 1.80 5 -2 -5 913.10 11.60 5 -2 -6 6.10 1.10 5 -2 -7 441.50 8.80 5 -2 -8 10.30 2.20 5 -3 8 24.20 3.40 5 -3 7 -1.60 1.50 5 -3 6 165.00 6.50 5 -3 5 -0.20 1.00 5 -3 4 799.50 10.50 5 -3 3 160.80 2.90 5 -3 2 149.10 2.70 5 -3 1 39.10 1.30 5 -3 0 422.60 5.80 5 -3 -1 28.20 0.90 5 -3 -2 15.20 0.80 5 -3 -3 8.80 0.70 5 -3 -4 424.50 5.90 5 -3 -5 195.20 3.40 5 -3 -6 174.20 2.90 5 -3 -7 2.10 1.20 5 -3 -8 133.50 5.70 5 -4 7 95.30 5.30 5 -4 6 34.40 3.30 5 -4 5 159.80 4.30 5 -4 4 572.80 10.10 5 -4 3 459.90 8.30 5 -4 2 172.80 3.00 5 -4 1 692.50 8.90 5 -4 0 239.00 3.80 5 -4 -1 180.00 2.60 5 -4 -2 170.50 2.60 5 -4 -3 538.70 6.30 5 -4 -4 2.10 0.70 5 -4 -5 8.00 1.00 5 -4 -6 43.60 2.20 5 -4 -7 215.00 4.90 5 -4 -8 31.00 2.20 5 -5 7 66.90 4.60 5 -5 6 8.60 2.10 5 -5 5 23.70 2.00 5 -5 4 38.60 3.20 5 -5 3 68.60 2.50 5 -5 2 225.60 7.10 5 -5 1 36.40 1.40 5 -5 0 138.10 2.70 5 -5 -1 311.00 4.80 5 -5 -2 127.50 2.00 5 -5 -3 87.00 1.80 5 -5 -4 43.10 1.70 5 -5 -5 82.20 2.70 5 -5 -6 22.30 1.80 5 -5 -7 69.80 2.90 5 -5 -8 11.90 2.40 5 -6 6 421.60 12.70 5 -6 5 104.10 3.60 5 -6 4 -0.30 1.20 5 -6 3 11.10 2.10 5 -6 2 1557.30 34.10 5 -6 1 449.20 8.30 5 -6 0 30.90 1.40 5 -6 -1 444.80 5.60 5 -6 -2 1306.60 12.60 5 -6 -3 220.40 3.80 5 -6 -4 77.20 2.60 5 -6 -5 635.80 10.60 5 -6 -6 287.10 6.00 5 -6 -7 12.20 1.70 5 -7 6 4.30 2.00 5 -7 5 61.80 2.90 5 -7 4 229.50 8.10 5 -7 3 55.80 4.00 5 -7 2 160.40 6.40 5 -7 1 26.20 3.00 5 -7 0 18.90 1.80 5 -7 -1 114.60 2.70 5 -7 -2 240.20 4.30 5 -7 -3 56.30 1.90 5 -7 -4 2.20 1.00 5 -7 -5 3.80 1.20 5 -7 -6 109.50 3.60 5 -8 5 16.20 1.90 5 -8 4 457.80 13.40 5 -8 3 91.60 5.10 5 -8 2 6.90 2.10 5 -8 1 52.50 2.90 5 -8 0 125.50 4.10 5 -8 -1 294.60 6.60 5 -8 -2 142.80 3.30 5 -8 -3 141.30 4.00 5 -8 -4 79.60 2.90 5 -8 -5 31.90 2.20 5 -9 4 49.80 4.20 5 -9 3 1.10 1.30 5 -9 2 82.90 3.60 5 -9 1 65.10 3.30 5 -9 0 235.50 6.10 5 -9 -1 7.60 1.60 5 -9 -2 11.60 1.70 5 -9 -3 110.10 3.70 5 -9 -4 238.60 9.00 5 -10 1 201.70 10.40 5 -10 0 92.40 5.70 5 -10 -1 3.10 2.20 5 -10 -2 30.10 3.70 4 8 2 26.20 4.00 4 8 1 8.00 2.20 4 8 0 97.60 5.00 4 8 -1 326.80 10.10 4 8 -2 4.10 2.00 4 7 4 2.30 2.00 4 7 3 24.90 2.90 4 7 2 12.40 2.20 4 7 1 213.00 7.00 4 7 0 -0.30 1.40 4 7 -1 10.00 2.20 4 7 -2 1.40 1.80 4 7 -3 123.10 5.60 4 7 -4 31.10 3.50 4 7 -5 5.80 2.30 4 6 5 86.50 2.80 4 6 4 15.80 1.80 4 6 3 380.90 7.70 4 6 2 15.50 1.70 4 6 1 108.80 2.70 4 6 0 22.60 1.80 4 6 -1 96.50 3.30 4 6 -2 56.10 3.70 4 6 -3 105.30 4.90 4 6 -4 35.00 3.50 4 6 -5 10.50 2.50 4 6 -6 6.20 1.50 4 5 6 54.20 3.70 4 5 5 100.70 3.30 4 5 4 122.60 3.60 4 5 3 182.70 3.50 4 5 2 11.60 1.10 4 5 1 0.80 0.70 4 5 0 51.50 1.90 4 5 -1 146.20 3.80 4 5 -2 28.20 2.00 4 5 -3 -1.50 1.40 4 5 -4 65.00 4.00 4 5 -5 162.30 4.30 4 5 -6 36.10 2.40 4 5 -7 8.60 1.70 4 4 7 14.00 2.50 4 4 6 390.10 10.60 4 4 5 624.60 10.70 4 4 4 46.30 2.20 4 4 3 11.50 1.00 4 4 2 1867.20 19.20 4 4 1 1785.10 18.30 4 4 0 2.30 0.70 4 4 -1 745.70 12.10 4 4 -2 1125.50 17.30 4 4 -3 1211.80 18.40 4 4 -4 177.80 4.20 4 4 -5 892.30 14.20 4 4 -6 68.80 2.80 4 4 -7 221.10 7.30 4 4 -8 184.50 7.00 4 3 7 7.60 1.90 4 3 6 192.40 6.50 4 3 5 7.20 1.20 4 3 4 168.90 3.10 4 3 3 148.30 2.80 4 3 2 290.50 3.70 4 3 1 17.30 1.00 4 3 0 225.70 3.00 4 3 -1 -0.10 0.80 4 3 -2 9.60 1.10 4 3 -3 229.30 4.70 4 3 -4 38.00 1.90 4 3 -5 18.50 1.50 4 3 -6 22.00 1.80 4 3 -7 5.80 1.70 4 3 -8 82.20 4.40 4 2 8 477.90 12.50 4 2 7 122.20 5.00 4 2 6 3.90 1.50 4 2 5 52.10 1.70 4 2 4 1117.70 13.60 4 2 3 84.80 1.90 4 2 2 289.90 3.60 4 2 1 157.50 2.30 4 2 0 1709.40 20.00 4 2 -1 835.50 10.30 4 2 -2 705.20 11.00 4 2 -3 53.00 2.00 4 2 -4 236.40 4.80 4 2 -5 1090.90 16.60 4 2 -6 80.90 2.70 4 2 -7 336.20 9.20 4 2 -8 8.00 2.00 4 2 -9 155.20 6.30 4 1 8 42.70 2.60 4 1 7 26.30 1.90 4 1 6 42.40 2.10 4 1 5 72.20 1.60 4 1 4 77.20 1.60 4 1 3 122.10 2.00 4 1 2 66.70 1.10 4 1 1 15.40 0.70 4 1 0 710.20 8.90 4 1 -1 101.80 2.00 4 1 -2 0.20 0.50 4 1 -3 2.00 0.60 4 1 -4 587.60 7.80 4 1 -5 61.50 1.80 4 1 -6 20.70 1.30 4 1 -7 139.30 3.70 4 1 -8 15.70 1.70 4 1 -9 96.20 3.50 4 0 9 -0.70 1.30 4 0 8 211.00 5.20 4 0 7 402.40 7.80 4 0 6 164.10 3.10 4 0 5 207.60 3.00 4 0 4 926.40 10.00 4 0 3 460.60 5.30 4 0 2 178.80 2.40 4 0 1 1019.80 10.50 4 0 0 735.60 9.00 4 0 -1 563.20 8.90 4 0 -2 319.60 4.30 4 0 -3 1744.50 15.80 4 0 -4 382.20 4.10 4 0 -5 132.20 2.20 4 0 -6 36.40 1.60 4 0 -7 483.80 8.40 4 0 -8 1.00 1.00 4 0 -9 1.20 1.90 4 -1 8 32.20 3.60 4 -1 7 25.80 1.80 4 -1 6 45.60 1.60 4 -1 5 1.00 0.50 4 -1 4 77.70 1.50 4 -1 3 32.00 1.10 4 -1 2 468.60 5.30 4 -1 1 3.90 0.30 4 -1 0 405.80 5.30 4 -1 -1 161.00 2.10 4 -1 -2 92.20 1.50 4 -1 -3 83.10 1.50 4 -1 -4 267.50 3.30 4 -1 -5 93.00 1.70 4 -1 -6 0.60 0.60 4 -1 -7 12.10 2.00 4 -1 -8 120.20 5.20 4 -1 -9 3.80 1.90 4 -2 8 118.20 6.00 4 -2 7 100.30 5.10 4 -2 6 1112.80 25.10 4 -2 5 122.20 2.60 4 -2 4 68.00 1.40 4 -2 3 50.80 1.10 4 -2 2 2796.40 32.40 4 -2 1 1140.50 13.60 4 -2 0 195.60 3.00 4 -2 -1 313.00 3.60 4 -2 -2 5170.80 50.70 4 -2 -3 1996.10 20.20 4 -2 -4 1099.60 11.50 4 -2 -5 885.40 9.60 4 -2 -6 550.40 6.50 4 -2 -7 63.80 2.00 4 -2 -8 154.70 4.20 4 -2 -9 735.40 18.30 4 -3 8 25.20 3.30 4 -3 7 48.10 2.50 4 -3 6 52.40 2.30 4 -3 5 24.80 1.10 4 -3 4 340.10 5.00 4 -3 3 65.00 1.30 4 -3 2 164.10 2.70 4 -3 1 62.40 1.50 4 -3 0 5.80 0.60 4 -3 -1 189.90 2.50 4 -3 -2 343.80 3.50 4 -3 -3 17.70 0.70 4 -3 -4 96.80 1.80 4 -3 -5 11.90 0.80 4 -3 -6 85.30 1.90 4 -3 -7 221.00 3.90 4 -3 -8 1.40 1.00 4 -3 -9 1.40 1.30 4 -4 8 518.70 9.90 4 -4 7 241.40 5.70 4 -4 6 198.60 4.70 4 -4 5 0.90 0.70 4 -4 4 1735.00 26.10 4 -4 3 396.00 7.10 4 -4 2 128.20 2.40 4 -4 1 2.40 0.50 4 -4 0 1186.00 12.20 4 -4 -1 359.90 4.30 4 -4 -2 796.90 7.80 4 -4 -3 28.40 1.00 4 -4 -4 378.20 4.70 4 -4 -5 378.70 4.80 4 -4 -6 317.90 5.00 4 -4 -7 137.90 3.00 4 -4 -8 24.50 1.50 4 -5 7 0.40 1.40 4 -5 6 60.20 3.90 4 -5 5 2.80 1.00 4 -5 4 224.00 4.90 4 -5 3 166.70 4.00 4 -5 2 654.50 11.00 4 -5 1 74.70 1.80 4 -5 0 1014.60 10.70 4 -5 -1 56.40 1.30 4 -5 -2 0.10 0.40 4 -5 -3 276.60 3.30 4 -5 -4 289.20 4.60 4 -5 -5 87.10 2.70 4 -5 -6 113.80 3.40 4 -5 -7 31.60 2.20 4 -5 -8 254.70 5.80 4 -6 7 1.70 1.70 4 -6 6 2.60 1.50 4 -6 5 147.50 4.20 4 -6 4 491.20 12.90 4 -6 3 1.70 1.30 4 -6 2 375.60 7.10 4 -6 1 496.90 8.80 4 -6 0 281.60 4.60 4 -6 -1 34.70 1.10 4 -6 -2 400.00 4.50 4 -6 -3 317.80 3.90 4 -6 -4 64.40 2.40 4 -6 -5 110.90 3.30 4 -6 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3 7 1 6.90 1.20 3 7 0 124.40 3.40 3 7 -1 43.20 3.40 3 7 -2 37.40 3.40 3 7 -3 17.40 2.60 3 7 -4 247.90 8.30 3 7 -5 0.10 1.20 3 7 -6 5.40 1.40 3 6 6 40.00 2.60 3 6 5 7.10 1.40 3 6 4 520.60 9.40 3 6 3 106.90 3.40 3 6 2 62.50 2.00 3 6 1 6.20 0.90 3 6 0 223.50 4.60 3 6 -1 497.80 8.50 3 6 -2 152.60 5.60 3 6 -3 27.50 2.80 3 6 -4 397.40 7.50 3 6 -5 275.60 6.00 3 6 -6 42.70 2.00 3 6 -7 104.80 5.30 3 5 7 78.40 4.40 3 5 6 11.00 2.10 3 5 5 41.20 2.30 3 5 4 2.60 1.00 3 5 3 289.00 4.70 3 5 2 42.90 1.20 3 5 1 272.70 4.40 3 5 0 41.50 1.50 3 5 -1 9.10 0.80 3 5 -2 43.50 2.90 3 5 -3 146.40 3.60 3 5 -4 94.00 2.90 3 5 -5 -0.30 0.70 3 5 -6 5.80 1.00 3 5 -7 119.30 3.70 3 4 7 144.50 5.60 3 4 6 14.70 2.20 3 4 5 217.40 4.80 3 4 4 242.20 4.00 3 4 3 678.50 9.00 3 4 2 251.40 3.30 3 4 1 817.40 8.90 3 4 0 34.60 1.30 3 4 -1 519.90 6.90 3 4 -2 135.30 3.30 3 4 -3 595.50 9.60 3 4 -4 3.70 0.70 3 4 -5 1.60 0.70 3 4 -6 7.00 1.00 3 4 -7 398.10 7.70 3 4 -8 16.20 1.70 3 3 8 124.10 5.30 3 3 7 9.40 1.90 3 3 6 237.10 7.10 3 3 5 16.10 1.10 3 3 4 757.70 9.70 3 3 3 0.40 0.50 3 3 2 116.50 1.90 3 3 1 42.90 1.00 3 3 0 84.60 1.50 3 3 -1 341.70 4.70 3 3 -2 6.00 0.60 3 3 -3 6.30 0.70 3 3 -4 299.50 4.50 3 3 -5 11.00 1.00 3 3 -6 6.60 0.90 3 3 -7 1.00 1.00 3 3 -8 112.90 3.60 3 3 -9 1.90 2.00 3 2 8 95.60 3.40 3 2 7 106.40 3.30 3 2 6 804.80 13.00 3 2 5 277.90 3.80 3 2 4 54.20 1.30 3 2 3 26.00 0.90 3 2 2 2589.90 26.10 3 2 1 1094.00 11.20 3 2 0 91.80 1.70 3 2 -1 454.50 5.00 3 2 -2 4846.00 47.50 3 2 -3 1933.40 22.70 3 2 -4 568.60 7.40 3 2 -5 1227.60 14.90 3 2 -6 571.40 7.80 3 2 -7 204.40 4.70 3 2 -8 247.50 5.50 3 2 -9 710.70 17.20 3 1 9 0.10 1.20 3 1 8 51.60 2.60 3 1 7 1.10 1.00 3 1 6 23.80 1.30 3 1 5 0.20 0.50 3 1 4 113.20 1.90 3 1 3 43.20 1.10 3 1 2 408.50 4.10 3 1 1 10.80 0.50 3 1 0 980.90 11.60 3 1 -1 455.90 5.70 3 1 -2 16.00 0.70 3 1 -3 4.20 0.50 3 1 -4 39.50 1.30 3 1 -5 22.10 1.00 3 1 -6 111.50 2.20 3 1 -7 118.80 2.70 3 1 -8 45.70 2.40 3 1 -9 7.90 1.50 3 0 9 19.10 2.00 3 0 8 760.20 12.90 3 0 7 249.40 5.30 3 0 6 150.30 2.90 3 0 5 61.50 1.50 3 0 4 2725.10 27.50 3 0 3 1724.90 17.60 3 0 2 672.50 7.20 3 0 1 110.50 1.80 3 0 0 3367.40 38.90 3 0 -1 3.10 0.60 3 0 -2 1088.00 10.90 3 0 -3 2.30 0.30 3 0 -4 704.40 6.80 3 0 -5 983.90 9.30 3 0 -6 936.80 11.80 3 0 -7 197.60 4.40 3 0 -8 2.00 1.10 3 0 -9 299.80 9.30 3 -1 9 10.00 2.60 3 -1 8 -0.80 1.50 3 -1 7 11.90 1.30 3 -1 6 0.30 0.60 3 -1 5 8.80 0.60 3 -1 4 143.80 2.10 3 -1 3 26.70 0.80 3 -1 2 384.80 4.90 3 -1 1 40.70 1.00 3 -1 0 1057.20 12.50 3 -1 -1 49.80 0.90 3 -1 -2 12.00 0.60 3 -1 -3 227.40 2.50 3 -1 -4 612.90 6.00 3 -1 -5 1.00 0.40 3 -1 -6 94.30 1.60 3 -1 -7 13.70 1.00 3 -1 -8 200.80 4.80 3 -1 -9 62.40 4.10 3 -2 9 2.00 2.00 3 -2 8 322.60 7.00 3 -2 7 30.00 2.10 3 -2 6 282.80 4.50 3 -2 5 5.40 0.50 3 -2 4 1219.20 11.40 3 -2 3 209.00 2.40 3 -2 2 1363.80 13.80 3 -2 1 3049.80 34.80 3 -2 0 2447.50 28.30 3 -2 -1 91.20 1.40 3 -2 -2 700.50 6.50 3 -2 -3 1728.50 15.60 3 -2 -4 3.40 0.40 3 -2 -5 18.30 0.80 3 -2 -6 413.10 5.10 3 -2 -7 361.00 5.50 3 -2 -8 75.10 2.90 3 -2 -9 40.80 2.50 3 -3 9 -0.70 1.60 3 -3 8 75.30 3.20 3 -3 7 13.00 1.60 3 -3 6 19.40 1.60 3 -3 5 35.10 1.20 3 -3 4 16.40 0.70 3 -3 3 447.20 5.10 3 -3 2 4.00 0.40 3 -3 1 71.60 1.40 3 -3 0 1.20 0.30 3 -3 -1 36.80 0.90 3 -3 -2 1178.30 10.00 3 -3 -3 1.60 0.30 3 -3 -4 49.00 1.20 3 -3 -5 136.70 2.30 3 -3 -6 56.70 1.60 3 -3 -7 0.70 0.80 3 -3 -8 33.50 1.70 3 -3 -9 13.10 1.70 3 -4 9 41.30 3.70 3 -4 8 112.80 3.80 3 -4 7 9.00 1.40 3 -4 6 533.10 9.50 3 -4 5 91.30 1.90 3 -4 4 38.40 1.40 3 -4 3 28.10 1.10 3 -4 2 1428.20 16.90 3 -4 1 236.20 2.90 3 -4 0 199.40 2.60 3 -4 -1 40.50 1.00 3 -4 -2 1804.20 15.00 3 -4 -3 455.40 4.30 3 -4 -4 497.00 5.80 3 -4 -5 245.70 3.50 3 -4 -6 689.50 9.10 3 -4 -7 165.20 3.30 3 -4 -8 316.20 5.30 3 -4 -9 255.80 9.40 3 -5 8 1.80 1.50 3 -5 7 14.40 1.80 3 -5 6 37.70 3.10 3 -5 5 15.00 1.40 3 -5 4 42.70 1.90 3 -5 3 6.90 0.90 3 -5 2 2.60 0.70 3 -5 1 213.10 3.30 3 -5 0 198.10 2.60 3 -5 -1 658.30 6.50 3 -5 -2 683.40 6.80 3 -5 -3 122.10 1.70 3 -5 -4 2.60 0.60 3 -5 -5 66.80 1.90 3 -5 -6 73.20 2.10 3 -5 -7 62.40 2.20 3 -5 -8 8.70 1.20 3 -6 7 204.30 7.90 3 -6 6 235.20 8.00 3 -6 5 112.00 3.80 3 -6 4 1749.40 37.00 3 -6 3 368.30 10.20 3 -6 2 190.90 4.20 3 -6 1 558.20 7.70 3 -6 0 1602.70 16.80 3 -6 -1 388.60 4.30 3 -6 -2 361.80 4.10 3 -6 -3 193.50 2.70 3 -6 -4 363.40 6.60 3 -6 -5 102.70 3.10 3 -6 -6 322.10 6.50 3 -6 -7 158.20 4.30 3 -7 7 0.90 1.50 3 -7 6 267.40 8.90 3 -7 5 38.40 3.10 3 -7 4 3.00 1.40 3 -7 3 6.00 1.10 3 -7 2 488.60 9.00 3 -7 1 6.70 0.90 3 -7 0 252.70 3.70 3 -7 -1 9.90 0.90 3 -7 -2 299.80 4.20 3 -7 -3 151.00 2.70 3 -7 -4 433.30 7.70 3 -7 -5 24.60 1.90 3 -7 -6 8.50 1.40 3 -8 6 29.80 2.40 3 -8 5 76.20 3.20 3 -8 4 4.10 1.20 3 -8 3 1.90 1.00 3 -8 2 82.30 3.20 3 -8 1 231.10 5.60 3 -8 0 57.80 2.80 3 -8 -1 9.30 1.10 3 -8 -2 511.00 7.70 3 -8 -3 54.00 1.80 3 -8 -4 33.30 2.20 3 -8 -5 65.10 2.80 3 -9 5 36.10 3.90 3 -9 4 103.90 4.00 3 -9 3 59.60 3.00 3 -9 2 46.80 2.80 3 -9 1 37.60 2.60 3 -9 0 231.90 5.90 3 -9 -1 107.70 3.20 3 -9 -2 150.10 3.60 3 -9 -3 2.60 1.00 3 -9 -4 45.90 2.50 3 -10 2 81.60 5.40 3 -10 1 22.40 3.40 3 -10 0 10.50 2.90 3 -10 -1 140.30 7.00 3 -10 -2 120.20 4.40 3 -10 -3 5.20 2.40 2 9 2 19.10 4.00 2 9 1 176.90 4.80 2 9 0 20.10 1.80 2 9 -1 26.50 3.30 2 8 4 85.40 5.00 2 8 3 194.30 7.30 2 8 2 64.90 2.80 2 8 1 286.20 6.10 2 8 0 9.70 1.40 2 8 -1 81.60 3.00 2 8 -2 13.10 2.40 2 8 -3 181.10 7.00 2 8 -4 11.00 2.40 2 8 -5 1.80 2.00 2 7 5 32.40 3.40 2 7 4 420.70 11.90 2 7 3 15.60 2.40 2 7 2 3.30 1.10 2 7 1 127.30 3.40 2 7 0 294.70 5.90 2 7 -1 85.60 2.80 2 7 -2 1.60 0.90 2 7 -3 1.30 1.50 2 7 -4 40.90 2.20 2 7 -5 98.10 3.30 2 7 -6 27.20 2.10 2 6 6 223.50 5.30 2 6 5 170.50 4.40 2 6 4 13.40 1.50 2 6 3 21.90 2.40 2 6 2 1335.60 16.40 2 6 1 440.70 7.60 2 6 0 1.90 0.80 2 6 -1 488.00 8.30 2 6 -2 962.60 14.80 2 6 -3 620.60 10.30 2 6 -4 14.90 1.40 2 6 -5 809.00 10.70 2 6 -6 381.80 6.10 2 6 -7 122.70 3.80 2 5 7 -0.20 1.50 2 5 6 24.40 2.60 2 5 5 20.40 2.20 2 5 4 8.60 1.20 2 5 3 62.50 1.50 2 5 2 839.50 8.20 2 5 1 12.20 0.90 2 5 0 378.20 6.50 2 5 -1 301.70 5.40 2 5 -2 210.90 3.40 2 5 -3 28.20 1.00 2 5 -4 220.30 3.70 2 5 -5 9.90 1.00 2 5 -6 3.30 0.80 2 5 -7 2.40 1.10 2 5 -8 122.00 3.90 2 4 8 483.70 12.60 2 4 7 166.50 6.00 2 4 6 207.90 6.50 2 4 5 0.10 1.20 2 4 4 1810.40 21.50 2 4 3 454.00 6.20 2 4 2 31.90 1.00 2 4 1 2.10 0.40 2 4 0 1354.40 16.40 2 4 -1 717.30 9.00 2 4 -2 1547.00 15.80 2 4 -3 1.50 0.40 2 4 -4 407.80 5.70 2 4 -5 418.60 6.00 2 4 -6 442.50 6.40 2 4 -7 126.20 3.60 2 4 -8 85.70 3.20 2 3 8 0.70 1.30 2 3 7 5.60 1.30 2 3 6 12.20 1.40 2 3 5 5.30 0.80 2 3 4 5.50 0.60 2 3 3 423.50 4.50 2 3 2 284.30 3.40 2 3 1 19.60 0.70 2 3 0 77.80 1.60 2 3 -1 24.30 0.90 2 3 -2 220.50 2.50 2 3 -3 53.50 1.10 2 3 -4 334.70 4.70 2 3 -5 120.20 2.40 2 3 -6 3.30 0.80 2 3 -7 26.60 1.80 2 3 -8 52.50 2.50 2 3 -9 22.80 2.00 2 2 9 0.70 1.20 2 2 8 355.40 7.30 2 2 7 38.70 2.20 2 2 6 338.60 5.10 2 2 5 2.00 0.60 2 2 4 947.40 10.10 2 2 3 446.60 5.00 2 2 2 1490.80 13.40 2 2 1 3188.40 31.30 2 2 0 1724.30 17.20 2 2 -1 42.10 1.00 2 2 -2 1260.60 11.50 2 2 -3 2125.80 21.30 2 2 -4 0.90 0.40 2 2 -5 12.10 0.90 2 2 -6 213.50 3.60 2 2 -7 496.50 7.10 2 2 -8 86.20 3.00 2 2 -9 38.10 2.40 2 1 9 18.50 1.80 2 1 8 2.20 1.10 2 1 7 2.80 1.00 2 1 6 151.50 2.90 2 1 5 12.30 0.90 2 1 4 57.40 1.20 2 1 3 0.40 0.30 2 1 2 439.30 4.80 2 1 1 3.50 0.30 2 1 0 247.00 3.20 2 1 -1 298.90 3.80 2 1 -2 32.80 0.80 2 1 -3 515.00 5.60 2 1 -4 68.00 1.30 2 1 -5 0.40 0.40 2 1 -6 7.50 0.80 2 1 -7 1.10 0.70 2 1 -8 114.90 2.80 2 1 -9 58.10 2.20 2 1 -10 2.00 2.60 2 0 9 13.20 2.70 2 0 8 223.40 5.10 2 0 7 0.60 0.90 2 0 6 1487.50 15.60 2 0 5 3.50 0.50 2 0 4 62.90 1.10 2 0 3 42.20 0.90 2 0 2 306.00 3.50 2 0 1 2361.60 27.20 2 0 0 851.70 9.90 2 0 -1 115.40 1.70 2 0 -2 2823.10 27.70 2 0 -3 796.30 6.20 2 0 -4 1340.10 10.30 2 0 -5 146.10 1.60 2 0 -6 1418.30 13.20 2 0 -7 288.90 3.60 2 0 -8 392.10 5.20 2 0 -9 533.10 9.80 2 0 -10 16.00 2.70 2 -1 9 58.30 3.10 2 -1 8 112.40 3.70 2 -1 7 1.30 0.70 2 -1 6 108.00 2.00 2 -1 5 9.40 0.70 2 -1 4 120.90 1.70 2 -1 3 7.00 0.40 2 -1 2 118.80 1.60 2 -1 1 86.90 1.40 2 -1 0 143.40 2.00 2 -1 -1 420.40 4.40 2 -1 -2 36.00 0.70 2 -1 -3 224.40 2.40 2 -1 -4 23.10 0.70 2 -1 -5 15.20 0.60 2 -1 -6 81.70 1.40 2 -1 -7 5.50 0.70 2 -1 -8 1.80 1.10 2 -1 -9 0.90 1.20 2 -2 9 27.20 2.40 2 -2 8 624.10 11.30 2 -2 7 214.50 3.90 2 -2 6 1080.80 13.50 2 -2 5 172.20 2.90 2 -2 4 6330.30 55.70 2 -2 3 1342.50 15.70 2 -2 2 7.80 0.40 2 -2 1 24.50 0.70 2 -2 0 9184.70 105.20 2 -2 -1 1175.10 11.70 2 -2 -2 336.60 3.30 2 -2 -3 899.60 7.60 2 -2 -4 1019.30 10.70 2 -2 -5 130.20 2.10 2 -2 -6 802.30 9.00 2 -2 -7 192.00 3.40 2 -2 -8 50.50 2.40 2 -2 -9 200.20 5.00 2 -3 9 0.60 1.30 2 -3 8 38.80 2.50 2 -3 7 1.10 0.90 2 -3 6 100.20 2.30 2 -3 5 41.80 1.20 2 -3 4 15.60 0.70 2 -3 3 10.00 0.70 2 -3 2 980.90 10.10 2 -3 1 553.20 8.20 2 -3 0 33.50 0.70 2 -3 -1 9.00 0.40 2 -3 -2 1100.90 9.30 2 -3 -3 178.10 1.90 2 -3 -4 482.10 5.60 2 -3 -5 90.30 1.80 2 -3 -6 35.30 1.30 2 -3 -7 264.90 4.40 2 -3 -8 205.20 3.90 2 -3 -9 28.90 2.20 2 -4 9 11.70 2.50 2 -4 8 225.10 5.60 2 -4 7 8.70 1.40 2 -4 6 116.50 3.30 2 -4 5 18.90 1.20 2 -4 4 140.80 2.30 2 -4 3 1.70 0.30 2 -4 2 1153.10 10.60 2 -4 1 354.40 4.80 2 -4 0 195.80 2.20 2 -4 -1 2.30 0.30 2 -4 -2 2123.30 17.50 2 -4 -3 766.20 6.70 2 -4 -4 23.00 0.90 2 -4 -5 68.90 1.60 2 -4 -6 491.80 6.90 2 -4 -7 76.90 2.30 2 -4 -8 36.10 1.80 2 -4 -9 50.20 4.50 2 -5 9 26.30 3.20 2 -5 8 68.80 3.10 2 -5 7 60.20 2.70 2 -5 6 43.20 2.20 2 -5 5 1.30 0.60 2 -5 4 236.10 3.40 2 -5 3 70.80 1.70 2 -5 2 74.40 1.40 2 -5 1 68.30 1.40 2 -5 0 39.00 0.80 2 -5 -1 199.40 2.20 2 -5 -2 682.50 6.70 2 -5 -3 93.70 1.60 2 -5 -4 127.50 2.00 2 -5 -5 1.80 0.70 2 -5 -6 639.30 8.60 2 -5 -7 4.10 1.00 2 -5 -8 1.60 1.00 2 -6 8 150.70 7.20 2 -6 7 147.60 6.30 2 -6 6 505.10 13.70 2 -6 5 112.50 4.80 2 -6 4 2.40 0.80 2 -6 3 82.50 2.50 2 -6 2 818.20 9.10 2 -6 1 4.00 0.60 2 -6 0 32.20 1.10 2 -6 -1 70.70 1.40 2 -6 -2 660.40 6.80 2 -6 -3 6.50 0.60 2 -6 -4 47.30 1.40 2 -6 -5 207.60 3.70 2 -6 -6 130.90 3.00 2 -6 -7 88.50 2.60 2 -6 -8 133.70 5.70 2 -7 7 40.70 3.50 2 -7 6 96.20 4.80 2 -7 5 95.10 3.20 2 -7 4 93.30 2.60 2 -7 3 12.80 1.20 2 -7 2 2.60 0.70 2 -7 1 68.30 1.70 2 -7 0 221.10 3.30 2 -7 -1 42.90 1.40 2 -7 -2 36.20 1.30 2 -7 -3 46.10 1.50 2 -7 -4 38.80 1.70 2 -7 -5 214.20 4.90 2 -7 -6 83.90 3.10 2 -8 5 22.60 2.90 2 -8 4 1218.20 19.80 2 -8 3 273.00 6.30 2 -8 2 2.90 1.10 2 -8 1 521.00 7.70 2 -8 0 986.50 13.00 2 -8 -1 265.10 4.80 2 -8 -2 52.20 2.00 2 -8 -3 392.80 5.40 2 -8 -4 591.20 8.60 2 -8 -5 3.10 1.20 2 -9 5 45.70 3.90 2 -9 4 36.80 2.50 2 -9 3 1.30 1.10 2 -9 2 408.30 8.70 2 -9 1 40.40 2.60 2 -9 0 134.40 3.40 2 -9 -1 16.60 1.40 2 -9 -2 252.50 4.90 2 -9 -3 2.90 1.00 2 -9 -4 372.60 6.30 2 -10 2 52.60 4.60 2 -10 1 134.50 6.70 2 -10 0 23.00 3.40 2 -10 -1 48.00 2.70 2 -10 -2 22.60 3.40 2 -10 -3 112.00 9.00 1 9 2 169.90 4.70 1 9 1 8.00 1.50 1 9 0 44.10 2.50 1 9 -1 21.50 2.00 1 9 -2 135.40 4.00 1 9 -3 30.50 3.60 1 8 4 332.10 10.40 1 8 3 147.90 6.10 1 8 2 6.60 1.30 1 8 1 12.70 1.60 1 8 0 400.50 7.50 1 8 -1 292.50 6.10 1 8 -2 270.90 5.80 1 8 -3 39.60 2.30 1 8 -4 157.10 6.30 1 8 -5 82.90 4.70 1 8 -6 76.50 6.80 1 7 6 69.60 4.50 1 7 5 -1.70 1.80 1 7 4 -3.00 1.50 1 7 3 142.30 5.50 1 7 2 30.20 1.90 1 7 1 86.10 2.80 1 7 0 29.00 1.80 1 7 -1 110.80 3.10 1 7 -2 19.80 1.60 1 7 -3 107.80 3.20 1 7 -4 0.30 0.90 1 7 -5 -0.40 0.90 1 7 -6 8.90 1.10 1 7 -7 50.80 3.70 1 6 7 12.00 1.70 1 6 6 3.40 1.30 1 6 5 113.30 3.40 1 6 4 191.30 4.30 1 6 3 96.60 1.90 1 6 2 531.10 7.20 1 6 1 299.40 5.60 1 6 0 285.70 5.40 1 6 -1 234.40 4.70 1 6 -2 763.30 9.70 1 6 -3 602.60 8.10 1 6 -4 4.80 0.70 1 6 -5 22.40 1.30 1 6 -6 5.90 1.00 1 6 -7 323.70 6.70 1 5 7 1.60 1.60 1 5 6 116.60 4.70 1 5 5 4.30 1.40 1 5 4 101.20 2.30 1 5 3 3.30 0.60 1 5 2 176.00 2.50 1 5 1 58.00 1.50 1 5 0 537.10 8.80 1 5 -1 164.30 3.40 1 5 -2 81.60 1.50 1 5 -3 265.90 3.40 1 5 -4 78.00 1.60 1 5 -5 77.00 2.00 1 5 -6 17.00 1.40 1 5 -7 1.80 1.00 1 5 -8 24.00 2.00 1 4 8 74.40 4.20 1 4 7 19.70 1.90 1 4 6 422.60 7.90 1 4 5 142.40 2.80 1 4 4 8.10 0.70 1 4 3 22.50 0.80 1 4 2 978.40 9.20 1 4 1 228.10 2.30 1 4 0 84.00 2.00 1 4 -1 36.90 0.90 1 4 -2 1199.60 12.40 1 4 -3 796.80 8.50 1 4 -4 533.60 6.00 1 4 -5 590.40 6.80 1 4 -6 320.70 6.20 1 4 -7 336.10 6.50 1 4 -8 280.40 6.00 1 3 9 1.90 1.40 1 3 8 449.70 8.60 1 3 7 8.80 1.30 1 3 6 34.20 2.00 1 3 5 21.90 1.20 1 3 4 157.80 2.40 1 3 3 14.40 0.60 1 3 2 269.10 2.90 1 3 1 128.30 1.40 1 3 0 69.60 1.40 1 3 -1 110.50 1.50 1 3 -2 1567.70 15.70 1 3 -3 7.10 0.50 1 3 -4 74.00 1.40 1 3 -5 0.00 0.40 1 3 -6 28.90 1.60 1 3 -7 62.50 2.40 1 3 -8 29.80 2.00 1 3 -9 -2.00 1.00 1 2 9 18.40 1.90 1 2 8 334.00 6.90 1 2 7 236.40 5.20 1 2 6 1261.30 15.50 1 2 5 124.70 2.40 1 2 4 6434.60 62.90 1 2 3 1003.00 10.40 1 2 2 73.00 1.00 1 2 1 27.60 0.70 1 2 0 9610.40 95.20 1 2 -1 1331.10 10.80 1 2 -2 392.70 4.20 1 2 -3 412.20 4.50 1 2 -4 1219.20 12.50 1 2 -5 305.50 3.80 1 2 -6 1096.20 13.60 1 2 -7 184.20 3.40 1 2 -8 45.80 1.80 1 2 -9 175.70 4.60 1 1 9 14.00 1.70 1 1 8 21.20 1.80 1 1 7 0.40 0.90 1 1 6 29.80 1.20 1 1 5 0.00 0.40 1 1 4 286.60 3.50 1 1 3 53.40 1.00 1 1 2 19.20 0.60 1 1 1 21.10 0.60 1 1 0 145.10 2.40 1 1 -1 332.40 4.10 1 1 -2 131.10 1.50 1 1 -3 26.60 0.70 1 1 -4 30.50 0.80 1 1 -5 18.10 0.70 1 1 -6 163.30 2.50 1 1 -7 0.10 0.60 1 1 -8 52.50 1.90 1 1 -9 18.50 1.70 1 1 -10 31.60 2.60 1 0 9 116.30 4.00 1 0 8 110.50 2.80 1 0 7 -0.50 0.60 1 0 6 306.80 4.00 1 0 5 63.70 1.40 1 0 4 1269.70 13.10 1 0 3 5.20 0.40 1 0 2 5407.20 47.60 1 0 1 84.40 1.50 1 0 0 261.60 5.30 1 0 -1 111.60 2.60 1 0 -2 3745.20 30.10 1 0 -3 5158.60 38.40 1 0 -4 41.60 0.70 1 0 -5 0.90 0.30 1 0 -6 1356.00 12.70 1 0 -7 176.40 2.80 1 0 -8 102.70 2.20 1 0 -9 28.60 1.40 1 -1 10 115.00 6.90 1 -1 9 12.00 1.80 1 -1 8 92.60 3.40 1 -1 7 37.60 1.60 1 -1 6 455.30 5.40 1 -1 5 0.10 0.40 1 -1 4 179.20 2.40 1 -1 3 6.10 0.30 1 -1 2 616.00 6.40 1 -1 1 105.40 2.00 1 -1 0 14.60 0.80 1 -1 -1 145.30 1.60 1 -1 -2 1714.50 17.10 1 -1 -3 4.50 0.30 1 -1 -4 4.70 0.30 1 -1 -5 50.60 1.00 1 -1 -6 386.60 3.80 1 -1 -7 6.50 0.60 1 -1 -8 -0.30 0.80 1 -1 -9 -0.60 1.10 1 -2 9 8.50 1.60 1 -2 8 238.20 5.70 1 -2 7 267.00 4.50 1 -2 6 1425.60 17.30 1 -2 5 7.10 0.70 1 -2 4 532.70 5.20 1 -2 3 565.20 6.10 1 -2 2 2764.90 31.70 1 -2 1 69.60 1.40 1 -2 0 162.40 2.10 1 -2 -1 55.80 0.70 1 -2 -2 303.90 3.10 1 -2 -3 479.30 4.70 1 -2 -4 354.10 3.70 1 -2 -5 164.20 1.90 1 -2 -6 562.00 5.90 1 -2 -7 45.70 1.70 1 -2 -8 190.20 4.60 1 -2 -9 184.40 4.70 1 -3 9 54.40 3.00 1 -3 8 5.80 1.30 1 -3 7 75.20 2.90 1 -3 6 260.10 4.20 1 -3 5 88.30 2.60 1 -3 4 115.40 1.70 1 -3 3 12.50 0.60 1 -3 2 502.90 5.40 1 -3 1 159.30 2.00 1 -3 0 7.80 0.30 1 -3 -1 50.40 0.80 1 -3 -2 3.60 0.30 1 -3 -3 336.50 3.50 1 -3 -4 312.70 3.50 1 -3 -5 144.00 2.30 1 -3 -6 2.70 0.70 1 -3 -7 3.80 0.90 1 -3 -8 31.70 1.70 1 -3 -9 20.90 1.90 1 -4 9 18.20 2.10 1 -4 8 299.10 6.70 1 -4 7 91.60 3.10 1 -4 6 707.50 11.80 1 -4 5 97.80 2.20 1 -4 4 4007.20 36.00 1 -4 3 381.60 4.40 1 -4 2 155.60 2.10 1 -4 1 968.00 10.00 1 -4 0 9350.50 81.60 1 -4 -1 689.10 6.60 1 -4 -2 480.80 4.80 1 -4 -3 482.70 4.90 1 -4 -4 2452.80 22.50 1 -4 -5 74.70 1.70 1 -4 -6 637.30 8.50 1 -4 -7 283.10 4.80 1 -4 -8 217.10 4.10 1 -4 -9 5.40 2.10 1 -5 9 1.20 1.90 1 -5 8 46.70 2.70 1 -5 7 16.40 1.60 1 -5 6 308.90 6.30 1 -5 5 3.40 0.70 1 -5 4 11.10 0.50 1 -5 3 148.40 2.00 1 -5 2 1075.10 10.20 1 -5 1 36.60 0.90 1 -5 0 161.20 2.00 1 -5 -1 1.60 0.40 1 -5 -2 965.80 9.30 1 -5 -3 100.00 1.60 1 -5 -4 456.60 4.90 1 -5 -5 -0.70 0.60 1 -5 -6 118.30 2.70 1 -5 -7 127.90 3.00 1 -5 -8 376.40 6.10 1 -6 8 224.40 5.70 1 -6 7 229.30 5.50 1 -6 6 35.90 2.00 1 -6 5 84.50 1.90 1 -6 4 73.30 1.40 1 -6 3 19.10 0.80 1 -6 2 252.60 3.20 1 -6 1 203.50 2.90 1 -6 0 74.70 1.50 1 -6 -1 18.80 0.80 1 -6 -2 544.10 5.70 1 -6 -3 83.40 1.60 1 -6 -4 -0.10 0.60 1 -6 -5 121.90 2.70 1 -6 -6 214.30 4.00 1 -6 -7 69.20 2.30 1 -7 5 124.60 5.30 1 -7 4 59.00 2.10 1 -7 3 52.00 1.60 1 -7 2 17.40 1.00 1 -7 1 5.10 0.80 1 -7 0 159.30 3.10 1 -7 -1 36.50 1.50 1 -7 -2 148.30 2.30 1 -7 -3 4.00 0.70 1 -7 -4 46.80 1.60 1 -7 -5 54.30 2.00 1 -7 -6 313.40 5.40 1 -7 -7 11.80 2.30 1 -8 5 3.30 1.70 1 -8 4 20.60 1.60 1 -8 3 100.70 3.50 1 -8 2 710.40 9.90 1 -8 1 3.40 0.80 1 -8 0 48.60 2.20 1 -8 -1 192.30 4.70 1 -8 -2 208.90 5.00 1 -8 -3 42.70 1.90 1 -8 -4 1.60 0.90 1 -8 -5 113.40 3.60 1 -9 4 49.10 2.30 1 -9 3 66.80 3.10 1 -9 2 2.30 1.20 1 -9 1 156.70 3.60 1 -9 0 264.60 5.00 1 -9 -1 37.70 2.00 1 -9 -2 23.40 2.10 1 -9 -3 17.60 1.90 1 -9 -4 50.80 2.80 1 -10 2 1.60 2.10 1 -10 1 106.90 6.10 1 -10 0 359.00 7.70 1 -10 -1 203.20 8.50 1 -10 -2 106.20 6.80 0 9 3 10.70 2.40 0 9 2 4.20 1.30 0 9 1 84.30 3.30 0 9 0 244.70 5.70 0 9 -1 47.90 2.60 0 9 -2 0.20 1.10 0 9 -3 6.70 1.30 0 9 -4 25.90 3.80 0 8 5 201.30 7.40 0 8 4 15.80 2.60 0 8 3 27.50 3.00 0 8 2 256.50 5.70 0 8 1 36.70 2.20 0 8 0 2.70 1.00 0 8 -1 40.90 2.20 0 8 -2 317.00 6.40 0 8 -3 250.00 5.50 0 8 -4 86.50 3.20 0 8 -5 310.00 9.70 0 7 6 81.00 3.10 0 7 5 9.90 1.50 0 7 4 293.60 8.80 0 7 3 7.20 1.20 0 7 2 271.80 4.40 0 7 1 33.80 1.90 0 7 0 18.60 1.50 0 7 -1 37.80 1.90 0 7 -2 398.70 7.30 0 7 -3 25.00 1.70 0 7 -4 102.50 3.10 0 7 -5 27.60 1.30 0 7 -6 52.50 2.40 0 7 -7 13.30 1.60 0 6 7 146.00 4.20 0 6 6 432.20 8.10 0 6 5 74.60 2.60 0 6 4 1260.30 16.20 0 6 3 476.00 5.70 0 6 2 319.40 4.70 0 6 1 457.80 7.90 0 6 0 2025.30 29.20 0 6 -1 451.70 7.70 0 6 -2 233.20 4.70 0 6 -3 11.80 0.80 0 6 -4 840.20 9.40 0 6 -5 184.70 3.00 0 6 -6 451.50 8.30 0 6 -7 172.50 4.50 0 5 8 15.30 2.50 0 5 7 12.70 2.10 0 5 6 21.20 1.90 0 5 5 0.70 0.70 0 5 4 306.50 4.00 0 5 3 80.60 1.40 0 5 2 35.70 0.90 0 5 1 15.30 0.70 0 5 0 11.00 0.70 0 5 -1 284.50 3.50 0 5 -2 5.50 0.50 0 5 -3 66.40 1.40 0 5 -4 55.40 1.30 0 5 -5 44.80 1.30 0 5 -6 130.20 2.80 0 5 -7 48.90 2.30 0 5 -8 0.00 1.00 0 4 9 51.90 4.60 0 4 8 104.50 3.60 0 4 7 0.90 1.00 0 4 6 123.50 3.50 0 4 5 28.20 1.40 0 4 4 188.60 3.20 0 4 3 60.00 1.30 0 4 2 1668.00 15.10 0 4 1 237.60 2.90 0 4 0 108.50 1.90 0 4 -1 73.50 1.20 0 4 -2 3531.70 35.30 0 4 -3 646.50 7.10 0 4 -4 2.90 0.50 0 4 -5 1.00 0.50 0 4 -6 699.00 9.20 0 4 -7 454.10 8.10 0 4 -8 148.90 4.10 0 4 -9 45.00 5.60 0 3 9 12.00 1.70 0 3 8 1.70 1.20 0 3 7 33.10 2.10 0 3 6 666.00 8.90 0 3 5 70.60 1.80 0 3 4 -0.20 0.50 0 3 3 3.30 0.50 0 3 2 1064.40 10.80 0 3 1 422.70 4.10 0 3 0 133.60 1.70 0 3 -1 97.90 1.40 0 3 -2 338.90 3.80 0 3 -3 331.40 3.80 0 3 -4 362.20 4.20 0 3 -5 94.20 1.70 0 3 -6 6.00 1.00 0 3 -7 77.00 2.50 0 3 -8 1.70 0.90 0 3 -9 5.20 1.30 0 2 9 37.10 2.60 0 2 8 114.40 3.60 0 2 7 265.90 5.60 0 2 6 871.00 11.10 0 2 5 3.20 0.60 0 2 4 586.70 7.50 0 2 3 739.80 7.70 0 2 2 2479.40 21.80 0 2 1 101.80 1.30 0 2 0 185.00 2.10 0 2 -1 73.10 1.00 0 2 -2 313.80 3.40 0 2 -3 338.20 3.80 0 2 -4 388.50 3.90 0 2 -5 119.30 2.30 0 2 -6 284.20 4.40 0 2 -7 169.50 3.20 0 2 -8 266.80 5.60 0 2 -9 299.80 6.30 0 1 10 9.20 2.50 0 1 9 23.50 1.70 0 1 8 181.50 4.50 0 1 7 24.50 1.40 0 1 6 216.70 3.10 0 1 5 53.10 1.30 0 1 4 440.90 5.00 0 1 3 115.30 1.60 0 1 2 1483.60 14.70 0 1 1 2.20 0.30 0 1 0 18.00 0.50 0 1 -2 1558.20 12.60 0 1 -3 336.10 3.00 0 1 -4 22.20 0.60 0 1 -5 47.30 1.20 0 1 -6 174.80 2.60 0 1 -7 11.70 0.80 0 1 -8 17.90 1.30 0 1 -9 6.20 1.00 0 1 -10 6.00 1.60 0 0 10 571.40 15.40 0 0 9 22.00 2.20 0 0 8 222.40 4.20 0 0 7 388.00 5.10 0 0 6 1041.10 11.20 0 0 5 336.20 4.10 0 0 4 4877.80 48.30 0 0 3 898.10 9.20 0 0 2 709.00 7.20 0 0 1 316.60 4.60 0 0 -1 313.10 6.50 0 0 -2 712.80 5.90 0 0 -3 894.20 7.50 0 0 -4 4912.40 39.40 0 0 -5 330.10 3.30 0 0 -6 1026.60 9.90 0 0 -7 388.40 4.90 0 0 -8 223.90 3.40 0 0 -9 21.30 1.50 0 -1 10 3.70 2.20 0 -1 9 3.80 1.50 0 -1 8 16.60 1.70 0 -1 7 8.90 1.00 0 -1 6 181.10 2.70 0 -1 5 48.10 1.10 0 -1 4 23.30 0.70 0 -1 3 333.30 4.40 0 -1 2 1564.30 22.10 0 -1 0 18.40 0.50 0 -1 -1 2.30 0.20 0 -1 -2 1474.30 13.20 0 -1 -3 115.20 1.30 0 -1 -4 441.40 4.00 0 -1 -5 53.60 1.00 0 -1 -6 215.50 2.50 0 -1 -7 25.40 1.10 0 -1 -8 189.20 4.50 0 -1 -9 16.90 2.50 0 -2 9 296.20 6.80 0 -2 8 267.20 6.10 0 -2 7 174.00 4.30 0 -2 6 293.60 4.60 0 -2 5 122.00 2.40 0 -2 4 385.30 5.30 0 -2 3 338.90 3.90 0 -2 2 312.20 4.00 0 -2 1 76.30 1.20 0 -2 0 186.90 2.10 0 -2 -1 101.10 1.20 0 -2 -2 2435.00 21.80 0 -2 -3 730.20 6.20 0 -2 -4 589.30 5.20 0 -2 -5 3.50 0.40 0 -2 -6 862.00 8.50 0 -2 -7 267.30 4.30 0 -2 -8 111.30 3.40 0 -2 -9 38.00 2.40 0 -3 9 4.70 1.40 0 -3 8 0.40 1.10 0 -3 7 66.30 2.70 0 -3 6 7.40 1.10 0 -3 5 92.80 2.10 0 -3 4 359.80 3.90 0 -3 3 329.60 3.50 0 -3 2 338.70 5.40 0 -3 1 100.40 1.40 0 -3 0 133.20 2.00 0 -3 -1 421.90 4.10 0 -3 -2 1048.40 9.70 0 -3 -3 1.90 0.40 0 -3 -4 2.00 0.50 0 -3 -5 71.50 1.60 0 -3 -6 659.50 7.60 0 -3 -7 38.70 1.60 0 -3 -8 2.20 0.90 0 -3 -9 13.60 1.70 0 -4 9 44.80 2.80 0 -4 8 155.30 4.40 0 -4 7 445.00 8.40 0 -4 6 696.20 9.40 0 -4 5 1.50 0.50 0 -4 4 3.70 0.40 0 -4 3 657.60 5.90 0 -4 2 3588.50 35.30 0 -4 1 76.50 1.30 0 -4 0 111.80 1.40 0 -4 -1 234.30 2.60 0 -4 -2 1669.50 15.20 0 -4 -3 59.00 1.20 0 -4 -4 186.00 2.50 0 -4 -5 27.40 1.10 0 -4 -6 120.10 2.60 0 -4 -7 0.20 0.80 0 -4 -8 106.00 2.80 0 -4 -9 52.80 4.00 0 -5 9 1.60 2.00 0 -5 8 0.00 1.10 0 -5 7 48.70 2.40 0 -5 6 130.40 3.60 0 -5 5 44.90 1.20 0 -5 4 52.20 0.90 0 -5 3 66.20 1.20 0 -5 2 5.30 0.50 0 -5 1 282.10 3.50 0 -5 0 13.00 0.60 0 -5 -1 16.80 0.70 0 -5 -2 34.40 1.00 0 -5 -3 75.60 1.50 0 -5 -4 305.10 3.70 0 -5 -5 0.70 0.60 0 -5 -6 24.40 1.40 0 -5 -7 15.80 1.30 0 -5 -8 14.10 1.40 0 -6 8 38.10 3.60 0 -6 7 170.10 6.40 0 -6 6 457.40 8.70 0 -6 5 190.40 3.00 0 -6 4 860.50 7.80 0 -6 3 11.40 0.90 0 -6 2 229.00 3.20 0 -6 1 452.40 5.40 0 -6 0 2005.40 20.60 0 -6 -1 466.00 4.90 0 -6 -2 322.00 3.70 0 -6 -3 478.90 5.20 0 -6 -4 1285.70 13.80 0 -6 -5 68.90 2.10 0 -6 -6 434.50 6.60 0 -6 -7 149.10 3.40 0 -7 7 18.20 2.60 0 -7 6 51.50 3.50 0 -7 5 29.40 2.00 0 -7 4 109.30 2.00 0 -7 3 23.90 1.40 0 -7 2 404.30 5.90 0 -7 1 37.40 1.50 0 -7 0 19.80 1.00 0 -7 -1 36.80 1.30 0 -7 -2 276.70 3.50 0 -7 -3 5.20 0.70 0 -7 -4 296.80 4.30 0 -7 -5 9.60 1.00 0 -7 -6 81.10 2.50 0 -8 5 336.80 10.40 0 -8 4 99.90 2.90 0 -8 3 249.90 4.60 0 -8 2 310.70 6.40 0 -8 1 39.20 2.20 0 -8 0 1.10 1.00 0 -8 -1 32.80 2.10 0 -8 -2 261.00 5.00 0 -8 -3 25.00 1.30 0 -8 -4 15.40 1.10 0 -8 -5 197.30 3.60 0 -9 5 69.70 4.80 0 -9 4 36.90 2.10 0 -9 3 6.90 1.20 0 -9 2 0.20 0.80 0 -9 1 43.80 2.40 0 -9 0 238.40 5.70 0 -9 -1 85.80 3.40 0 -9 -2 2.60 1.30 0 -9 -3 10.40 1.70 0 -9 -4 123.80 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