data_fleetite _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common 'fleetite' _chemical_melting_point ? _chemical_formula_moiety 'Cu32.96 Ir16 Rh13.62 Sb32' _chemical_formula_sum 'Cu32.96 Ir16 Rh13.62 Sb32' _chemical_formula_weight 10467.67 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ir' 'Ir' -1.4442 7.9887 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Rh' 'Rh' -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Sb' 'Sb' -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting 'cubic' _symmetry_space_group_name_H-M 'Fd-3m' loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y+1/4, -z+1/4' '-x+3/4, -y+1/4, z+1/2' '-x+3/4, y, -z+3/4' '-y, x+1/4, z+1/4' 'y+3/4, x+1/4, -z+1/2' 'y+3/4, -x, z+3/4' '-y, -x, -z' 'y, z, x' '-y+3/4, -z+1/4, x+1/2' 'y, -z+1/4, -x+1/4' '-y+3/4, z, -x+3/4' '-z, y+1/4, x+1/4' '-z, -y, -x' 'z+3/4, -y, x+3/4' 'z+3/4, y+1/4, -x+1/2' 'z, x, y' '-z+1/4, x+1/2, -y+3/4' '-z+1/4, -x+1/4, y' 'z, -x+3/4, -y+3/4' '-x, -z, -y' '-x, z+3/4, y+3/4' 'x+1/4, -z+1/2, y+3/4' 'x+3/4, z+1/4, -y+1/2' 'x, y+1/2, z+1/2' 'x, -y+3/4, -z+3/4' '-x+3/4, -y+3/4, z+1' '-x+3/4, y+1/2, -z+5/4' '-y, x+3/4, z+3/4' 'y+3/4, x+3/4, -z+1' 'y+3/4, -x+1/2, z+5/4' '-y, -x+1/2, -z+1/2' 'y, z+1/2, x+1/2' '-y+3/4, -z+3/4, x+1' 'y, -z+3/4, -x+3/4' '-y+3/4, z+1/2, -x+5/4' '-z, y+3/4, x+3/4' '-z, -y+1/2, -x+1/2' 'z+3/4, -y+1/2, x+5/4' 'z+3/4, y+3/4, -x+1' 'z, x+1/2, y+1/2' '-z+1/4, x+1, -y+5/4' '-z+1/4, -x+3/4, y+1/2' 'z, -x+5/4, -y+5/4' '-x, -z+1/2, -y+1/2' '-x, z+5/4, y+5/4' 'x+1/4, -z+1, y+5/4' 'x+3/4, z+3/4, -y+1' 'x+1/2, y, z+1/2' 'x+1/2, -y+1/4, -z+3/4' '-x+5/4, -y+1/4, z+1' '-x+5/4, y, -z+5/4' '-y+1/2, x+1/4, z+3/4' 'y+5/4, x+1/4, -z+1' 'y+5/4, -x, z+5/4' '-y+1/2, -x, -z+1/2' 'y+1/2, z, x+1/2' '-y+5/4, -z+1/4, x+1' 'y+1/2, -z+1/4, -x+3/4' '-y+5/4, z, -x+5/4' '-z+1/2, y+1/4, x+3/4' '-z+1/2, -y, -x+1/2' 'z+5/4, -y, x+5/4' 'z+5/4, y+1/4, -x+1' 'z+1/2, x, y+1/2' '-z+3/4, x+1/2, -y+5/4' '-z+3/4, -x+1/4, y+1/2' 'z+1/2, -x+3/4, -y+5/4' '-x+1/2, -z, -y+1/2' '-x+1/2, z+3/4, y+5/4' 'x+3/4, -z+1/2, y+5/4' 'x+5/4, z+1/4, -y+1' 'x+1/2, y+1/2, z' 'x+1/2, -y+3/4, -z+1/4' '-x+5/4, -y+3/4, z+1/2' '-x+5/4, y+1/2, -z+3/4' '-y+1/2, x+3/4, z+1/4' 'y+5/4, x+3/4, -z+1/2' 'y+5/4, -x+1/2, z+3/4' '-y+1/2, -x+1/2, -z' 'y+1/2, z+1/2, x' '-y+5/4, -z+3/4, x+1/2' 'y+1/2, -z+3/4, -x+1/4' '-y+5/4, z+1/2, -x+3/4' '-z+1/2, y+3/4, x+1/4' '-z+1/2, -y+1/2, -x' 'z+5/4, -y+1/2, x+3/4' 'z+5/4, y+3/4, -x+1/2' 'z+1/2, x+1/2, y' '-z+3/4, x+1, -y+3/4' '-z+3/4, -x+3/4, y' 'z+1/2, -x+5/4, -y+3/4' '-x+1/2, -z+1/2, -y' '-x+1/2, z+5/4, y+3/4' 'x+3/4, -z+1, y+3/4' 'x+5/4, z+3/4, -y+1/2' '-x, -y, -z' '-x, y-1/4, z-1/4' 'x-3/4, y-1/4, -z-1/2' 'x-3/4, -y, z-3/4' 'y, -x-1/4, -z-1/4' '-y-3/4, -x-1/4, z-1/2' '-y-3/4, x, -z-3/4' 'y, x, z' '-y, -z, -x' 'y-3/4, z-1/4, -x-1/2' '-y, z-1/4, x-1/4' 'y-3/4, -z, x-3/4' 'z, -y-1/4, -x-1/4' 'z, y, x' '-z-3/4, y, -x-3/4' '-z-3/4, -y-1/4, x-1/2' '-z, -x, -y' 'z-1/4, -x-1/2, y-3/4' 'z-1/4, x-1/4, -y' '-z, x-3/4, y-3/4' 'x, z, y' 'x, -z-3/4, -y-3/4' '-x-1/4, z-1/2, -y-3/4' '-x-3/4, -z-1/4, y-1/2' '-x, -y+1/2, -z+1/2' '-x, y+1/4, z+1/4' 'x-3/4, y+1/4, -z' 'x-3/4, -y+1/2, z-1/4' 'y, -x+1/4, -z+1/4' '-y-3/4, -x+1/4, z' '-y-3/4, x+1/2, -z-1/4' 'y, x+1/2, z+1/2' '-y, -z+1/2, -x+1/2' 'y-3/4, z+1/4, -x' '-y, z+1/4, x+1/4' 'y-3/4, -z+1/2, x-1/4' 'z, -y+1/4, -x+1/4' 'z, y+1/2, x+1/2' '-z-3/4, y+1/2, -x-1/4' '-z-3/4, -y+1/4, x' '-z, -x+1/2, -y+1/2' 'z-1/4, -x, y-1/4' 'z-1/4, x+1/4, -y+1/2' '-z, x-1/4, y-1/4' 'x, z+1/2, y+1/2' 'x, -z-1/4, -y-1/4' '-x-1/4, z, -y-1/4' '-x-3/4, -z+1/4, y' '-x+1/2, -y, -z+1/2' '-x+1/2, y-1/4, z+1/4' 'x-1/4, y-1/4, -z' 'x-1/4, -y, z-1/4' 'y+1/2, -x-1/4, -z+1/4' '-y-1/4, -x-1/4, z' '-y-1/4, x, -z-1/4' 'y+1/2, x, z+1/2' '-y+1/2, -z, -x+1/2' 'y-1/4, z-1/4, -x' '-y+1/2, z-1/4, x+1/4' 'y-1/4, -z, x-1/4' 'z+1/2, -y-1/4, -x+1/4' 'z+1/2, y, x+1/2' '-z-1/4, y, -x-1/4' '-z-1/4, -y-1/4, x' '-z+1/2, -x, -y+1/2' 'z+1/4, -x-1/2, y-1/4' 'z+1/4, x-1/4, -y+1/2' '-z+1/2, x-3/4, y-1/4' 'x+1/2, z, y+1/2' 'x+1/2, -z-3/4, -y-1/4' '-x+1/4, z-1/2, -y-1/4' '-x-1/4, -z-1/4, y' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/4, z-1/4' 'x-1/4, y+1/4, -z-1/2' 'x-1/4, -y+1/2, z-3/4' 'y+1/2, -x+1/4, -z-1/4' '-y-1/4, -x+1/4, z-1/2' '-y-1/4, x+1/2, -z-3/4' 'y+1/2, x+1/2, z' '-y+1/2, -z+1/2, -x' 'y-1/4, z+1/4, -x-1/2' '-y+1/2, z+1/4, x-1/4' 'y-1/4, -z+1/2, x-3/4' 'z+1/2, -y+1/4, -x-1/4' 'z+1/2, y+1/2, x' '-z-1/4, y+1/2, -x-3/4' '-z-1/4, -y+1/4, x-1/2' '-z+1/2, -x+1/2, -y' 'z+1/4, -x, y-3/4' 'z+1/4, x+1/4, -y' '-z+1/2, x-1/4, y-3/4' 'x+1/2, z+1/2, y' 'x+1/2, -z-1/4, -y-3/4' '-x+1/4, z, -y-3/4' '-x-1/4, -z+1/4, y-1/2' _cell_length_a 11.6682(8) _cell_length_b 11.6682(8) _cell_length_c 11.6682(8) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 1588.59(19) _cell_formula_units_Z 1 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 325 _cell_measurement_theta_min 7.5 _cell_measurement_theta_max 12.9 _exptl_crystal_description block _exptl_crystal_colour black _exptl_crystal_size_max 0.035 _exptl_crystal_size_mid 0.030 _exptl_crystal_size_min 0.018 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 10.942 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 4452 _exptl_absorpt_coefficient_mu 60.840 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.125 _exptl_absorpt_correction_T_max 0.188 _exptl_absorpt_process_details '(ABSPACK; Oxford Diffraction, 2006)' _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Oxford Xcalibur 3' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count . _diffrn_standards_interval_time . _diffrn_standards_decay_% ? _diffrn_reflns_number 17985 _diffrn_reflns_av_R_equivalents 0.0395 _diffrn_reflns_av_sigmaI/netI 0.0452 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 3.02 _diffrn_reflns_theta_max 31.30 _reflns_number_total 153 _reflns_number_gt 44 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'Oxford Diffraction (2006)' _computing_cell_refinement 'Oxford Diffraction (2006)' _computing_data_reduction 'Oxford Diffraction (2006)' _computing_structure_solution 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'DIAMOND (Brandenburg, 2001)' _computing_publication_material 'SHELXL-97 (Sheldrick, 1997)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment . _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 153 _refine_ls_number_parameters 10 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0340 _refine_ls_R_factor_gt 0.0212 _refine_ls_wR_factor_ref 0.0528 _refine_ls_wR_factor_gt 0.0467 _refine_ls_goodness_of_fit_ref 0.958 _refine_ls_restrained_S_all 0.958 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb Sb 0.25625(9) 0.25625(9) 0.25625(9) 0.0103(6) Uiso 1 6 d S . . Ir Ir 0.0000 0.0000 0.0000 0.0193(14) Uiso 1 12 d S . . Rh Rh 0.5000 0.5000 0.5000 0.022(3) Uiso 0.851(15) 12 d SP . . Cu1 Cu 0.1250 0.1250 0.1250 0.0159(13) Uiso 1 24 d S . . Cu2 Cu 0.3619(5) 0.1250 0.1250 0.015(2) Uiso 0.52(2) 4 d SP . . _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb Cu2 2.492(3) 9 ? Sb Cu2 2.492(3) 103_656 ? Sb Cu2 2.492(3) . ? Sb Cu2 2.584(4) 179 ? Sb Cu2 2.584(4) 77_545 ? Sb Cu2 2.584(4) 171_556 ? Sb Cu1 2.6526(18) . ? Sb Rh 2.8460(10) 27_554 ? Sb Rh 2.8460(10) 4 ? Sb Rh 2.8460(10) 26 ? Sb Ir 2.9918(11) 51_454 ? Sb Ir 2.9918(11) 2 ? Ir Cu2 2.441(3) 107 ? Ir Cu2 2.441(3) 11 ? Ir Cu2 2.441(3) 125 ? Ir Cu2 2.441(3) 29_544 ? Ir Cu2 2.441(3) 147 ? Ir Cu2 2.441(3) 51_454 ? Ir Cu1 2.52624(17) . ? Ir Cu1 2.52624(17) 97 ? Ir Sb 2.9918(11) 51_454 ? Ir Sb 2.9918(11) 147 ? Ir Sb 2.9918(11) 148 ? Ir Sb 2.9918(11) 52_454 ? Rh Cu2 2.617(3) 151_656 ? Rh Cu2 2.617(3) 55_464 ? Rh Cu2 2.617(3) 121_655 ? Rh Cu2 2.617(3) 25 ? Rh Cu2 2.617(3) 177_556 ? Rh Cu2 2.617(3) 81 ? Rh Sb 2.8460(10) 4 ? Rh Sb 2.8460(10) 100_666 ? Rh Sb 2.8460(10) 26 ? Rh Sb 2.8460(10) 122_655 ? Rh Sb 2.8460(10) 123_656 ? Rh Sb 2.8460(10) 27_554 ? Cu1 Ir 2.52624(17) 52_454 ? Cu1 Ir 2.52624(18) 51_454 ? Cu1 Ir 2.52624(17) 2 ? Cu1 Sb 2.6526(18) 51_454 ? Cu1 Sb 2.6526(18) 52_454 ? Cu1 Sb 2.6526(18) 2 ? Cu1 Cu2 2.764(6) 11 ? Cu1 Cu2 2.764(6) 9 ? Cu1 Cu2 2.764(6) 51_454 ? Cu1 Cu2 2.764(6) 125 ? Cu2 Ir 2.441(3) 52_454 ? Cu2 Ir 2.441(3) 51_454 ? Cu2 Sb 2.492(3) 2 ? Cu2 Sb 2.584(4) 99_656 ? Cu2 Sb 2.584(4) 124_655 ? Cu2 Rh 2.617(3) 26 ? Cu2 Rh 2.617(3) 25_544 ? Cu2 Cu2 2.9250(6) 179 ? Cu2 Cu2 2.9250(6) 77_545 ? Cu2 Cu2 2.9250(6) 79_454 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cu2 Sb Cu2 103.32(14) 9 103_656 ? Cu2 Sb Cu2 103.32(14) 9 . ? Cu2 Sb Cu2 103.32(14) 103_656 . ? Cu2 Sb Cu2 169.0(2) 9 179 ? Cu2 Sb Cu2 70.348(5) 103_656 179 ? Cu2 Sb Cu2 70.348(5) . 179 ? Cu2 Sb Cu2 70.348(5) 9 77_545 ? Cu2 Sb Cu2 169.0(2) 103_656 77_545 ? Cu2 Sb Cu2 70.348(5) . 77_545 ? Cu2 Sb Cu2 114.30(8) 179 77_545 ? Cu2 Sb Cu2 70.348(5) 9 171_556 ? Cu2 Sb Cu2 70.348(5) 103_656 171_556 ? Cu2 Sb Cu2 169.0(2) . 171_556 ? Cu2 Sb Cu2 114.30(8) 179 171_556 ? Cu2 Sb Cu2 114.30(8) 77_545 171_556 ? Cu2 Sb Cu1 64.91(12) 9 . ? Cu2 Sb Cu1 64.91(12) 103_656 . ? Cu2 Sb Cu1 64.91(12) . . ? Cu2 Sb Cu1 104.06(11) 179 . ? Cu2 Sb Cu1 104.06(11) 77_545 . ? Cu2 Sb Cu1 104.06(11) 171_556 . ? Cu2 Sb Rh 58.27(11) 9 27_554 ? Cu2 Sb Rh 127.66(5) 103_656 27_554 ? Cu2 Sb Rh 127.66(5) . 27_554 ? Cu2 Sb Rh 132.76(12) 179 27_554 ? Cu2 Sb Rh 57.39(5) 77_545 27_554 ? Cu2 Sb Rh 57.39(5) 171_556 27_554 ? Cu1 Sb Rh 123.19(3) . 27_554 ? Cu2 Sb Rh 127.66(5) 9 4 ? Cu2 Sb Rh 58.27(11) 103_656 4 ? Cu2 Sb Rh 127.66(5) . 4 ? Cu2 Sb Rh 57.39(5) 179 4 ? Cu2 Sb Rh 132.76(12) 77_545 4 ? Cu2 Sb Rh 57.39(5) 171_556 4 ? Cu1 Sb Rh 123.19(3) . 4 ? Rh Sb Rh 92.90(4) 27_554 4 ? Cu2 Sb Rh 127.66(5) 9 26 ? Cu2 Sb Rh 127.67(5) 103_656 26 ? Cu2 Sb Rh 58.27(11) . 26 ? Cu2 Sb Rh 57.39(5) 179 26 ? Cu2 Sb Rh 57.39(5) 77_545 26 ? Cu2 Sb Rh 132.76(12) 171_556 26 ? Cu1 Sb Rh 123.19(3) . 26 ? Rh Sb Rh 92.90(4) 27_554 26 ? Rh Sb Rh 92.90(4) 4 26 ? Cu2 Sb Ir 117.67(14) 9 51_454 ? Cu2 Sb Ir 51.90(6) 103_656 51_454 ? Cu2 Sb Ir 51.90(6) . 51_454 ? Cu2 Sb Ir 51.30(10) 179 51_454 ? Cu2 Sb Ir 122.22(6) 77_545 51_454 ? Cu2 Sb Ir 122.22(6) 171_556 51_454 ? Cu1 Sb Ir 52.76(3) . 51_454 ? Rh Sb Ir 175.95(6) 27_554 51_454 ? Rh Sb Ir 89.893(3) 4 51_454 ? Rh Sb Ir 89.893(3) 26 51_454 ? Cu2 Sb Ir 51.90(6) 9 2 ? Cu2 Sb Ir 51.90(6) 103_656 2 ? Cu2 Sb Ir 117.67(14) . 2 ? Cu2 Sb Ir 122.22(6) 179 2 ? Cu2 Sb Ir 122.22(6) 77_545 2 ? Cu2 Sb Ir 51.30(10) 171_556 2 ? Cu1 Sb Ir 52.76(3) . 2 ? Rh Sb Ir 89.893(3) 27_554 2 ? Rh Sb Ir 89.893(3) 4 2 ? Rh Sb Ir 175.95(6) 26 2 ? Ir Sb Ir 87.17(4) 51_454 2 ? Cu2 Ir Cu2 180.0(2) 107 11 ? Cu2 Ir Cu2 73.61(12) 107 125 ? Cu2 Ir Cu2 106.39(12) 11 125 ? Cu2 Ir Cu2 106.39(12) 107 29_544 ? Cu2 Ir Cu2 73.61(12) 11 29_544 ? Cu2 Ir Cu2 180.0(2) 125 29_544 ? Cu2 Ir Cu2 106.39(12) 107 147 ? Cu2 Ir Cu2 73.61(12) 11 147 ? Cu2 Ir Cu2 73.61(12) 125 147 ? Cu2 Ir Cu2 106.39(12) 29_544 147 ? Cu2 Ir Cu2 73.61(12) 107 51_454 ? Cu2 Ir Cu2 106.39(12) 11 51_454 ? Cu2 Ir Cu2 106.39(12) 125 51_454 ? Cu2 Ir Cu2 73.61(12) 29_544 51_454 ? Cu2 Ir Cu2 180.0(2) 147 51_454 ? Cu2 Ir Cu1 112.40(11) 107 . ? Cu2 Ir Cu1 67.60(11) 11 . ? Cu2 Ir Cu1 67.60(11) 125 . ? Cu2 Ir Cu1 112.40(11) 29_544 . ? Cu2 Ir Cu1 112.40(11) 147 . ? Cu2 Ir Cu1 67.60(11) 51_454 . ? Cu2 Ir Cu1 67.60(11) 107 97 ? Cu2 Ir Cu1 112.40(11) 11 97 ? Cu2 Ir Cu1 112.40(11) 125 97 ? Cu2 Ir Cu1 67.60(11) 29_544 97 ? Cu2 Ir Cu1 67.60(11) 147 97 ? Cu2 Ir Cu1 112.40(11) 51_454 97 ? Cu1 Ir Cu1 180.0 . 97 ? Cu2 Ir Sb 55.69(11) 107 51_454 ? Cu2 Ir Sb 124.31(11) 11 51_454 ? Cu2 Ir Sb 53.45(5) 125 51_454 ? Cu2 Ir Sb 126.55(5) 29_544 51_454 ? Cu2 Ir Sb 126.55(5) 147 51_454 ? Cu2 Ir Sb 53.45(5) 51_454 51_454 ? Cu1 Ir Sb 56.71(3) . 51_454 ? Cu1 Ir Sb 123.29(3) 97 51_454 ? Cu2 Ir Sb 124.31(11) 107 147 ? Cu2 Ir Sb 55.69(11) 11 147 ? Cu2 Ir Sb 126.55(5) 125 147 ? Cu2 Ir Sb 53.45(5) 29_544 147 ? Cu2 Ir Sb 53.45(5) 147 147 ? Cu2 Ir Sb 126.55(5) 51_454 147 ? Cu1 Ir Sb 123.29(3) . 147 ? Cu1 Ir Sb 56.71(3) 97 147 ? Sb Ir Sb 180.0 51_454 147 ? Cu2 Ir Sb 53.45(5) 107 148 ? Cu2 Ir Sb 126.55(5) 11 148 ? Cu2 Ir Sb 55.69(11) 125 148 ? Cu2 Ir Sb 124.31(11) 29_544 148 ? Cu2 Ir Sb 53.45(5) 147 148 ? Cu2 Ir Sb 126.55(5) 51_454 148 ? Cu1 Ir Sb 123.29(3) . 148 ? Cu1 Ir Sb 56.71(3) 97 148 ? Sb Ir Sb 87.24(4) 51_454 148 ? Sb Ir Sb 92.76(4) 147 148 ? Cu2 Ir Sb 126.55(5) 107 52_454 ? Cu2 Ir Sb 53.45(5) 11 52_454 ? Cu2 Ir Sb 124.31(11) 125 52_454 ? Cu2 Ir Sb 55.69(11) 29_544 52_454 ? Cu2 Ir Sb 126.55(5) 147 52_454 ? Cu2 Ir Sb 53.45(5) 51_454 52_454 ? Cu1 Ir Sb 56.71(3) . 52_454 ? Cu1 Ir Sb 123.29(3) 97 52_454 ? Sb Ir Sb 92.76(4) 51_454 52_454 ? Sb Ir Sb 87.24(4) 147 52_454 ? Sb Ir Sb 180.00(4) 148 52_454 ? Cu2 Rh Cu2 180.0 151_656 55_464 ? Cu2 Rh Cu2 67.94(9) 151_656 121_655 ? Cu2 Rh Cu2 112.06(9) 55_464 121_655 ? Cu2 Rh Cu2 112.06(9) 151_656 25 ? Cu2 Rh Cu2 67.94(9) 55_464 25 ? Cu2 Rh Cu2 180.000(1) 121_655 25 ? Cu2 Rh Cu2 67.94(9) 151_656 177_556 ? Cu2 Rh Cu2 112.06(9) 55_464 177_556 ? Cu2 Rh Cu2 112.06(9) 121_655 177_556 ? Cu2 Rh Cu2 67.94(9) 25 177_556 ? Cu2 Rh Cu2 112.06(9) 151_656 81 ? Cu2 Rh Cu2 67.94(9) 55_464 81 ? Cu2 Rh Cu2 67.94(9) 121_655 81 ? Cu2 Rh Cu2 112.06(9) 25 81 ? Cu2 Rh Cu2 180.0 177_556 81 ? Cu2 Rh Sb 54.08(10) 151_656 4 ? Cu2 Rh Sb 125.92(10) 55_464 4 ? Cu2 Rh Sb 56.26(5) 121_655 4 ? Cu2 Rh Sb 123.74(5) 25 4 ? Cu2 Rh Sb 56.26(5) 177_556 4 ? Cu2 Rh Sb 123.74(5) 81 4 ? Cu2 Rh Sb 125.92(10) 151_656 100_666 ? Cu2 Rh Sb 54.08(10) 55_464 100_666 ? Cu2 Rh Sb 123.74(5) 121_655 100_666 ? Cu2 Rh Sb 56.26(5) 25 100_666 ? Cu2 Rh Sb 123.74(5) 177_556 100_666 ? Cu2 Rh Sb 56.26(5) 81 100_666 ? Sb Rh Sb 180.00(4) 4 100_666 ? Cu2 Rh Sb 123.74(5) 151_656 26 ? Cu2 Rh Sb 56.26(5) 55_464 26 ? Cu2 Rh Sb 125.92(10) 121_655 26 ? Cu2 Rh Sb 54.08(10) 25 26 ? Cu2 Rh Sb 56.26(5) 177_556 26 ? Cu2 Rh Sb 123.74(5) 81 26 ? Sb Rh Sb 87.03(4) 4 26 ? Sb Rh Sb 92.97(4) 100_666 26 ? Cu2 Rh Sb 56.26(5) 151_656 122_655 ? Cu2 Rh Sb 123.74(5) 55_464 122_655 ? Cu2 Rh Sb 54.08(10) 121_655 122_655 ? Cu2 Rh Sb 125.92(10) 25 122_655 ? Cu2 Rh Sb 123.74(5) 177_556 122_655 ? Cu2 Rh Sb 56.26(5) 81 122_655 ? Sb Rh Sb 92.97(4) 4 122_655 ? Sb Rh Sb 87.03(4) 100_666 122_655 ? Sb Rh Sb 180.00(4) 26 122_655 ? Cu2 Rh Sb 56.26(5) 151_656 123_656 ? Cu2 Rh Sb 123.74(5) 55_464 123_656 ? Cu2 Rh Sb 123.74(5) 121_655 123_656 ? Cu2 Rh Sb 56.26(5) 25 123_656 ? Cu2 Rh Sb 54.08(10) 177_556 123_656 ? Cu2 Rh Sb 125.92(10) 81 123_656 ? Sb Rh Sb 92.97(4) 4 123_656 ? Sb Rh Sb 87.03(4) 100_666 123_656 ? Sb Rh Sb 92.97(4) 26 123_656 ? Sb Rh Sb 87.03(4) 122_655 123_656 ? Cu2 Rh Sb 123.74(5) 151_656 27_554 ? Cu2 Rh Sb 56.26(5) 55_464 27_554 ? Cu2 Rh Sb 56.26(5) 121_655 27_554 ? Cu2 Rh Sb 123.74(5) 25 27_554 ? Cu2 Rh Sb 125.92(10) 177_556 27_554 ? Cu2 Rh Sb 54.08(10) 81 27_554 ? Sb Rh Sb 87.03(4) 4 27_554 ? Sb Rh Sb 92.97(4) 100_666 27_554 ? Sb Rh Sb 87.03(4) 26 27_554 ? Sb Rh Sb 92.97(4) 122_655 27_554 ? Sb Rh Sb 180.0 123_656 27_554 ? Ir Cu1 Ir 109.5 . 52_454 ? Ir Cu1 Ir 109.5 . 51_454 ? Ir Cu1 Ir 109.5 52_454 51_454 ? Ir Cu1 Ir 109.5 . 2 ? Ir Cu1 Ir 109.5 52_454 2 ? Ir Cu1 Ir 109.5 51_454 2 ? Ir Cu1 Sb 180.000(18) . . ? Ir Cu1 Sb 70.5 52_454 . ? Ir Cu1 Sb 70.5 51_454 . ? Ir Cu1 Sb 70.5 2 . ? Ir Cu1 Sb 70.5 . 51_454 ? Ir Cu1 Sb 70.5 52_454 51_454 ? Ir Cu1 Sb 180.000(18) 51_454 51_454 ? Ir Cu1 Sb 70.5 2 51_454 ? Sb Cu1 Sb 109.5 . 51_454 ? Ir Cu1 Sb 70.5 . 52_454 ? Ir Cu1 Sb 180.000(18) 52_454 52_454 ? Ir Cu1 Sb 70.5 51_454 52_454 ? Ir Cu1 Sb 70.5 2 52_454 ? Sb Cu1 Sb 109.5 . 52_454 ? Sb Cu1 Sb 109.5 51_454 52_454 ? Ir Cu1 Sb 70.5 . 2 ? Ir Cu1 Sb 70.5 52_454 2 ? Ir Cu1 Sb 70.5 51_454 2 ? Ir Cu1 Sb 180.000(18) 2 2 ? Sb Cu1 Sb 109.5 . 2 ? Sb Cu1 Sb 109.5 51_454 2 ? Sb Cu1 Sb 109.5 52_454 2 ? Ir Cu1 Cu2 54.7 . 11 ? Ir Cu1 Cu2 125.3 52_454 11 ? Ir Cu1 Cu2 54.7 51_454 11 ? Ir Cu1 Cu2 125.3 2 11 ? Sb Cu1 Cu2 125.3 . 11 ? Sb Cu1 Cu2 125.3 51_454 11 ? Sb Cu1 Cu2 54.7 52_454 11 ? Sb Cu1 Cu2 54.7 2 11 ? Ir Cu1 Cu2 125.3 . 9 ? Ir Cu1 Cu2 54.7 52_454 9 ? Ir Cu1 Cu2 125.3 51_454 9 ? Ir Cu1 Cu2 54.7 2 9 ? Sb Cu1 Cu2 54.7 . 9 ? Sb Cu1 Cu2 54.7 51_454 9 ? Sb Cu1 Cu2 125.3 52_454 9 ? Sb Cu1 Cu2 125.3 2 9 ? Cu2 Cu1 Cu2 180.0 11 9 ? Ir Cu1 Cu2 54.7 . 51_454 ? Ir Cu1 Cu2 125.3 52_454 51_454 ? Ir Cu1 Cu2 125.3 51_454 51_454 ? Ir Cu1 Cu2 54.7 2 51_454 ? Sb Cu1 Cu2 125.3 . 51_454 ? Sb Cu1 Cu2 54.7 51_454 51_454 ? Sb Cu1 Cu2 54.7 52_454 51_454 ? Sb Cu1 Cu2 125.3 2 51_454 ? Cu2 Cu1 Cu2 90.0 11 51_454 ? Cu2 Cu1 Cu2 90.0 9 51_454 ? Ir Cu1 Cu2 54.7 . 125 ? Ir Cu1 Cu2 54.7 52_454 125 ? Ir Cu1 Cu2 125.3 51_454 125 ? Ir Cu1 Cu2 125.3 2 125 ? Sb Cu1 Cu2 125.3 . 125 ? Sb Cu1 Cu2 54.7 51_454 125 ? Sb Cu1 Cu2 125.3 52_454 125 ? Sb Cu1 Cu2 54.7 2 125 ? Cu2 Cu1 Cu2 90.0 11 125 ? Cu2 Cu1 Cu2 90.0 9 125 ? Cu2 Cu1 Cu2 90.0 51_454 125 ? Ir Cu2 Ir 115.3(2) 52_454 51_454 ? Ir Cu2 Sb 74.66(10) 52_454 2 ? Ir Cu2 Sb 74.66(10) 51_454 2 ? Ir Cu2 Sb 74.66(10) 52_454 . ? Ir Cu2 Sb 74.66(10) 51_454 . ? Sb Cu2 Sb 120.7(2) 2 . ? Ir Cu2 Sb 73.02(4) 52_454 99_656 ? Ir Cu2 Sb 171.7(2) 51_454 99_656 ? Sb Cu2 Sb 108.81(3) 2 99_656 ? Sb Cu2 Sb 108.81(3) . 99_656 ? Ir Cu2 Sb 171.7(2) 52_454 124_655 ? Ir Cu2 Sb 73.02(4) 51_454 124_655 ? Sb Cu2 Sb 108.81(3) 2 124_655 ? Sb Cu2 Sb 108.81(3) . 124_655 ? Sb Cu2 Sb 98.6(2) 99_656 124_655 ? Ir Cu2 Rh 109.225(18) 52_454 26 ? Ir Cu2 Rh 109.225(18) 51_454 26 ? Sb Cu2 Rh 171.7(2) 2 26 ? Sb Cu2 Rh 67.64(4) . 26 ? Sb Cu2 Rh 66.34(11) 99_656 26 ? Sb Cu2 Rh 66.34(11) 124_655 26 ? Ir Cu2 Rh 109.225(18) 52_454 25_544 ? Ir Cu2 Rh 109.225(18) 51_454 25_544 ? Sb Cu2 Rh 67.64(4) 2 25_544 ? Sb Cu2 Rh 171.7(2) . 25_544 ? Sb Cu2 Rh 66.34(11) 99_656 25_544 ? Sb Cu2 Rh 66.34(11) 124_655 25_544 ? Rh Cu2 Rh 104.01(19) 26 25_544 ? Ir Cu2 Cu1 57.66(11) 52_454 . ? Ir Cu2 Cu1 57.66(11) 51_454 . ? Sb Cu2 Cu1 60.35(12) 2 . ? Sb Cu2 Cu1 60.35(12) . . ? Sb Cu2 Cu1 130.68(11) 99_656 . ? Sb Cu2 Cu1 130.68(11) 124_655 . ? Rh Cu2 Cu1 127.99(10) 26 . ? Rh Cu2 Cu1 127.99(10) 25_544 . ? Ir Cu2 Cu2 130.9(2) 52_454 179 ? Ir Cu2 Cu2 53.20(6) 51_454 179 ? Sb Cu2 Cu2 127.34(2) 2 179 ? Sb Cu2 Cu2 56.29(10) . 179 ? Sb Cu2 Cu2 121.92(9) 99_656 179 ? Sb Cu2 Cu2 53.36(10) 124_655 179 ? Rh Cu2 Cu2 56.03(4) 26 179 ? Rh Cu2 Cu2 119.6(2) 25_544 179 ? Cu1 Cu2 Cu2 92.99(11) . 179 ? Ir Cu2 Cu2 53.20(6) 52_454 77_545 ? Ir Cu2 Cu2 130.9(2) 51_454 77_545 ? Sb Cu2 Cu2 127.34(2) 2 77_545 ? Sb Cu2 Cu2 56.29(10) . 77_545 ? Sb Cu2 Cu2 53.36(10) 99_656 77_545 ? Sb Cu2 Cu2 121.92(9) 124_655 77_545 ? Rh Cu2 Cu2 56.03(4) 26 77_545 ? Rh Cu2 Cu2 119.6(2) 25_544 77_545 ? Cu1 Cu2 Cu2 92.99(11) . 77_545 ? Cu2 Cu2 Cu2 95.8(2) 179 77_545 ? Ir Cu2 Cu2 130.9(2) 52_454 79_454 ? Ir Cu2 Cu2 53.20(6) 51_454 79_454 ? Sb Cu2 Cu2 56.29(10) 2 79_454 ? Sb Cu2 Cu2 127.34(2) . 79_454 ? Sb Cu2 Cu2 121.92(9) 99_656 79_454 ? Sb Cu2 Cu2 53.36(10) 124_655 79_454 ? Rh Cu2 Cu2 119.6(2) 26 79_454 ? Rh Cu2 Cu2 56.03(4) 25_544 79_454 ? Cu1 Cu2 Cu2 92.99(11) . 79_454 ? Cu2 Cu2 Cu2 83.9(2) 179 79_454 ? Cu2 Cu2 Cu2 174.0(2) 77_545 79_454 ? _diffrn_measured_fraction_theta_max 0.994 _diffrn_reflns_theta_full 31.30 _diffrn_measured_fraction_theta_full 0.994 _refine_diff_density_max 0.667 _refine_diff_density_min -0.884 _refine_diff_density_rms 0.226