data_shelx
 
_audit_creation_method            'SHELXL-2018/1'
_shelx_SHELXL_version_number      '2018/1'
_chemical_name_mineral            'tsugaruite'
_chemical_compound_source         'Yunosawa mine, Japan'
_chemical_formula_analytical
;      
As7.37 Cl0.76 Pb14.13 S24.54
; 
_chemical_formula_sum
 'As7.55 Cl0.5 Pb13.95 S25'
_chemical_formula_weight          4275.71

loop_
 _atom_type_symbol
 _atom_type_description
 _atom_type_scat_dispersion_real
 _atom_type_scat_dispersion_imag
 _atom_type_scat_source
 'As'  'As'   0.0499   2.0058
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Pb'  'Pb'  -3.3944  10.1111
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'S'  'S'   0.1246   0.1234
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Cl'  'Cl'   0.1484   0.1585
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Sb'  'Sb'  -0.5866   1.5461
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
_space_group_crystal_system       orthorhombic
_space_group_IT_number            ?
_space_group_name_H-M_alt         'P 2 n n'
_space_group_name_Hall            'P -2n 2'
 
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
 
loop_
 _space_group_symop_operation_xyz
 'x, y, z'
 'x+1/2, y+1/2, -z+1/2'
 'x, -y, -z'
 'x+1/2, -y+1/2, z+1/2'
 
_cell_length_a                    8.0774(10)
_cell_length_b                    15.1772(16)
_cell_length_c                    38.129(4)
_cell_angle_alpha                 90
_cell_angle_beta                  90
_cell_angle_gamma                 90
_cell_volume                      4674.3(9)
_cell_formula_units_Z             4
_cell_measurement_temperature     293(2)
_cell_measurement_reflns_used     2879
_cell_measurement_theta_min       2.889
_cell_measurement_theta_max       28.542
 
_exptl_crystal_description        'acicular'
_exptl_crystal_colour             'black'
_exptl_crystal_density_meas       'not measured'
_exptl_crystal_density_method     ?
_exptl_crystal_density_diffrn     6.076          
_exptl_crystal_F_000              7206.8
_exptl_transmission_factor_min    ?
_exptl_transmission_factor_max    ?
_exptl_crystal_size_max           0.100
_exptl_crystal_size_mid           0.010
_exptl_crystal_size_min           0.010
_exptl_absorpt_coefficient_mu     56.505
_shelx_estimated_absorpt_T_min    ?
_shelx_estimated_absorpt_T_max    ?
_exptl_absorpt_correction_type    'multi-scan'
_exptl_absorpt_correction_T_min   0.864
_exptl_absorpt_correction_T_max   0.885
_exptl_absorpt_process_details    'SADABS (Sheldrick, 1996)'
_exptl_absorpt_special_details    ?
_diffrn_ambient_temperature       293(2)
_diffrn_radiation_wavelength      0.71073
_diffrn_radiation_type            MoK\a
_diffrn_radiation_source          'fine-focus sealed tube'
_diffrn_radiation_monochromator   graphite
_diffrn_measurement_device_type   'Bruker Smart Breeze'
_diffrn_reflns_number             8315
_diffrn_reflns_av_unetI/netI      0.1850
_diffrn_reflns_av_R_equivalents   0.1052
_diffrn_reflns_limit_h_min        -10
_diffrn_reflns_limit_h_max        4
_diffrn_reflns_limit_k_min        -20
_diffrn_reflns_limit_k_max        5
_diffrn_reflns_limit_l_min        -52
_diffrn_reflns_limit_l_max        34
_diffrn_reflns_theta_min          1.068
_diffrn_reflns_theta_max          29.305
_diffrn_reflns_theta_full         25.242
_diffrn_measured_fraction_theta_max   0.973
_diffrn_measured_fraction_theta_full  0.995
_diffrn_reflns_Laue_measured_fraction_max    0.973
_diffrn_reflns_Laue_measured_fraction_full   0.995
_diffrn_reflns_point_group_measured_fraction_max   0.650
_diffrn_reflns_point_group_measured_fraction_full  0.719
_reflns_number_total              8315
_reflns_number_gt                 3488
_reflns_threshold_expression      'I > 2\s(I)'
_reflns_Friedel_coverage          0.252
_reflns_Friedel_fraction_max      0.280
_reflns_Friedel_fraction_full     0.397
 
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
 
_computing_data_collection      'Apex2 (Bruker AXS Inc., 2004)'
_computing_cell_refinement      'Apex2 (Bruker AXS Inc., 2004)'
_computing_data_reduction       'Apex2 (Bruker AXS Inc., 2004)'
_computing_structure_solution   'SHELXS-1997 (Sheldrick, 1997)'
_computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)'
_computing_molecular_graphics     ?
_computing_publication_material   ?
_refine_special_details           ?
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0001P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary      ?
_atom_sites_solution_secondary    ?
_atom_sites_solution_hydrogens    .
_refine_ls_hydrogen_treatment     undef
_refine_ls_extinction_method      none
_refine_ls_extinction_coef        .
_refine_ls_abs_structure_details
;
 Flack x determined using 587 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack    0.002(4)
_chemical_absolute_configuration  ?
_refine_ls_number_reflns          8315
_refine_ls_number_parameters      424
_refine_ls_number_restraints      1
_refine_ls_R_factor_all           0.0539
_refine_ls_R_factor_gt            0.0427
_refine_ls_wR_factor_ref          0.0936
_refine_ls_wR_factor_gt           0.0926
_refine_ls_goodness_of_fit_ref    0.593
_refine_ls_restrained_S_all       0.593
_refine_ls_shift/su_max           0.001
_refine_ls_shift/su_mean          0.000
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_site_symmetry_order  
 _atom_site_calc_flag
 _atom_site_refinement_flags_posn
 _atom_site_refinement_flags_adp
 _atom_site_refinement_flags_occupancy
 _atom_site_disorder_assembly
 _atom_site_disorder_group
Pb1 Pb 0.4911(3) 0.45802(15) 0.82334(7) 0.0264(6) Uani 1 1 d . . . . .
Pb2 Pb 0.9965(3) 0.18951(17) 0.87405(6) 0.0307(6) Uani 1 1 d . . . . .
Pb3 Pb 0.9946(3) 0.69008(17) 0.62585(5) 0.0252(6) Uani 1 1 d . . . . .
Pb4 Pb 0.9977(3) 0.79718(17) 0.52316(6) 0.0274(6) Uani 1 1 d . . . . .
Pb5 Pb 0.4891(3) 0.08931(16) 0.57486(6) 0.0241(6) Uani 1 1 d . . . . .
Pb6 Pb 0.4965(2) 0.56219(15) 0.72471(6) 0.0188(5) Uani 1 1 d . . . . .
Pb7 Pb 0.4915(3) 0.58989(15) 0.92453(5) 0.0191(5) Uani 1 1 d . . . . .
Pb8 Pb 0.9911(3) 0.46034(15) 0.82291(5) 0.0221(5) Uani 1 1 d . . . . .
Pb9 Pb 0.4989(2) 0.94052(16) 0.22482(6) 0.0216(5) Uani 1 1 d . . . . .
Pb10 Pb 0.9929(3) 0.29549(17) 0.97666(6) 0.0260(6) Uani 1 1 d . . . . .
Pb11 Pb 0.2440(4) 0.30978(7) 0.74438(2) 0.0225(3) Uani 1 1 d . . . . .
Pb12 Pb 0.7440(6) 0.86403(9) 0.93201(3) 0.0499(4) Uani 1 1 d . . . . .
Pb13 Pb 0.2391(6) 0.74618(11) 0.83146(3) 0.0596(5) Uani 1 1 d . . . . .
As14 As 0.249(2) 0.9719(5) 0.87007(18) 0.0273(11) Uani 0.640(5) 1 d . . P . .
Pb14 Pb 0.2502(16) 0.9454(3) 0.85665(11) 0.0273(11) Uani 0.360(5) 1 d . . P . .
As15 As 0.7412(10) 0.08156(15) 0.97063(6) 0.0137(5) Uani 1 1 d . . . . .
As16 As 0.2424(12) 0.80706(17) 0.93041(6) 0.0215(6) Uani 1 1 d . . . . .
As17 As 0.2373(10) 0.18969(16) 0.66428(6) 0.0149(6) Uani 1 1 d . . . . .
As18 As 0.7441(11) 0.93241(16) 0.84388(6) 0.0168(6) Uani 1 1 d . . . . .
As19 As 0.2372(10) 0.80569(16) 0.74518(6) 0.0130(5) Uani 1 1 d . . . . .
As20 As 0.2381(13) 0.60355(19) 0.09896(7) 0.0360(8) Uani 1 1 d . . . . .
As21 As 0.741(5) 0.5425(10) 0.5568(4) 0.0701(14) Uani 0.407(5) 1 d . . P . .
Pb21 Pb 0.7402(11) 0.5324(2) 0.53686(9) 0.0701(14) Uani 0.593(5) 1 d . . P . .
As22 As 0.247(2) 0.000000 0.500000 0.0415(13) Uani 1 2 d S T P . .
S1 S 0.750(2) 0.1980(4) 0.93439(15) 0.0162(17) Uani 1 1 d . . . . .
S2 S 0.740(3) 0.4527(4) 0.76441(15) 0.0247(17) Uani 1 1 d . . . . .
S3 S 0.249(2) 0.0707(4) 0.62876(15) 0.0161(17) Uani 1 1 d . . . . .
S4 S 0.244(2) 0.6958(4) 0.96780(14) 0.0150(14) Uani 1 1 d . . . . .
S5 S 0.752(3) 0.7008(5) 0.56997(18) 0.031(2) Uani 1 1 d . . . . .
S6 S 0.9643(16) 0.8943(7) 0.8113(3) 0.004(2) Uiso 1 1 d . . . . .
S7 S 0.247(2) 0.4797(4) 0.77138(15) 0.0153(16) Uani 1 1 d . . . . .
S8 S 0.754(2) 0.0800(4) 0.83048(16) 0.017(2) Uani 1 1 d . . . . .
S9 S 0.9700(19) 0.1200(8) 0.0068(3) 0.015(3) Uani 1 1 d . . . . .
S10 S 0.0272(19) 0.7663(9) 0.8986(3) 0.018(3) Uani 1 1 d . . . . .
S11 S 0.4667(17) 0.7625(8) 0.8931(3) 0.014(3) Uani 1 1 d . . . . .
S12 S 0.475(2) 0.0060(10) 0.9048(3) 0.025(3) Uani 1 1 d . . . . .
S13 S 0.520(2) 0.8930(9) 0.8079(3) 0.024(3) Uani 1 1 d . . . . .
S14 S 0.4629(15) 0.7765(6) 0.7111(3) 0.006(2) Uiso 1 1 d . . . . .
S15 S 0.2587(18) 0.6771(4) 0.14936(16) 0.014(2) Uani 1 1 d . . . . .
S16 S 0.0442(17) 0.7619(8) 0.7097(3) 0.028(3) Uani 1 1 d . . . . .
S17 S 0.0290(17) 0.0173(8) 0.9070(3) 0.015(3) Uani 1 1 d . . . . .
S18 S 0.460(2) 0.1392(9) 0.6974(3) 0.019(3) Uani 1 1 d . . . . .
S19 S 0.254(2) 0.0949(5) 0.83193(16) 0.023(2) Uani 1 1 d . . . . .
S20 S 0.240(3) 0.1729(5) 0.53164(19) 0.039(2) Uani 1 1 d . . . . .
S21 S 0.024(2) 0.1585(9) 0.6985(4) 0.024(3) Uani 1 1 d . . . . .
S22 S 0.238(3) 0.4568(4) 0.12717(16) 0.0267(16) Uani 1 1 d . . . . .
S23 S 0.5337(18) 0.1216(8) 0.0047(3) 0.015(3) Uani 1 1 d . . . . .
S24 S 0.5304(11) 0.6126(5) 0.0956(2) 0.0209(19) Uani 1 1 d . . . . .
Cl25 Cl 0.9536(15) 0.000000 0.500000 0.029(3) Uani 1 2 d S T P . .
S26 S 0.260(3) 0.0583(6) 0.4473(2) 0.054(4) Uani 1 1 d . . . . .
 
loop_
 _atom_site_aniso_label
 _atom_site_aniso_U_11
 _atom_site_aniso_U_22
 _atom_site_aniso_U_33
 _atom_site_aniso_U_23
 _atom_site_aniso_U_13
 _atom_site_aniso_U_12
Pb1 0.0133(11) 0.0295(13) 0.0364(13) 0.0041(11) -0.0056(10) 0.0023(11)
Pb2 0.0197(14) 0.0298(14) 0.0426(14) -0.0053(12) 0.0014(12) 0.0164(11)
Pb3 0.0224(14) 0.0353(14) 0.0179(11) -0.0008(10) 0.0065(11) 0.0096(11)
Pb4 0.0278(15) 0.0278(13) 0.0265(12) -0.0001(10) 0.0003(11) 0.0002(11)
Pb5 0.0132(12) 0.0265(13) 0.0325(13) 0.0025(11) 0.0036(10) 0.0029(10)
Pb6 0.0182(13) 0.0209(11) 0.0174(11) 0.0007(9) -0.0001(10) 0.0002(10)
Pb7 0.0198(13) 0.0208(12) 0.0167(11) 0.0004(9) 0.0010(10) -0.0007(10)
Pb8 0.0224(12) 0.0352(13) 0.0086(9) -0.0030(10) -0.0040(9) 0.0088(11)
Pb9 0.0116(12) 0.0309(13) 0.0224(11) 0.0010(10) -0.0001(9) -0.0070(10)
Pb10 0.0185(13) 0.0376(15) 0.0219(11) -0.0018(10) -0.0045(11) 0.0186(11)
Pb11 0.0223(6) 0.0231(6) 0.0221(5) 0.0013(4) -0.0021(14) 0.0166(13)
Pb12 0.0398(9) 0.0694(9) 0.0405(7) -0.0290(7) 0.008(2) -0.003(2)
Pb13 0.0475(10) 0.1071(12) 0.0242(6) -0.0114(7) 0.0041(18) -0.014(3)
As14 0.0241(15) 0.031(3) 0.027(3) -0.0011(15) -0.002(5) -0.002(5)
Pb14 0.0241(15) 0.031(3) 0.027(3) -0.0011(15) -0.002(5) -0.002(5)
As15 0.0152(14) 0.0141(13) 0.0119(12) 0.0014(10) 0.000(3) -0.001(3)
As16 0.0219(15) 0.0205(14) 0.0221(14) 0.0015(12) -0.001(4) 0.003(4)
As17 0.0172(15) 0.0142(12) 0.0134(12) 0.0015(10) -0.002(3) 0.002(3)
As18 0.0170(15) 0.0151(13) 0.0184(13) 0.0010(10) -0.001(4) -0.001(4)
As19 0.0138(14) 0.0136(12) 0.0117(11) 0.0021(10) 0.003(3) 0.000(3)
As20 0.036(2) 0.0327(18) 0.0388(17) 0.0002(14) 0.002(5) 0.000(5)
As21 0.0249(14) 0.0855(19) 0.100(3) 0.080(2) 0.011(6) 0.006(4)
Pb21 0.0249(14) 0.0855(19) 0.100(3) 0.080(2) 0.011(6) 0.006(4)
As22 0.042(3) 0.039(3) 0.044(3) 0.000(2) 0.000 0.000
S1 0.014(4) 0.017(3) 0.017(3) -0.001(3) 0.001(6) -0.001(6)
S2 0.031(5) 0.025(4) 0.018(3) -0.001(3) -0.008(9) -0.008(10)
S3 0.016(5) 0.017(3) 0.015(3) 0.000(3) 0.000(6) -0.004(6)
S4 0.014(4) 0.015(3) 0.016(3) -0.005(3) -0.001(7) -0.001(7)
S5 0.032(7) 0.033(4) 0.029(4) 0.007(3) 0.006(7) 0.000(8)
S7 0.016(4) 0.020(3) 0.010(3) -0.002(2) 0.001(6) -0.003(7)
S8 0.016(6) 0.015(3) 0.021(3) 0.006(3) -0.003(5) 0.003(5)
S9 0.020(6) 0.011(5) 0.013(5) -0.005(4) 0.000(5) 0.000(5)
S10 0.019(6) 0.025(6) 0.009(5) 0.006(4) 0.001(4) 0.003(5)
S11 0.007(5) 0.013(5) 0.024(6) 0.002(4) -0.002(5) -0.001(5)
S12 0.021(6) 0.030(7) 0.024(6) -0.008(5) 0.003(6) 0.002(6)
S13 0.025(6) 0.023(5) 0.024(5) 0.007(4) 0.000(4) 0.004(4)
S15 0.009(6) 0.013(3) 0.021(3) 0.005(3) 0.000(4) -0.003(4)
S16 0.037(8) 0.027(6) 0.018(5) 0.002(4) 0.001(4) 0.007(5)
S17 0.015(5) 0.012(5) 0.020(6) -0.003(4) 0.000(4) 0.003(4)
S18 0.020(6) 0.032(7) 0.006(5) 0.000(4) 0.003(5) -0.004(5)
S19 0.020(6) 0.029(4) 0.019(3) -0.002(3) 0.001(6) 0.000(6)
S20 0.034(5) 0.038(5) 0.045(4) 0.007(4) -0.006(12) 0.007(12)
S21 0.019(7) 0.019(6) 0.034(7) -0.003(5) 0.000(5) -0.002(5)
S22 0.025(4) 0.030(4) 0.025(4) 0.008(3) 0.001(10) 0.001(10)
S23 0.015(5) 0.016(6) 0.014(6) 0.000(5) -0.004(5) -0.001(5)
S24 0.018(5) 0.018(4) 0.027(5) -0.003(4) -0.002(3) 0.003(4)
Cl25 0.020(7) 0.033(7) 0.034(7) 0.002(6) 0.000 0.000
S26 0.050(13) 0.052(6) 0.061(6) 0.003(5) 0.001(8) -0.014(9)
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
Pb1 S7 2.812(15) . ?
Pb1 S15 2.969(11) 3_566 ?
Pb1 S2 3.015(17) . ?
Pb1 S22 3.066(16) 3_566 ?
Pb1 S21 3.166(13) 2_556 ?
Pb1 S3 3.256(13) 2_556 ?
Pb1 S16 3.260(12) 2_546 ?
Pb1 S24 3.285(8) 3_566 ?
Pb1 As20 3.719(7) 3_566 ?
Pb1 As19 4.015(5) 2_546 ?
Pb1 Pb8 4.0386(18) 1_455 ?
Pb1 Pb8 4.0392(18) . ?
Pb2 S17 2.911(13) 1_655 ?
Pb2 S5 2.974(17) 2_546 ?
Pb2 S19 2.994(14) 1_655 ?
Pb2 S1 3.047(13) . ?
Pb2 S8 3.061(13) . ?
Pb2 S15 3.062(12) 3_666 ?
Pb2 S14 3.515(10) 2_546 ?
Pb2 As20 3.838(7) 3_666 ?
Pb2 As14 3.883(13) 1_645 ?
Pb2 As21 3.98(2) 2_546 ?
Pb2 Pb3 4.0233(16) 2_546 ?
Pb2 Pb3 4.0541(16) 2_446 ?
Pb3 S5 2.899(17) . ?
Pb3 S19 2.909(14) 2_556 ?
Pb3 S15 2.915(11) 4_565 ?
Pb3 S12 3.032(15) 2_556 ?
Pb3 S1 3.088(13) 2_556 ?
Pb3 S8 3.153(13) 2_556 ?
Pb3 S24 3.222(8) 4_565 ?
Pb3 S16 3.400(11) 1_655 ?
Pb3 As14 3.866(12) 2_546 ?
Pb3 As20 3.893(7) 4_565 ?
Pb3 As21 4.02(3) . ?
Pb4 S23 2.884(13) 2 ?
Pb4 S20 2.900(18) 3_666 ?
Pb4 S4 2.945(15) 4_564 ?
Pb4 S1 3.005(14) 2_556 ?
Pb4 S5 3.044(16) . ?
Pb4 S24 3.095(8) 4_565 ?
Pb4 Cl25 3.222(3) 1_565 ?
Pb4 S26 3.254(19) 3_666 ?
Pb4 As22 3.784(9) 1_665 ?
Pb4 As15 3.825(5) 2_556 ?
Pb4 As20 3.875(7) 4_565 ?
Pb4 Pb10 4.0006(16) 2_556 ?
Pb5 S3 2.839(14) . ?
Pb5 S10 2.887(13) 2_546 ?
Pb5 S20 2.892(19) . ?
Pb5 S22 2.919(16) 4 ?
Pb5 S26 3.024(18) 3_556 ?
Pb5 S4 3.081(14) 2_546 ?
Pb5 As20 3.668(7) 4 ?
Pb5 As22 3.715(9) . ?
Pb5 As16 3.892(6) 2_546 ?
Pb5 Pb7 4.0192(17) 2_446 ?
Pb5 Pb7 4.0584(17) 2_546 ?
Pb5 Pb10 4.133(3) 4_454 ?
Pb6 S8 2.890(14) 2_456 ?
Pb6 S6 2.907(11) 2_446 ?
Pb6 S7 2.964(14) . ?
Pb6 S2 2.985(16) . ?
Pb6 S19 3.037(14) 2_556 ?
Pb6 S21 3.281(14) 2_556 ?
Pb6 S14 3.305(10) . ?
Pb6 As18 3.857(5) 2_446 ?
Pb6 Pb9 4.0197(16) 4_465 ?
Pb6 Pb9 4.0581(16) 4_565 ?
Pb6 Pb14 4.119(8) 2_546 ?
Pb7 S11 2.888(12) . ?
Pb7 S20 2.90(2) 2_556 ?
Pb7 S3 2.923(14) 2_556 ?
Pb7 S22 2.928(17) 3_566 ?
Pb7 S4 3.051(14) . ?
Pb7 S24 3.183(8) 3_566 ?
Pb7 Cl25 3.199(2) 2_456 ?
Pb7 S26 3.245(18) 4 ?
Pb7 As20 3.690(7) 3_566 ?
Pb7 As22 3.795(9) 2_556 ?
Pb7 As16 3.868(6) . ?
Pb8 S18 2.834(13) 2_556 ?
Pb8 S7 2.869(15) 1_655 ?
Pb8 S2 3.018(16) . ?
Pb8 S22 3.031(16) 3_666 ?
Pb8 S14 3.085(10) 2_546 ?
Pb8 S3 3.166(13) 2_556 ?
Pb8 S15 3.185(11) 3_666 ?
Pb8 As20 3.714(7) 3_666 ?
Pb8 Pb9 4.032(3) 4_565 ?
Pb8 As19 4.056(5) 2_546 ?
Pb9 S13 2.823(14) 3_576 ?
Pb9 S7 2.940(14) 4_564 ?
Pb9 S8 2.962(14) 3_566 ?
Pb9 S19 2.982(14) 3_566 ?
Pb9 S2 3.047(17) 4_464 ?
Pb9 S16 3.147(12) 4_564 ?
Pb9 S18 3.218(12) 3_566 ?
Pb9 As18 3.808(5) 3_576 ?
Pb9 Pb14 4.085(8) 3_576 ?
Pb10 S9 2.907(13) 1_556 ?
Pb10 S4 2.934(15) 3_667 ?
Pb10 S1 2.941(14) . ?
Pb10 S20 2.97(2) 4 ?
Pb10 S5 3.099(17) 2_546 ?
Pb10 S26 3.115(17) 4 ?
Pb10 As22 3.791(9) 2_556 ?
Pb10 As20 3.818(7) 3_666 ?
Pb10 As15 3.838(6) . ?
Pb11 S7 2.776(6) . ?
Pb11 S14 2.880(11) 2_446 ?
Pb11 S13 2.976(14) 2_446 ?
Pb11 S6 3.053(12) 2_446 ?
Pb11 S16 3.078(12) 2_546 ?
Pb11 S21 3.390(14) . ?
Pb11 As17 3.557(2) . ?
Pb11 S18 3.598(13) . ?
Pb11 As18 3.845(3) 2_446 ?
Pb11 As19 4.004(9) 2_546 ?
Pb11 S15 4.058(6) 3_566 ?
Pb11 As19 4.114(9) 2_446 ?
Pb12 S23 2.960(13) 3_566 ?
Pb12 S9 2.972(14) 3_566 ?
Pb12 S10 3.009(15) 1_655 ?
Pb12 S11 3.098(14) . ?
Pb12 S20 3.215(8) 2_556 ?
Pb12 S12 3.233(15) 1_565 ?
Pb12 S17 3.409(14) 1_665 ?
Pb12 As18 3.517(3) . ?
Pb12 As15 3.615(3) 1_565 ?
Pb12 As15 3.803(2) 3_567 ?
Pb12 As16 4.118(10) 1_655 ?
Pb12 As16 4.144(10) . ?
Pb13 S21 2.893(16) 2_556 ?
Pb13 S18 2.991(15) 2_456 ?
Pb13 S11 2.994(13) . ?
Pb13 S10 3.094(13) . ?
Pb13 Pb14 3.174(5) . ?
Pb13 S6 3.250(12) 1_455 ?
Pb13 S13 3.304(15) . ?
Pb13 As19 3.411(3) . ?
Pb13 S22 3.462(7) 3_566 ?
Pb13 As14 3.729(7) . ?
Pb13 As16 3.884(3) . ?
Pb13 As17 4.118(9) 2_556 ?
As14 Pb14 0.651(5) . ?
As14 S12 2.31(2) 1_565 ?
As14 S17 2.37(2) 1_565 ?
As14 S19 2.367(10) 1_565 ?
As14 As21 2.990(14) 2_456 ?
As14 As16 3.399(8) . ?
As14 S6 3.417(18) 1_455 ?
As14 S13 3.44(2) . ?
As14 Pb21 3.666(7) 2_456 ?
As14 S11 3.738(17) . ?
As14 S10 3.757(18) . ?
Pb14 S19 2.457(8) 1_565 ?
Pb14 S12 2.739(18) 1_565 ?
Pb14 S17 2.840(16) 1_565 ?
Pb14 S13 2.971(17) . ?
Pb14 S6 2.987(16) 1_455 ?
Pb14 As16 3.510(5) . ?
Pb14 S11 3.563(15) . ?
Pb14 As21 3.617(13) 2_456 ?
Pb14 S10 3.632(16) . ?
Pb14 As18 4.023(15) . ?
As15 S23 2.206(15) 1_556 ?
As15 S1 2.244(7) . ?
As15 S9 2.379(15) 1_556 ?
As15 As15 3.339(5) 3_557 ?
As15 S17 3.500(14) 1_655 ?
As15 S12 3.500(16) . ?
As15 S23 3.633(14) 3_556 ?
As15 S9 3.676(14) 3_556 ?
As16 S10 2.208(16) . ?
As16 S4 2.210(6) . ?
As16 S11 2.401(15) . ?
As16 S9 3.434(14) 3_466 ?
As16 S23 3.582(15) 3_566 ?
As16 As21 3.607(15) 2_456 ?
As16 Pb21 3.640(4) 2_456 ?
As16 S12 3.687(16) 1_565 ?
As16 S17 3.735(14) 1_565 ?
As17 S21 2.211(17) . ?
As17 S3 2.259(7) . ?
As17 S18 2.326(16) . ?
As17 S11 3.283(14) 2_446 ?
As17 S10 3.548(15) 2_546 ?
As17 As18 3.697(3) 2_446 ?
As17 S13 3.706(15) 2_446 ?
As17 S6 3.724(12) 2_446 ?
As18 S6 2.245(14) . ?
As18 S8 2.298(7) 1_565 ?
As18 S13 2.349(17) . ?
As18 S12 3.373(15) 1_565 ?
As18 S17 3.570(14) 1_665 ?
As18 S11 3.897(14) . ?
As18 S10 3.992(14) 1_655 ?
As19 S16 2.169(15) . ?
As19 S2 2.261(7) 2_456 ?
As19 S14 2.283(13) . ?
As19 S13 3.562(15) . ?
As19 S6 3.609(12) 1_455 ?
As19 S21 3.870(16) 2_556 ?
As19 S18 4.026(15) 2_456 ?
As20 S15 2.229(7) . ?
As20 S24 2.369(13) . ?
As20 S22 2.473(7) . ?
As20 S5 3.171(8) 4_464 ?
As21 Pb21 0.774(15) . ?
As21 S17 2.24(3) 2_556 ?
As21 S12 2.45(4) 2_556 ?
As21 S5 2.455(18) . ?
As21 S9 3.47(3) 2_455 ?
As21 S23 3.54(3) 2 ?
As21 Pb21 3.746(18) 3_566 ?
As21 S9 3.81(3) 4_455 ?
As21 S23 3.97(3) 4 ?
Pb21 S17 2.748(13) 2_556 ?
Pb21 S5 2.852(8) . ?
Pb21 S12 2.950(15) 2_556 ?
Pb21 Pb21 2.977(8) 3_566 ?
Pb21 S9 3.050(15) 2_455 ?
Pb21 S23 3.157(15) 2 ?
Pb21 S9 3.380(15) 4_455 ?
Pb21 S23 3.547(15) 4 ?
As22 S26 2.199(9) 3_556 ?
As22 S26 2.199(9) . ?
As22 Cl25 2.37(2) 1_455 ?
As22 S20 2.888(8) 3_556 ?
As22 S20 2.888(8) . ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
S7 Pb1 S15 83.4(3) . 3_566 ?
S7 Pb1 S2 86.8(4) . . ?
S15 Pb1 S2 131.6(2) 3_566 . ?
S7 Pb1 S22 85.3(4) . 3_566 ?
S15 Pb1 S22 69.8(3) 3_566 3_566 ?
S2 Pb1 S22 156.0(2) . 3_566 ?
S7 Pb1 S21 76.2(3) . 2_556 ?
S15 Pb1 S21 144.0(4) 3_566 2_556 ?
S2 Pb1 S21 76.9(3) . 2_556 ?
S22 Pb1 S21 79.2(3) 3_566 2_556 ?
S7 Pb1 S3 141.4(2) . 2_556 ?
S15 Pb1 S3 124.8(2) 3_566 2_556 ?
S2 Pb1 S3 90.3(4) . 2_556 ?
S22 Pb1 S3 81.9(4) 3_566 2_556 ?
S21 Pb1 S3 65.7(3) 2_556 2_556 ?
S7 Pb1 S16 85.8(3) . 2_546 ?
S15 Pb1 S16 65.7(3) 3_566 2_546 ?
S2 Pb1 S16 66.4(3) . 2_546 ?
S22 Pb1 S16 135.2(4) 3_566 2_546 ?
S21 Pb1 S16 139.9(3) 2_556 2_546 ?
S3 Pb1 S16 127.7(3) 2_556 2_546 ?
S7 Pb1 S24 140.2(3) . 3_566 ?
S15 Pb1 S24 60.4(2) 3_566 3_566 ?
S2 Pb1 S24 128.9(4) . 3_566 ?
S22 Pb1 S24 67.9(2) 3_566 3_566 ?
S21 Pb1 S24 123.5(3) 2_556 3_566 ?
S3 Pb1 S24 65.28(19) 2_556 3_566 ?
S16 Pb1 S24 93.0(2) 2_546 3_566 ?
S7 Pb1 As20 101.9(3) . 3_566 ?
S15 Pb1 As20 36.83(14) 3_566 3_566 ?
S2 Pb1 As20 162.4(2) . 3_566 ?
S22 Pb1 As20 41.37(15) 3_566 3_566 ?
S21 Pb1 As20 119.8(3) 2_556 3_566 ?
S3 Pb1 As20 92.1(2) 2_556 3_566 ?
S16 Pb1 As20 98.7(2) 2_546 3_566 ?
S24 Pb1 As20 38.9(2) 3_566 3_566 ?
S7 Pb1 As19 87.4(3) . 2_546 ?
S15 Pb1 As19 98.24(19) 3_566 2_546 ?
S2 Pb1 As19 33.89(15) . 2_546 ?
S22 Pb1 As19 166.6(3) 3_566 2_546 ?
S21 Pb1 As19 109.9(3) 2_556 2_546 ?
S3 Pb1 As19 110.5(3) 2_556 2_546 ?
S16 Pb1 As19 32.6(2) 2_546 2_546 ?
S24 Pb1 As19 112.10(16) 3_566 2_546 ?
As20 Pb1 As19 130.22(10) 3_566 2_546 ?
S7 Pb1 Pb8 45.3(3) . 1_455 ?
S15 Pb1 Pb8 51.3(2) 3_566 1_455 ?
S2 Pb1 Pb8 131.6(3) . 1_455 ?
S22 Pb1 Pb8 48.2(3) 3_566 1_455 ?
S21 Pb1 Pb8 94.3(3) 2_556 1_455 ?
S3 Pb1 Pb8 129.6(3) 2_556 1_455 ?
S16 Pb1 Pb8 97.9(3) 2_546 1_455 ?
S24 Pb1 Pb8 95.94(17) 3_566 1_455 ?
As20 Pb1 Pb8 57.04(15) 3_566 1_455 ?
As19 Pb1 Pb8 119.83(13) 2_546 1_455 ?
S7 Pb1 Pb8 134.1(3) . . ?
S15 Pb1 Pb8 129.8(3) 3_566 . ?
S2 Pb1 Pb8 48.0(3) . . ?
S22 Pb1 Pb8 131.7(3) 3_566 . ?
S21 Pb1 Pb8 84.6(3) 2_556 . ?
S3 Pb1 Pb8 50.0(3) 2_556 . ?
S16 Pb1 Pb8 82.8(3) 2_546 . ?
S24 Pb1 Pb8 84.83(17) 3_566 . ?
As20 Pb1 Pb8 123.71(17) 3_566 . ?
As19 Pb1 Pb8 60.48(12) 2_546 . ?
Pb8 Pb1 Pb8 178.90(13) 1_455 . ?
S17 Pb2 S5 71.3(3) 1_655 2_546 ?
S17 Pb2 S19 74.8(3) 1_655 1_655 ?
S5 Pb2 S19 86.0(4) 2_546 1_655 ?
S17 Pb2 S1 76.8(3) 1_655 . ?
S5 Pb2 S1 84.8(4) 2_546 . ?
S19 Pb2 S1 151.6(2) 1_655 . ?
S17 Pb2 S8 78.7(3) 1_655 . ?
S5 Pb2 S8 149.9(2) 2_546 . ?
S19 Pb2 S8 83.9(4) 1_655 . ?
S1 Pb2 S8 90.8(4) . . ?
S17 Pb2 S15 131.0(4) 1_655 3_666 ?
S5 Pb2 S15 72.0(3) 2_546 3_666 ?
S19 Pb2 S15 71.4(3) 1_655 3_666 ?
S1 Pb2 S15 130.1(2) . 3_666 ?
S8 Pb2 S15 130.1(2) . 3_666 ?
S17 Pb2 S14 137.9(3) 1_655 2_546 ?
S5 Pb2 S14 134.0(4) 2_546 2_546 ?
S19 Pb2 S14 74.8(2) 1_655 2_546 ?
S1 Pb2 S14 129.1(3) . 2_546 ?
S8 Pb2 S14 69.7(2) . 2_546 ?
S15 Pb2 S14 62.4(2) 3_666 2_546 ?
S17 Pb2 As20 125.0(3) 1_655 3_666 ?
S5 Pb2 As20 53.68(19) 2_546 3_666 ?
S19 Pb2 As20 100.6(3) 1_655 3_666 ?
S1 Pb2 As20 95.5(2) . 3_666 ?
S8 Pb2 As20 156.31(18) . 3_666 ?
S15 Pb2 As20 35.49(16) 3_666 3_666 ?
S14 Pb2 As20 88.83(18) 2_546 3_666 ?
S17 Pb2 As14 37.4(3) 1_655 1_645 ?
S5 Pb2 As14 73.3(3) 2_546 1_645 ?
S19 Pb2 As14 37.5(2) 1_655 1_645 ?
S1 Pb2 As14 114.1(2) . 1_645 ?
S8 Pb2 As14 81.5(3) . 1_645 ?
S15 Pb2 As14 100.9(3) 3_666 1_645 ?
S14 Pb2 As14 108.9(2) 2_546 1_645 ?
As20 Pb2 As14 116.1(3) 3_666 1_645 ?
S17 Pb2 As21 33.5(5) 1_655 2_546 ?
S5 Pb2 As21 38.0(4) 2_546 2_546 ?
S19 Pb2 As21 75.1(4) 1_655 2_546 ?
S1 Pb2 As21 81.3(5) . 2_546 ?
S8 Pb2 As21 111.9(4) . 2_546 ?
S15 Pb2 As21 102.7(6) 3_666 2_546 ?
S14 Pb2 As21 149.4(5) 2_546 2_546 ?
As20 Pb2 As21 91.6(4) 3_666 2_546 ?
As14 Pb2 As21 44.7(2) 1_645 2_546 ?
S17 Pb2 Pb3 84.9(3) 1_655 2_546 ?
S5 Pb2 Pb3 46.0(3) 2_546 2_546 ?
S19 Pb2 Pb3 46.2(3) 1_655 2_546 ?
S1 Pb2 Pb3 130.8(3) . 2_546 ?
S8 Pb2 Pb3 130.0(3) . 2_546 ?
S15 Pb2 Pb3 46.2(2) 3_666 2_546 ?
S14 Pb2 Pb3 94.4(2) 2_546 2_546 ?
As20 Pb2 Pb3 59.31(15) 3_666 2_546 ?
As14 Pb2 Pb3 58.5(3) 1_645 2_546 ?
As21 Pb2 Pb3 60.3(5) 2_546 2_546 ?
S17 Pb2 Pb3 95.3(3) 1_655 2_446 ?
S5 Pb2 Pb3 133.9(4) 2_546 2_446 ?
S19 Pb2 Pb3 134.1(3) 1_655 2_446 ?
S1 Pb2 Pb3 49.1(3) . 2_446 ?
S8 Pb2 Pb3 50.3(3) . 2_446 ?
S15 Pb2 Pb3 133.7(2) 3_666 2_446 ?
S14 Pb2 Pb3 85.6(2) 2_546 2_446 ?
As20 Pb2 Pb3 120.42(17) 3_666 2_446 ?
As14 Pb2 Pb3 121.7(3) 1_645 2_446 ?
As21 Pb2 Pb3 119.8(5) 2_546 2_446 ?
Pb3 Pb2 Pb3 179.74(15) 2_546 2_446 ?
S5 Pb3 S19 89.0(4) . 2_556 ?
S5 Pb3 S15 75.3(3) . 4_565 ?
S19 Pb3 S15 74.7(3) 2_556 4_565 ?
S5 Pb3 S12 74.5(3) . 2_556 ?
S19 Pb3 S12 73.7(3) 2_556 2_556 ?
S15 Pb3 S12 136.1(4) 4_565 2_556 ?
S5 Pb3 S1 84.4(4) . 2_556 ?
S19 Pb3 S1 151.3(2) 2_556 2_556 ?
S15 Pb3 S1 129.6(2) 4_565 2_556 ?
S12 Pb3 S1 77.6(3) 2_556 2_556 ?
S5 Pb3 S8 150.0(2) . 2_556 ?
S19 Pb3 S8 83.6(4) 2_556 2_556 ?
S15 Pb3 S8 129.6(2) 4_565 2_556 ?
S12 Pb3 S8 75.5(3) 2_556 2_556 ?
S1 Pb3 S8 88.3(3) 2_556 2_556 ?
S5 Pb3 S24 75.3(3) . 4_565 ?
S19 Pb3 S24 136.0(3) 2_556 4_565 ?
S15 Pb3 S24 61.7(2) 4_565 4_565 ?
S12 Pb3 S24 136.3(3) 2_556 4_565 ?
S1 Pb3 S24 68.8(2) 2_556 4_565 ?
S8 Pb3 S24 128.5(3) 2_556 4_565 ?
S5 Pb3 S16 138.8(4) . 1_655 ?
S19 Pb3 S16 73.6(3) 2_556 1_655 ?
S15 Pb3 S16 64.3(3) 4_565 1_655 ?
S12 Pb3 S16 131.6(3) 2_556 1_655 ?
S1 Pb3 S16 127.4(4) 2_556 1_655 ?
S8 Pb3 S16 66.1(2) 2_556 1_655 ?
S24 Pb3 S16 91.6(3) 4_565 1_655 ?
S5 Pb3 As14 74.3(3) . 2_546 ?
S19 Pb3 As14 37.7(2) 2_556 2_546 ?
S15 Pb3 As14 104.1(3) 4_565 2_546 ?
S12 Pb3 As14 36.8(4) 2_556 2_546 ?
S1 Pb3 As14 114.0(2) 2_556 2_546 ?
S8 Pb3 As14 82.3(3) 2_556 2_546 ?
S24 Pb3 As14 149.0(3) 4_565 2_546 ?
S16 Pb3 As14 107.3(2) 1_655 2_546 ?
S5 Pb3 As20 53.25(19) . 4_565 ?
S19 Pb3 As20 100.9(3) 2_556 4_565 ?
S15 Pb3 As20 34.59(15) 4_565 4_565 ?
S12 Pb3 As20 127.7(3) 2_556 4_565 ?
S1 Pb3 As20 97.4(2) 2_556 4_565 ?
S8 Pb3 As20 156.74(17) 2_556 4_565 ?
S24 Pb3 As20 37.4(2) 4_565 4_565 ?
S16 Pb3 As20 93.0(2) 1_655 4_565 ?
As14 Pb3 As20 115.2(3) 2_546 4_565 ?
S5 Pb3 As21 37.3(3) . . ?
S19 Pb3 As21 75.2(4) 2_556 . ?
S15 Pb3 As21 104.7(5) 4_565 . ?
S12 Pb3 As21 37.5(4) 2_556 . ?
S1 Pb3 As21 82.8(5) 2_556 . ?
S8 Pb3 As21 112.9(4) 2_556 . ?
S24 Pb3 As21 109.2(2) 4_565 . ?
S16 Pb3 As21 148.7(4) 1_655 . ?
As14 Pb3 As21 44.5(2) 2_546 . ?
As20 Pb3 As21 90.3(4) 4_565 . ?
S5 Pb3 Pb2 47.5(4) . 2_456 ?
S19 Pb3 Pb2 47.9(3) 2_556 2_456 ?
S15 Pb3 Pb2 49.3(2) 4_565 2_456 ?
S12 Pb3 Pb2 86.9(3) 2_556 2_456 ?
S1 Pb3 Pb2 131.9(3) 2_556 2_456 ?
S8 Pb3 Pb2 131.4(3) 2_556 2_456 ?
S24 Pb3 Pb2 95.28(18) 4_565 2_456 ?
S16 Pb3 Pb2 96.8(2) 1_655 2_456 ?
As14 Pb3 Pb2 58.9(3) 2_546 2_456 ?
As20 Pb3 Pb2 57.97(15) 4_565 2_456 ?
As21 Pb3 Pb2 59.3(5) . 2_456 ?
S23 Pb4 S20 79.1(3) 2 3_666 ?
S23 Pb4 S4 80.8(3) 2 4_564 ?
S20 Pb4 S4 87.0(5) 3_666 4_564 ?
S23 Pb4 S1 70.6(3) 2 2_556 ?
S20 Pb4 S1 90.5(5) 3_666 2_556 ?
S4 Pb4 S1 151.2(2) 4_564 2_556 ?
S23 Pb4 S5 80.6(3) 2 . ?
S20 Pb4 S5 159.8(2) 3_666 . ?
S4 Pb4 S5 89.1(5) 4_564 . ?
S1 Pb4 S5 83.4(5) 2_556 . ?
S23 Pb4 S24 136.8(3) 2 4_565 ?
S20 Pb4 S24 121.1(3) 3_666 4_565 ?
S4 Pb4 S24 133.1(3) 4_564 4_565 ?
S1 Pb4 S24 71.5(2) 2_556 4_565 ?
S5 Pb4 S24 75.2(2) . 4_565 ?
S23 Pb4 Cl25 142.5(3) 2 1_565 ?
S20 Pb4 Cl25 74.2(3) 3_666 1_565 ?
S4 Pb4 Cl25 72.1(2) 4_564 1_565 ?
S1 Pb4 Cl25 134.5(3) 2_556 1_565 ?
S5 Pb4 Cl25 123.2(3) . 1_565 ?
S24 Pb4 Cl25 80.29(16) 4_565 1_565 ?
S23 Pb4 S26 133.2(5) 2 3_666 ?
S20 Pb4 S26 72.7(4) 3_666 3_666 ?
S4 Pb4 S26 132.7(3) 4_564 3_666 ?
S1 Pb4 S26 73.1(3) 2_556 3_666 ?
S5 Pb4 S26 123.1(3) . 3_666 ?
S24 Pb4 S26 48.5(3) 4_565 3_666 ?
Cl25 Pb4 S26 61.5(3) 1_565 3_666 ?
S23 Pb4 As22 127.8(3) 2 1_665 ?
S20 Pb4 As22 49.05(19) 3_666 1_665 ?
S4 Pb4 As22 100.0(3) 4_564 1_665 ?
S1 Pb4 As22 99.9(3) 2_556 1_665 ?
S5 Pb4 As22 151.07(19) . 1_665 ?
S24 Pb4 As22 78.63(16) 4_565 1_665 ?
Cl25 Pb4 As22 38.5(3) 1_565 1_665 ?
S26 Pb4 As22 35.41(18) 3_666 1_665 ?
S23 Pb4 As15 34.9(3) 2 2_556 ?
S20 Pb4 As15 80.3(3) 3_666 2_556 ?
S4 Pb4 As15 115.68(18) 4_564 2_556 ?
S1 Pb4 As15 35.88(14) 2_556 2_556 ?
S5 Pb4 As15 83.6(3) . 2_556 ?
S24 Pb4 As15 106.22(17) 4_565 2_556 ?
Cl25 Pb4 As15 153.0(2) 1_565 2_556 ?
S26 Pb4 As15 102.7(3) 3_666 2_556 ?
As22 Pb4 As15 115.9(2) 1_665 2_556 ?
S23 Pb4 As20 133.5(3) 2 4_565 ?
S20 Pb4 As20 147.34(19) 3_666 4_565 ?
S4 Pb4 As20 98.3(3) 4_564 4_565 ?
S1 Pb4 As20 99.2(2) 2_556 4_565 ?
S5 Pb4 As20 52.90(19) . 4_565 ?
S24 Pb4 As20 37.7(2) 4_565 4_565 ?
Cl25 Pb4 As20 76.89(14) 1_565 4_565 ?
S26 Pb4 As20 80.4(4) 3_666 4_565 ?
As22 Pb4 As20 98.39(14) 1_665 4_565 ?
As15 Pb4 As20 124.38(10) 2_556 4_565 ?
S23 Pb4 Pb10 83.9(3) 2 2_556 ?
S20 Pb4 Pb10 47.7(4) 3_666 2_556 ?
S4 Pb4 Pb10 134.2(3) 4_564 2_556 ?
S1 Pb4 Pb10 47.0(3) 2_556 2_556 ?
S5 Pb4 Pb10 130.4(4) . 2_556 ?
S24 Pb4 Pb10 85.18(18) 4_565 2_556 ?
Cl25 Pb4 Pb10 96.7(2) 1_565 2_556 ?
S26 Pb4 Pb10 49.6(4) 3_666 2_556 ?
As22 Pb4 Pb10 58.2(2) 1_665 2_556 ?
As15 Pb4 Pb10 58.68(13) 2_556 2_556 ?
As20 Pb4 Pb10 122.85(16) 4_565 2_556 ?
S3 Pb5 S10 84.9(3) . 2_546 ?
S3 Pb5 S20 88.9(5) . . ?
S10 Pb5 S20 82.3(3) 2_546 . ?
S3 Pb5 S22 87.3(4) . 4 ?
S10 Pb5 S22 84.8(3) 2_546 4 ?
S20 Pb5 S22 166.9(2) . 4 ?
S3 Pb5 S26 73.2(4) . 3_556 ?
S10 Pb5 S26 148.5(5) 2_546 3_556 ?
S20 Pb5 S26 75.0(4) . 3_556 ?
S22 Pb5 S26 115.7(3) 4 3_556 ?
S3 Pb5 S4 152.9(2) . 2_546 ?
S10 Pb5 S4 68.0(3) 2_546 2_546 ?
S20 Pb5 S4 86.2(5) . 2_546 ?
S22 Pb5 S4 91.5(4) 4 2_546 ?
S26 Pb5 S4 130.5(3) 3_556 2_546 ?
S3 Pb5 As20 96.5(3) . 4 ?
S10 Pb5 As20 126.6(3) 2_546 4 ?
S20 Pb5 As20 150.9(2) . 4 ?
S22 Pb5 As20 42.22(15) 4 4 ?
S26 Pb5 As20 79.2(4) 3_556 4 ?
S4 Pb5 As20 100.6(3) 2_546 4 ?
S3 Pb5 As22 99.2(3) . . ?
S10 Pb5 As22 131.7(3) 2_546 . ?
S20 Pb5 As22 50.0(2) . . ?
S22 Pb5 As22 143.15(19) 4 . ?
S26 Pb5 As22 36.29(19) 3_556 . ?
S4 Pb5 As22 97.9(2) 2_546 . ?
As20 Pb5 As22 100.93(15) 4 . ?
S3 Pb5 As16 118.74(18) . 2_546 ?
S10 Pb5 As16 34.1(3) 2_546 2_546 ?
S20 Pb5 As16 87.9(4) . 2_546 ?
S22 Pb5 As16 82.9(3) 4 2_546 ?
S26 Pb5 As16 159.4(2) 3_556 2_546 ?
S4 Pb5 As16 34.54(13) 2_546 2_546 ?
As20 Pb5 As16 113.7(2) 4 2_546 ?
As22 Pb5 As16 123.13(11) . 2_546 ?
S3 Pb5 Pb7 46.6(3) . 2_446 ?
S10 Pb5 Pb7 95.9(3) 2_546 2_446 ?
S20 Pb5 Pb7 46.2(4) . 2_446 ?
S22 Pb5 Pb7 133.3(3) 4 2_446 ?
S26 Pb5 Pb7 52.6(4) 3_556 2_446 ?
S4 Pb5 Pb7 132.1(3) 2_546 2_446 ?
As20 Pb5 Pb7 123.27(17) 4 2_446 ?
As22 Pb5 Pb7 58.6(2) . 2_446 ?
As16 Pb5 Pb7 121.61(15) 2_546 2_446 ?
S3 Pb5 Pb7 132.8(3) . 2_546 ?
S10 Pb5 Pb7 83.6(3) 2_546 2_546 ?
S20 Pb5 Pb7 134.2(4) . 2_546 ?
S22 Pb5 Pb7 46.1(3) 4 2_546 ?
S26 Pb5 Pb7 127.9(4) 3_556 2_546 ?
S4 Pb5 Pb7 48.2(3) 2_546 2_546 ?
As20 Pb5 Pb7 56.78(15) 4 2_546 ?
As22 Pb5 Pb7 122.1(2) . 2_546 ?
As16 Pb5 Pb7 58.18(13) 2_546 2_546 ?
Pb7 Pb5 Pb7 179.30(12) 2_446 2_546 ?
S3 Pb5 Pb10 134.7(3) . 4_454 ?
S10 Pb5 Pb10 85.6(2) 2_546 4_454 ?
S20 Pb5 Pb10 45.8(4) . 4_454 ?
S22 Pb5 Pb10 135.7(3) 4 4_454 ?
S26 Pb5 Pb10 93.73(18) 3_556 4_454 ?
S4 Pb5 Pb10 45.1(3) 2_546 4_454 ?
As20 Pb5 Pb10 124.08(10) 4 4_454 ?
As22 Pb5 Pb10 57.47(10) . 4_454 ?
As16 Pb5 Pb10 65.80(7) 2_546 4_454 ?
Pb7 Pb5 Pb10 90.68(8) 2_446 4_454 ?
Pb7 Pb5 Pb10 89.81(7) 2_546 4_454 ?
S8 Pb6 S6 71.1(3) 2_456 2_446 ?
S8 Pb6 S7 90.9(4) 2_456 . ?
S6 Pb6 S7 81.5(3) 2_446 . ?
S8 Pb6 S2 150.2(2) 2_456 . ?
S6 Pb6 S2 79.1(3) 2_446 . ?
S7 Pb6 S2 84.7(4) . . ?
S8 Pb6 S19 86.1(4) 2_456 2_556 ?
S6 Pb6 S19 82.4(3) 2_446 2_556 ?
S7 Pb6 S19 163.8(2) . 2_556 ?
S2 Pb6 S19 90.1(4) . 2_556 ?
S8 Pb6 S21 130.9(4) 2_456 2_556 ?
S6 Pb6 S21 145.0(3) 2_446 2_556 ?
S7 Pb6 S21 72.5(3) . 2_556 ?
S2 Pb6 S21 75.6(3) . 2_556 ?
S19 Pb6 S21 121.0(4) 2_556 2_556 ?
S8 Pb6 S14 74.8(2) 2_456 . ?
S6 Pb6 S14 141.4(3) 2_446 . ?
S7 Pb6 S14 117.0(3) . . ?
S2 Pb6 S14 133.0(3) . . ?
S19 Pb6 S14 77.5(3) 2_556 . ?
S21 Pb6 S14 73.0(3) 2_556 . ?
S8 Pb6 As18 36.38(14) 2_456 2_446 ?
S6 Pb6 As18 35.4(3) 2_446 2_446 ?
S7 Pb6 As18 80.3(2) . 2_446 ?
S2 Pb6 As18 114.05(18) . 2_446 ?
S19 Pb6 As18 87.9(3) 2_556 2_446 ?
S21 Pb6 As18 150.3(3) 2_556 2_446 ?
S14 Pb6 As18 110.64(19) . 2_446 ?
S8 Pb6 Pb9 47.4(3) 2_456 4_465 ?
S6 Pb6 Pb9 84.4(3) 2_446 4_465 ?
S7 Pb6 Pb9 46.8(3) . 4_465 ?
S2 Pb6 Pb9 130.7(4) . 4_465 ?
S19 Pb6 Pb9 133.3(3) 2_556 4_465 ?
S21 Pb6 Pb9 94.1(3) 2_556 4_465 ?
S14 Pb6 Pb9 85.9(2) . 4_465 ?
As18 Pb6 Pb9 57.78(12) 2_446 4_465 ?
S8 Pb6 Pb9 132.9(3) 2_456 4_565 ?
S6 Pb6 Pb9 94.7(3) 2_446 4_565 ?
S7 Pb6 Pb9 132.4(3) . 4_565 ?
S2 Pb6 Pb9 48.4(4) . 4_565 ?
S19 Pb6 Pb9 47.0(3) 2_556 4_565 ?
S21 Pb6 Pb9 86.3(3) 2_556 4_565 ?
S14 Pb6 Pb9 95.3(2) . 4_565 ?
As18 Pb6 Pb9 121.62(14) 2_446 4_565 ?
Pb9 Pb6 Pb9 178.83(13) 4_465 4_565 ?
S8 Pb6 Pb1 134.4(3) 2_456 . ?
S6 Pb6 Pb1 95.5(2) 2_446 . ?
S7 Pb6 Pb1 43.6(3) . . ?
S2 Pb6 Pb1 47.5(3) . . ?
S19 Pb6 Pb1 136.6(3) 2_556 . ?
S21 Pb6 Pb1 49.5(2) 2_556 . ?
S14 Pb6 Pb1 121.69(18) . . ?
As18 Pb6 Pb1 114.92(8) 2_446 . ?
Pb9 Pb6 Pb1 89.10(7) 4_465 . ?
Pb9 Pb6 Pb1 90.34(7) 4_565 . ?
S8 Pb6 Pb14 80.2(3) 2_456 2_546 ?
S6 Pb6 Pb14 46.5(3) 2_446 2_546 ?
S7 Pb6 Pb14 127.45(18) . 2_546 ?
S2 Pb6 Pb14 79.3(2) . 2_546 ?
S19 Pb6 Pb14 36.34(17) 2_556 2_546 ?
S21 Pb6 Pb14 146.1(3) 2_556 2_546 ?
S14 Pb6 Pb14 110.2(2) . 2_546 ?
As18 Pb6 Pb14 62.13(19) 2_446 2_546 ?
Pb9 Pb6 Pb14 119.59(18) 4_465 2_546 ?
Pb9 Pb6 Pb14 59.93(17) 4_565 2_546 ?
Pb1 Pb6 Pb14 122.21(10) . 2_546 ?
S11 Pb7 S20 83.9(3) . 2_556 ?
S11 Pb7 S3 81.4(3) . 2_556 ?
S20 Pb7 S3 87.2(5) 2_556 2_556 ?
S11 Pb7 S22 83.8(3) . 3_566 ?
S20 Pb7 S22 167.6(2) 2_556 3_566 ?
S3 Pb7 S22 90.3(4) 2_556 3_566 ?
S11 Pb7 S4 72.6(3) . . ?
S20 Pb7 S4 85.1(5) 2_556 . ?
S3 Pb7 S4 153.6(2) 2_556 . ?
S22 Pb7 S4 91.9(4) 3_566 . ?
S11 Pb7 S24 141.5(3) . 3_566 ?
S20 Pb7 S24 119.3(3) 2_556 3_566 ?
S3 Pb7 S24 70.5(2) 2_556 3_566 ?
S22 Pb7 S24 70.9(3) 3_566 3_566 ?
S4 Pb7 S24 134.7(3) . 3_566 ?
S11 Pb7 Cl25 138.9(3) . 2_456 ?
S20 Pb7 Cl25 74.5(3) 2_556 2_456 ?
S3 Pb7 Cl25 130.6(3) 2_556 2_456 ?
S22 Pb7 Cl25 115.8(3) 3_566 2_456 ?
S4 Pb7 Cl25 71.1(2) . 2_456 ?
S24 Pb7 Cl25 79.34(15) 3_566 2_456 ?
S11 Pb7 S26 141.8(5) . 4 ?
S20 Pb7 S26 71.5(4) 2_556 4 ?
S3 Pb7 S26 68.9(3) 2_556 4 ?
S22 Pb7 S26 118.7(3) 3_566 4 ?
S4 Pb7 S26 131.3(3) . 4 ?
S24 Pb7 S26 47.9(3) 3_566 4 ?
Cl25 Pb7 S26 61.8(3) 2_456 4 ?
S11 Pb7 As20 125.6(3) . 3_566 ?
S20 Pb7 As20 150.41(19) 2_556 3_566 ?
S3 Pb7 As20 98.4(2) 2_556 3_566 ?
S22 Pb7 As20 41.95(15) 3_566 3_566 ?
S4 Pb7 As20 100.8(3) . 3_566 ?
S24 Pb7 As20 39.5(2) 3_566 3_566 ?
Cl25 Pb7 As20 79.97(14) 2_456 3_566 ?
S26 Pb7 As20 83.4(4) 4 3_566 ?
S11 Pb7 As22 132.7(3) . 2_556 ?
S20 Pb7 As22 48.89(19) 2_556 2_556 ?
S3 Pb7 As22 96.0(3) 2_556 2_556 ?
S22 Pb7 As22 143.46(19) 3_566 2_556 ?
S4 Pb7 As22 97.8(2) . 2_556 ?
S24 Pb7 As22 77.43(16) 3_566 2_556 ?
Cl25 Pb7 As22 38.5(3) 2_456 2_556 ?
S26 Pb7 As22 35.31(18) 4 2_556 ?
As20 Pb7 As22 101.53(14) 3_566 2_556 ?
S11 Pb7 As16 38.3(3) . . ?
S20 Pb7 As16 87.5(3) 2_556 . ?
S3 Pb7 As16 119.71(17) 2_556 . ?
S22 Pb7 As16 83.2(3) 3_566 . ?
S4 Pb7 As16 34.78(13) . . ?
S24 Pb7 As16 152.6(2) 3_566 . ?
Cl25 Pb7 As16 105.15(15) 2_456 . ?
S26 Pb7 As16 157.4(2) 4 . ?
As20 Pb7 As16 113.8(2) 3_566 . ?
As22 Pb7 As16 123.05(10) 2_556 . ?
S11 Pb7 Pb5 94.2(3) . 2_556 ?
S20 Pb7 Pb5 46.0(4) 2_556 2_556 ?
S3 Pb7 Pb5 44.9(3) 2_556 2_556 ?
S22 Pb7 Pb5 134.6(3) 3_566 2_556 ?
S4 Pb7 Pb5 130.8(3) . 2_556 ?
S24 Pb7 Pb5 84.29(17) 3_566 2_556 ?
Cl25 Pb7 Pb5 95.1(2) 2_456 2_556 ?
S26 Pb7 Pb5 47.7(4) 4 2_556 ?
As20 Pb7 Pb5 123.68(17) 3_566 2_556 ?
As22 Pb7 Pb5 56.7(2) 2_556 2_556 ?
As16 Pb7 Pb5 121.45(15) . 2_556 ?
S18 Pb8 S7 77.3(3) 2_556 1_655 ?
S18 Pb8 S2 77.0(3) 2_556 . ?
S7 Pb8 S2 89.0(4) 1_655 . ?
S18 Pb8 S22 80.4(3) 2_556 3_666 ?
S7 Pb8 S22 85.0(4) 1_655 3_666 ?
S2 Pb8 S22 157.4(2) . 3_666 ?
S18 Pb8 S14 138.1(3) 2_556 2_546 ?
S7 Pb8 S14 81.8(2) 1_655 2_546 ?
S2 Pb8 S14 66.8(3) . 2_546 ?
S22 Pb8 S14 133.4(3) 3_666 2_546 ?
S18 Pb8 S3 66.2(3) 2_556 2_556 ?
S7 Pb8 S3 142.2(2) 1_655 2_556 ?
S2 Pb8 S3 92.0(4) . 2_556 ?
S22 Pb8 S3 79.7(4) 3_666 2_556 ?
S14 Pb8 S3 132.6(3) 2_546 2_556 ?
S18 Pb8 S15 141.2(4) 2_556 3_666 ?
S7 Pb8 S15 78.7(3) 1_655 3_666 ?
S2 Pb8 S15 132.6(2) . 3_666 ?
S22 Pb8 S15 67.4(3) 3_666 3_666 ?
S14 Pb8 S15 66.2(3) 2_546 3_666 ?
S3 Pb8 S15 124.9(2) 2_556 3_666 ?
S18 Pb8 As20 121.2(3) 2_556 3_666 ?
S7 Pb8 As20 100.9(3) 1_655 3_666 ?
S2 Pb8 As20 160.7(2) . 3_666 ?
S22 Pb8 As20 41.49(15) 3_666 3_666 ?
S14 Pb8 As20 98.1(2) 2_546 3_666 ?
S3 Pb8 As20 90.2(2) 2_556 3_666 ?
S15 Pb8 As20 36.69(14) 3_666 3_666 ?
S18 Pb8 Pb9 52.4(2) 2_556 4_565 ?
S7 Pb8 Pb9 46.8(3) 1_655 4_565 ?
S2 Pb8 Pb9 48.7(3) . 4_565 ?
S22 Pb8 Pb9 114.67(19) 3_666 4_565 ?
S14 Pb8 Pb9 87.07(19) 2_546 4_565 ?
S3 Pb8 Pb9 110.62(14) 2_556 4_565 ?
S15 Pb8 Pb9 122.81(17) 3_666 4_565 ?
As20 Pb8 Pb9 146.42(16) 3_666 4_565 ?
S18 Pb8 Pb1 95.7(3) 2_556 1_655 ?
S7 Pb8 Pb1 44.1(3) 1_655 1_655 ?
S2 Pb8 Pb1 132.5(4) . 1_655 ?
S22 Pb8 Pb1 48.9(3) 3_666 1_655 ?
S14 Pb8 Pb1 93.9(2) 2_546 1_655 ?
S3 Pb8 Pb1 128.3(3) 2_556 1_655 ?
S15 Pb8 Pb1 46.7(2) 3_666 1_655 ?
As20 Pb8 Pb1 57.14(16) 3_666 1_655 ?
Pb9 Pb8 Pb1 89.51(8) 4_565 1_655 ?
S18 Pb8 Pb1 85.4(3) 2_556 . ?
S7 Pb8 Pb1 136.5(3) 1_655 . ?
S2 Pb8 Pb1 47.9(4) . . ?
S22 Pb8 Pb1 131.3(3) 3_666 . ?
S14 Pb8 Pb1 85.4(2) 2_546 . ?
S3 Pb8 Pb1 52.0(3) 2_556 . ?
S15 Pb8 Pb1 132.2(2) 3_666 . ?
As20 Pb8 Pb1 122.10(17) 3_666 . ?
Pb9 Pb8 Pb1 91.30(7) 4_565 . ?
Pb1 Pb8 Pb1 178.90(13) 1_655 . ?
S18 Pb8 As19 109.5(3) 2_556 2_546 ?
S7 Pb8 As19 89.2(2) 1_655 2_546 ?
S2 Pb8 As19 33.37(15) . 2_546 ?
S22 Pb8 As19 167.1(3) 3_666 2_546 ?
S14 Pb8 As19 33.9(2) 2_546 2_546 ?
S3 Pb8 As19 111.5(3) 2_556 2_546 ?
S15 Pb8 As19 100.17(18) 3_666 2_546 ?
As20 Pb8 As19 129.33(10) 3_666 2_546 ?
Pb9 Pb8 As19 68.30(6) 4_565 2_546 ?
Pb1 Pb8 As19 120.21(13) 1_655 2_546 ?
Pb1 Pb8 As19 59.47(12) . 2_546 ?
S13 Pb9 S7 81.8(3) 3_576 4_564 ?
S13 Pb9 S8 74.8(3) 3_576 3_566 ?
S7 Pb9 S8 89.9(4) 4_564 3_566 ?
S13 Pb9 S19 83.1(3) 3_576 3_566 ?
S7 Pb9 S19 164.9(2) 4_564 3_566 ?
S8 Pb9 S19 85.7(4) 3_566 3_566 ?
S13 Pb9 S2 77.5(4) 3_576 4_464 ?
S7 Pb9 S2 87.2(4) 4_564 4_464 ?
S8 Pb9 S2 152.3(2) 3_566 4_464 ?
S19 Pb9 S2 89.9(4) 3_566 4_464 ?
S13 Pb9 S16 141.8(3) 3_576 4_564 ?
S7 Pb9 S16 115.7(3) 4_564 4_564 ?
S8 Pb9 S16 71.7(3) 3_566 4_564 ?
S19 Pb9 S16 76.6(3) 3_566 4_564 ?
S2 Pb9 S16 133.6(3) 4_464 4_564 ?
S13 Pb9 S18 138.6(4) 3_576 3_566 ?
S7 Pb9 S18 70.5(3) 4_564 3_566 ?
S8 Pb9 S18 133.2(4) 3_566 3_566 ?
S19 Pb9 S18 122.4(4) 3_566 3_566 ?
S2 Pb9 S18 71.1(3) 4_464 3_566 ?
S16 Pb9 S18 79.3(3) 4_564 3_566 ?
S13 Pb9 As18 38.0(3) 3_576 3_576 ?
S7 Pb9 As18 81.5(2) 4_564 3_576 ?
S8 Pb9 As18 37.10(15) 3_566 3_576 ?
S19 Pb9 As18 86.4(3) 3_566 3_576 ?
S2 Pb9 As18 115.39(19) 4_464 3_576 ?
S16 Pb9 As18 107.9(2) 4_564 3_576 ?
S18 Pb9 As18 151.1(3) 3_566 3_576 ?
S13 Pb9 Pb6 87.1(3) 3_576 4_564 ?
S7 Pb9 Pb6 47.3(3) 4_564 4_564 ?
S8 Pb9 Pb6 45.9(3) 3_566 4_564 ?
S19 Pb9 Pb6 131.4(3) 3_566 4_564 ?
S2 Pb9 Pb6 133.9(3) 4_464 4_564 ?
S16 Pb9 Pb6 82.7(3) 4_564 4_564 ?
S18 Pb9 Pb6 95.5(3) 3_566 4_564 ?
As18 Pb9 Pb6 58.97(12) 3_576 4_564 ?
S13 Pb9 Pb8 94.4(3) 3_576 4_464 ?
S7 Pb9 Pb8 45.3(3) 4_564 4_464 ?
S8 Pb9 Pb8 135.3(3) 3_566 4_464 ?
S19 Pb9 Pb8 136.9(3) 3_566 4_464 ?
S2 Pb9 Pb8 48.0(3) 4_464 4_464 ?
S16 Pb9 Pb8 122.4(2) 4_564 4_464 ?
S18 Pb9 Pb8 44.3(2) 3_566 4_464 ?
As18 Pb9 Pb8 117.21(8) 3_576 4_464 ?
Pb6 Pb9 Pb8 91.17(7) 4_564 4_464 ?
S13 Pb9 Pb6 93.9(3) 3_576 4_464 ?
S7 Pb9 Pb6 133.4(3) 4_564 4_464 ?
S8 Pb9 Pb6 133.8(3) 3_566 4_464 ?
S19 Pb9 Pb6 48.2(3) 3_566 4_464 ?
S2 Pb9 Pb6 47.1(3) 4_464 4_464 ?
S16 Pb9 Pb6 96.1(3) 4_564 4_464 ?
S18 Pb9 Pb6 84.2(3) 3_566 4_464 ?
As18 Pb9 Pb6 121.63(14) 3_576 4_464 ?
Pb6 Pb9 Pb6 178.83(13) 4_564 4_464 ?
Pb8 Pb9 Pb6 89.37(7) 4_464 4_464 ?
S13 Pb9 Pb14 46.7(3) 3_576 3_576 ?
S7 Pb9 Pb14 128.33(17) 4_564 3_576 ?
S8 Pb9 Pb14 81.1(3) 3_566 3_576 ?
S19 Pb9 Pb14 36.66(17) 3_566 3_576 ?
S2 Pb9 Pb14 79.3(2) 4_464 3_576 ?
S16 Pb9 Pb14 109.3(2) 4_564 3_576 ?
S18 Pb9 Pb14 144.3(3) 3_566 3_576 ?
As18 Pb9 Pb14 61.18(19) 3_576 3_576 ?
Pb6 Pb9 Pb14 119.69(18) 4_564 3_576 ?
Pb8 Pb9 Pb14 122.66(11) 4_464 3_576 ?
Pb6 Pb9 Pb14 60.77(17) 4_464 3_576 ?
S9 Pb10 S4 78.5(3) 1_556 3_667 ?
S9 Pb10 S1 73.3(3) 1_556 . ?
S4 Pb10 S1 151.6(2) 3_667 . ?
S9 Pb10 S20 79.9(3) 1_556 4 ?
S4 Pb10 S20 87.6(5) 3_667 4 ?
S1 Pb10 S20 90.5(5) . 4 ?
S9 Pb10 S5 81.1(3) 1_556 2_546 ?
S4 Pb10 S5 88.2(4) 3_667 2_546 ?
S1 Pb10 S5 84.4(4) . 2_546 ?
S20 Pb10 S5 161.0(2) 4 2_546 ?
S9 Pb10 S26 139.2(5) 1_556 4 ?
S4 Pb10 S26 130.1(3) 3_667 4 ?
S1 Pb10 S26 76.0(4) . 4 ?
S20 Pb10 S26 74.0(4) 4 4 ?
S5 Pb10 S26 122.1(3) 2_546 4 ?
S9 Pb10 As22 128.6(3) 1_556 2_556 ?
S4 Pb10 As22 98.9(3) 3_667 2_556 ?
S1 Pb10 As22 101.0(3) . 2_556 ?
S20 Pb10 As22 48.76(19) 4 2_556 ?
S5 Pb10 As22 150.2(2) 2_546 2_556 ?
S26 Pb10 As22 35.46(18) 4 2_556 ?
S9 Pb10 As20 134.4(3) 1_556 3_666 ?
S4 Pb10 As20 99.7(3) 3_667 3_666 ?
S1 Pb10 As20 97.7(2) . 3_666 ?
S20 Pb10 As20 145.7(2) 4 3_666 ?
S5 Pb10 As20 53.34(18) 2_546 3_666 ?
S26 Pb10 As20 75.8(4) 4 3_666 ?
As22 Pb10 As20 96.91(15) 2_556 3_666 ?
S9 Pb10 As15 38.3(3) 1_556 . ?
S4 Pb10 As15 116.58(19) 3_667 . ?
S1 Pb10 As15 35.65(14) . . ?
S20 Pb10 As15 79.3(3) 4 . ?
S5 Pb10 As15 86.0(3) 2_546 . ?
S26 Pb10 As15 105.2(4) 4 . ?
As22 Pb10 As15 115.4(2) 2_556 . ?
As20 Pb10 As15 124.68(10) 3_666 . ?
S9 Pb10 Pb4 86.6(3) 1_556 2_446 ?
S4 Pb10 Pb4 133.6(3) 3_667 2_446 ?
S1 Pb10 Pb4 48.4(3) . 2_446 ?
S20 Pb10 Pb4 46.3(4) 4 2_446 ?
S5 Pb10 Pb4 132.8(4) 2_546 2_446 ?
S26 Pb10 Pb4 52.6(4) 4 2_446 ?
As22 Pb10 Pb4 58.0(2) 2_556 2_446 ?
As20 Pb10 Pb4 121.15(16) 3_666 2_446 ?
As15 Pb10 Pb4 58.38(12) . 2_446 ?
S9 Pb10 Pb4 93.9(3) 1_556 2_546 ?
S4 Pb10 Pb4 46.2(3) 3_667 2_546 ?
S1 Pb10 Pb4 132.2(3) . 2_546 ?
S20 Pb10 Pb4 133.3(4) 4 2_546 ?
S5 Pb10 Pb4 47.8(3) 2_546 2_546 ?
S26 Pb10 Pb4 126.8(4) 4 2_546 ?
As22 Pb10 Pb4 121.2(2) 2_556 2_546 ?
As20 Pb10 Pb4 58.68(15) 3_666 2_546 ?
As15 Pb10 Pb4 122.36(14) . 2_546 ?
Pb4 Pb10 Pb4 179.24(14) 2_446 2_546 ?
S9 Pb10 Pb5 91.6(2) 1_556 4 ?
S4 Pb10 Pb5 48.1(3) 3_667 4 ?
S1 Pb10 Pb5 134.8(3) . 4 ?
S20 Pb10 Pb5 44.4(4) 4 4 ?
S5 Pb10 Pb5 136.1(3) 2_546 4 ?
S26 Pb10 Pb5 91.14(17) 4 4 ?
As22 Pb10 Pb5 55.73(10) 2_556 4 ?
As20 Pb10 Pb5 121.21(10) 3_666 4 ?
As15 Pb10 Pb5 114.09(8) . 4 ?
Pb4 Pb10 Pb5 89.32(8) 2_446 4 ?
Pb4 Pb10 Pb5 90.19(8) 2_546 4 ?
S7 Pb11 S14 87.2(4) . 2_446 ?
S7 Pb11 S13 81.9(4) . 2_446 ?
S14 Pb11 S13 89.4(4) 2_446 2_446 ?
S7 Pb11 S6 82.1(3) . 2_446 ?
S14 Pb11 S6 160.6(3) 2_446 2_446 ?
S13 Pb11 S6 73.17(17) 2_446 2_446 ?
S7 Pb11 S16 90.0(4) . 2_546 ?
S14 Pb11 S16 104.12(18) 2_446 2_546 ?
S13 Pb11 S16 164.0(4) 2_446 2_546 ?
S6 Pb11 S16 92.1(3) 2_446 2_546 ?
S7 Pb11 S21 145.6(5) . . ?
S14 Pb11 S21 76.8(3) 2_446 . ?
S13 Pb11 S21 67.8(4) 2_446 . ?
S6 Pb11 S21 103.3(3) 2_446 . ?
S16 Pb11 S21 123.1(3) 2_546 . ?
S7 Pb11 As17 142.60(13) . . ?
S14 Pb11 As17 113.8(2) 2_446 . ?
S13 Pb11 As17 68.5(3) 2_446 . ?
S6 Pb11 As17 68.1(2) 2_446 . ?
S16 Pb11 As17 112.3(2) 2_546 . ?
S21 Pb11 As17 37.0(3) . . ?
S7 Pb11 S18 148.0(5) . . ?
S14 Pb11 S18 123.3(3) 2_446 . ?
S13 Pb11 S18 105.5(3) 2_446 . ?
S6 Pb11 S18 71.0(3) 2_446 . ?
S16 Pb11 S18 74.5(3) 2_546 . ?
S21 Pb11 S18 60.62(18) . . ?
As17 Pb11 S18 37.9(2) . . ?
S7 Pb11 As18 82.82(13) . 2_446 ?
S14 Pb11 As18 126.9(3) 2_446 2_446 ?
S13 Pb11 As18 37.6(3) 2_446 2_446 ?
S6 Pb11 As18 35.7(3) 2_446 2_446 ?
S16 Pb11 As18 127.8(3) 2_546 2_446 ?
S21 Pb11 As18 82.9(2) . 2_446 ?
As17 Pb11 As18 59.78(5) . 2_446 ?
S18 Pb11 As18 85.0(2) . 2_446 ?
S7 Pb11 As19 88.2(4) . 2_546 ?
S14 Pb11 As19 136.3(2) 2_446 2_546 ?
S13 Pb11 As19 132.8(3) 2_446 2_546 ?
S6 Pb11 As19 59.7(2) 2_446 2_546 ?
S16 Pb11 As19 32.5(2) 2_546 2_546 ?
S21 Pb11 As19 124.2(3) . 2_546 ?
As17 Pb11 As19 95.32(15) . 2_546 ?
S18 Pb11 As19 63.7(3) . 2_546 ?
As18 Pb11 As19 95.43(14) 2_446 2_546 ?
S7 Pb11 S15 65.42(15) . 3_566 ?
S14 Pb11 S15 56.1(3) 2_446 3_566 ?
S13 Pb11 S15 131.8(3) 2_446 3_566 ?
S6 Pb11 S15 131.1(3) 2_446 3_566 ?
S16 Pb11 S15 54.6(3) 2_546 3_566 ?
S21 Pb11 S15 124.3(3) . 3_566 ?
As17 Pb11 S15 151.98(10) . 3_566 ?
S18 Pb11 S15 121.2(2) . 3_566 ?
As18 Pb11 S15 148.20(10) 2_446 3_566 ?
As19 Pb11 S15 82.7(2) 2_546 3_566 ?
S7 Pb11 As19 89.3(4) . 2_446 ?
S14 Pb11 As19 32.4(2) 2_446 2_446 ?
S13 Pb11 As19 57.7(3) 2_446 2_446 ?
S6 Pb11 As19 130.8(2) 2_446 2_446 ?
S16 Pb11 As19 136.5(2) 2_546 2_446 ?
S21 Pb11 As19 61.2(3) . 2_446 ?
As17 Pb11 As19 93.44(15) . 2_446 ?
S18 Pb11 As19 121.3(3) . 2_446 ?
As18 Pb11 As19 95.28(14) 2_446 2_446 ?
As19 Pb11 As19 168.60(6) 2_546 2_446 ?
S15 Pb11 As19 86.2(2) 3_566 2_446 ?
S23 Pb12 S9 72.9(2) 3_566 3_566 ?
S23 Pb12 S10 144.9(4) 3_566 1_655 ?
S9 Pb12 S10 84.6(4) 3_566 1_655 ?
S23 Pb12 S11 90.7(4) 3_566 . ?
S9 Pb12 S11 149.4(3) 3_566 . ?
S10 Pb12 S11 95.8(2) 1_655 . ?
S23 Pb12 S20 73.1(4) 3_566 2_556 ?
S9 Pb12 S20 75.0(4) 3_566 2_556 ?
S10 Pb12 S20 75.2(4) 1_655 2_556 ?
S11 Pb12 S20 75.6(4) . 2_556 ?
S23 Pb12 S12 80.0(4) 3_566 1_565 ?
S9 Pb12 S12 127.7(4) 3_566 1_565 ?
S10 Pb12 S12 134.7(3) 1_655 1_565 ?
S11 Pb12 S12 72.0(4) . 1_565 ?
S20 Pb12 S12 137.2(6) 2_556 1_565 ?
S23 Pb12 S17 124.5(3) 3_566 1_665 ?
S9 Pb12 S17 75.5(3) 3_566 1_665 ?
S10 Pb12 S17 72.8(3) 1_655 1_665 ?
S11 Pb12 S17 133.9(3) . 1_665 ?
S20 Pb12 S17 138.0(6) 2_556 1_665 ?
S12 Pb12 S17 84.82(19) 1_565 1_665 ?
S23 Pb12 As18 139.2(3) 3_566 . ?
S9 Pb12 As18 136.5(3) 3_566 . ?
S10 Pb12 As18 75.0(3) 1_655 . ?
S11 Pb12 As18 71.9(2) . . ?
S20 Pb12 As18 132.69(14) 2_556 . ?
S12 Pb12 As18 59.8(3) 1_565 . ?
S17 Pb12 As18 62.0(2) 1_665 . ?
S23 Pb12 As15 66.2(3) 3_566 1_565 ?
S9 Pb12 As15 67.0(3) 3_566 1_565 ?
S10 Pb12 As15 128.9(3) 1_655 1_565 ?
S11 Pb12 As15 130.2(3) . 1_565 ?
S20 Pb12 As15 130.42(13) 2_556 1_565 ?
S12 Pb12 As15 61.2(3) 1_565 1_565 ?
S17 Pb12 As15 59.7(2) 1_665 1_565 ?
As18 Pb12 As15 96.87(6) . 1_565 ?
S23 Pb12 As15 35.4(3) 3_566 3_567 ?
S9 Pb12 As15 38.7(3) 3_566 3_567 ?
S10 Pb12 As15 121.7(3) 1_655 3_567 ?
S11 Pb12 As15 124.9(3) . 3_567 ?
S20 Pb12 As15 77.00(13) 2_556 3_567 ?
S12 Pb12 As15 99.5(2) 1_565 3_567 ?
S17 Pb12 As15 97.4(2) 1_665 3_567 ?
As18 Pb12 As15 150.30(7) . 3_567 ?
As15 Pb12 As15 53.42(6) 1_565 3_567 ?
S23 Pb12 As16 126.1(3) 3_566 1_655 ?
S9 Pb12 As16 55.1(3) 3_566 1_655 ?
S10 Pb12 As16 31.5(3) 1_655 1_655 ?
S11 Pb12 As16 126.5(3) . 1_655 ?
S20 Pb12 As16 80.0(5) 2_556 1_655 ?
S12 Pb12 As16 142.5(3) 1_565 1_655 ?
S17 Pb12 As16 58.6(2) 1_665 1_655 ?
As18 Pb12 As16 92.73(16) . 1_655 ?
As15 Pb12 As16 101.77(16) 1_565 1_655 ?
As15 Pb12 As16 93.78(14) 3_567 1_655 ?
S23 Pb12 As16 57.7(3) 3_566 . ?
S9 Pb12 As16 129.0(3) 3_566 . ?
S10 Pb12 As16 129.4(3) 1_655 . ?
S11 Pb12 As16 35.1(2) . . ?
S20 Pb12 As16 79.0(5) 2_556 . ?
S12 Pb12 As16 58.4(3) 1_565 . ?
S17 Pb12 As16 143.0(2) 1_665 . ?
As18 Pb12 As16 92.72(16) . . ?
As15 Pb12 As16 100.98(16) 1_565 . ?
As15 Pb12 As16 93.09(14) 3_567 . ?
As16 Pb12 As16 155.77(8) 1_655 . ?
S21 Pb13 S18 101.9(2) 2_556 2_456 ?
S21 Pb13 S11 81.9(4) 2_556 . ?
S18 Pb13 S11 142.9(3) 2_456 . ?
S21 Pb13 S10 144.3(4) 2_556 . ?
S18 Pb13 S10 86.6(4) 2_456 . ?
S11 Pb13 S10 71.5(2) . . ?
S21 Pb13 Pb14 122.3(4) 2_556 . ?
S18 Pb13 Pb14 130.6(4) 2_456 . ?
S11 Pb13 Pb14 70.5(3) . . ?
S10 Pb13 Pb14 70.8(3) . . ?
S21 Pb13 S6 140.2(3) 2_556 1_455 ?
S18 Pb13 S6 76.9(4) 2_456 1_455 ?
S11 Pb13 S6 123.2(3) . 1_455 ?
S10 Pb13 S6 75.5(3) . 1_455 ?
Pb14 Pb13 S6 55.4(3) . 1_455 ?
S21 Pb13 S13 69.9(4) 2_556 . ?
S18 Pb13 S13 141.7(3) 2_456 . ?
S11 Pb13 S13 74.7(3) . . ?
S10 Pb13 S13 122.5(4) . . ?
Pb14 Pb13 S13 54.5(3) . . ?
S6 Pb13 S13 86.44(16) 1_455 . ?
S21 Pb13 As19 75.2(3) 2_556 . ?
S18 Pb13 As19 77.6(2) 2_456 . ?
S11 Pb13 As19 137.5(3) . . ?
S10 Pb13 As19 140.3(3) . . ?
Pb14 Pb13 As19 92.28(10) . . ?
S6 Pb13 As19 65.6(2) 1_455 . ?
S13 Pb13 As19 64.1(2) . . ?
S21 Pb13 S22 76.8(4) 2_556 3_566 ?
S18 Pb13 S22 71.5(4) 2_456 3_566 ?
S11 Pb13 S22 73.6(3) . 3_566 ?
S10 Pb13 S22 73.1(3) . 3_566 ?
Pb14 Pb13 S22 135.24(14) . 3_566 ?
S6 Pb13 S22 136.2(5) 1_455 3_566 ?
S13 Pb13 S22 136.5(5) . 3_566 ?
As19 Pb13 S22 132.47(12) . 3_566 ?
S21 Pb13 As14 124.2(4) 2_556 . ?
S18 Pb13 As14 131.3(4) 2_456 . ?
S11 Pb13 As14 66.5(3) . . ?
S10 Pb13 As14 66.0(3) . . ?
Pb14 Pb13 As14 5.65(16) . . ?
S6 Pb13 As14 58.1(3) 1_455 . ?
S13 Pb13 As14 58.2(4) . . ?
As19 Pb13 As14 97.91(12) . . ?
S22 Pb13 As14 129.62(15) 3_566 . ?
S21 Pb13 As16 119.1(3) 2_556 . ?
S18 Pb13 As16 119.5(3) 2_456 . ?
S11 Pb13 As16 38.2(3) . . ?
S10 Pb13 As16 34.6(3) . . ?
Pb14 Pb13 As16 58.62(9) . . ?
S6 Pb13 As16 94.0(2) 1_455 . ?
S13 Pb13 As16 95.7(2) . . ?
As19 Pb13 As16 150.89(8) . . ?
S22 Pb13 As16 76.65(12) 3_566 . ?
As14 Pb13 As16 52.98(12) . . ?
S21 Pb13 As17 30.9(3) 2_556 2_556 ?
S18 Pb13 As17 129.7(3) 2_456 2_556 ?
S11 Pb13 As17 52.1(3) . 2_556 ?
S10 Pb13 As17 121.9(3) . 2_556 ?
Pb14 Pb13 As17 99.1(3) . 2_556 ?
S6 Pb13 As17 145.1(2) 1_455 2_556 ?
S13 Pb13 As17 58.7(3) . 2_556 ?
As19 Pb13 As17 95.60(16) . 2_556 ?
S22 Pb13 As17 78.4(4) 3_566 2_556 ?
As14 Pb13 As17 99.0(3) . 2_556 ?
As16 Pb13 As17 90.26(15) . 2_556 ?
Pb14 As14 S12 125(3) . 1_565 ?
Pb14 As14 S17 132(3) . 1_565 ?
S12 As14 S17 100.7(4) 1_565 1_565 ?
Pb14 As14 S19 90.2(10) . 1_565 ?
S12 As14 S19 99.3(7) 1_565 1_565 ?
S17 As14 S19 98.5(7) 1_565 1_565 ?
Pb14 As14 As21 162.9(11) . 2_456 ?
S12 As14 As21 53.3(8) 1_565 2_456 ?
S17 As14 As21 47.6(8) 1_565 2_456 ?
S19 As14 As21 106.9(4) 1_565 2_456 ?
Pb14 As14 As16 94.5(10) . . ?
S12 As14 As16 77.8(5) 1_565 . ?
S17 As14 As16 78.5(4) 1_565 . ?
S19 As14 As16 175.3(3) 1_565 . ?
As21 As14 As16 68.4(4) 2_456 . ?
Pb14 As14 S6 44(2) . 1_455 ?
S12 As14 S6 169.2(7) 1_565 1_455 ?
S17 As14 S6 89.2(7) 1_565 1_455 ?
S19 As14 S6 83.2(5) 1_565 1_455 ?
As21 As14 S6 136.2(10) 2_456 1_455 ?
As16 As14 S6 100.4(4) . 1_455 ?
Pb14 As14 S13 40(2) . . ?
S12 As14 S13 88.2(7) 1_565 . ?
S17 As14 S13 171.0(7) 1_565 . ?
S19 As14 S13 80.8(5) 1_565 . ?
As21 As14 S13 141.3(10) 2_456 . ?
As16 As14 S13 102.7(4) . . ?
S6 As14 S13 81.8(2) 1_455 . ?
Pb14 As14 Pb21 156.4(11) . 2_456 ?
S12 As14 Pb21 53.5(4) 1_565 2_456 ?
S17 As14 Pb21 48.5(3) 1_565 2_456 ?
S19 As14 Pb21 113.4(3) 1_565 2_456 ?
As21 As14 Pb21 6.5(4) 2_456 2_456 ?
As16 As14 Pb21 61.89(13) . 2_456 ?
S6 As14 Pb21 135.1(6) 1_455 2_456 ?
S13 As14 Pb21 139.9(6) . 2_456 ?
Pb14 As14 Pb13 28.7(9) . . ?
S12 As14 Pb13 116.6(6) 1_565 . ?
S17 As14 Pb13 119.1(6) 1_565 . ?
S19 As14 Pb13 118.8(3) 1_565 . ?
As21 As14 Pb13 134.2(4) 2_456 . ?
As16 As14 Pb13 65.86(13) . . ?
S6 As14 Pb13 53.9(2) 1_455 . ?
S13 As14 Pb13 54.7(3) . . ?
Pb21 As14 Pb13 127.7(2) 2_456 . ?
Pb14 As14 S11 69.5(15) . . ?
S12 As14 S11 71.6(5) 1_565 . ?
S17 As14 S11 117.5(5) 1_565 . ?
S19 As14 S11 143.7(8) 1_565 . ?
As21 As14 S11 95.5(5) 2_456 . ?
As16 As14 S11 39.0(2) . . ?
S6 As14 S11 100.2(3) 1_455 . ?
S13 As14 S11 64.3(4) . . ?
Pb21 As14 S11 89.7(3) 2_456 . ?
Pb13 As14 S11 47.3(2) . . ?
Pb14 As14 S10 74.0(15) . . ?
S12 As14 S10 113.3(5) 1_565 . ?
S17 As14 S10 73.3(5) 1_565 . ?
S19 As14 S10 147.3(8) 1_565 . ?
As21 As14 S10 91.0(6) 2_456 . ?
As16 As14 S10 35.5(3) . . ?
S6 As14 S10 65.4(4) 1_455 . ?
S13 As14 S10 102.3(4) . . ?
Pb21 As14 S10 85.3(3) 2_456 . ?
Pb13 As14 S10 48.8(2) . . ?
S11 As14 S10 56.66(19) . . ?
As14 Pb14 S19 74.5(10) . 1_565 ?
As14 Pb14 S12 44(2) . 1_565 ?
S19 Pb14 S12 86.5(5) 1_565 1_565 ?
As14 Pb14 S17 39(2) . 1_565 ?
S19 Pb14 S17 84.9(5) 1_565 1_565 ?
S12 Pb14 S17 80.5(3) 1_565 1_565 ?
As14 Pb14 S13 132(3) . . ?
S19 Pb14 S13 89.9(5) 1_565 . ?
S12 Pb14 S13 91.4(6) 1_565 . ?
S17 Pb14 S13 170.6(5) 1_565 . ?
As14 Pb14 S6 127(3) . 1_455 ?
S19 Pb14 S6 91.5(5) 1_565 1_455 ?
S12 Pb14 S6 170.7(5) 1_565 1_455 ?
S17 Pb14 S6 90.2(5) 1_565 1_455 ?
S13 Pb14 S6 97.8(2) . 1_455 ?
As14 Pb14 Pb13 145.6(10) . . ?
S19 Pb14 Pb13 139.8(2) 1_565 . ?
S12 Pb14 Pb13 122.8(4) 1_565 . ?
S17 Pb14 Pb13 123.6(4) 1_565 . ?
S13 Pb14 Pb13 65.0(3) . . ?
S6 Pb14 Pb13 63.6(3) 1_455 . ?
As14 Pb14 As16 74.9(9) . . ?
S19 Pb14 As16 149.3(2) 1_565 . ?
S12 Pb14 As16 71.1(3) 1_565 . ?
S17 Pb14 As16 71.2(3) 1_565 . ?
S13 Pb14 As16 110.8(4) . . ?
S6 Pb14 As16 107.1(3) 1_455 . ?
Pb13 Pb14 As16 70.86(10) . . ?
As14 Pb14 S11 100.6(16) . . ?
S19 Pb14 S11 149.7(7) 1_565 . ?
S12 Pb14 S11 71.1(4) 1_565 . ?
S17 Pb14 S11 110.2(3) 1_565 . ?
S13 Pb14 S11 71.1(4) . . ?
S6 Pb14 S11 113.7(3) 1_455 . ?
Pb13 Pb14 S11 52.4(2) . . ?
As16 Pb14 S11 39.7(2) . . ?
As14 Pb14 As21 14.1(9) . 2_456 ?
S19 Pb14 As21 88.5(3) 1_565 2_456 ?
S12 Pb14 As21 42.7(7) 1_565 2_456 ?
S17 Pb14 As21 38.2(7) 1_565 2_456 ?
S13 Pb14 As21 134.0(8) . 2_456 ?
S6 Pb14 As21 128.2(8) 1_455 2_456 ?
Pb13 Pb14 As21 131.6(3) . 2_456 ?
As16 Pb14 As21 60.8(3) . 2_456 ?
S11 Pb14 As21 88.4(4) . 2_456 ?
As14 Pb14 S10 96.1(16) . . ?
S19 Pb14 S10 150.0(7) 1_565 . ?
S12 Pb14 S10 106.5(4) 1_565 . ?
S17 Pb14 S10 71.2(4) 1_565 . ?
S13 Pb14 S10 116.0(4) . . ?
S6 Pb14 S10 71.2(4) 1_455 . ?
Pb13 Pb14 S10 53.6(2) . . ?
As16 Pb14 S10 36.0(2) . . ?
S11 Pb14 S10 59.24(18) . . ?
As21 Pb14 S10 83.9(5) 2_456 . ?
As14 Pb14 As18 98(3) . . ?
S19 Pb14 As18 89.3(6) 1_565 . ?
S12 Pb14 As18 56.0(4) 1_565 . ?
S17 Pb14 As18 136.4(4) 1_565 . ?
S13 Pb14 As18 35.4(3) . . ?
S6 Pb14 As18 133.1(3) 1_455 . ?
Pb13 Pb14 As18 86.8(2) . . ?
As16 Pb14 As18 94.9(3) . . ?
S11 Pb14 As18 61.5(3) . . ?
As21 Pb14 As18 98.7(7) 2_456 . ?
S10 Pb14 As18 120.6(3) . . ?
S23 As15 S1 99.7(5) 1_556 . ?
S23 As15 S9 100.4(2) 1_556 1_556 ?
S1 As15 S9 98.1(5) . 1_556 ?
S23 As15 As15 79.0(3) 1_556 3_557 ?
S1 As15 As15 175.5(3) . 3_557 ?
S9 As15 As15 78.0(3) 1_556 3_557 ?
S23 As15 S17 171.9(5) 1_556 1_655 ?
S1 As15 S17 76.8(4) . 1_655 ?
S9 As15 S17 87.4(4) 1_556 1_655 ?
As15 As15 S17 105.0(2) 3_557 1_655 ?
S23 As15 S12 92.6(5) 1_556 . ?
S1 As15 S12 80.5(4) . . ?
S9 As15 S12 166.9(5) 1_556 . ?
As15 As15 S12 103.8(3) 3_557 . ?
S17 As15 S12 79.6(2) 1_655 . ?
S23 As15 Pb12 119.7(4) 1_556 1_545 ?
S1 As15 Pb12 117.92(18) . 1_545 ?
S9 As15 Pb12 117.1(4) 1_556 1_545 ?
As15 As15 Pb12 66.17(8) 3_557 1_545 ?
S17 As15 Pb12 57.2(2) 1_655 1_545 ?
S12 As15 Pb12 54.0(2) . 1_545 ?
S23 As15 S23 74.4(5) 1_556 3_556 ?
S1 As15 S23 147.3(5) . 3_556 ?
S9 As15 S23 114.6(4) 1_556 3_556 ?
As15 As15 S23 36.6(2) 3_557 3_556 ?
S17 As15 S23 104.5(3) 1_655 3_556 ?
S12 As15 S23 67.9(3) . 3_556 ?
Pb12 As15 S23 48.2(2) 1_545 3_556 ?
S23 As15 S9 118.3(4) 1_556 3_556 ?
S1 As15 S9 141.6(6) . 3_556 ?
S9 As15 S9 71.2(5) 1_556 3_556 ?
As15 As15 S9 39.3(2) 3_557 3_556 ?
S17 As15 S9 66.2(3) 1_655 3_556 ?
S12 As15 S9 101.8(3) . 3_556 ?
Pb12 As15 S9 48.1(2) 1_545 3_556 ?
S23 As15 S9 57.67(18) 3_556 3_556 ?
S23 As15 Pb12 50.9(3) 1_556 3_567 ?
S1 As15 Pb12 115.46(18) . 3_567 ?
S9 As15 Pb12 51.4(3) 1_556 3_567 ?
As15 As15 Pb12 60.40(7) 3_557 3_567 ?
S17 As15 Pb12 137.2(3) 1_655 3_567 ?
S12 As15 Pb12 140.8(3) . 3_567 ?
Pb12 As15 Pb12 126.57(6) 1_545 3_567 ?
S23 As15 Pb12 86.2(2) 3_556 3_567 ?
S9 As15 Pb12 87.1(2) 3_556 3_567 ?
S23 As15 Pb4 48.5(3) 1_556 2_446 ?
S1 As15 Pb4 51.7(4) . 2_446 ?
S9 As15 Pb4 98.8(3) 1_556 2_446 ?
As15 As15 Pb4 126.36(10) 3_557 2_446 ?
S17 As15 Pb4 128.5(2) 1_655 2_446 ?
S12 As15 Pb4 90.5(3) . 2_446 ?
Pb12 As15 Pb4 144.1(2) 1_545 2_446 ?
S23 As15 Pb4 118.2(3) 3_556 2_446 ?
S9 As15 Pb4 162.9(2) 3_556 2_446 ?
Pb12 As15 Pb4 75.93(8) 3_567 2_446 ?
S23 As15 Pb10 97.7(4) 1_556 . ?
S1 As15 Pb10 49.8(4) . . ?
S9 As15 Pb10 49.2(3) 1_556 . ?
As15 As15 Pb10 125.95(9) 3_557 . ?
S17 As15 Pb10 85.7(3) 1_655 . ?
S12 As15 Pb10 130.2(3) . . ?
Pb12 As15 Pb10 142.5(2) 1_545 . ?
S23 As15 Pb10 161.2(2) 3_556 . ?
S9 As15 Pb10 115.1(3) 3_556 . ?
Pb12 As15 Pb10 75.80(8) 3_567 . ?
Pb4 As15 Pb10 62.94(4) 2_446 . ?
S10 As16 S4 98.3(6) . . ?
S10 As16 S11 100.9(3) . . ?
S4 As16 S11 99.4(5) . . ?
S10 As16 As14 81.1(4) . . ?
S4 As16 As14 177.3(4) . . ?
S11 As16 As14 78.2(4) . . ?
S10 As16 S9 88.2(5) . 3_466 ?
S4 As16 S9 78.5(4) . 3_466 ?
S11 As16 S9 170.8(5) . 3_466 ?
As14 As16 S9 104.1(3) . 3_466 ?
S10 As16 Pb14 75.0(4) . . ?
S4 As16 Pb14 166.8(2) . . ?
S11 As16 Pb14 71.3(3) . . ?
As14 As16 Pb14 10.65(9) . . ?
S9 As16 Pb14 112.2(3) 3_466 . ?
S10 As16 S23 168.9(5) . 3_566 ?
S4 As16 S23 77.4(4) . 3_566 ?
S11 As16 S23 89.9(4) . 3_566 ?
As14 As16 S23 103.6(3) . 3_566 ?
S9 As16 S23 80.90(17) 3_466 3_566 ?
Pb14 As16 S23 111.1(3) . 3_566 ?
S10 As16 As21 110.5(7) . 2_456 ?
S4 As16 As21 132.0(3) . 2_456 ?
S11 As16 As21 111.2(7) . 2_456 ?
As14 As16 As21 50.4(3) . 2_456 ?
S9 As16 As21 65.4(5) 3_466 2_456 ?
Pb14 As16 As21 61.1(3) . 2_456 ?
S23 As16 As21 67.0(5) 3_566 2_456 ?
S10 As16 Pb21 116.6(4) . 2_456 ?
S4 As16 Pb21 119.77(19) . 2_456 ?
S11 As16 Pb21 118.1(4) . 2_456 ?
As14 As16 Pb21 62.67(13) . 2_456 ?
S9 As16 Pb21 57.0(3) 3_466 2_456 ?
Pb14 As16 Pb21 73.32(11) . 2_456 ?
S23 As16 Pb21 58.8(2) 3_566 2_456 ?
As21 As16 Pb21 12.3(2) 2_456 2_456 ?
S10 As16 S12 119.0(4) . 1_565 ?
S4 As16 S12 142.6(6) . 1_565 ?
S11 As16 S12 71.9(4) . 1_565 ?
As14 As16 S12 37.9(4) . 1_565 ?
S9 As16 S12 104.3(3) 3_466 1_565 ?
Pb14 As16 S12 44.7(3) . 1_565 ?
S23 As16 S12 66.5(3) 3_566 1_565 ?
As21 As16 S12 39.3(6) 2_456 1_565 ?
Pb21 As16 S12 47.5(2) 2_456 1_565 ?
S10 As16 S17 75.2(4) . 1_565 ?
S4 As16 S17 144.1(5) . 1_565 ?
S11 As16 S17 116.6(4) . 1_565 ?
As14 As16 S17 38.4(3) . 1_565 ?
S9 As16 S17 66.2(3) 3_466 1_565 ?
Pb14 As16 S17 46.0(2) . 1_565 ?
S23 As16 S17 102.1(3) 3_566 1_565 ?
As21 As16 S17 35.4(5) 2_456 1_565 ?
Pb21 As16 S17 43.7(2) 2_456 1_565 ?
S12 As16 S17 58.1(2) 1_565 1_565 ?
S10 As16 Pb7 98.0(4) . . ?
S4 As16 Pb7 51.9(4) . . ?
S11 As16 Pb7 48.2(3) . . ?
As14 As16 Pb7 125.5(3) . . ?
S9 As16 Pb7 130.4(2) 3_466 . ?
Pb14 As16 Pb7 116.99(19) . . ?
S23 As16 Pb7 87.5(3) 3_566 . ?
As21 As16 Pb7 148.6(7) 2_456 . ?
Pb21 As16 Pb7 145.4(3) 2_456 . ?
S12 As16 Pb7 114.7(3) 1_565 . ?
S17 As16 Pb7 162.6(2) 1_565 . ?
S21 As17 S3 102.4(6) . . ?
S21 As17 S18 102.2(3) . . ?
S3 As17 S18 91.7(5) . . ?
S21 As17 S11 86.9(5) . 2_446 ?
S3 As17 S11 84.1(4) . 2_446 ?
S18 As17 S11 170.7(5) . 2_446 ?
S21 As17 S10 169.3(5) . 2_546 ?
S3 As17 S10 80.2(4) . 2_546 ?
S18 As17 S10 88.0(5) . 2_546 ?
S11 As17 S10 83.05(17) 2_446 2_546 ?
S21 As17 Pb11 67.4(4) . . ?
S3 As17 Pb11 157.5(2) . . ?
S18 As17 Pb11 72.0(3) . . ?
S11 As17 Pb11 114.2(3) 2_446 . ?
S10 As17 Pb11 113.7(3) 2_546 . ?
S21 As17 As18 105.9(4) . 2_446 ?
S3 As17 As18 138.20(18) . 2_446 ?
S18 As17 As18 111.3(4) . 2_446 ?
S11 As17 As18 67.6(2) 2_446 2_446 ?
S10 As17 As18 66.8(2) 2_546 2_446 ?
Pb11 As17 As18 63.98(5) . 2_446 ?
S21 As17 S13 68.9(4) . 2_446 ?
S3 As17 S13 149.0(6) . 2_446 ?
S18 As17 S13 119.0(4) . 2_446 ?
S11 As17 S13 66.1(3) 2_446 2_446 ?
S10 As17 S13 103.5(3) 2_546 2_446 ?
Pb11 As17 S13 48.3(2) . 2_446 ?
As18 As17 S13 37.0(3) 2_446 2_446 ?
S21 As17 S6 114.5(4) . 2_446 ?
S3 As17 S6 142.7(5) . 2_446 ?
S18 As17 S6 76.0(4) . 2_446 ?
S11 As17 S6 102.3(3) 2_446 2_446 ?
S10 As17 S6 64.6(3) 2_546 2_446 ?
Pb11 As17 S6 49.51(17) . 2_446 ?
As18 As17 S6 35.2(2) 2_446 2_446 ?
S13 As17 S6 57.84(15) 2_446 2_446 ?
S21 As17 Pb1 50.6(4) . 2_446 ?
S3 As17 Pb1 53.1(3) . 2_446 ?
S18 As17 Pb1 91.7(4) . 2_446 ?
S11 As17 Pb1 92.4(3) 2_446 2_446 ?
S10 As17 Pb1 133.2(2) 2_546 2_446 ?
Pb11 As17 Pb1 110.54(11) . 2_446 ?
As18 As17 Pb1 151.4(3) 2_446 2_446 ?
S13 As17 Pb1 117.1(3) 2_446 2_446 ?
S6 As17 Pb1 158.84(17) 2_446 2_446 ?
S21 As17 Pb8 98.0(4) . 2_446 ?
S3 As17 Pb8 50.7(3) . 2_446 ?
S18 As17 Pb8 42.6(3) . 2_446 ?
S11 As17 Pb8 134.7(2) 2_446 2_446 ?
S10 As17 Pb8 91.7(3) 2_546 2_446 ?
Pb11 As17 Pb8 109.11(11) . 2_446 ?
As18 As17 Pb8 148.7(3) 2_446 2_446 ?
S13 As17 Pb8 156.5(2) 2_446 2_446 ?
S6 As17 Pb8 115.8(3) 2_446 2_446 ?
Pb1 As17 Pb8 59.53(4) 2_446 2_446 ?
S21 As17 Pb13 42.3(4) . 2_446 ?
S3 As17 Pb13 103.4(5) . 2_446 ?
S18 As17 Pb13 143.3(4) . 2_446 ?
S11 As17 Pb13 46.0(3) 2_446 2_446 ?
S10 As17 Pb13 127.1(3) 2_546 2_446 ?
Pb11 As17 Pb13 82.78(13) . 2_446 ?
As18 As17 Pb13 79.07(17) 2_446 2_446 ?
S13 As17 Pb13 49.6(3) 2_446 2_446 ?
S6 As17 Pb13 107.3(2) 2_446 2_446 ?
Pb1 As17 Pb13 72.39(13) 2_446 2_446 ?
Pb8 As17 Pb13 131.74(14) 2_446 2_446 ?
S6 As18 S8 95.8(5) . 1_565 ?
S6 As18 S13 102.9(2) . . ?
S8 As18 S13 98.3(5) 1_565 . ?
S6 As18 S12 167.8(5) . 1_565 ?
S8 As18 S12 81.5(4) 1_565 1_565 ?
S13 As18 S12 89.3(5) . 1_565 ?
S6 As18 Pb12 116.9(4) . . ?
S8 As18 Pb12 119.99(18) 1_565 . ?
S13 As18 Pb12 118.8(4) . . ?
S12 As18 Pb12 55.9(3) 1_565 . ?
S6 As18 S17 87.4(4) . 1_665 ?
S8 As18 S17 77.1(4) 1_565 1_665 ?
S13 As18 S17 169.2(5) . 1_665 ?
S12 As18 S17 80.36(19) 1_565 1_665 ?
Pb12 As18 S17 57.5(2) . 1_665 ?
S6 As18 As17 73.0(3) . 2_556 ?
S8 As18 As17 162.30(19) 1_565 2_556 ?
S13 As18 As17 71.7(4) . 2_556 ?
S12 As18 As17 112.2(3) 1_565 2_556 ?
Pb12 As18 As17 77.66(6) . 2_556 ?
S17 As18 As17 115.2(3) 1_665 2_556 ?
S6 As18 Pb9 99.3(3) . 3_576 ?
S8 As18 Pb9 51.0(4) 1_565 3_576 ?
S13 As18 Pb9 47.7(3) . 3_576 ?
S12 As18 Pb9 88.3(3) 1_565 3_576 ?
Pb12 As18 Pb9 143.8(2) . 3_576 ?
S17 As18 Pb9 128.0(2) 1_665 3_576 ?
As17 As18 Pb9 116.04(15) 2_556 3_576 ?
S6 As18 Pb11 52.5(3) . 2_556 ?
S8 As18 Pb11 106.09(18) 1_565 2_556 ?
S13 As18 Pb11 50.7(4) . 2_556 ?
S12 As18 Pb11 139.7(4) 1_565 2_556 ?
Pb12 As18 Pb11 133.89(7) . 2_556 ?
S17 As18 Pb11 139.9(3) 1_665 2_556 ?
As17 As18 Pb11 56.23(5) 2_556 2_556 ?
Pb9 As18 Pb11 69.09(7) 3_576 2_556 ?
S6 As18 Pb6 48.5(3) . 2_556 ?
S8 As18 Pb6 48.2(4) 1_565 2_556 ?
S13 As18 Pb6 98.2(3) . 2_556 ?
S12 As18 Pb6 129.7(3) 1_565 2_556 ?
Pb12 As18 Pb6 143.0(2) . 2_556 ?
S17 As18 Pb6 86.1(3) 1_665 2_556 ?
As17 As18 Pb6 117.36(15) 2_556 2_556 ?
Pb9 As18 Pb6 63.25(4) 3_576 2_556 ?
Pb11 As18 Pb6 69.75(7) 2_556 2_556 ?
S6 As18 S11 123.4(4) . . ?
S8 As18 S11 140.5(6) 1_565 . ?
S13 As18 S11 70.7(4) . . ?
S12 As18 S11 61.1(3) 1_565 . ?
Pb12 As18 S11 49.1(2) . . ?
S17 As18 S11 106.6(3) 1_665 . ?
As17 As18 S11 51.1(2) 2_556 . ?
Pb9 As18 S11 111.6(3) 3_576 . ?
Pb11 As18 S11 95.8(2) 2_556 . ?
Pb6 As18 S11 165.51(19) 2_556 . ?
S6 As18 S10 70.9(4) . 1_655 ?
S8 As18 S10 135.4(6) 1_565 1_655 ?
S13 As18 S10 125.9(4) . 1_655 ?
S12 As18 S10 102.6(3) 1_565 1_655 ?
Pb12 As18 S10 46.7(2) . 1_655 ?
S17 As18 S10 60.4(3) 1_665 1_655 ?
As17 As18 S10 54.8(2) 2_556 1_655 ?
Pb9 As18 S10 167.7(2) 3_576 1_655 ?
Pb11 As18 S10 98.7(2) 2_556 1_655 ?
Pb6 As18 S10 112.0(3) 2_556 1_655 ?
S11 As18 S10 70.12(15) . 1_655 ?
S16 As19 S2 102.0(6) . 2_456 ?
S16 As19 S14 99.2(3) . . ?
S2 As19 S14 95.3(6) 2_456 . ?
S16 As19 Pb13 121.6(4) . . ?
S2 As19 Pb13 114.65(17) 2_456 . ?
S14 As19 Pb13 119.6(4) . . ?
S16 As19 S13 173.6(4) . . ?
S2 As19 S13 74.7(5) 2_456 . ?
S14 As19 S13 86.7(4) . . ?
Pb13 As19 S13 56.5(2) . . ?
S16 As19 S6 96.4(4) . 1_455 ?
S2 As19 S6 75.6(4) 2_456 1_455 ?
S14 As19 S6 163.3(4) . 1_455 ?
Pb13 As19 S6 55.07(19) . 1_455 ?
S13 As19 S6 77.49(16) . 1_455 ?
S16 As19 S21 126.9(4) . 2_556 ?
S2 As19 S21 130.8(6) 2_456 2_556 ?
S14 As19 S21 74.1(4) . 2_556 ?
Pb13 As19 S21 46.3(2) . 2_556 ?
S13 As19 S21 57.2(3) . 2_556 ?
S6 As19 S21 101.1(3) 1_455 2_556 ?
S16 As19 Pb11 49.6(3) . 2_456 ?
S2 As19 Pb11 90.6(6) 2_456 2_456 ?
S14 As19 Pb11 148.7(3) . 2_456 ?
Pb13 As19 Pb11 84.99(15) . 2_456 ?
S13 As19 Pb11 124.4(3) . 2_456 ?
S6 As19 Pb11 46.9(2) 1_455 2_456 ?
S21 As19 Pb11 123.3(3) 2_556 2_456 ?
S16 As19 Pb1 54.2(3) . 2_456 ?
S2 As19 Pb1 48.0(4) 2_456 2_456 ?
S14 As19 Pb1 97.9(3) . 2_456 ?
Pb13 As19 Pb1 141.5(2) . 2_456 ?
S13 As19 Pb1 122.7(2) . 2_456 ?
S6 As19 Pb1 86.4(2) 1_455 2_456 ?
S21 As19 Pb1 171.9(3) 2_556 2_456 ?
Pb11 As19 Pb1 64.10(12) 2_456 2_456 ?
S16 As19 S18 75.3(4) . 2_456 ?
S2 As19 S18 135.4(6) 2_456 2_456 ?
S14 As19 S18 129.2(3) . 2_456 ?
Pb13 As19 S18 46.52(19) . 2_456 ?
S13 As19 S18 103.0(3) . 2_456 ?
S6 As19 S18 60.9(3) 1_455 2_456 ?
S21 As19 S18 70.68(17) 2_556 2_456 ?
Pb11 As19 S18 53.2(2) 2_456 2_456 ?
Pb1 As19 S18 116.1(3) 2_456 2_456 ?
S16 As19 Pb8 98.1(3) . 2_456 ?
S2 As19 Pb8 47.2(4) 2_456 2_456 ?
S14 As19 Pb8 49.0(3) . 2_456 ?
Pb13 As19 Pb8 140.2(2) . 2_456 ?
S13 As19 Pb8 83.7(2) . 2_456 ?
S6 As19 Pb8 122.71(19) 1_455 2_456 ?
S21 As19 Pb8 112.7(3) 2_556 2_456 ?
Pb11 As19 Pb8 123.90(12) 2_456 2_456 ?
Pb1 As19 Pb8 60.05(4) 2_456 2_456 ?
S18 As19 Pb8 173.1(2) 2_456 2_456 ?
S16 As19 Pb11 141.3(4) . 2_556 ?
S2 As19 Pb11 89.5(6) 2_456 2_556 ?
S14 As19 Pb11 42.5(3) . 2_556 ?
Pb13 As19 Pb11 84.61(15) . 2_556 ?
S13 As19 Pb11 44.9(2) . 2_556 ?
S6 As19 Pb11 122.3(2) 1_455 2_556 ?
S21 As19 Pb11 50.1(2) 2_556 2_556 ?
Pb11 As19 Pb11 168.60(6) 2_456 2_556 ?
Pb1 As19 Pb11 123.16(12) 2_456 2_556 ?
S18 As19 Pb11 120.7(2) 2_456 2_556 ?
Pb8 As19 Pb11 63.26(11) 2_456 2_556 ?
S15 As20 S24 86.7(5) . . ?
S15 As20 S22 94.4(2) . . ?
S24 As20 S22 94.3(6) . . ?
S15 As20 S5 80.1(2) . 4_464 ?
S24 As20 S5 83.8(5) . 4_464 ?
S22 As20 S5 174.2(4) . 4_464 ?
S15 As20 Pb5 131.0(4) . 4_454 ?
S24 As20 Pb5 125.4(3) . 4_454 ?
S22 As20 Pb5 52.5(4) . 4_454 ?
S5 As20 Pb5 132.8(4) 4_464 4_454 ?
S15 As20 Pb7 124.5(4) . 3_566 ?
S24 As20 Pb7 58.7(3) . 3_566 ?
S22 As20 Pb7 52.3(4) . 3_566 ?
S5 As20 Pb7 129.9(4) 4_464 3_566 ?
Pb5 As20 Pb7 66.95(6) 4_454 3_566 ?
S15 As20 Pb8 58.6(3) . 3_466 ?
S24 As20 Pb8 126.4(3) . 3_466 ?
S22 As20 Pb8 54.3(4) . 3_466 ?
S5 As20 Pb8 122.9(3) 4_464 3_466 ?
Pb5 As20 Pb8 72.43(15) 4_454 3_466 ?
Pb7 As20 Pb8 106.56(9) 3_566 3_466 ?
S15 As20 Pb1 53.0(3) . 3_566 ?
S24 As20 Pb1 60.6(3) . 3_566 ?
S22 As20 Pb1 55.0(4) . 3_566 ?
S5 As20 Pb1 119.6(4) 4_464 3_566 ?
Pb5 As20 Pb1 107.47(9) 4_454 3_566 ?
Pb7 As20 Pb1 71.85(15) 3_566 3_566 ?
Pb8 As20 Pb1 65.82(5) 3_466 3_566 ?
S15 As20 Pb10 119.3(3) . 3_466 ?
S24 As20 Pb10 117.0(2) . 3_466 ?
S22 As20 Pb10 133.6(5) . 3_466 ?
S5 As20 Pb10 51.6(3) 4_464 3_466 ?
Pb5 As20 Pb10 81.19(17) 4_454 3_466 ?
Pb7 As20 Pb10 115.07(9) 3_566 3_466 ?
Pb8 As20 Pb10 115.6(3) 3_466 3_466 ?
Pb1 As20 Pb10 170.90(12) 3_566 3_466 ?
S15 As20 Pb2 52.9(3) . 3_466 ?
S24 As20 Pb2 118.3(3) . 3_466 ?
S22 As20 Pb2 128.4(4) . 3_466 ?
S5 As20 Pb2 49.1(3) 4_464 3_466 ?
Pb5 As20 Pb2 116.2(3) 4_454 3_466 ?
Pb7 As20 Pb2 176.7(3) 3_566 3_466 ?
Pb8 As20 Pb2 74.07(15) 3_466 3_466 ?
Pb1 As20 Pb2 105.75(9) 3_566 3_466 ?
Pb10 As20 Pb2 67.08(13) 3_466 3_466 ?
S15 As20 Pb4 114.1(4) . 4_464 ?
S24 As20 Pb4 53.0(2) . 4_464 ?
S22 As20 Pb4 132.4(5) . 4_464 ?
S5 As20 Pb4 50.0(3) 4_464 4_464 ?
Pb5 As20 Pb4 114.84(9) 4_454 4_464 ?
Pb7 As20 Pb4 80.10(16) 3_566 4_464 ?
Pb8 As20 Pb4 171.99(10) 3_466 4_464 ?
Pb1 As20 Pb4 113.2(3) 3_566 4_464 ?
Pb10 As20 Pb4 63.99(5) 3_466 4_464 ?
Pb2 As20 Pb4 99.03(8) 3_466 4_464 ?
S15 As20 Pb3 47.9(3) . 4_464 ?
S24 As20 Pb3 55.7(2) . 4_464 ?
S22 As20 Pb3 127.6(5) . 4_464 ?
S5 As20 Pb3 47.1(3) 4_464 4_464 ?
Pb5 As20 Pb3 178.8(3) 4_454 4_464 ?
Pb7 As20 Pb3 114.1(3) 3_566 4_464 ?
Pb8 As20 Pb3 106.54(8) 3_466 4_464 ?
Pb1 As20 Pb3 72.53(15) 3_566 4_464 ?
Pb10 As20 Pb3 98.75(8) 3_466 4_464 ?
Pb2 As20 Pb3 62.72(5) 3_466 4_464 ?
Pb4 As20 Pb3 66.15(13) 4_464 4_464 ?
Pb21 As21 S17 124(4) . 2_556 ?
Pb21 As21 S12 123(3) . 2_556 ?
S17 As21 S12 100.4(5) 2_556 2_556 ?
Pb21 As21 S5 113.4(12) . . ?
S17 As21 S5 93.9(10) 2_556 . ?
S12 As21 S5 94.1(12) 2_556 . ?
Pb21 As21 As14 147.5(15) . 2_546 ?
S17 As21 As14 51.4(6) 2_556 2_546 ?
S12 As21 As14 49.1(6) 2_556 2_546 ?
S5 As21 As14 99.1(6) . 2_546 ?
Pb21 As21 S9 51(2) . 2_455 ?
S17 As21 S9 90.4(12) 2_556 2_455 ?
S12 As21 S9 168.3(12) 2_556 2_455 ?
S5 As21 S9 80.5(7) . 2_455 ?
As14 As21 S9 141.8(13) 2_546 2_455 ?
Pb21 As21 S23 55(2) . 2 ?
S17 As21 S23 168.5(10) 2_556 2 ?
S12 As21 S23 87.7(11) 2_556 2 ?
S5 As21 S23 77.3(8) . 2 ?
As14 As21 S23 136.6(13) 2_546 2 ?
S9 As21 S23 81.0(3) 2_455 2 ?
Pb21 As21 As16 86.3(13) . 2_546 ?
S17 As21 As16 75.4(6) 2_556 2_546 ?
S12 As21 As16 72.1(5) 2_556 2_546 ?
S5 As21 As16 160.2(6) . 2_546 ?
As14 As21 As16 61.2(3) 2_546 2_546 ?
S9 As21 As16 115.6(8) 2_455 2_546 ?
S23 As21 As16 115.1(8) 2 2_546 ?
Pb21 As21 Pb14 144.4(14) . 2_546 ?
S17 As21 Pb14 51.7(5) 2_556 2_546 ?
S12 As21 Pb14 49.2(5) 2_556 2_546 ?
S5 As21 Pb14 102.2(5) . 2_546 ?
As14 As21 Pb14 3.0(2) 2_546 2_546 ?
S9 As21 Pb14 142.0(12) 2_455 2_546 ?
S23 As21 Pb14 136.8(12) 2 2_546 ?
As16 As21 Pb14 58.1(2) 2_546 2_546 ?
Pb21 As21 Pb21 6.2(10) . 3_566 ?
S17 As21 Pb21 122.4(13) 2_556 3_566 ?
S12 As21 Pb21 120.2(11) 2_556 3_566 ?
S5 As21 Pb21 119.5(4) . 3_566 ?
As14 As21 Pb21 141.3(5) 2_546 3_566 ?
S9 As21 Pb21 55.7(4) 2_455 3_566 ?
S23 As21 Pb21 58.2(4) 2 3_566 ?
As16 As21 Pb21 80.1(3) 2_546 3_566 ?
Pb14 As21 Pb21 138.3(4) 2_546 3_566 ?
Pb21 As21 S9 51(2) . 4_455 ?
S17 As21 S9 76.0(9) 2_556 4_455 ?
S12 As21 S9 126.5(7) 2_556 4_455 ?
S5 As21 S9 139.2(13) . 4_455 ?
As14 As21 S9 104.2(7) 2_546 4_455 ?
S9 As21 S9 60.5(6) 2_455 4_455 ?
S23 As21 S9 105.8(5) 2 4_455 ?
As16 As21 S9 55.1(4) 2_546 4_455 ?
Pb14 As21 S9 101.8(6) 2_546 4_455 ?
Pb21 As21 S9 47.6(4) 3_566 4_455 ?
Pb21 As21 S23 52(2) . 4 ?
S17 As21 S23 131.2(7) 2_556 4 ?
S12 As21 S23 72.5(8) 2_556 4 ?
S5 As21 S23 134.1(13) . 4 ?
As14 As21 S23 103.3(7) 2_546 4 ?
S9 As21 S23 103.8(5) 2_455 4 ?
S23 As21 S23 58.9(6) 2 4 ?
As16 As21 S23 56.2(4) 2_546 4 ?
Pb14 As21 S23 100.9(6) 2_546 4 ?
Pb21 As21 S23 48.2(3) 3_566 4 ?
S9 As21 S23 71.7(3) 4_455 4 ?
As21 Pb21 S17 42(3) . 2_556 ?
As21 Pb21 S5 52.2(12) . . ?
S17 Pb21 S5 75.5(4) 2_556 . ?
As21 Pb21 S12 44(3) . 2_556 ?
S17 Pb21 S12 78.4(2) 2_556 2_556 ?
S5 Pb21 S12 76.5(5) . 2_556 ?
As21 Pb21 Pb21 172.2(13) . 3_566 ?
S17 Pb21 Pb21 135.1(3) 2_556 3_566 ?
S5 Pb21 Pb21 135.52(19) . 3_566 ?
S12 Pb21 Pb21 131.9(3) 2_556 3_566 ?
As21 Pb21 S9 117(3) . 2_455 ?
S17 Pb21 S9 91.0(4) 2_556 2_455 ?
S5 Pb21 S9 82.8(4) . 2_455 ?
S12 Pb21 S9 158.5(4) 2_556 2_455 ?
Pb21 Pb21 S9 68.2(3) 3_566 2_455 ?
As21 Pb21 S23 113(3) . 2 ?
S17 Pb21 S23 153.3(4) 2_556 2 ?
S5 Pb21 S23 79.2(5) . 2 ?
S12 Pb21 S23 87.4(4) 2_556 2 ?
Pb21 Pb21 S23 70.6(2) 3_566 2 ?
S9 Pb21 S23 94.4(2) 2_455 2 ?
As21 Pb21 S9 118(3) . 4_455 ?
S17 Pb21 S9 78.8(4) 2_556 4_455 ?
S5 Pb21 S9 141.7(6) . 4_455 ?
S12 Pb21 S9 125.3(4) 2_556 4_455 ?
Pb21 Pb21 S9 56.9(2) 3_566 4_455 ?
S9 Pb21 S9 69.6(5) 2_455 4_455 ?
S23 Pb21 S9 127.5(4) 2 4_455 ?
As21 Pb21 S23 118(3) . 4 ?
S17 Pb21 S23 129.0(4) 2_556 4 ?
S5 Pb21 S23 136.1(6) . 4 ?
S12 Pb21 S23 75.1(4) 2_556 4 ?
Pb21 Pb21 S23 57.1(2) 3_566 4 ?
S9 Pb21 S23 125.2(4) 2_455 4 ?
S23 Pb21 S23 66.9(5) 2 4 ?
S9 Pb21 S23 82.16(19) 4_455 4 ?
As21 Pb21 As16 81.4(11) . 2_546 ?
S17 Pb21 As16 70.0(3) 2_556 2_546 ?
S5 Pb21 As16 133.61(19) . 2_546 ?
S12 Pb21 As16 67.1(3) 2_556 2_546 ?
Pb21 Pb21 As16 90.79(15) 3_566 2_546 ?
S9 Pb21 As16 126.9(4) 2_455 2_546 ?
S23 Pb21 As16 124.8(4) 2 2_546 ?
S9 Pb21 As16 58.4(2) 4_455 2_546 ?
S23 Pb21 As16 59.8(2) 4 2_546 ?
As21 Pb21 As14 26.0(11) . 2_546 ?
S17 Pb21 As14 40.2(4) 2_556 2_546 ?
S5 Pb21 As14 78.2(2) . 2_546 ?
S12 Pb21 As14 39.1(4) 2_556 2_546 ?
Pb21 Pb21 As14 146.2(2) 3_566 2_546 ?
S9 Pb21 As14 130.6(4) 2_455 2_546 ?
S23 Pb21 As14 125.4(4) 2 2_546 ?
S9 Pb21 As14 99.7(3) 4_455 2_546 ?
S23 Pb21 As14 99.1(3) 4 2_546 ?
As16 Pb21 As14 55.44(12) 2_546 2_546 ?
As21 Pb21 As21 173.8(11) . 3_566 ?
S17 Pb21 As21 136.0(8) 2_556 3_566 ?
S5 Pb21 As21 133.9(2) . 3_566 ?
S12 Pb21 As21 132.6(7) 2_556 3_566 ?
Pb21 Pb21 As21 1.6(2) 3_566 3_566 ?
S9 Pb21 As21 67.3(6) 2_455 3_566 ?
S23 Pb21 As21 69.5(6) 2 3_566 ?
S9 Pb21 As21 58.1(5) 4_455 3_566 ?
S23 Pb21 As21 57.9(6) 4 3_566 ?
As16 Pb21 As21 92.39(18) 2_546 3_566 ?
As14 Pb21 As21 147.8(2) 2_546 3_566 ?
S26 As22 S26 174.4(16) 3_556 . ?
S26 As22 Cl25 92.8(8) 3_556 1_455 ?
S26 As22 Cl25 92.8(8) . 1_455 ?
S26 As22 S20 91.0(3) 3_556 3_556 ?
S26 As22 S20 89.1(3) . 3_556 ?
Cl25 As22 S20 88.9(6) 1_455 3_556 ?
S26 As22 S20 89.1(3) 3_556 . ?
S26 As22 S20 91.0(3) . . ?
Cl25 As22 S20 88.9(6) 1_455 . ?
S20 As22 S20 177.8(13) 3_556 . ?
S26 As22 Pb5 54.5(5) 3_556 . ?
S26 As22 Pb5 122.0(6) . . ?
Cl25 As22 Pb5 121.7(2) 1_455 . ?
S20 As22 Pb5 131.5(5) 3_556 . ?
S20 As22 Pb5 50.0(4) . . ?
S26 As22 Pb5 122.0(6) 3_556 3_556 ?
S26 As22 Pb5 54.5(5) . 3_556 ?
Cl25 As22 Pb5 121.7(2) 1_455 3_556 ?
S20 As22 Pb5 50.0(4) 3_556 3_556 ?
S20 As22 Pb5 131.5(5) . 3_556 ?
Pb5 As22 Pb5 116.5(4) . 3_556 ?
S26 As22 Pb4 59.0(5) 3_556 1_445 ?
S26 As22 Pb4 124.5(6) . 1_445 ?
Cl25 As22 Pb4 57.8(2) 1_455 1_445 ?
S20 As22 Pb4 49.3(4) 3_556 1_445 ?
S20 As22 Pb4 129.1(5) . 1_445 ?
Pb5 As22 Pb4 113.43(5) . 1_445 ?
Pb5 As22 Pb4 99.36(5) 3_556 1_445 ?
S26 As22 Pb4 124.5(6) 3_556 3_466 ?
S26 As22 Pb4 59.0(5) . 3_466 ?
Cl25 As22 Pb4 57.8(2) 1_455 3_466 ?
S20 As22 Pb4 129.1(5) 3_556 3_466 ?
S20 As22 Pb4 49.3(4) . 3_466 ?
Pb5 As22 Pb4 99.36(5) . 3_466 ?
Pb5 As22 Pb4 113.43(5) 3_556 3_466 ?
Pb4 As22 Pb4 115.6(4) 1_445 3_466 ?
S26 As22 Pb10 121.2(6) 3_556 4_454 ?
S26 As22 Pb10 55.3(5) . 4_454 ?
Cl25 As22 Pb10 121.6(2) 1_455 4_454 ?
S20 As22 Pb10 131.0(5) 3_556 4_454 ?
S20 As22 Pb10 50.5(4) . 4_454 ?
Pb5 As22 Pb10 66.80(17) . 4_454 ?
Pb5 As22 Pb10 81.0(2) 3_556 4_454 ?
Pb4 As22 Pb10 179.4(4) 1_445 4_454 ?
Pb4 As22 Pb10 63.77(3) 3_466 4_454 ?
S26 As22 Pb10 55.3(5) 3_556 2_446 ?
S26 As22 Pb10 121.2(6) . 2_446 ?
Cl25 As22 Pb10 121.6(2) 1_455 2_446 ?
S20 As22 Pb10 50.5(4) 3_556 2_446 ?
S20 As22 Pb10 131.0(5) . 2_446 ?
Pb5 As22 Pb10 81.0(2) . 2_446 ?
Pb5 As22 Pb10 66.81(17) 3_556 2_446 ?
Pb4 As22 Pb10 63.77(3) 1_445 2_446 ?
Pb4 As22 Pb10 179.4(4) 3_466 2_446 ?
Pb10 As22 Pb10 116.8(4) 4_454 2_446 ?
S26 As22 Pb7 125.1(6) 3_556 4_454 ?
S26 As22 Pb7 58.6(5) . 4_454 ?
Cl25 As22 Pb7 57.0(2) 1_455 4_454 ?
S20 As22 Pb7 49.2(4) 3_556 4_454 ?
S20 As22 Pb7 129.3(5) . 4_454 ?
Pb5 As22 Pb7 178.8(4) . 4_454 ?
Pb5 As22 Pb7 64.69(3) 3_556 4_454 ?
Pb4 As22 Pb7 66.10(17) 1_445 4_454 ?
Pb4 As22 Pb7 80.0(2) 3_466 4_454 ?
Pb10 As22 Pb7 113.66(5) 4_454 4_454 ?
Pb10 As22 Pb7 99.71(5) 2_446 4_454 ?
As15 S1 Pb10 94.5(4) . . ?
As15 S1 Pb4 92.4(4) . 2_446 ?
Pb10 S1 Pb4 84.57(16) . 2_446 ?
As15 S1 Pb2 116.9(5) . . ?
Pb10 S1 Pb2 89.9(5) . . ?
Pb4 S1 Pb2 150.6(2) 2_446 . ?
As15 S1 Pb3 114.0(5) . 2_446 ?
Pb10 S1 Pb3 150.8(2) . 2_446 ?
Pb4 S1 Pb3 88.2(5) 2_446 2_446 ?
Pb2 S1 Pb3 82.72(15) . 2_446 ?
As15 S1 As21 65.2(5) . 2_546 ?
Pb10 S1 As21 69.1(4) . 2_546 ?
Pb4 S1 As21 142.8(3) 2_446 2_546 ?
Pb2 S1 As21 58.2(4) . 2_546 ?
Pb3 S1 As21 127.3(3) 2_446 2_546 ?
As15 S1 As21 62.5(5) . 2_446 ?
Pb10 S1 As21 142.1(3) . 2_446 ?
Pb4 S1 As21 67.9(4) 2_446 2_446 ?
Pb2 S1 As21 126.8(3) . 2_446 ?
Pb3 S1 As21 57.1(3) 2_446 2_446 ?
As21 S1 As21 118.9(4) 2_546 2_446 ?
As15 S1 Pb21 58.3(4) . 2_546 ?
Pb10 S1 Pb21 65.7(3) . 2_546 ?
Pb4 S1 Pb21 134.1(2) 2_446 2_546 ?
Pb2 S1 Pb21 67.2(3) . 2_546 ?
Pb3 S1 Pb21 134.2(2) 2_446 2_546 ?
As21 S1 Pb21 9.1(2) 2_546 2_546 ?
As21 S1 Pb21 115.8(3) 2_446 2_546 ?
As15 S1 Pb21 55.8(4) . 2_446 ?
Pb10 S1 Pb21 133.6(2) . 2_446 ?
Pb4 S1 Pb21 64.6(3) 2_446 2_446 ?
Pb2 S1 Pb21 133.7(2) . 2_446 ?
Pb3 S1 Pb21 65.8(3) 2_446 2_446 ?
As21 S1 Pb21 116.0(4) 2_546 2_446 ?
As21 S1 Pb21 8.86(18) 2_446 2_446 ?
Pb21 S1 Pb21 111.63(15) 2_546 2_446 ?
As15 S1 Pb12 39.06(13) . 1_545 ?
Pb10 S1 Pb12 121.3(3) . 1_545 ?
Pb4 S1 Pb12 120.3(3) 2_446 1_545 ?
Pb2 S1 Pb12 87.15(19) . 1_545 ?
Pb3 S1 Pb12 86.66(19) 2_446 1_545 ?
As21 S1 Pb12 60.0(3) 2_546 1_545 ?
As21 S1 Pb12 59.8(3) 2_446 1_545 ?
Pb21 S1 Pb12 59.33(14) 2_546 1_545 ?
Pb21 S1 Pb12 59.22(14) 2_446 1_545 ?
As15 S1 As20 129.7(6) . 3_666 ?
Pb10 S1 As20 47.6(2) . 3_666 ?
Pb4 S1 As20 111.1(2) 2_446 3_666 ?
Pb2 S1 As20 48.2(2) . 3_666 ?
Pb3 S1 As20 110.6(2) 2_446 3_666 ?
As21 S1 As20 70.0(4) 2_546 3_666 ?
As21 S1 As20 167.3(3) 2_446 3_666 ?
Pb21 S1 As20 74.3(3) 2_546 3_666 ?
Pb21 S1 As20 174.0(3) 2_446 3_666 ?
Pb12 S1 As20 126.2(3) 1_545 3_666 ?
As15 S1 Pb12 41.52(13) . 3_567 ?
Pb10 S1 Pb12 63.79(13) . 3_567 ?
Pb4 S1 Pb12 63.60(12) 2_446 3_567 ?
Pb2 S1 Pb12 137.8(5) . 3_567 ?
Pb3 S1 Pb12 135.9(5) 2_446 3_567 ?
As21 S1 Pb12 81.0(3) 2_546 3_567 ?
As21 S1 Pb12 80.3(3) 2_446 3_567 ?
Pb21 S1 Pb12 71.87(16) 2_546 3_567 ?
Pb21 S1 Pb12 71.47(15) 2_446 3_567 ?
Pb12 S1 Pb12 80.55(9) 1_545 3_567 ?
As20 S1 Pb12 111.0(3) 3_666 3_567 ?
As19 S2 Pb6 117.5(6) 2_546 . ?
As19 S2 Pb1 98.1(5) 2_546 . ?
Pb6 S2 Pb1 85.7(6) . . ?
As19 S2 Pb8 99.4(5) 2_546 . ?
Pb6 S2 Pb8 142.8(2) . . ?
Pb1 S2 Pb8 84.05(15) . . ?
As19 S2 Pb9 116.8(7) 2_546 4_565 ?
Pb6 S2 Pb9 84.55(16) . 4_565 ?
Pb1 S2 Pb9 144.4(2) . 4_565 ?
Pb8 S2 Pb9 83.3(5) . 4_565 ?
As19 S2 As17 152.2(2) 2_546 2_556 ?
Pb6 S2 As17 81.9(2) . 2_556 ?
Pb1 S2 As17 61.73(16) . 2_556 ?
Pb8 S2 As17 61.76(15) . 2_556 ?
Pb9 S2 As17 83.0(2) 4_565 2_556 ?
As19 S2 Pb11 60.1(5) 2_546 . ?
Pb6 S2 Pb11 66.9(4) . . ?
Pb1 S2 Pb11 63.8(4) . . ?
Pb8 S2 Pb11 136.3(3) . . ?
Pb9 S2 Pb11 139.8(3) 4_565 . ?
As17 S2 Pb11 118.1(4) 2_556 . ?
As19 S2 Pb14 79.33(17) 2_546 2_546 ?
Pb6 S2 Pb14 61.22(17) . 2_546 ?
Pb1 S2 Pb14 139.3(6) . 2_546 ?
Pb8 S2 Pb14 136.6(7) . 2_546 ?
Pb9 S2 Pb14 60.34(19) 4_565 2_546 ?
As17 S2 Pb14 128.47(16) 2_556 2_546 ?
Pb11 S2 Pb14 80.7(3) . 2_546 ?
As19 S2 Pb11 61.6(5) 2_546 1_655 ?
Pb6 S2 Pb11 138.4(3) . 1_655 ?
Pb1 S2 Pb11 135.6(3) . 1_655 ?
Pb8 S2 Pb11 63.4(4) . 1_655 ?
Pb9 S2 Pb11 64.4(4) 4_565 1_655 ?
As17 S2 Pb11 118.2(4) 2_556 1_655 ?
Pb11 S2 Pb11 120.67(14) . 1_655 ?
Pb14 S2 Pb11 79.0(3) 2_546 1_655 ?
As19 S2 Pb13 40.08(12) 2_546 2_546 ?
Pb6 S2 Pb13 88.7(2) . 2_546 ?
Pb1 S2 Pb13 125.6(4) . 2_546 ?
Pb8 S2 Pb13 125.9(5) . 2_546 ?
Pb9 S2 Pb13 88.3(2) 4_565 2_546 ?
As17 S2 Pb13 167.71(15) 2_556 2_546 ?
Pb11 S2 Pb13 64.38(16) . 2_546 ?
Pb14 S2 Pb13 39.25(8) 2_546 2_546 ?
Pb11 S2 Pb13 64.85(18) 1_655 2_546 ?
As19 S2 As14 83.95(18) 2_546 2_546 ?
Pb6 S2 As14 58.1(2) . 2_546 ?
Pb1 S2 As14 138.7(6) . 2_546 ?
Pb8 S2 As14 136.6(6) . 2_546 ?
Pb9 S2 As14 57.7(2) 4_565 2_546 ?
As17 S2 As14 123.85(16) 2_556 2_546 ?
Pb11 S2 As14 82.7(3) . 2_546 ?
Pb14 S2 As14 4.63(11) 2_546 2_546 ?
Pb11 S2 As14 81.4(3) 1_655 2_546 ?
Pb13 S2 As14 43.87(10) 2_546 2_546 ?
As19 S2 Pb11 167.2(2) 2_546 2_556 ?
Pb6 S2 Pb11 54.37(11) . 2_556 ?
Pb1 S2 Pb11 91.4(2) . 2_556 ?
Pb8 S2 Pb11 90.2(2) . 2_556 ?
Pb9 S2 Pb11 55.55(11) 4_565 2_556 ?
As17 S2 Pb11 40.63(6) 2_556 2_556 ?
Pb11 S2 Pb11 117.7(4) . 2_556 ?
Pb14 S2 Pb11 87.84(11) 2_546 2_556 ?
Pb11 S2 Pb11 116.6(4) 1_655 2_556 ?
Pb13 S2 Pb11 127.08(12) 2_546 2_556 ?
As14 S2 Pb11 83.22(12) 2_546 2_556 ?
As17 S3 Pb5 112.5(5) . . ?
As17 S3 Pb7 107.9(5) . 2_446 ?
Pb5 S3 Pb7 88.44(17) . 2_446 ?
As17 S3 Pb8 95.7(4) . 2_446 ?
Pb5 S3 Pb8 93.0(5) . 2_446 ?
Pb7 S3 Pb8 153.8(3) 2_446 2_446 ?
As17 S3 Pb1 93.2(4) . 2_446 ?
Pb5 S3 Pb1 153.5(2) . 2_446 ?
Pb7 S3 Pb1 89.2(5) 2_446 2_446 ?
Pb8 S3 Pb1 77.94(14) 2_446 2_446 ?
As17 S3 As20 127.3(6) . 4 ?
Pb5 S3 As20 48.2(2) . 4 ?
Pb7 S3 As20 117.9(2) 2_446 4 ?
Pb8 S3 As20 49.5(2) 2_446 4 ?
Pb1 S3 As20 111.3(2) 2_446 4 ?
As17 S3 Pb13 55.0(4) . 2_546 ?
Pb5 S3 Pb13 68.1(3) . 2_546 ?
Pb7 S3 Pb13 136.1(2) 2_446 2_546 ?
Pb8 S3 Pb13 67.5(3) 2_446 2_546 ?
Pb1 S3 Pb13 128.0(2) 2_446 2_546 ?
As20 S3 Pb13 73.7(3) 4 2_546 ?
As17 S3 Pb12 64.36(15) . 2_446 ?
Pb5 S3 Pb12 65.36(13) . 2_446 ?
Pb7 S3 Pb12 65.47(13) 2_446 2_446 ?
Pb8 S3 Pb12 138.0(4) 2_446 2_446 ?
Pb1 S3 Pb12 136.0(4) 2_446 2_446 ?
As20 S3 Pb12 112.3(3) 4 2_446 ?
Pb13 S3 Pb12 71.00(14) 2_546 2_446 ?
As17 S3 As22 139.1(2) . . ?
Pb5 S3 As22 46.9(2) . . ?
Pb7 S3 As22 48.69(19) 2_446 . ?
Pb8 S3 As22 117.2(3) 2_446 . ?
Pb1 S3 As22 115.7(3) 2_446 . ?
As20 S3 As22 70.1(2) 4 . ?
Pb13 S3 As22 114.3(3) 2_546 . ?
Pb12 S3 As22 74.83(8) 2_446 . ?
As17 S3 As20 121.4(6) . 4_455 ?
Pb5 S3 As20 116.7(2) . 4_455 ?
Pb7 S3 As20 46.5(2) 2_446 4_455 ?
Pb8 S3 As20 111.1(2) 2_446 4_455 ?
Pb1 S3 As20 47.6(2) 2_446 4_455 ?
As20 S3 As20 109.03(13) 4 4_455 ?
Pb13 S3 As20 175.3(2) 2_546 4_455 ?
Pb12 S3 As20 110.8(3) 2_446 4_455 ?
As22 S3 As20 70.4(2) . 4_455 ?
As17 S3 Pb13 51.3(4) . 2_446 ?
Pb5 S3 Pb13 135.2(2) . 2_446 ?
Pb7 S3 Pb13 65.3(3) 2_446 2_446 ?
Pb8 S3 Pb13 126.7(2) 2_446 2_446 ?
Pb1 S3 Pb13 66.0(3) 2_446 2_446 ?
As20 S3 Pb13 176.16(15) 4 2_446 ?
Pb13 S3 Pb13 105.59(11) 2_546 2_446 ?
Pb12 S3 Pb13 70.72(15) 2_446 2_446 ?
As22 S3 Pb13 113.4(3) . 2_446 ?
As20 S3 Pb13 71.4(3) 4_455 2_446 ?
As16 S4 Pb10 115.3(6) . 3_467 ?
As16 S4 Pb4 116.0(6) . 4_465 ?
Pb10 S4 Pb4 87.82(15) 3_467 4_465 ?
As16 S4 Pb7 93.3(4) . . ?
Pb10 S4 Pb7 150.1(2) 3_467 . ?
Pb4 S4 Pb7 87.1(5) 4_465 . ?
As16 S4 Pb5 93.2(4) . 2_456 ?
Pb10 S4 Pb5 86.8(5) 3_467 2_456 ?
Pb4 S4 Pb5 149.6(2) 4_465 2_456 ?
Pb7 S4 Pb5 82.88(14) . 2_456 ?
As16 S4 Pb21 72.72(17) . 4_465 ?
Pb10 S4 Pb21 64.50(15) 3_467 4_465 ?
Pb4 S4 Pb21 65.67(15) 4_465 4_465 ?
Pb7 S4 Pb21 137.6(5) . 4_465 ?
Pb5 S4 Pb21 136.2(5) 2_456 4_465 ?
As16 S4 Pb12 54.9(5) . 1_455 ?
Pb10 S4 Pb12 67.3(3) 3_467 1_455 ?
Pb4 S4 Pb12 138.1(2) 4_465 1_455 ?
Pb7 S4 Pb12 130.9(2) . 1_455 ?
Pb5 S4 Pb12 65.3(3) 2_456 1_455 ?
Pb21 S4 Pb12 73.11(19) 4_465 1_455 ?
As16 S4 Pb12 55.6(5) . . ?
Pb10 S4 Pb12 137.4(2) 3_467 . ?
Pb4 S4 Pb12 67.2(3) 4_465 . ?
Pb7 S4 Pb12 65.7(3) . . ?
Pb5 S4 Pb12 131.9(2) 2_456 . ?
Pb21 S4 Pb12 73.71(18) 4_465 . ?
Pb12 S4 Pb12 108.73(12) 1_455 . ?
As16 S4 Pb21 38.18(13) . 2_456 ?
Pb10 S4 Pb21 88.6(2) 3_467 2_456 ?
Pb4 S4 Pb21 89.6(2) 4_465 2_456 ?
Pb7 S4 Pb21 120.8(4) . 2_456 ?
Pb5 S4 Pb21 120.1(4) 2_456 2_456 ?
Pb21 S4 Pb21 34.54(10) 4_465 2_456 ?
Pb12 S4 Pb21 58.13(15) 1_455 2_456 ?
Pb12 S4 Pb21 58.79(15) . 2_456 ?
As16 S4 As22 126.3(7) . 2_456 ?
Pb10 S4 As22 46.7(2) 3_467 2_456 ?
Pb4 S4 As22 113.1(2) 4_465 2_456 ?
Pb7 S4 As22 109.7(2) . 2_456 ?
Pb5 S4 As22 45.7(2) 2_456 2_456 ?
Pb21 S4 As22 110.7(3) 4_465 2_456 ?
Pb12 S4 As22 74.2(3) 1_455 2_456 ?
Pb12 S4 As22 175.4(2) . 2_456 ?
Pb21 S4 As22 125.5(4) 2_456 2_456 ?
As16 S4 As22 126.5(7) . 2_556 ?
Pb10 S4 As22 113.4(2) 3_467 2_556 ?
Pb4 S4 As22 46.0(2) 4_465 2_556 ?
Pb7 S4 As22 46.5(2) . 2_556 ?
Pb5 S4 As22 110.4(2) 2_456 2_556 ?
Pb21 S4 As22 111.1(3) 4_465 2_556 ?
Pb12 S4 As22 175.7(2) 1_455 2_556 ?
Pb12 S4 As22 73.9(3) . 2_556 ?
Pb21 S4 As22 125.9(4) 2_456 2_556 ?
As22 S4 As22 102.95(10) 2_456 2_556 ?
As16 S4 As20 145.8(2) . 1_556 ?
Pb10 S4 As20 46.45(15) 3_467 1_556 ?
Pb4 S4 As20 47.61(16) 4_465 1_556 ?
Pb7 S4 As20 112.6(3) . 1_556 ?
Pb5 S4 As20 111.2(3) 2_456 1_556 ?
Pb21 S4 As20 73.09(10) 4_465 1_556 ?
Pb12 S4 As20 113.3(3) 1_455 1_556 ?
Pb12 S4 As20 114.2(3) . 1_556 ?
Pb21 S4 As20 107.63(11) 2_456 1_556 ?
As22 S4 As20 66.87(17) 2_456 1_556 ?
As22 S4 As20 67.94(17) 2_556 1_556 ?
As21 S5 Pb21 14.4(3) . . ?
As21 S5 Pb3 96.9(8) . . ?
Pb21 S5 Pb3 107.3(5) . . ?
As21 S5 Pb2 93.8(8) . 2_456 ?
Pb21 S5 Pb2 104.1(5) . 2_456 ?
Pb3 S5 Pb2 86.47(18) . 2_456 ?
As21 S5 Pb4 111.9(8) . . ?
Pb21 S5 Pb4 101.1(4) . . ?
Pb3 S5 Pb4 91.0(6) . . ?
Pb2 S5 Pb4 154.3(3) 2_456 . ?
As21 S5 Pb10 108.2(9) . 2_456 ?
Pb21 S5 Pb10 98.0(4) . 2_456 ?
Pb3 S5 Pb10 154.7(3) . 2_456 ?
Pb2 S5 Pb10 88.3(6) 2_456 2_456 ?
Pb4 S5 Pb10 83.15(17) . 2_456 ?
As21 S5 As20 170.5(7) . 4_565 ?
Pb21 S5 As20 172.9(6) . 4_565 ?
Pb3 S5 As20 79.7(3) . 4_565 ?
Pb2 S5 As20 77.2(3) 2_456 4_565 ?
Pb4 S5 As20 77.1(3) . 4_565 ?
Pb10 S5 As20 75.0(3) 2_456 4_565 ?
As21 S5 As14 45.2(3) . 2_546 ?
Pb21 S5 As14 59.64(17) . 2_546 ?
Pb3 S5 As14 63.5(3) . 2_546 ?
Pb2 S5 As14 63.4(3) 2_456 2_546 ?
Pb4 S5 As14 136.7(7) . 2_546 ?
Pb10 S5 As14 134.3(7) 2_456 2_546 ?
As20 S5 As14 126.2(2) 4_565 2_546 ?
As21 S5 As15 65.0(10) . 2_556 ?
Pb21 S5 As15 61.9(4) . 2_556 ?
Pb3 S5 As15 69.3(4) . 2_556 ?
Pb2 S5 As15 144.4(3) 2_456 2_556 ?
Pb4 S5 As15 55.5(3) . 2_556 ?
Pb10 S5 As15 124.6(3) 2_456 2_556 ?
As20 S5 As15 121.0(6) 4_565 2_556 ?
As14 S5 As15 82.1(4) 2_546 2_556 ?
As21 S5 As15 62.0(10) . 2_456 ?
Pb21 S5 As15 59.1(4) . 2_456 ?
Pb3 S5 As15 143.4(3) . 2_456 ?
Pb2 S5 As15 67.1(4) 2_456 2_456 ?
Pb4 S5 As15 123.8(3) . 2_456 ?
Pb10 S5 As15 53.5(3) 2_456 2_456 ?
As20 S5 As15 116.0(6) 4_565 2_456 ?
As14 S5 As15 81.7(4) 2_546 2_456 ?
As15 S5 As15 118.94(16) 2_556 2_456 ?
As21 S5 Pb14 47.7(3) . 2_546 ?
Pb21 S5 Pb14 62.12(15) . 2_546 ?
Pb3 S5 Pb14 61.74(19) . 2_546 ?
Pb2 S5 Pb14 62.05(19) 2_456 2_546 ?
Pb4 S5 Pb14 137.3(6) . 2_546 ?
Pb10 S5 Pb14 135.2(6) 2_456 2_546 ?
As20 S5 Pb14 123.7(2) 4_565 2_546 ?
As14 S5 Pb14 2.48(14) 2_546 2_546 ?
As15 S5 Pb14 83.2(3) 2_556 2_546 ?
As15 S5 Pb14 83.1(3) 2_456 2_546 ?
As21 S5 As16 76.9(3) . 4_564 ?
Pb21 S5 As16 62.42(14) . 4_564 ?
Pb3 S5 As16 138.0(6) . 4_564 ?
Pb2 S5 As16 134.9(6) 2_456 4_564 ?
Pb4 S5 As16 55.54(14) . 4_564 ?
Pb10 S5 As16 55.04(14) 2_456 4_564 ?
As20 S5 As16 111.64(18) 4_565 4_564 ?
As14 S5 As16 122.06(19) 2_546 4_564 ?
As15 S5 As16 70.63(19) 2_556 4_564 ?
As15 S5 As16 69.8(2) 2_456 4_564 ?
Pb14 S5 As16 124.54(17) 2_546 4_564 ?
As18 S6 Pb6 96.1(4) . 2_556 ?
As18 S6 Pb14 103.1(4) . 1_655 ?
Pb6 S6 Pb14 88.7(3) 2_556 1_655 ?
As18 S6 Pb11 91.8(4) . 2_556 ?
Pb6 S6 Pb11 95.2(3) 2_556 2_556 ?
Pb14 S6 Pb11 164.2(5) 1_655 2_556 ?
As18 S6 Pb13 126.1(4) . 1_655 ?
Pb6 S6 Pb13 131.0(4) 2_556 1_655 ?
Pb14 S6 Pb13 61.0(3) 1_655 1_655 ?
Pb11 S6 Pb13 105.8(3) 2_556 1_655 ?
As18 S6 As14 94.7(4) . 1_655 ?
Pb6 S6 As14 87.0(3) 2_556 1_655 ?
Pb14 S6 As14 8.8(4) 1_655 1_655 ?
Pb11 S6 As14 172.9(5) 2_556 1_655 ?
Pb13 S6 As14 68.0(3) 1_655 1_655 ?
As18 S6 As19 165.1(5) . 1_655 ?
Pb6 S6 As19 86.6(3) 2_556 1_655 ?
Pb14 S6 As19 91.7(4) 1_655 1_655 ?
Pb11 S6 As19 73.3(2) 2_556 1_655 ?
Pb13 S6 As19 59.4(2) 1_655 1_655 ?
As14 S6 As19 100.1(4) 1_655 1_655 ?
As18 S6 As17 71.7(3) . 2_556 ?
Pb6 S6 As17 153.3(4) 2_556 2_556 ?
Pb14 S6 As17 116.9(3) 1_655 2_556 ?
Pb11 S6 As17 62.4(2) 2_556 2_556 ?
Pb13 S6 As17 72.6(2) 1_655 2_556 ?
As14 S6 As17 117.0(3) 1_655 2_556 ?
As19 S6 As17 99.5(3) 1_655 2_556 ?
As18 S6 Pb9 52.7(3) . 3_576 ?
Pb6 S6 Pb9 57.9(2) 2_556 3_576 ?
Pb14 S6 Pb9 130.2(3) 1_655 3_576 ?
Pb11 S6 Pb9 63.7(2) 2_556 3_576 ?
Pb13 S6 Pb9 168.3(3) 1_655 3_576 ?
As14 S6 Pb9 122.9(3) 1_655 3_576 ?
As19 S6 Pb9 118.7(3) 1_655 3_576 ?
As17 S6 Pb9 97.1(3) 2_556 3_576 ?
As18 S6 Pb12 39.3(2) . . ?
Pb6 S6 Pb12 123.5(3) 2_556 . ?
Pb14 S6 Pb12 76.4(3) 1_655 . ?
Pb11 S6 Pb12 113.4(3) 2_556 . ?
Pb13 S6 Pb12 87.8(2) 1_655 . ?
As14 S6 Pb12 70.4(3) 1_655 . ?
As19 S6 Pb12 146.5(3) 1_655 . ?
As17 S6 Pb12 60.92(15) 2_556 . ?
Pb9 S6 Pb12 92.0(2) 3_576 . ?
As18 S6 Pb2 63.5(3) . 1_565 ?
Pb6 S6 Pb2 56.31(18) 2_556 1_565 ?
Pb14 S6 Pb2 57.3(2) 1_655 1_565 ?
Pb11 S6 Pb2 136.6(3) 2_556 1_565 ?
Pb13 S6 Pb2 117.6(3) 1_655 1_565 ?
As14 S6 Pb2 49.7(2) 1_655 1_565 ?
As19 S6 Pb2 128.7(3) 1_655 1_565 ?
As17 S6 Pb2 130.0(3) 2_556 1_565 ?
Pb9 S6 Pb2 73.15(16) 3_576 1_565 ?
Pb12 S6 Pb2 70.32(14) . 1_565 ?
As18 S6 Pb9 133.1(4) . 3_676 ?
Pb6 S6 Pb9 51.34(19) 2_556 3_676 ?
Pb14 S6 Pb9 52.0(2) 1_655 3_676 ?
Pb11 S6 Pb9 120.3(3) 2_556 3_676 ?
Pb13 S6 Pb9 80.1(2) 1_655 3_676 ?
As14 S6 Pb9 56.5(3) 1_655 3_676 ?
As19 S6 Pb9 59.03(19) 1_655 3_676 ?
As17 S6 Pb9 151.7(3) 2_556 3_676 ?
Pb9 S6 Pb9 109.2(2) 3_576 3_676 ?
Pb12 S6 Pb9 126.3(2) . 3_676 ?
Pb2 S6 Pb9 69.88(15) 1_565 3_676 ?
Pb11 S7 Pb1 99.2(4) . . ?
Pb11 S7 Pb8 98.8(4) . 1_455 ?
Pb1 S7 Pb8 90.61(17) . 1_455 ?
Pb11 S7 Pb9 98.8(4) . 4_465 ?
Pb1 S7 Pb9 162.0(3) . 4_465 ?
Pb8 S7 Pb9 87.9(5) 1_455 4_465 ?
Pb11 S7 Pb6 100.2(4) . . ?
Pb1 S7 Pb6 89.8(5) . . ?
Pb8 S7 Pb6 160.8(3) 1_455 . ?
Pb9 S7 Pb6 85.81(16) 4_465 . ?
Pb11 S7 As18 58.96(11) . 2_446 ?
Pb1 S7 As18 132.9(5) . 2_446 ?
Pb8 S7 As18 130.9(5) 1_455 2_446 ?
Pb9 S7 As18 57.75(14) 4_465 2_446 ?
Pb6 S7 As18 58.65(14) . 2_446 ?
Pb11 S7 Pb13 172.1(2) . . ?
Pb1 S7 Pb13 76.38(17) . . ?
Pb8 S7 Pb13 75.00(17) 1_455 . ?
Pb9 S7 Pb13 85.9(2) 4_465 . ?
Pb6 S7 Pb13 86.4(2) . . ?
As18 S7 Pb13 128.78(14) 2_446 . ?
Pb11 S7 As19 56.5(3) . 2_546 ?
Pb1 S7 As19 56.7(3) . 2_546 ?
Pb8 S7 As19 129.0(2) 1_455 2_546 ?
Pb9 S7 As19 135.2(2) 4_465 2_546 ?
Pb6 S7 As19 66.0(3) . 2_546 ?
As18 S7 As19 77.7(2) 2_446 2_546 ?
Pb13 S7 As19 123.7(4) . 2_546 ?
Pb11 S7 As19 56.5(3) . 2_446 ?
Pb1 S7 As19 127.8(2) . 2_446 ?
Pb8 S7 As19 55.3(3) 1_455 2_446 ?
Pb9 S7 As19 64.7(3) 4_465 2_446 ?
Pb6 S7 As19 135.8(2) . 2_446 ?
As18 S7 As19 77.4(2) 2_446 2_446 ?
Pb13 S7 As19 121.1(4) . 2_446 ?
As19 S7 As19 112.17(13) 2_546 2_446 ?
Pb11 S7 As19 146.78(18) . . ?
Pb1 S7 As19 105.4(3) . . ?
Pb8 S7 As19 102.9(3) 1_455 . ?
Pb9 S7 As19 57.70(14) 4_465 . ?
Pb6 S7 As19 58.54(14) . . ?
As18 S7 As19 87.85(11) 2_446 . ?
Pb13 S7 As19 40.93(6) . . ?
As19 S7 As19 121.8(4) 2_546 . ?
As19 S7 As19 119.1(4) 2_446 . ?
Pb11 S7 As20 97.43(15) . 3_566 ?
Pb1 S7 As20 45.48(17) . 3_566 ?
Pb8 S7 As20 45.63(16) 1_455 3_566 ?
Pb9 S7 As20 132.6(5) 4_465 3_566 ?
Pb6 S7 As20 134.1(5) . 3_566 ?
As18 S7 As20 156.38(16) 2_446 3_566 ?
Pb13 S7 As20 74.80(9) . 3_566 ?
As19 S7 As20 90.2(2) 2_546 3_566 ?
As19 S7 As20 88.8(2) 2_446 3_566 ?
As19 S7 As20 115.72(12) . 3_566 ?
As18 S8 Pb6 95.4(4) 1_545 2_546 ?
As18 S8 Pb9 91.9(4) 1_545 3_566 ?
Pb6 S8 Pb9 86.75(17) 2_546 3_566 ?
As18 S8 Pb2 115.5(5) 1_545 . ?
Pb6 S8 Pb2 90.6(5) 2_546 . ?
Pb9 S8 Pb2 152.7(2) 3_566 . ?
As18 S8 Pb3 112.1(5) 1_545 2_446 ?
Pb6 S8 Pb3 152.2(2) 2_546 2_446 ?
Pb9 S8 Pb3 88.3(5) 3_566 2_446 ?
Pb2 S8 Pb3 81.42(16) . 2_446 ?
As18 S8 As19 152.5(3) 1_545 2_546 ?
Pb6 S8 As19 67.83(16) 2_546 2_546 ?
Pb9 S8 As19 66.51(16) 3_566 2_546 ?
Pb2 S8 As19 87.3(2) . 2_546 ?
Pb3 S8 As19 85.1(2) 2_446 2_546 ?
As18 S8 As14 66.8(4) 1_545 1_645 ?
Pb6 S8 As14 67.3(4) 2_546 1_645 ?
Pb9 S8 As14 143.5(3) 3_566 1_645 ?
Pb2 S8 As14 57.1(3) . 1_645 ?
Pb3 S8 As14 126.5(2) 2_446 1_645 ?
As19 S8 As14 120.8(4) 2_546 1_645 ?
As18 S8 Pb14 63.2(4) 1_545 1_645 ?
Pb6 S8 Pb14 61.7(3) 2_546 1_645 ?
Pb9 S8 Pb14 135.4(3) 3_566 1_645 ?
Pb2 S8 Pb14 64.3(3) . 1_645 ?
Pb3 S8 Pb14 134.3(2) 2_446 1_645 ?
As19 S8 Pb14 120.3(4) 2_546 1_645 ?
As14 S8 Pb14 8.11(7) 1_645 1_645 ?
As18 S8 As14 63.5(5) 1_545 1_545 ?
Pb6 S8 As14 143.1(3) 2_546 1_545 ?
Pb9 S8 As14 65.5(3) 3_566 1_545 ?
Pb2 S8 As14 125.3(3) . 1_545 ?
Pb3 S8 As14 55.5(3) 2_446 1_545 ?
As19 S8 As14 116.9(4) 2_546 1_545 ?
As14 S8 As14 122.2(2) 1_645 1_545 ?
Pb14 S8 As14 122.5(2) 1_645 1_545 ?
As18 S8 Pb14 59.7(4) 1_545 1_545 ?
Pb6 S8 Pb14 135.0(3) 2_546 1_545 ?
Pb9 S8 Pb14 60.0(3) 3_566 1_545 ?
Pb2 S8 Pb14 132.9(3) . 1_545 ?
Pb3 S8 Pb14 62.6(3) 2_446 1_545 ?
As19 S8 Pb14 116.6(4) 2_546 1_545 ?
As14 S8 Pb14 122.3(2) 1_645 1_545 ?
Pb14 S8 Pb14 121.26(16) 1_645 1_545 ?
As14 S8 Pb14 8.01(7) 1_545 1_545 ?
As18 S8 Pb11 47.68(14) 1_545 2_546 ?
Pb6 S8 Pb11 61.18(13) 2_546 2_546 ?
Pb9 S8 Pb11 59.77(13) 3_566 2_546 ?
Pb2 S8 Pb11 140.0(5) . 2_546 ?
Pb3 S8 Pb11 136.6(5) 2_446 2_546 ?
As19 S8 Pb11 105.02(12) 2_546 2_546 ?
As14 S8 Pb11 84.7(2) 1_645 2_546 ?
Pb14 S8 Pb11 76.91(18) 1_645 2_546 ?
As14 S8 Pb11 83.2(2) 1_545 2_546 ?
Pb14 S8 Pb11 75.47(18) 1_545 2_546 ?
As18 S8 Pb12 36.91(12) 1_545 1_545 ?
Pb6 S8 Pb12 120.4(3) 2_546 1_545 ?
Pb9 S8 Pb12 117.7(3) 3_566 1_545 ?
Pb2 S8 Pb12 86.94(18) . 1_545 ?
Pb3 S8 Pb12 85.95(18) 2_446 1_545 ?
As19 S8 Pb12 170.01(19) 2_546 1_545 ?
As14 S8 Pb12 61.98(19) 1_645 1_545 ?
Pb14 S8 Pb12 64.02(15) 1_645 1_545 ?
As14 S8 Pb12 60.71(19) 1_545 1_545 ?
Pb14 S8 Pb12 62.61(16) 1_545 1_545 ?
Pb11 S8 Pb12 84.58(10) 2_546 1_545 ?
As15 S9 Pb10 92.6(4) 1_554 1_554 ?
As15 S9 Pb12 89.9(5) 1_554 3_566 ?
Pb10 S9 Pb12 106.0(4) 1_554 3_566 ?
As15 S9 Pb21 97.6(4) 1_554 2_545 ?
Pb10 S9 Pb21 97.9(4) 1_554 2_545 ?
Pb12 S9 Pb21 154.6(5) 3_566 2_545 ?
As15 S9 Pb21 122.0(4) 1_554 4_554 ?
Pb10 S9 Pb21 136.0(5) 1_554 4_554 ?
Pb12 S9 Pb21 100.7(4) 3_566 4_554 ?
Pb21 S9 Pb21 54.9(3) 2_545 4_554 ?
As15 S9 As16 168.8(6) 1_554 3_666 ?
Pb10 S9 As16 86.5(3) 1_554 3_666 ?
Pb12 S9 As16 79.6(3) 3_566 3_666 ?
Pb21 S9 As16 93.6(4) 2_545 3_666 ?
Pb21 S9 As16 64.6(3) 4_554 3_666 ?
As15 S9 As21 90.1(6) 1_554 2_545 ?
Pb10 S9 As21 89.7(4) 1_554 2_545 ?
Pb12 S9 As21 164.4(5) 3_566 2_545 ?
Pb21 S9 As21 11.5(4) 2_545 2_545 ?
Pb21 S9 As21 66.3(4) 4_554 2_545 ?
As16 S9 As21 101.1(6) 3_666 2_545 ?
As15 S9 As15 62.7(3) 1_554 3_556 ?
Pb10 S9 As15 152.5(5) 1_554 3_556 ?
Pb12 S9 As15 64.9(3) 3_566 3_556 ?
Pb21 S9 As15 97.1(3) 2_545 3_556 ?
Pb21 S9 As15 71.1(3) 4_554 3_556 ?
As16 S9 As15 115.3(3) 3_666 3_556 ?
As21 S9 As15 101.4(5) 2_545 3_556 ?
As15 S9 As21 125.3(6) 1_554 4_554 ?
Pb10 S9 As21 139.0(7) 1_554 4_554 ?
Pb12 S9 As21 90.8(5) 3_566 4_554 ?
Pb21 S9 As21 65.1(4) 2_545 4_554 ?
Pb21 S9 As21 10.3(3) 4_554 4_554 ?
As16 S9 As21 59.5(4) 3_666 4_554 ?
As21 S9 As21 76.5(7) 2_545 4_554 ?
As15 S9 As21 68.5(5) 3_556 4_554 ?
As15 S9 Pb4 51.9(3) 1_554 2_445 ?
Pb10 S9 Pb4 56.2(2) 1_554 2_445 ?
Pb12 S9 Pb4 69.7(3) 3_566 2_445 ?
Pb21 S9 Pb4 133.0(4) 2_545 2_445 ?
Pb21 S9 Pb4 167.5(4) 4_554 2_445 ?
As16 S9 Pb4 119.6(3) 3_666 2_445 ?
As21 S9 Pb4 121.6(5) 2_545 2_445 ?
As15 S9 Pb4 97.0(3) 3_556 2_445 ?
As21 S9 Pb4 159.7(6) 4_554 2_445 ?
As15 S9 Pb5 121.9(4) 1_554 4_554 ?
Pb10 S9 Pb5 53.78(19) 1_554 4_554 ?
Pb12 S9 Pb5 63.3(2) 3_566 4_554 ?
Pb21 S9 Pb5 129.1(4) 2_545 4_554 ?
Pb21 S9 Pb5 113.5(3) 4_554 4_554 ?
As16 S9 Pb5 49.45(18) 3_666 4_554 ?
As21 S9 Pb5 128.8(5) 2_545 4_554 ?
As15 S9 Pb5 127.9(3) 3_556 4_554 ?
As21 S9 Pb5 106.7(3) 4_554 4_554 ?
Pb4 S9 Pb5 70.27(17) 2_445 4_554 ?
As15 S9 Pb12 38.6(2) 1_554 1_544 ?
Pb10 S9 Pb12 119.6(3) 1_554 1_544 ?
Pb12 S9 Pb12 106.1(3) 3_566 1_544 ?
Pb21 S9 Pb12 67.8(2) 2_545 1_544 ?
Pb21 S9 Pb12 84.3(2) 4_554 1_544 ?
As16 S9 Pb12 148.8(4) 3_666 1_544 ?
As21 S9 Pb12 65.3(5) 2_545 1_544 ?
As15 S9 Pb12 47.47(15) 3_556 1_544 ?
As21 S9 Pb12 89.5(4) 4_554 1_544 ?
Pb4 S9 Pb12 90.5(2) 2_445 1_544 ?
Pb5 S9 Pb12 160.1(3) 4_554 1_544 ?
As16 S10 Pb5 98.7(5) . 2_456 ?
As16 S10 Pb12 103.2(5) . 1_455 ?
Pb5 S10 Pb12 103.2(4) 2_456 1_455 ?
As16 S10 Pb13 92.7(5) . . ?
Pb5 S10 Pb13 104.9(4) 2_456 . ?
Pb12 S10 Pb13 145.0(5) 1_455 . ?
As16 S10 As17 169.4(6) . 2_456 ?
Pb5 S10 As17 82.0(3) 2_456 2_456 ?
Pb12 S10 As17 86.9(4) 1_455 2_456 ?
Pb13 S10 As17 76.9(3) . 2_456 ?
As16 S10 Pb14 69.0(4) . . ?
Pb5 S10 Pb14 154.6(6) 2_456 . ?
Pb12 S10 Pb14 101.2(4) 1_455 . ?
Pb13 S10 Pb14 55.6(2) . . ?
As17 S10 Pb14 106.0(3) 2_456 . ?
As16 S10 As14 63.4(4) . . ?
Pb5 S10 As14 157.7(6) 2_456 . ?
Pb12 S10 As14 94.3(4) 1_455 . ?
Pb13 S10 As14 65.1(3) . . ?
As17 S10 As14 113.0(4) 2_456 . ?
Pb14 S10 As14 9.92(11) . . ?
As16 S10 As18 124.1(5) . 1_455 ?
Pb5 S10 As18 135.2(5) 2_456 1_455 ?
Pb12 S10 As18 58.3(2) 1_455 1_455 ?
Pb13 S10 As18 87.0(3) . 1_455 ?
As17 S10 As18 58.4(2) 2_456 1_455 ?
Pb14 S10 As18 65.3(3) . 1_455 ?
As14 S10 As18 66.2(4) . 1_455 ?
As16 S10 Pb7 54.4(3) . . ?
Pb5 S10 Pb7 58.9(2) 2_456 . ?
Pb12 S10 Pb7 142.8(3) 1_455 . ?
Pb13 S10 Pb7 71.2(3) . . ?
As17 S10 Pb7 118.7(3) 2_456 . ?
Pb14 S10 Pb7 97.1(4) . . ?
As14 S10 Pb7 98.9(4) . . ?
As18 S10 Pb7 157.6(3) 1_455 . ?
As16 S10 As21 44.2(5) . 2_456 ?
Pb5 S10 As21 136.1(4) 2_456 2_456 ?
Pb12 S10 As21 72.3(5) 1_455 2_456 ?
Pb13 S10 As21 100.3(5) . 2_456 ?
As17 S10 As21 139.2(5) 2_456 2_456 ?
Pb14 S10 As21 47.9(3) . 2_456 ?
As14 S10 As21 38.1(3) . 2_456 ?
As18 S10 As21 80.9(4) 1_455 2_456 ?
Pb7 S10 As21 97.7(5) . 2_456 ?
As16 S10 Pb10 63.9(3) . 3_467 ?
Pb5 S10 Pb10 58.1(2) 2_456 3_467 ?
Pb12 S10 Pb10 68.7(2) 1_455 3_467 ?
Pb13 S10 Pb10 145.4(4) . 3_467 ?
As17 S10 Pb10 124.1(4) 2_456 3_467 ?
Pb14 S10 Pb10 127.2(3) . 3_467 ?
As14 S10 Pb10 118.1(3) . 3_467 ?
As18 S10 Pb10 127.0(3) 1_455 3_467 ?
Pb7 S10 Pb10 74.34(18) . 3_467 ?
As21 S10 Pb10 81.0(3) 2_456 3_467 ?
As16 S10 Pb21 40.3(3) . 2_456 ?
Pb5 S10 Pb21 127.7(3) 2_456 2_456 ?
Pb12 S10 Pb21 70.0(3) 1_455 2_456 ?
Pb13 S10 Pb21 107.1(4) . 2_456 ?
As17 S10 Pb21 145.0(4) 2_456 2_456 ?
Pb14 S10 Pb21 56.3(2) . 2_456 ?
As14 S10 Pb21 46.57(19) . 2_456 ?
As18 S10 Pb21 86.8(3) 1_455 2_456 ?
Pb7 S10 Pb21 94.7(3) . 2_456 ?
As21 S10 Pb21 8.7(2) 2_456 2_456 ?
Pb10 S10 Pb21 72.27(17) 3_467 2_456 ?
As16 S11 Pb7 93.5(4) . . ?
As16 S11 Pb13 91.4(5) . . ?
Pb7 S11 Pb13 107.1(4) . . ?
As16 S11 Pb12 97.0(4) . . ?
Pb7 S11 Pb12 101.7(4) . . ?
Pb13 S11 Pb12 149.5(4) . . ?
As16 S11 As17 172.7(6) . 2_556 ?
Pb7 S11 As17 85.7(3) . 2_556 ?
Pb13 S11 As17 81.8(3) . 2_556 ?
Pb12 S11 As17 90.3(4) . 2_556 ?
As16 S11 Pb14 69.0(3) . . ?
Pb7 S11 Pb14 154.5(5) . . ?
Pb13 S11 Pb14 57.1(2) . . ?
Pb12 S11 Pb14 98.9(4) . . ?
As17 S11 Pb14 109.2(3) 2_556 . ?
As16 S11 As14 62.9(4) . . ?
Pb7 S11 As14 154.3(6) . . ?
Pb13 S11 As14 66.2(3) . . ?
Pb12 S11 As14 91.7(4) . . ?
As17 S11 As14 116.3(4) 2_556 . ?
Pb14 S11 As14 9.85(10) . . ?
As16 S11 As18 122.2(4) . . ?
Pb7 S11 As18 139.5(5) . . ?
Pb13 S11 As18 91.7(3) . . ?
Pb12 S11 As18 59.1(2) . . ?
As17 S11 As18 61.3(2) 2_556 . ?
Pb14 S11 As18 65.1(3) . . ?
As14 S11 As18 66.1(3) . . ?
As16 S11 Pb5 53.1(3) . 2_456 ?
Pb7 S11 Pb5 57.1(2) . 2_456 ?
Pb13 S11 Pb5 70.3(3) . 2_456 ?
Pb12 S11 Pb5 136.7(3) . 2_456 ?
As17 S11 Pb5 121.2(3) 2_556 2_456 ?
Pb14 S11 Pb5 97.5(4) . 2_456 ?
As14 S11 Pb5 98.4(4) . 2_456 ?
As18 S11 Pb5 160.4(3) . 2_456 ?
As16 S11 As21 42.2(4) . 2_456 ?
Pb7 S11 As21 129.6(4) . 2_456 ?
Pb13 S11 As21 98.4(4) . 2_456 ?
Pb12 S11 As21 70.0(5) . 2_456 ?
As17 S11 As21 141.5(5) 2_556 2_456 ?
Pb14 S11 As21 46.3(3) . 2_456 ?
As14 S11 As21 36.5(3) . 2_456 ?
As18 S11 As21 80.3(4) . 2_456 ?
Pb5 S11 As21 94.3(5) 2_456 2_456 ?
As16 S11 Pb4 60.4(3) . 4_465 ?
Pb7 S11 Pb4 55.0(2) . 4_465 ?
Pb13 S11 Pb4 141.9(4) . 4_465 ?
Pb12 S11 Pb4 65.3(2) . 4_465 ?
As17 S11 Pb4 124.1(3) 2_556 4_465 ?
Pb14 S11 Pb4 123.2(3) . 4_465 ?
As14 S11 Pb4 114.0(3) . 4_465 ?
As18 S11 Pb4 124.3(3) . 4_465 ?
Pb5 S11 Pb4 72.13(17) 2_456 4_465 ?
As21 S11 Pb4 78.2(3) 2_456 4_465 ?
As16 S11 Pb5 128.7(4) . 2_556 ?
Pb7 S11 Pb5 51.5(2) . 2_556 ?
Pb13 S11 Pb5 130.6(3) . 2_556 ?
Pb12 S11 Pb5 62.9(2) . 2_556 ?
As17 S11 Pb5 55.8(2) 2_556 2_556 ?
Pb14 S11 Pb5 153.9(4) . 2_556 ?
As14 S11 Pb5 151.8(4) . 2_556 ?
As18 S11 Pb5 88.9(3) . 2_556 ?
Pb5 S11 Pb5 108.6(2) 2_456 2_556 ?
As21 S11 Pb5 130.2(4) 2_456 2_556 ?
Pb4 S11 Pb5 68.44(16) 4_465 2_556 ?
As14 S12 As21 77.6(9) 1_545 2_446 ?
As14 S12 Pb14 11.2(5) 1_545 1_545 ?
As21 S12 Pb14 88.1(8) 2_446 1_545 ?
As14 S12 Pb21 87.4(6) 1_545 2_446 ?
As21 S12 Pb21 12.7(6) 2_446 2_446 ?
Pb14 S12 Pb21 97.2(5) 1_545 2_446 ?
As14 S12 Pb3 91.6(5) 1_545 2_446 ?
As21 S12 Pb3 93.6(6) 2_446 2_446 ?
Pb14 S12 Pb3 95.0(4) 1_545 2_446 ?
Pb21 S12 Pb3 101.5(4) 2_446 2_446 ?
As14 S12 Pb12 124.4(6) 1_545 1_545 ?
As21 S12 Pb12 118.4(7) 2_446 1_545 ?
Pb14 S12 Pb12 115.9(5) 1_545 1_545 ?
Pb21 S12 Pb12 106.3(4) 2_446 1_545 ?
Pb3 S12 Pb12 134.6(6) 2_446 1_545 ?
As14 S12 As18 92.4(5) 1_545 1_545 ?
As21 S12 As18 169.3(9) 2_446 1_545 ?
Pb14 S12 As18 81.6(4) 1_545 1_545 ?
Pb21 S12 As18 168.2(5) 2_446 1_545 ?
Pb3 S12 As18 90.3(4) 2_446 1_545 ?
Pb12 S12 As18 64.3(3) 1_545 1_545 ?
As14 S12 As15 165.7(7) 1_545 . ?
As21 S12 As15 88.3(7) 2_446 . ?
Pb14 S12 As15 176.2(6) 1_545 . ?
Pb21 S12 As15 79.0(3) 2_446 . ?
Pb3 S12 As15 86.7(4) 2_446 . ?
Pb12 S12 As15 64.8(3) 1_545 . ?
As18 S12 As15 101.9(4) 1_545 . ?
As14 S12 As16 64.3(4) 1_545 1_545 ?
As21 S12 As16 68.6(6) 2_446 1_545 ?
Pb14 S12 As16 64.3(3) 1_545 1_545 ?
Pb21 S12 As16 65.4(3) 2_446 1_545 ?
Pb3 S12 As16 152.1(6) 2_446 1_545 ?
Pb12 S12 As16 73.2(3) 1_545 1_545 ?
As18 S12 As16 103.9(4) 1_545 1_545 ?
As15 S12 As16 113.0(4) . 1_545 ?
As14 S12 Pb2 50.9(4) 1_545 1_455 ?
As21 S12 Pb2 53.8(6) 2_446 1_455 ?
Pb14 S12 Pb2 60.6(3) 1_545 1_455 ?
Pb21 S12 Pb2 66.3(3) 2_446 1_455 ?
Pb3 S12 Pb2 55.0(2) 2_446 1_455 ?
Pb12 S12 Pb2 170.1(5) 1_545 1_455 ?
As18 S12 Pb2 122.1(4) 1_545 1_455 ?
As15 S12 Pb2 118.0(3) . 1_455 ?
As16 S12 Pb2 97.3(4) 1_545 1_455 ?
As14 S12 Pb9 60.2(4) 1_545 3_566 ?
As21 S12 Pb9 125.7(7) 2_446 3_566 ?
Pb14 S12 Pb9 54.5(3) 1_545 3_566 ?
Pb21 S12 Pb9 138.3(5) 2_446 3_566 ?
Pb3 S12 Pb9 57.9(2) 2_446 3_566 ?
Pb12 S12 Pb9 113.5(3) 1_545 3_566 ?
As18 S12 Pb9 49.42(19) 1_545 3_566 ?
As15 S12 Pb9 129.1(4) . 3_566 ?
As16 S12 Pb9 114.4(3) 1_545 3_566 ?
Pb2 S12 Pb9 72.7(2) 1_455 3_566 ?
As14 S12 Pb2 129.2(5) 1_545 . ?
As21 S12 Pb2 129.7(7) 2_446 . ?
Pb14 S12 Pb2 124.5(4) 1_545 . ?
Pb21 S12 Pb2 128.3(4) 2_446 . ?
Pb3 S12 Pb2 51.3(2) 2_446 . ?
Pb12 S12 Pb2 83.3(3) 1_545 . ?
As18 S12 Pb2 59.9(3) 1_545 . ?
As15 S12 Pb2 59.1(2) . . ?
As16 S12 Pb2 156.0(4) 1_545 . ?
Pb2 S12 Pb2 106.3(3) 1_455 . ?
Pb9 S12 Pb2 70.03(19) 3_566 . ?
As18 S13 Pb9 94.4(5) . 3_576 ?
As18 S13 Pb14 97.6(5) . . ?
Pb9 S13 Pb14 89.6(4) 3_576 . ?
As18 S13 Pb11 91.7(5) . 2_556 ?
Pb9 S13 Pb11 96.9(4) 3_576 2_556 ?
Pb14 S13 Pb11 168.2(6) . 2_556 ?
As18 S13 Pb13 122.8(5) . . ?
Pb9 S13 Pb13 133.1(5) 3_576 . ?
Pb14 S13 Pb13 60.5(3) . . ?
Pb11 S13 Pb13 108.3(4) 2_556 . ?
As18 S13 As14 90.0(5) . . ?
Pb9 S13 As14 87.5(4) 3_576 . ?
Pb14 S13 As14 8.0(4) . . ?
Pb11 S13 As14 175.2(5) 2_556 . ?
Pb13 S13 As14 67.1(3) . . ?
As18 S13 As19 168.7(6) . . ?
Pb9 S13 As19 89.9(4) 3_576 . ?
Pb14 S13 As19 92.9(4) . . ?
Pb11 S13 As19 77.4(3) 2_556 . ?
Pb13 S13 As19 59.4(3) . . ?
As14 S13 As19 100.6(5) . . ?
As18 S13 As17 71.3(4) . 2_556 ?
Pb9 S13 As17 154.2(5) 3_576 2_556 ?
Pb14 S13 As17 113.0(4) . 2_556 ?
Pb11 S13 As17 63.2(3) 2_556 2_556 ?
Pb13 S13 As17 71.7(3) . 2_556 ?
As14 S13 As17 113.2(4) . 2_556 ?
As19 S13 As17 100.7(4) . 2_556 ?
As18 S13 Pb6 52.8(3) . 2_556 ?
Pb9 S13 Pb6 56.9(3) 3_576 2_556 ?
Pb14 S13 Pb6 127.4(4) . 2_556 ?
Pb11 S13 Pb6 64.2(3) 2_556 2_556 ?
Pb13 S13 Pb6 169.5(4) . 2_556 ?
As14 S13 Pb6 120.3(4) . 2_556 ?
As19 S13 Pb6 122.7(3) . 2_556 ?
As17 S13 Pb6 98.0(3) 2_556 2_556 ?
As18 S13 Pb12 37.3(2) . . ?
Pb9 S13 Pb12 120.7(4) 3_576 . ?
Pb14 S13 Pb12 72.7(3) . . ?
Pb11 S13 Pb12 111.7(4) 2_556 . ?
Pb13 S13 Pb12 86.2(3) . . ?
As14 S13 Pb12 67.4(3) . . ?
As19 S13 Pb12 145.2(4) . . ?
As17 S13 Pb12 59.53(18) 2_556 . ?
Pb6 S13 Pb12 90.1(3) 2_556 . ?
As18 S13 Pb8 123.7(5) . 2_456 ?
Pb9 S13 Pb8 52.1(2) 3_576 2_456 ?
Pb14 S13 Pb8 121.7(4) . 2_456 ?
Pb11 S13 Pb8 57.1(2) 2_556 2_456 ?
Pb13 S13 Pb8 111.7(3) . 2_456 ?
As14 S13 Pb8 125.1(4) . 2_456 ?
As19 S13 Pb8 52.29(17) . 2_456 ?
As17 S13 Pb8 117.9(3) 2_556 2_456 ?
Pb6 S13 Pb8 71.04(18) 2_556 2_456 ?
Pb12 S13 Pb8 160.7(3) . 2_456 ?
As18 S13 Pb6 130.8(5) . 2_456 ?
Pb9 S13 Pb6 52.6(2) 3_576 2_456 ?
Pb14 S13 Pb6 53.9(3) . 2_456 ?
Pb11 S13 Pb6 123.7(3) 2_556 2_456 ?
Pb13 S13 Pb6 80.6(3) . 2_456 ?
As14 S13 Pb6 57.7(3) . 2_456 ?
As19 S13 Pb6 59.5(2) . 2_456 ?
As17 S13 Pb6 151.9(4) 2_556 2_456 ?
Pb6 S13 Pb6 109.5(3) 2_556 2_456 ?
Pb12 S13 Pb6 124.5(3) . 2_456 ?
Pb8 S13 Pb6 67.83(17) 2_456 2_456 ?
As19 S14 Pb11 105.1(4) . 2_556 ?
As19 S14 Pb8 97.0(4) . 2_456 ?
Pb11 S14 Pb8 91.8(3) 2_556 2_456 ?
As19 S14 Pb6 99.6(3) . . ?
Pb11 S14 Pb6 90.9(3) 2_556 . ?
Pb8 S14 Pb6 161.8(4) 2_456 . ?
As19 S14 Pb2 131.3(4) . 2_456 ?
Pb11 S14 Pb2 123.3(4) 2_556 2_456 ?
Pb8 S14 Pb2 86.9(2) 2_456 2_456 ?
Pb6 S14 Pb2 76.7(2) . 2_456 ?
As19 S14 Pb1 54.6(2) . 2_456 ?
Pb11 S14 Pb1 132.5(3) 2_556 2_456 ?
Pb8 S14 Pb1 55.55(18) 2_456 2_456 ?
Pb6 S14 Pb1 131.4(3) . 2_456 ?
Pb2 S14 Pb1 91.4(2) 2_456 2_456 ?
As19 S14 Pb9 66.3(2) . 3_576 ?
Pb11 S14 Pb9 60.69(17) 2_556 3_576 ?
Pb8 S14 Pb9 54.43(15) 2_456 3_576 ?
Pb6 S14 Pb9 140.5(3) . 3_576 ?
Pb2 S14 Pb9 141.0(3) 2_456 3_576 ?
Pb1 S14 Pb9 71.88(14) 2_456 3_576 ?
As19 S14 Pb13 36.8(2) . . ?
Pb11 S14 Pb13 76.0(2) 2_556 . ?
Pb8 S14 Pb13 120.0(3) 2_456 . ?
Pb6 S14 Pb13 78.05(19) . . ?
Pb2 S14 Pb13 148.1(3) 2_456 . ?
Pb1 S14 Pb13 90.95(19) 2_456 . ?
Pb9 S14 Pb13 69.19(13) 3_576 . ?
As19 S14 Pb9 58.1(2) . 4_465 ?
Pb11 S14 Pb9 130.0(3) 2_556 4_465 ?
Pb8 S14 Pb9 133.8(3) 2_456 4_465 ?
Pb6 S14 Pb9 53.05(15) . 4_465 ?
Pb2 S14 Pb9 84.69(19) 2_456 4_465 ?
Pb1 S14 Pb9 79.36(18) 2_456 4_465 ?
Pb9 S14 Pb9 124.2(2) 3_576 4_465 ?
Pb13 S14 Pb9 64.51(13) . 4_465 ?
As19 S14 As20 138.5(4) . 4_565 ?
Pb11 S14 As20 95.0(3) 2_556 4_565 ?
Pb8 S14 As20 45.56(15) 2_456 4_565 ?
Pb6 S14 As20 116.3(3) . 4_565 ?
Pb2 S14 As20 48.15(14) 2_456 4_565 ?
Pb1 S14 As20 85.08(18) 2_456 4_565 ?
Pb9 S14 As20 94.46(16) 3_576 4_565 ?
Pb13 S14 As20 163.6(2) . 4_565 ?
Pb9 S14 As20 129.9(2) 4_465 4_565 ?
As19 S14 Pb3 79.8(3) . 1_455 ?
Pb11 S14 Pb3 174.0(3) 2_556 1_455 ?
Pb8 S14 Pb3 91.1(2) 2_456 1_455 ?
Pb6 S14 Pb3 84.8(2) . 1_455 ?
Pb2 S14 Pb3 51.61(14) 2_456 1_455 ?
Pb1 S14 Pb3 53.23(12) 2_456 1_455 ?
Pb9 S14 Pb3 125.1(2) 3_576 1_455 ?
Pb13 S14 Pb3 107.0(2) . 1_455 ?
Pb9 S14 Pb3 49.52(11) 4_465 1_455 ?
As20 S14 Pb3 83.30(18) 4_565 1_455 ?
As19 S14 Pb1 133.6(3) . 2_556 ?
Pb11 S14 Pb1 54.14(18) 2_556 2_556 ?
Pb8 S14 Pb1 50.19(16) 2_456 2_556 ?
Pb6 S14 Pb1 119.3(3) . 2_556 ?
Pb2 S14 Pb1 84.5(2) 2_456 2_556 ?
Pb1 S14 Pb1 105.74(17) 2_456 2_556 ?
Pb9 S14 Pb1 67.67(13) 3_576 2_556 ?
Pb13 S14 Pb1 125.3(2) . 2_556 ?
Pb9 S14 Pb1 168.1(2) 4_465 2_556 ?
As20 S14 Pb1 41.90(13) 4_565 2_556 ?
Pb3 S14 Pb1 124.92(19) 1_455 2_556 ?
As20 S15 Pb3 97.5(4) . 4_464 ?
As20 S15 Pb1 90.2(3) . 3_566 ?
Pb3 S15 Pb1 99.9(4) 4_464 3_566 ?
As20 S15 Pb2 91.6(4) . 3_466 ?
Pb3 S15 Pb2 84.57(16) 4_464 3_466 ?
Pb1 S15 Pb2 174.9(4) 3_566 3_466 ?
As20 S15 Pb8 84.7(4) . 3_466 ?
Pb3 S15 Pb8 177.1(4) 4_464 3_466 ?
Pb1 S15 Pb8 81.96(15) 3_566 3_466 ?
Pb2 S15 Pb8 93.5(4) 3_466 3_466 ?
As20 S15 Pb11 152.0(3) . 3_566 ?
Pb3 S15 Pb11 107.0(2) 4_464 3_566 ?
Pb1 S15 Pb11 72.68(15) 3_566 3_566 ?
Pb2 S15 Pb11 103.8(3) 3_466 3_566 ?
Pb8 S15 Pb11 71.39(15) 3_466 3_566 ?
As20 S15 Pb4 42.9(3) . 4_464 ?
Pb3 S15 Pb4 54.61(13) 4_464 4_464 ?
Pb1 S15 Pb4 98.1(3) 3_566 4_464 ?
Pb2 S15 Pb4 86.41(14) 3_466 4_464 ?
Pb8 S15 Pb4 127.5(2) 3_466 4_464 ?
Pb11 S15 Pb4 158.6(3) 3_566 4_464 ?
As20 S15 Pb10 39.1(2) . 3_466 ?
Pb3 S15 Pb10 86.07(14) 4_464 3_466 ?
Pb1 S15 Pb10 129.1(2) 3_566 3_466 ?
Pb2 S15 Pb10 53.24(13) 3_466 3_466 ?
Pb8 S15 Pb10 94.5(3) 3_466 3_466 ?
Pb11 S15 Pb10 153.3(3) 3_566 3_466 ?
Pb4 S15 Pb10 45.79(6) 4_464 3_466 ?
As20 S15 Pb7 35.1(3) . 3_566 ?
Pb3 S15 Pb7 97.7(3) 4_464 3_566 ?
Pb1 S15 Pb7 55.37(14) 3_566 3_566 ?
Pb2 S15 Pb7 126.7(2) 3_466 3_566 ?
Pb8 S15 Pb7 85.19(14) 3_466 3_566 ?
Pb11 S15 Pb7 125.49(18) 3_566 3_566 ?
Pb4 S15 Pb7 55.37(9) 4_464 3_566 ?
Pb10 S15 Pb7 73.72(9) 3_466 3_566 ?
As20 S15 Pb9 151.0(4) . . ?
Pb3 S15 Pb9 53.51(13) 4_464 . ?
Pb1 S15 Pb9 95.7(3) 3_566 . ?
Pb2 S15 Pb9 85.00(14) 3_466 . ?
Pb8 S15 Pb9 124.27(19) 3_466 . ?
Pb11 S15 Pb9 55.33(10) 3_566 . ?
Pb4 S15 Pb9 108.07(19) 4_464 . ?
Pb10 S15 Pb9 125.75(12) 3_466 . ?
Pb7 S15 Pb9 137.6(3) 3_566 . ?
As20 S15 As19 132.1(5) . 4_564 ?
Pb3 S15 As19 72.7(3) 4_464 4_564 ?
Pb1 S15 As19 48.27(17) 3_566 4_564 ?
Pb2 S15 As19 132.03(19) 3_466 4_564 ?
Pb8 S15 As19 107.27(17) 3_466 4_564 ?
Pb11 S15 As19 48.22(14) 3_566 4_564 ?
Pb4 S15 As19 111.2(3) 4_464 4_564 ?
Pb10 S15 As19 156.3(3) 3_466 4_564 ?
Pb7 S15 As19 98.3(2) 3_566 4_564 ?
Pb9 S15 As19 47.47(10) . 4_564 ?
As20 S15 Pb6 143.8(5) . 4_464 ?
Pb3 S15 Pb6 84.96(15) 4_464 4_464 ?
Pb1 S15 Pb6 125.12(18) 3_566 4_464 ?
Pb2 S15 Pb6 52.53(13) 3_466 4_464 ?
Pb8 S15 Pb6 92.2(2) 3_466 4_464 ?
Pb11 S15 Pb6 54.11(10) 3_566 4_464 ?
Pb4 S15 Pb6 126.22(13) 4_464 4_464 ?
Pb10 S15 Pb6 105.71(19) 3_466 4_464 ?
Pb7 S15 Pb6 177.2(3) 3_566 4_464 ?
Pb9 S15 Pb6 44.92(6) . 4_464 ?
As19 S15 Pb6 83.23(11) 4_564 4_464 ?
As19 S16 Pb11 98.0(4) . 2_456 ?
As19 S16 Pb9 105.6(4) . 4_465 ?
Pb11 S16 Pb9 92.0(3) 2_456 4_465 ?
As19 S16 Pb1 93.2(4) . 2_456 ?
Pb11 S16 Pb1 84.3(3) 2_456 2_456 ?
Pb9 S16 Pb1 161.2(5) 4_465 2_456 ?
As19 S16 Pb3 140.3(5) . 1_455 ?
Pb11 S16 Pb3 121.2(4) 2_456 1_455 ?
Pb9 S16 Pb3 81.1(3) 4_465 1_455 ?
Pb1 S16 Pb3 85.1(3) 2_456 1_455 ?
As19 S16 Pb6 64.5(3) . . ?
Pb11 S16 Pb6 133.1(3) 2_456 . ?
Pb9 S16 Pb6 56.50(18) 4_465 . ?
Pb1 S16 Pb6 136.5(4) 2_456 . ?
Pb3 S16 Pb6 90.0(2) 1_455 . ?
As19 S16 Pb8 55.7(3) . 2_456 ?
Pb11 S16 Pb8 125.7(3) 2_456 2_456 ?
Pb9 S16 Pb8 137.5(4) 4_465 2_456 ?
Pb1 S16 Pb8 55.5(2) 2_456 2_456 ?
Pb3 S16 Pb8 92.6(3) 1_455 2_456 ?
Pb6 S16 Pb8 81.7(2) . 2_456 ?
As19 S16 Pb13 36.3(2) . . ?
Pb11 S16 Pb13 74.1(2) 2_456 . ?
Pb9 S16 Pb13 79.4(2) 4_465 . ?
Pb1 S16 Pb13 116.9(3) 2_456 . ?
Pb3 S16 Pb13 155.7(3) 1_455 . ?
Pb6 S16 Pb13 67.09(16) . . ?
Pb8 S16 Pb13 91.9(2) 2_456 . ?
As19 S16 Pb2 86.6(4) . 2_456 ?
Pb11 S16 Pb2 174.8(4) 2_456 2_456 ?
Pb9 S16 Pb2 89.3(2) 4_465 2_456 ?
Pb1 S16 Pb2 92.9(3) 2_456 2_456 ?
Pb3 S16 Pb2 54.03(16) 1_455 2_456 ?
Pb6 S16 Pb2 51.38(13) . 2_456 ?
Pb8 S16 Pb2 55.08(15) 2_456 2_456 ?
Pb13 S16 Pb2 111.1(3) . 2_456 ?
As19 S16 Pb6 59.0(3) . 2_456 ?
Pb11 S16 Pb6 57.47(18) 2_456 2_456 ?
Pb9 S16 Pb6 139.2(3) 4_465 2_456 ?
Pb1 S16 Pb6 51.49(16) 2_456 2_456 ?
Pb3 S16 Pb6 136.3(3) 1_455 2_456 ?
Pb6 S16 Pb6 123.6(3) . 2_456 ?
Pb8 S16 Pb6 68.65(16) 2_456 2_456 ?
Pb13 S16 Pb6 67.18(15) . 2_456 ?
Pb2 S16 Pb6 123.7(3) 2_456 2_456 ?
As19 S16 As20 135.6(4) . 4_465 ?
Pb11 S16 As20 89.7(3) 2_456 4_465 ?
Pb9 S16 As20 117.9(3) 4_465 4_465 ?
Pb1 S16 As20 43.90(16) 2_456 4_465 ?
Pb3 S16 As20 47.16(15) 1_455 4_465 ?
Pb6 S16 As20 134.1(2) . 4_465 ?
Pb8 S16 As20 84.5(2) 2_456 4_465 ?
Pb13 S16 As20 157.1(2) . 4_465 ?
Pb2 S16 As20 85.22(19) 2_456 4_465 ?
Pb6 S16 As20 90.62(17) 2_456 4_465 ?
As19 S16 Pb6 134.1(4) . 1_455 ?
Pb11 S16 Pb6 55.0(2) 2_456 1_455 ?
Pb9 S16 Pb6 48.44(19) 4_465 1_455 ?
Pb1 S16 Pb6 116.5(3) 2_456 1_455 ?
Pb3 S16 Pb6 79.8(3) 1_455 1_455 ?
Pb6 S16 Pb6 104.9(2) . 1_455 ?
Pb8 S16 Pb6 169.8(3) 2_456 1_455 ?
Pb13 S16 Pb6 97.8(2) . 1_455 ?
Pb2 S16 Pb6 123.1(2) 2_456 1_455 ?
Pb6 S16 Pb6 112.3(2) 2_456 1_455 ?
As20 S16 Pb6 85.3(2) 4_465 1_455 ?
As21 S17 As14 81.0(9) 2_446 1_545 ?
As21 S17 Pb21 13.5(8) 2_446 2_446 ?
As14 S17 Pb21 91.3(6) 1_545 2_446 ?
As21 S17 Pb14 90.1(9) 2_446 1_545 ?
As14 S17 Pb14 9.9(5) 1_545 1_545 ?
Pb21 S17 Pb14 99.7(5) 2_446 1_545 ?
As21 S17 Pb2 100.5(6) 2_446 1_455 ?
As14 S17 Pb2 94.2(5) 1_545 1_455 ?
Pb21 S17 Pb2 108.5(4) 2_446 1_455 ?
Pb14 S17 Pb2 96.3(4) 1_545 1_455 ?
As21 S17 Pb12 117.5(7) 2_446 1_445 ?
As14 S17 Pb12 118.3(5) 1_545 1_445 ?
Pb21 S17 Pb12 104.9(4) 2_446 1_445 ?
Pb14 S17 Pb12 110.6(4) 1_545 1_445 ?
Pb2 S17 Pb12 132.3(5) 1_455 1_445 ?
As21 S17 As15 91.9(8) 2_446 1_455 ?
As14 S17 As15 172.5(6) 1_545 1_455 ?
Pb21 S17 As15 81.3(3) 2_446 1_455 ?
Pb14 S17 As15 173.5(5) 1_545 1_455 ?
Pb2 S17 As15 89.4(3) 1_455 1_455 ?
Pb12 S17 As15 63.1(2) 1_445 1_455 ?
As21 S17 As18 166.7(8) 2_446 1_445 ?
As14 S17 As18 88.7(5) 1_545 1_445 ?
Pb21 S17 As18 162.9(5) 2_446 1_445 ?
Pb14 S17 As18 79.1(4) 1_545 1_445 ?
Pb2 S17 As18 88.6(3) 1_455 1_445 ?
Pb12 S17 As18 60.5(2) 1_445 1_445 ?
As15 S17 As18 98.0(4) 1_455 1_445 ?
As21 S17 As16 69.2(5) 2_446 1_545 ?
As14 S17 As16 63.1(4) 1_545 1_545 ?
Pb21 S17 As16 66.3(3) 2_446 1_545 ?
Pb14 S17 As16 62.8(3) 1_545 1_545 ?
Pb2 S17 As16 155.7(5) 1_455 1_545 ?
Pb12 S17 As16 70.2(3) 1_445 1_545 ?
As15 S17 As16 112.3(3) 1_455 1_545 ?
As18 S17 As16 98.6(3) 1_445 1_545 ?
As21 S17 Pb3 57.4(7) 2_446 2_446 ?
As14 S17 Pb3 53.9(4) 1_545 2_446 ?
Pb21 S17 Pb3 70.6(3) 2_446 2_446 ?
Pb14 S17 Pb3 62.4(3) 1_545 2_446 ?
Pb2 S17 Pb3 57.5(2) 1_455 2_446 ?
Pb12 S17 Pb3 169.9(4) 1_445 2_446 ?
As15 S17 Pb3 123.7(3) 1_455 2_446 ?
As18 S17 Pb3 122.1(3) 1_445 2_446 ?
As16 S17 Pb3 99.7(3) 1_545 2_446 ?
As21 S17 Pb10 64.6(6) 2_446 1_455 ?
As14 S17 Pb10 127.3(5) 1_545 1_455 ?
Pb21 S17 Pb10 63.3(2) 2_446 1_455 ?
Pb14 S17 Pb10 136.1(4) 1_545 1_455 ?
Pb2 S17 Pb10 57.7(2) 1_455 1_455 ?
Pb12 S17 Pb10 112.8(3) 1_445 1_455 ?
As15 S17 Pb10 49.99(18) 1_455 1_455 ?
As18 S17 Pb10 128.7(4) 1_445 1_455 ?
As16 S17 Pb10 128.4(3) 1_545 1_455 ?
Pb3 S17 Pb10 73.74(18) 2_446 1_455 ?
As21 S17 Pb6 129.0(9) 2_446 2_446 ?
As14 S17 Pb6 59.3(4) 1_545 2_446 ?
Pb21 S17 Pb6 142.4(4) 2_446 2_446 ?
Pb14 S17 Pb6 54.2(3) 1_545 2_446 ?
Pb2 S17 Pb6 56.5(2) 1_455 2_446 ?
Pb12 S17 Pb6 109.5(3) 1_445 2_446 ?
As15 S17 Pb6 127.9(3) 1_455 2_446 ?
As18 S17 Pb6 49.33(17) 1_445 2_446 ?
As16 S17 Pb6 112.0(3) 1_545 2_446 ?
Pb3 S17 Pb6 72.92(18) 2_446 2_446 ?
Pb10 S17 Pb6 114.2(2) 1_455 2_446 ?
As17 S18 Pb8 103.7(5) . 2_446 ?
As17 S18 Pb13 101.8(4) . 2_546 ?
Pb8 S18 Pb13 110.6(5) 2_446 2_546 ?
As17 S18 Pb9 134.5(6) . 3_566 ?
Pb8 S18 Pb9 83.3(3) 2_446 3_566 ?
Pb13 S18 Pb9 118.0(5) 2_546 3_566 ?
As17 S18 Pb11 70.1(4) . . ?
Pb8 S18 Pb11 150.3(5) 2_446 . ?
Pb13 S18 Pb11 99.1(4) 2_546 . ?
Pb9 S18 Pb11 81.9(3) 3_566 . ?
As17 S18 As19 121.2(5) . 2_546 ?
Pb8 S18 As19 134.4(5) 2_446 2_546 ?
Pb13 S18 As19 55.9(2) 2_546 2_546 ?
Pb9 S18 As19 71.3(2) 3_566 2_546 ?
Pb11 S18 As19 63.1(2) . 2_546 ?
As17 S18 Pb5 63.6(3) . . ?
Pb8 S18 Pb5 64.7(2) 2_446 . ?
Pb13 S18 Pb5 71.7(2) 2_546 . ?
Pb9 S18 Pb5 147.5(4) 3_566 . ?
Pb11 S18 Pb5 129.0(3) . . ?
As19 S18 Pb5 127.5(3) 2_546 . ?
As17 S18 Pb1 59.0(3) . 2_446 ?
Pb8 S18 Pb1 58.1(3) 2_446 2_446 ?
Pb13 S18 Pb1 148.8(3) 2_546 2_446 ?
Pb9 S18 Pb1 90.8(3) 3_566 2_446 ?
Pb11 S18 Pb1 96.5(3) . 2_446 ?
As19 S18 Pb1 154.0(3) 2_546 2_446 ?
Pb5 S18 Pb1 77.5(2) . 2_446 ?
As17 S18 Pb6 79.6(4) . 2_446 ?
Pb8 S18 Pb6 90.3(3) 2_446 2_446 ?
Pb13 S18 Pb6 157.7(4) 2_546 2_446 ?
Pb9 S18 Pb6 55.2(2) 3_566 2_446 ?
Pb11 S18 Pb6 60.1(2) . 2_446 ?
As19 S18 Pb6 104.2(2) 2_546 2_446 ?
Pb5 S18 Pb6 126.6(3) . 2_446 ?
Pb1 S18 Pb6 49.92(16) 2_446 2_446 ?
As17 S18 As18 43.2(3) . 2_446 ?
Pb8 S18 As18 142.4(4) 2_446 2_446 ?
Pb13 S18 As18 70.5(3) 2_546 2_446 ?
Pb9 S18 As18 130.9(3) 3_566 2_446 ?
Pb11 S18 As18 49.57(17) . 2_446 ?
As19 S18 As18 78.9(2) 2_546 2_446 ?
Pb5 S18 As18 81.38(19) . 2_446 ?
Pb1 S18 As18 100.6(3) 2_446 2_446 ?
Pb6 S18 As18 97.8(3) 2_446 2_446 ?
As17 S18 Pb1 137.3(4) . 2_546 ?
Pb8 S18 Pb1 51.2(3) 2_446 2_546 ?
Pb13 S18 Pb1 66.7(3) 2_546 2_546 ?
Pb9 S18 Pb1 81.9(3) 3_566 2_546 ?
Pb11 S18 Pb1 149.6(4) . 2_546 ?
As19 S18 Pb1 87.4(3) 2_546 2_546 ?
Pb5 S18 Pb1 73.86(19) . 2_546 ?
Pb1 S18 Pb1 109.2(2) 2_446 2_546 ?
Pb6 S18 Pb1 126.8(3) 2_446 2_546 ?
As18 S18 Pb1 135.3(3) 2_446 2_546 ?
As17 S18 Pb6 173.2(5) . 2_546 ?
Pb8 S18 Pb6 82.6(3) 2_446 2_546 ?
Pb13 S18 Pb6 73.3(3) 2_546 2_546 ?
Pb9 S18 Pb6 48.0(2) 3_566 2_546 ?
Pb11 S18 Pb6 105.8(3) . 2_546 ?
As19 S18 Pb6 52.25(19) 2_546 2_546 ?
Pb5 S18 Pb6 117.9(3) . 2_546 ?
Pb1 S18 Pb6 127.5(3) 2_446 2_546 ?
Pb6 S18 Pb6 103.2(2) 2_446 2_546 ?
As18 S18 Pb6 130.0(3) 2_446 2_546 ?
Pb1 S18 Pb6 45.47(14) 2_546 2_546 ?
As14 S19 Pb14 15.35(14) 1_545 1_545 ?
As14 S19 Pb3 93.7(5) 1_545 2_446 ?
Pb14 S19 Pb3 104.7(5) 1_545 2_446 ?
As14 S19 Pb9 108.4(6) 1_545 3_566 ?
Pb14 S19 Pb9 96.9(4) 1_545 3_566 ?
Pb3 S19 Pb9 92.7(5) 2_446 3_566 ?
As14 S19 Pb2 92.1(5) 1_545 1_455 ?
Pb14 S19 Pb2 103.2(5) 1_545 1_455 ?
Pb3 S19 Pb2 85.92(18) 2_446 1_455 ?
Pb9 S19 Pb2 159.5(3) 3_566 1_455 ?
As14 S19 Pb6 107.2(6) 1_545 2_446 ?
Pb14 S19 Pb6 96.6(5) 1_545 2_446 ?
Pb3 S19 Pb6 158.7(3) 2_446 2_446 ?
Pb9 S19 Pb6 84.77(16) 3_566 2_446 ?
Pb2 S19 Pb6 89.1(5) 1_455 2_446 ?
As14 S19 As21 41.5(3) 1_545 2_446 ?
Pb14 S19 As21 56.8(2) 1_545 2_446 ?
Pb3 S19 As21 64.1(4) 2_446 2_446 ?
Pb9 S19 As21 134.1(7) 3_566 2_446 ?
Pb2 S19 As21 62.9(4) 1_455 2_446 ?
Pb6 S19 As21 130.7(7) 2_446 2_446 ?
As14 S19 Pb11 172.0(4) 1_545 . ?
Pb14 S19 Pb11 156.9(3) 1_545 . ?
Pb3 S19 Pb11 93.4(2) 2_446 . ?
Pb9 S19 Pb11 67.55(15) 3_566 . ?
Pb2 S19 Pb11 92.1(2) 1_455 . ?
Pb6 S19 Pb11 66.05(14) 2_446 . ?
As21 S19 Pb11 146.2(3) 2_446 . ?
As14 S19 As18 62.6(6) 1_545 1_545 ?
Pb14 S19 As18 59.1(5) 1_545 1_545 ?
Pb3 S19 As18 69.1(3) 2_446 1_545 ?
Pb9 S19 As18 54.2(3) 3_566 1_545 ?
Pb2 S19 As18 141.9(3) 1_455 1_545 ?
Pb6 S19 As18 124.1(2) 2_446 1_545 ?
As21 S19 As18 80.1(5) 2_446 1_545 ?
Pb11 S19 As18 116.8(3) . 1_545 ?
As14 S19 As18 61.5(6) 1_545 1_445 ?
Pb14 S19 As18 58.8(5) 1_545 1_445 ?
Pb3 S19 As18 140.6(3) 2_446 1_445 ?
Pb9 S19 As18 122.9(2) 3_566 1_445 ?
Pb2 S19 As18 66.5(3) 1_455 1_445 ?
Pb6 S19 As18 53.1(3) 2_446 1_445 ?
As21 S19 As18 78.1(5) 2_446 1_445 ?
Pb11 S19 As18 114.2(3) . 1_445 ?
As18 S19 As18 116.32(15) 1_545 1_445 ?
As14 S19 Pb21 41.3(2) 1_545 2_446 ?
Pb14 S19 Pb21 56.69(16) 1_545 2_446 ?
Pb3 S19 Pb21 64.11(15) 2_446 2_446 ?
Pb9 S19 Pb21 133.9(5) 3_566 2_446 ?
Pb2 S19 Pb21 63.09(15) 1_455 2_446 ?
Pb6 S19 Pb21 130.8(5) 2_446 2_446 ?
As21 S19 Pb21 0.2(4) 2_446 2_446 ?
Pb11 S19 Pb21 146.33(16) . 2_446 ?
As18 S19 Pb21 79.91(19) 1_545 2_446 ?
As18 S19 Pb21 78.1(2) 1_445 2_446 ?
As14 S19 As20 112.1(3) 1_545 3_566 ?
Pb14 S19 As20 127.5(2) 1_545 3_566 ?
Pb3 S19 As20 46.34(17) 2_446 3_566 ?
Pb9 S19 As20 122.3(3) 3_566 3_566 ?
Pb2 S19 As20 45.57(16) 1_455 3_566 ?
Pb6 S19 As20 118.7(4) 2_446 3_566 ?
As21 S19 As20 70.6(2) 2_446 3_566 ?
Pb11 S19 As20 75.58(10) . 3_566 ?
As18 S19 As20 115.3(3) 1_545 3_566 ?
As18 S19 As20 112.1(3) 1_445 3_566 ?
Pb21 S19 As20 70.78(9) 2_446 3_566 ?
As22 S20 Pb5 80.0(4) . . ?
As22 S20 Pb4 81.6(4) . 3_466 ?
Pb5 S20 Pb4 161.6(3) . 3_466 ?
As22 S20 Pb7 81.9(4) . 2_446 ?
Pb5 S20 Pb7 87.9(2) . 2_446 ?
Pb4 S20 Pb7 90.9(7) 3_466 2_446 ?
As22 S20 Pb10 80.7(4) . 4_454 ?
Pb5 S20 Pb10 89.7(7) . 4_454 ?
Pb4 S20 Pb10 86.00(19) 3_466 4_454 ?
Pb7 S20 Pb10 162.6(3) 2_446 4_454 ?
As22 S20 Pb12 178.2(10) . 2_446 ?
Pb5 S20 Pb12 98.3(4) . 2_446 ?
Pb4 S20 Pb12 100.1(4) 3_466 2_446 ?
Pb7 S20 Pb12 98.6(4) 2_446 2_446 ?
Pb10 S20 Pb12 98.7(5) 4_454 2_446 ?
As22 S20 As15 123.3(2) . 4_454 ?
Pb5 S20 As15 132.3(7) . 4_454 ?
Pb4 S20 As15 59.12(17) 3_466 4_454 ?
Pb7 S20 As15 132.4(7) 2_446 4_454 ?
Pb10 S20 As15 59.14(18) 4_454 4_454 ?
Pb12 S20 As15 57.51(12) 2_446 4_454 ?
As22 S20 As16 122.3(8) . 2_446 ?
Pb5 S20 As16 127.2(3) . 2_446 ?
Pb4 S20 As16 65.1(4) 3_466 2_446 ?
Pb7 S20 As16 54.7(4) 2_446 2_446 ?
Pb10 S20 As16 137.0(3) 4_454 2_446 ?
Pb12 S20 As16 59.2(3) 2_446 2_446 ?
As15 S20 As16 78.4(3) 4_454 2_446 ?
As22 S20 As16 119.9(8) . 2_546 ?
Pb5 S20 As16 54.7(4) . 2_546 ?
Pb4 S20 As16 136.6(3) 3_466 2_546 ?
Pb7 S20 As16 126.9(3) 2_446 2_546 ?
Pb10 S20 As16 63.9(4) 4_454 2_546 ?
Pb12 S20 As16 58.3(3) 2_446 2_546 ?
As15 S20 As16 78.3(3) 4_454 2_546 ?
As16 S20 As16 116.52(16) 2_446 2_546 ?
As22 S20 As17 117.6(2) . . ?
Pb5 S20 As17 57.06(15) . . ?
Pb4 S20 As17 135.1(7) 3_466 . ?
Pb7 S20 As17 56.17(15) 2_446 . ?
Pb10 S20 As17 134.5(7) 4_454 . ?
Pb12 S20 As17 61.58(12) 2_446 . ?
As15 S20 As17 119.09(16) 4_454 . ?
As16 S20 As17 70.7(2) 2_446 . ?
As16 S20 As17 71.3(2) 2_546 . ?
As17 S21 Pb13 106.8(5) . 2_446 ?
As17 S21 Pb1 96.7(5) . 2_446 ?
Pb13 S21 Pb1 105.7(4) 2_446 2_446 ?
As17 S21 Pb6 132.4(6) . 2_446 ?
Pb13 S21 Pb6 120.2(5) 2_446 2_446 ?
Pb1 S21 Pb6 78.5(3) 2_446 2_446 ?
As17 S21 Pb11 75.6(4) . . ?
Pb13 S21 Pb11 108.0(4) 2_446 . ?
Pb1 S21 Pb11 146.2(5) 2_446 . ?
Pb6 S21 Pb11 82.9(3) 2_446 . ?
As17 S21 As19 132.1(5) . 2_446 ?
Pb13 S21 As19 58.5(3) 2_446 2_446 ?
Pb1 S21 As19 130.6(5) 2_446 2_446 ?
Pb6 S21 As19 73.8(3) 2_446 2_446 ?
Pb11 S21 As19 68.7(3) . 2_446 ?
As17 S21 As18 47.8(3) . 2_446 ?
Pb13 S21 As18 76.3(3) 2_446 2_446 ?
Pb1 S21 As18 140.8(4) 2_446 2_446 ?
Pb6 S21 As18 135.3(4) 2_446 2_446 ?
Pb11 S21 As18 52.64(19) . 2_446 ?
As19 S21 As18 84.8(3) 2_446 2_446 ?
As17 S21 Pb7 60.9(3) . 2_446 ?
Pb13 S21 Pb7 70.8(3) 2_446 2_446 ?
Pb1 S21 Pb7 62.0(2) 2_446 2_446 ?
Pb6 S21 Pb7 140.3(4) 2_446 2_446 ?
Pb11 S21 Pb7 132.7(4) . 2_446 ?
As19 S21 Pb7 129.3(4) 2_446 2_446 ?
As18 S21 Pb7 83.1(2) 2_446 2_446 ?
As17 S21 Pb8 55.4(3) . 2_446 ?
Pb13 S21 Pb8 146.1(4) 2_446 2_446 ?
Pb1 S21 Pb8 55.3(2) 2_446 2_446 ?
Pb6 S21 Pb8 85.8(3) 2_446 2_446 ?
Pb11 S21 Pb8 95.6(4) . 2_446 ?
As19 S21 Pb8 155.4(4) 2_446 2_446 ?
As18 S21 Pb8 101.0(3) 2_446 2_446 ?
Pb7 S21 Pb8 75.3(2) 2_446 2_446 ?
As17 S21 Pb9 79.3(4) . 3_566 ?
Pb13 S21 Pb9 165.7(4) 2_446 3_566 ?
Pb1 S21 Pb9 86.0(3) 2_446 3_566 ?
Pb6 S21 Pb9 53.3(2) 2_446 3_566 ?
Pb11 S21 Pb9 60.3(2) . 3_566 ?
As19 S21 Pb9 107.8(3) 2_446 3_566 ?
As18 S21 Pb9 99.9(3) 2_446 3_566 ?
Pb7 S21 Pb9 122.8(3) 2_446 3_566 ?
Pb8 S21 Pb9 47.80(15) 2_446 3_566 ?
As17 S21 Pb8 131.4(5) . 2_346 ?
Pb13 S21 Pb8 63.6(3) 2_446 2_346 ?
Pb1 S21 Pb8 49.3(2) 2_446 2_346 ?
Pb6 S21 Pb8 80.2(3) 2_446 2_346 ?
Pb11 S21 Pb8 152.5(4) . 2_346 ?
As19 S21 Pb8 85.8(3) 2_446 2_346 ?
As18 S21 Pb8 137.6(3) 2_446 2_346 ?
Pb7 S21 Pb8 71.56(19) 2_446 2_346 ?
Pb8 S21 Pb8 104.5(2) 2_446 2_346 ?
Pb9 S21 Pb8 122.4(3) 3_566 2_346 ?
As17 S21 Pb14 85.2(4) . 2_446 ?
Pb13 S21 Pb14 30.3(2) 2_446 2_446 ?
Pb1 S21 Pb14 130.4(4) 2_446 2_446 ?
Pb6 S21 Pb14 133.6(4) 2_446 2_446 ?
Pb11 S21 Pb14 82.4(3) . 2_446 ?
As19 S21 Pb14 59.8(2) 2_446 2_446 ?
As18 S21 Pb14 46.5(2) 2_446 2_446 ?
Pb7 S21 Pb14 76.7(2) 2_446 2_446 ?
Pb8 S21 Pb14 139.3(3) 2_446 2_446 ?
Pb9 S21 Pb14 142.0(3) 3_566 2_446 ?
Pb8 S21 Pb14 93.8(3) 2_346 2_446 ?
As20 S22 Pb5 85.3(4) . 4_454 ?
As20 S22 Pb7 85.7(4) . 3_566 ?
Pb5 S22 Pb7 87.92(17) 4_454 3_566 ?
As20 S22 Pb8 84.2(4) . 3_466 ?
Pb5 S22 Pb8 94.3(6) 4_454 3_466 ?
Pb7 S22 Pb8 169.5(3) 3_566 3_466 ?
As20 S22 Pb1 83.6(4) . 3_566 ?
Pb5 S22 Pb1 168.8(3) 4_454 3_566 ?
Pb7 S22 Pb1 92.9(6) 3_566 3_566 ?
Pb8 S22 Pb1 82.95(16) 3_466 3_566 ?
As20 S22 Pb13 178.7(3) . 3_566 ?
Pb5 S22 Pb13 95.7(3) 4_454 3_566 ?
Pb7 S22 Pb13 95.2(3) 3_566 3_566 ?
Pb8 S22 Pb13 94.8(3) 3_466 3_566 ?
Pb1 S22 Pb13 95.4(3) 3_566 3_566 ?
As20 S22 As16 125.5(2) . 3_566 ?
Pb5 S22 As16 57.74(16) 4_454 3_566 ?
Pb7 S22 As16 57.25(16) 3_566 3_566 ?
Pb8 S22 As16 132.1(5) 3_466 3_566 ?
Pb1 S22 As16 131.3(5) 3_566 3_566 ?
Pb13 S22 As16 55.84(10) 3_566 3_566 ?
As20 S22 As17 123.0(7) . 4_554 ?
Pb5 S22 As17 131.8(3) 4_454 4_554 ?
Pb7 S22 As17 60.1(3) 3_566 4_554 ?
Pb8 S22 As17 123.9(2) 3_466 4_554 ?
Pb1 S22 As17 57.1(3) 3_566 4_554 ?
Pb13 S22 As17 56.9(2) 3_566 4_554 ?
As16 S22 As17 74.3(2) 3_566 4_554 ?
As20 S22 As17 122.8(7) . 4_454 ?
Pb5 S22 As17 60.8(3) 4_454 4_454 ?
Pb7 S22 As17 132.2(3) 3_566 4_454 ?
Pb8 S22 As17 57.0(3) 3_466 4_454 ?
Pb1 S22 As17 124.9(2) 3_566 4_454 ?
Pb13 S22 As17 57.2(2) 3_566 4_454 ?
As16 S22 As17 75.1(2) 3_566 4_454 ?
As17 S22 As17 113.74(13) 4_554 4_454 ?
As15 S23 Pb4 96.6(5) 1_554 2_445 ?
As15 S23 Pb12 93.7(5) 1_554 3_566 ?
Pb4 S23 Pb12 106.9(4) 2_445 3_566 ?
As15 S23 Pb21 99.0(5) 1_554 2_445 ?
Pb4 S23 Pb21 97.8(4) 2_445 2_445 ?
Pb12 S23 Pb21 150.7(5) 3_566 2_445 ?
As15 S23 As21 91.4(7) 1_554 2_445 ?
Pb4 S23 As21 90.1(4) 2_445 2_445 ?
Pb12 S23 As21 161.6(6) 3_566 2_445 ?
Pb21 S23 As21 11.6(4) 2_445 2_445 ?
As15 S23 Pb21 122.0(5) 1_554 4_454 ?
Pb4 S23 Pb21 132.0(5) 2_445 4_454 ?
Pb12 S23 Pb21 98.6(4) 3_566 4_454 ?
Pb21 S23 Pb21 52.3(3) 2_445 4_454 ?
As21 S23 Pb21 63.8(5) 2_445 4_454 ?
As15 S23 As16 171.5(6) 1_554 3_566 ?
Pb4 S23 As16 84.8(3) 2_445 3_566 ?
Pb12 S23 As16 78.0(3) 3_566 3_566 ?
Pb21 S23 As16 89.0(4) 2_445 3_566 ?
As21 S23 As16 97.0(6) 2_445 3_566 ?
Pb21 S23 As16 61.4(2) 4_454 3_566 ?
As15 S23 As15 64.4(3) 1_554 3_556 ?
Pb4 S23 As15 157.8(5) 2_445 3_556 ?
Pb12 S23 As15 65.6(3) 3_566 3_556 ?
Pb21 S23 As15 96.5(3) 2_445 3_556 ?
As21 S23 As15 101.1(5) 2_445 3_556 ?
Pb21 S23 As15 70.1(3) 4_454 3_556 ?
As16 S23 As15 112.4(3) 3_566 3_556 ?
As15 S23 As21 125.1(6) 1_554 4_454 ?
Pb4 S23 As21 134.8(6) 2_445 4_454 ?
Pb12 S23 As21 88.9(5) 3_566 4_454 ?
Pb21 S23 As21 62.2(4) 2_445 4_454 ?
As21 S23 As21 73.8(8) 2_445 4_454 ?
Pb21 S23 As21 10.0(3) 4_454 4_454 ?
As16 S23 As21 56.8(3) 3_566 4_454 ?
As15 S23 As21 67.2(5) 3_556 4_454 ?
As15 S23 Pb10 54.4(3) 1_554 1_554 ?
Pb4 S23 Pb10 58.3(2) 2_445 1_554 ?
Pb12 S23 Pb10 71.9(3) 3_566 1_554 ?
Pb21 S23 Pb10 136.3(4) 2_445 1_554 ?
As21 S23 Pb10 124.7(5) 2_445 1_554 ?
Pb21 S23 Pb10 168.8(4) 4_454 1_554 ?
As16 S23 Pb10 120.5(3) 3_566 1_554 ?
As15 S23 Pb10 99.9(3) 3_556 1_554 ?
As21 S23 Pb10 160.3(6) 4_454 1_554 ?
As15 S23 Pb12 38.1(3) 1_554 1_544 ?
Pb4 S23 Pb12 122.9(3) 2_445 1_544 ?
Pb12 S23 Pb12 108.0(4) 3_566 1_544 ?
Pb21 S23 Pb12 69.4(3) 2_445 1_544 ?
As21 S23 Pb12 66.5(5) 2_445 1_544 ?
Pb21 S23 Pb12 84.6(3) 4_454 1_544 ?
As16 S23 Pb12 145.9(4) 3_566 1_544 ?
As15 S23 Pb12 48.28(16) 3_556 1_544 ?
As21 S23 Pb12 89.4(3) 4_454 1_544 ?
Pb10 S23 Pb12 92.5(2) 1_554 1_544 ?
As15 S23 Pb3 61.8(3) 1_554 2_445 ?
Pb4 S23 Pb3 56.3(2) 2_445 2_445 ?
Pb12 S23 Pb3 144.8(4) 3_566 2_445 ?
Pb21 S23 Pb3 63.3(2) 2_445 2_445 ?
As21 S23 Pb3 51.7(4) 2_445 2_445 ?
Pb21 S23 Pb3 115.5(3) 4_454 2_445 ?
As16 S23 Pb3 124.9(3) 3_566 2_445 ?
As15 S23 Pb3 117.1(3) 3_556 2_445 ?
As21 S23 Pb3 125.5(5) 4_454 2_445 ?
Pb10 S23 Pb3 73.18(19) 1_554 2_445 ?
Pb12 S23 Pb3 69.21(16) 1_544 2_445 ?
As20 S24 Pb4 89.3(3) . 4_464 ?
As20 S24 Pb7 81.9(2) . 3_566 ?
Pb4 S24 Pb7 101.7(2) 4_464 3_566 ?
As20 S24 Pb3 86.9(3) . 4_464 ?
Pb4 S24 Pb3 84.3(2) 4_464 4_464 ?
Pb7 S24 Pb3 167.1(3) 3_566 4_464 ?
As20 S24 Pb1 80.5(2) . 3_566 ?
Pb4 S24 Pb1 167.3(3) 4_464 3_566 ?
Pb7 S24 Pb1 84.4(2) 3_566 3_566 ?
Pb3 S24 Pb1 87.6(2) 4_464 3_566 ?
As20 S24 As22 114.8(3) . 2 ?
Pb4 S24 As22 57.65(15) 4_464 2 ?
Pb7 S24 As22 57.53(15) 3_566 2 ?
Pb3 S24 As22 134.0(2) 4_464 2 ?
Pb1 S24 As22 133.8(2) 3_566 2 ?
As20 S24 Pb10 144.6(3) . 3_566 ?
Pb4 S24 Pb10 55.31(14) 4_464 3_566 ?
Pb7 S24 Pb10 102.5(2) 3_566 3_566 ?
Pb3 S24 Pb10 90.29(19) 4_464 3_566 ?
Pb1 S24 Pb10 134.7(2) 3_566 3_566 ?
As22 S24 Pb10 48.13(17) 2 3_566 ?
As20 S24 Pb5 136.9(3) . 4_554 ?
Pb4 S24 Pb5 101.4(2) 4_464 4_554 ?
Pb7 S24 Pb5 55.16(13) 3_566 4_554 ?
Pb3 S24 Pb5 135.3(2) 4_464 4_554 ?
Pb1 S24 Pb5 91.22(18) 3_566 4_554 ?
As22 S24 Pb5 46.94(16) 2 4_554 ?
Pb10 S24 Pb5 60.17(11) 3_566 4_554 ?
As20 S24 Pb2 141.3(3) . 3_566 ?
Pb4 S24 Pb2 90.3(2) 4_464 3_566 ?
Pb7 S24 Pb2 135.8(2) 3_566 3_566 ?
Pb3 S24 Pb2 54.62(13) 4_464 3_566 ?
Pb1 S24 Pb2 92.97(18) 3_566 3_566 ?
As22 S24 Pb2 97.3(2) 2 3_566 ?
Pb10 S24 Pb2 51.13(10) 3_566 3_566 ?
Pb5 S24 Pb2 80.87(14) 4_554 3_566 ?
As20 S24 Pb8 134.4(3) . 3_566 ?
Pb4 S24 Pb8 136.1(3) 4_464 3_566 ?
Pb7 S24 Pb8 90.57(18) 3_566 3_566 ?
Pb3 S24 Pb8 92.90(18) 4_464 3_566 ?
Pb1 S24 Pb8 54.01(12) 3_566 3_566 ?
As22 S24 Pb8 97.7(2) 2 3_566 ?
Pb10 S24 Pb8 80.94(14) 3_566 3_566 ?
Pb5 S24 Pb8 52.59(10) 4_554 3_566 ?
Pb2 S24 Pb8 54.57(10) 3_566 3_566 ?
As20 S24 Pb10 39.70(16) . 3_466 ?
Pb4 S24 Pb10 49.66(13) 4_464 3_466 ?
Pb7 S24 Pb10 92.72(18) 3_566 3_466 ?
Pb3 S24 Pb10 82.44(17) 4_464 3_466 ?
Pb1 S24 Pb10 119.5(2) 3_566 3_466 ?
As22 S24 Pb10 89.8(2) 2 3_466 ?
Pb10 S24 Pb10 104.97(15) 3_566 3_466 ?
Pb5 S24 Pb10 134.44(17) 4_554 3_466 ?
Pb2 S24 Pb10 125.54(16) 3_566 3_466 ?
Pb8 S24 Pb10 172.42(18) 3_566 3_466 ?
As20 S24 Pb2 38.91(16) . 3_466 ?
Pb4 S24 Pb2 82.90(17) 4_464 3_466 ?
Pb7 S24 Pb2 120.8(2) 3_566 3_466 ?
Pb3 S24 Pb2 48.12(12) 4_464 3_466 ?
Pb1 S24 Pb2 84.40(17) 3_566 3_466 ?
As22 S24 Pb2 135.7(2) 2 3_466 ?
Pb10 S24 Pb2 125.39(16) 3_566 3_466 ?
Pb5 S24 Pb2 174.44(19) 4_554 3_466 ?
Pb2 S24 Pb2 102.74(14) 3_566 3_466 ?
Pb8 S24 Pb2 126.15(16) 3_566 3_466 ?
Pb10 S24 Pb2 46.53(8) 3_466 3_466 ?
As22 Cl25 Pb7 84.5(2) 1_655 2_546 ?
As22 Cl25 Pb7 84.5(2) 1_655 4_554 ?
Pb7 Cl25 Pb7 169.0(4) 2_546 4_554 ?
As22 Cl25 Pb4 83.7(2) 1_655 3_566 ?
Pb7 Cl25 Pb4 80.13(7) 2_546 3_566 ?
Pb7 Cl25 Pb4 98.64(8) 4_554 3_566 ?
As22 Cl25 Pb4 83.7(2) 1_655 1_545 ?
Pb7 Cl25 Pb4 98.64(8) 2_546 1_545 ?
Pb7 Cl25 Pb4 80.13(7) 4_554 1_545 ?
Pb4 Cl25 Pb4 167.3(4) 3_566 1_545 ?
As22 Cl25 As20 113.07(19) 1_655 2_545 ?
Pb7 Cl25 As20 130.59(14) 2_546 2_545 ?
Pb7 Cl25 As20 54.87(10) 4_554 2_545 ?
Pb4 Cl25 As20 58.17(10) 3_566 2_545 ?
Pb4 Cl25 As20 127.89(13) 1_545 2_545 ?
As22 Cl25 As20 113.07(19) 1_655 4 ?
Pb7 Cl25 As20 54.87(10) 2_546 4 ?
Pb7 Cl25 As20 130.59(14) 4_554 4 ?
Pb4 Cl25 As20 127.89(13) 3_566 4 ?
Pb4 Cl25 As20 58.17(10) 1_545 4 ?
As20 Cl25 As20 133.9(4) 2_545 4 ?
As22 Cl25 Pb5 139.89(10) 1_655 . ?
Pb7 Cl25 Pb5 55.39(13) 2_546 . ?
Pb7 Cl25 Pb5 135.6(3) 4_554 . ?
Pb4 Cl25 Pb5 88.86(16) 3_566 . ?
Pb4 Cl25 Pb5 100.90(18) 1_545 . ?
As20 Cl25 Pb5 95.6(2) 2_545 . ?
As20 Cl25 Pb5 45.88(13) 4 . ?
As22 Cl25 Pb5 139.89(10) 1_655 3_556 ?
Pb7 Cl25 Pb5 135.6(3) 2_546 3_556 ?
Pb7 Cl25 Pb5 55.39(13) 4_554 3_556 ?
Pb4 Cl25 Pb5 100.90(18) 3_566 3_556 ?
Pb4 Cl25 Pb5 88.86(16) 1_545 3_556 ?
As20 Cl25 Pb5 45.88(13) 2_545 3_556 ?
As20 Cl25 Pb5 95.6(2) 4 3_556 ?
Pb5 Cl25 Pb5 80.2(2) . 3_556 ?
As22 Cl25 Pb10 139.05(10) 1_655 2_446 ?
Pb7 Cl25 Pb10 100.29(18) 2_546 2_446 ?
Pb7 Cl25 Pb10 88.06(16) 4_554 2_446 ?
Pb4 Cl25 Pb10 137.3(3) 3_566 2_446 ?
Pb4 Cl25 Pb10 55.40(13) 1_545 2_446 ?
As20 Cl25 Pb10 94.6(2) 2_545 2_446 ?
As20 Cl25 Pb10 47.76(13) 4 2_446 ?
Pb5 Cl25 Pb10 59.43(13) . 2_446 ?
Pb5 Cl25 Pb10 49.71(11) 3_556 2_446 ?
As22 Cl25 Pb10 139.05(10) 1_655 4_454 ?
Pb7 Cl25 Pb10 88.06(16) 2_546 4_454 ?
Pb7 Cl25 Pb10 100.29(18) 4_554 4_454 ?
Pb4 Cl25 Pb10 55.40(13) 3_566 4_454 ?
Pb4 Cl25 Pb10 137.3(3) 1_545 4_454 ?
As20 Cl25 Pb10 47.76(13) 2_545 4_454 ?
As20 Cl25 Pb10 94.6(2) 4 4_454 ?
Pb5 Cl25 Pb10 49.71(11) . 4_454 ?
Pb5 Cl25 Pb10 59.43(13) 3_556 4_454 ?
Pb10 Cl25 Pb10 81.9(2) 2_446 4_454 ?
As22 Cl25 Pb5 36.15(8) 1_655 1_655 ?
Pb7 Cl25 Pb5 48.35(15) 2_546 1_655 ?
Pb7 Cl25 Pb5 120.7(3) 4_554 1_655 ?
Pb4 Cl25 Pb5 79.34(18) 3_566 1_655 ?
Pb4 Cl25 Pb5 90.4(2) 1_545 1_655 ?
As20 Cl25 Pb5 132.80(18) 2_545 1_655 ?
As20 Cl25 Pb5 87.33(14) 4 1_655 ?
Pb5 Cl25 Pb5 103.74(4) . 1_655 ?
Pb5 Cl25 Pb5 176.04(17) 3_556 1_655 ?
Pb10 Cl25 Pb5 132.30(4) 2_446 1_655 ?
Pb10 Cl25 Pb5 123.14(4) 4_454 1_655 ?
As22 S26 Pb5 89.3(5) . 3_556 ?
As22 S26 Pb10 89.3(5) . 4_454 ?
Pb5 S26 Pb10 105.1(8) 3_556 4_454 ?
As22 S26 Pb7 86.1(6) . 4_454 ?
Pb5 S26 Pb7 79.7(2) 3_556 4_454 ?
Pb10 S26 Pb7 173.4(6) 4_454 4_454 ?
As22 S26 Pb4 85.6(6) . 3_466 ?
Pb5 S26 Pb4 174.1(5) 3_556 3_466 ?
Pb10 S26 Pb4 77.8(2) 4_454 3_466 ?
Pb7 S26 Pb4 97.1(7) 4_454 3_466 ?
As22 S26 As20 118.9(9) . 2_545 ?
Pb5 S26 As20 57.0(4) 3_556 2_545 ?
Pb10 S26 As20 59.5(4) 4_454 2_545 ?
Pb7 S26 As20 127.0(3) 4_454 2_545 ?
Pb4 S26 As20 128.3(3) 3_466 2_545 ?
As22 S26 As20 111.3(9) . 2_445 ?
Pb5 S26 As20 124.1(4) 3_556 2_445 ?
Pb10 S26 As20 125.5(4) 4_454 2_445 ?
Pb7 S26 As20 52.4(3) 4_454 2_445 ?
Pb4 S26 As20 55.7(4) 3_466 2_445 ?
As20 S26 As20 129.7(2) 2_545 2_445 ?
As22 S26 Pb8 147.7(7) . 4_454 ?
Pb5 S26 Pb8 58.4(2) 3_556 4_454 ?
Pb10 S26 Pb8 98.8(4) 4_454 4_454 ?
Pb7 S26 Pb8 87.57(19) 4_454 4_454 ?
Pb4 S26 Pb8 126.7(3) 3_466 4_454 ?
As20 S26 Pb8 45.56(16) 2_545 4_454 ?
As20 S26 Pb8 89.3(2) 2_445 4_454 ?
As22 S26 Pb2 145.1(6) . 4_454 ?
Pb5 S26 Pb2 100.1(5) 3_556 4_454 ?
Pb10 S26 Pb2 55.8(2) 4_454 4_454 ?
Pb7 S26 Pb2 128.6(3) 4_454 4_454 ?
Pb4 S26 Pb2 85.86(19) 3_466 4_454 ?
As20 S26 Pb2 47.21(17) 2_545 4_454 ?
As20 S26 Pb2 91.2(2) 2_445 4_454 ?
Pb8 S26 Pb2 52.93(14) 4_454 4_454 ?
As22 S26 Pb3 140.0(7) . 3_466 ?
Pb5 S26 Pb3 130.4(3) 3_556 3_466 ?
Pb10 S26 Pb3 85.3(2) 4_454 3_466 ?
Pb7 S26 Pb3 95.1(4) 4_454 3_466 ?
Pb4 S26 Pb3 54.6(2) 3_466 3_466 ?
As20 S26 Pb3 91.9(2) 2_545 3_466 ?
As20 S26 Pb3 46.27(18) 2_445 3_466 ?
Pb8 S26 Pb3 72.11(12) 4_454 3_466 ?
Pb2 S26 Pb3 46.35(8) 4_454 3_466 ?
As22 S26 Pb1 142.2(8) . 4_454 ?
Pb5 S26 Pb1 88.1(2) 3_556 4_454 ?
Pb10 S26 Pb1 127.7(3) 4_454 4_454 ?
Pb7 S26 Pb1 56.3(2) 4_454 4_454 ?
Pb4 S26 Pb1 94.2(4) 3_466 4_454 ?
As20 S26 Pb1 90.6(2) 2_545 4_454 ?
As20 S26 Pb1 43.94(16) 2_445 4_454 ?
Pb8 S26 Pb1 46.11(8) 4_454 4_454 ?
Pb2 S26 Pb1 72.28(12) 4_454 4_454 ?
Pb3 S26 Pb1 51.32(14) 3_466 4_454 ?
As22 S26 Pb5 37.1(4) . . ?
Pb5 S26 Pb5 96.4(4) 3_556 . ?
Pb10 S26 Pb5 52.26(18) 4_454 . ?
Pb7 S26 Pb5 123.2(3) 4_454 . ?
Pb4 S26 Pb5 81.22(18) 3_466 . ?
As20 S26 Pb5 92.9(4) 2_545 . ?
As20 S26 Pb5 131.6(4) 2_445 . ?
Pb8 S26 Pb5 137.8(5) 4_454 . ?
Pb2 S26 Pb5 108.0(3) 4_454 . ?
Pb3 S26 Pb5 125.44(19) 3_466 . ?
Pb1 S26 Pb5 175.4(5) 4_454 . ?
 
_refine_diff_density_max    5.917
_refine_diff_density_min   -5.512
_refine_diff_density_rms    0.591

_shelx_res_file
;

TITL  tsugaruite_0m8 in P 2 n n
    shelx.res
    created by SHELXL-2018/1 at 08:27:16 on 29-Nov-2018
CELL   0.71073   8.0774  15.1772  38.1290  90.000  90.000  90.000
ZERR     1       0.0010   0.0016   0.0038   0.000   0.000   0.000
LATT   -1
SYMM   1/2+X,1/2+Y,1/2-Z
SYMM   +X,-Y,-Z
SYMM   1/2+X,1/2-Y,1/2+Z
SFAC  As   Pb   S    Cl  Sb
UNIT  6    12   21   1   1
ACTA
L.S. 10
BOND
CONN 12 4 $Pb
CONN 12 4 $As
FMAP 2
PLAN 100
EADP AS14 PB14
EADP AS21 PB21
rem   WGHT    0.022000
WGHT    0.000100
FVAR       1.03626   0.40691   0.35955   0.73689
PB1   2    0.491051    0.458023    0.823340    11.00000    0.01330    0.02949 =
         0.03643    0.00406   -0.00561    0.00228
PB2   2    0.996494    0.189515    0.874048    11.00000    0.01970    0.02980 =
         0.04261   -0.00526    0.00137    0.01644
PB3   2    0.994590    0.690079    0.625853    11.00000    0.02237    0.03533 =
         0.01792   -0.00083    0.00653    0.00957
PB4   2    0.997674    0.797183    0.523164    11.00000    0.02784    0.02777 =
         0.02651   -0.00014    0.00029    0.00016
PB5   2    0.489079    0.089308    0.574864    11.00000    0.01323    0.02654 =
         0.03254    0.00252    0.00365    0.00294
PB6   2    0.496537    0.562188    0.724714    11.00000    0.01824    0.02086 =
         0.01742    0.00070   -0.00007    0.00021
PB7   2    0.491510    0.589892    0.924529    11.00000    0.01981    0.02075 =
         0.01673    0.00043    0.00096   -0.00070
PB8   2    0.991088    0.460341    0.822906    11.00000    0.02244    0.03516 =
         0.00860   -0.00301   -0.00399    0.00878
PB9   2    0.498915    0.940524    0.224823    11.00000    0.01162    0.03086 =
         0.02242    0.00097   -0.00011   -0.00703
PB10  2    0.992941    0.295485    0.976659    11.00000    0.01848    0.03763 =
         0.02195   -0.00182   -0.00453    0.01862
PB11  2    0.244040    0.309784    0.744376    11.00000    0.02230    0.02313 =
         0.02214    0.00131   -0.00213    0.01663
PB12  2    0.744017    0.864032    0.932012    11.00000    0.03982    0.06938 =
         0.04050   -0.02901    0.00836   -0.00324
PB13  2    0.239080    0.746181    0.831455    11.00000    0.04750    0.10706 =
         0.02419   -0.01139    0.00405   -0.01433
AS14  1    0.248562    0.971860    0.870066   -31.00000    0.02410    0.03058 =
         0.02718   -0.00108   -0.00189   -0.00181
PB14  2    0.250206    0.945404    0.856648    31.00000    0.02410    0.03058 =
         0.02718   -0.00108   -0.00189   -0.00181
AS15  1    0.741191    0.081564    0.970626    11.00000    0.01518    0.01408 =
         0.01190    0.00141    0.00049   -0.00116
AS16  1    0.242363    0.807063    0.930406    11.00000    0.02191    0.02046 =
         0.02208    0.00146   -0.00090    0.00288
AS17  1    0.237264    0.189688    0.664276    11.00000    0.01723    0.01421 =
         0.01339    0.00154   -0.00178    0.00178
AS18  1    0.744057    0.932410    0.843876    11.00000    0.01696    0.01511 =
         0.01840    0.00103   -0.00108   -0.00136
AS19  1    0.237173    0.805690    0.745178    11.00000    0.01382    0.01364 =
         0.01166    0.00213    0.00256    0.00015
AS20  1    0.238052    0.603552    0.098957    11.00000    0.03649    0.03272 =
         0.03881    0.00020    0.00202   -0.00023
AS21  1    0.741163    0.542535    0.556758    21.00000    0.02492    0.08554 =
         0.09997    0.07970    0.01114    0.00645
PB21  2    0.740166    0.532362    0.536857   -21.00000    0.02492    0.08554 =
         0.09997    0.07970    0.01114    0.00645
AS22  1    0.247146    0.000000    0.500000    10.50000    0.04198    0.03876 =
         0.04389    0.00013    0.00000    0.00000
S1    3    0.749734    0.197987    0.934387    11.00000    0.01385    0.01736 =
         0.01744   -0.00116    0.00075   -0.00110
S2    3    0.739712    0.452729    0.764410    11.00000    0.03124    0.02453 =
         0.01832   -0.00081   -0.00758   -0.00763
S3    3    0.249052    0.070681    0.628763    11.00000    0.01643    0.01665 =
         0.01526    0.00013    0.00016   -0.00419
S4    3    0.243859    0.695784    0.967804    11.00000    0.01440    0.01474 =
         0.01592   -0.00531   -0.00133   -0.00145
S5    3    0.752014    0.700771    0.569973    11.00000    0.03191    0.03297 =
         0.02913    0.00727    0.00563    0.00035
S6    3    0.964330    0.894267    0.811326    11.00000    0.00383
S7    3    0.247300    0.479652    0.771380    11.00000    0.01588    0.02022 =
         0.00973   -0.00194    0.00129   -0.00312
S8    3    0.753622    0.079964    0.830483    11.00000    0.01642    0.01484 =
         0.02095    0.00623   -0.00257    0.00267
S9    3    0.970019    0.120027    0.006819    11.00000    0.01972    0.01144 =
         0.01332   -0.00478    0.00041   -0.00018
S10   3    0.027223    0.766312    0.898595    11.00000    0.01871    0.02517 =
         0.00877    0.00569    0.00055    0.00294
S11   3    0.466709    0.762478    0.893080    11.00000    0.00663    0.01262 =
         0.02400    0.00157   -0.00241   -0.00076
S12   3    0.474660    0.006006    0.904781    11.00000    0.02057    0.03038 =
         0.02415   -0.00777    0.00320    0.00191
S13   3    0.519756    0.893044    0.807917    11.00000    0.02510    0.02265 =
         0.02364    0.00709    0.00021    0.00382
S14   3    0.462908    0.776495    0.711089    11.00000    0.00560
S15   3    0.258676    0.677119    0.149364    11.00000    0.00891    0.01347 =
         0.02055    0.00546   -0.00012   -0.00313
S16   3    0.044177    0.761882    0.709672    11.00000    0.03693    0.02736 =
         0.01845    0.00161    0.00149    0.00710
S17   3    0.029009    0.017309    0.906971    11.00000    0.01477    0.01207 =
         0.01960   -0.00334   -0.00001    0.00288
S18   3    0.459648    0.139150    0.697413    11.00000    0.02022    0.03218 =
         0.00571    0.00004    0.00258   -0.00382
S19   3    0.253744    0.094854    0.831927    11.00000    0.02008    0.02944 =
         0.01928   -0.00184    0.00075    0.00048
S20   3    0.240251    0.172876    0.531642    11.00000    0.03449    0.03808 =
         0.04457    0.00661   -0.00573    0.00748
S21   3    0.024053    0.158531    0.698478    11.00000    0.01859    0.01896 =
         0.03418   -0.00276    0.00021   -0.00246
S22   3    0.238241    0.456825    0.127167    11.00000    0.02487    0.03002 =
         0.02521    0.00797    0.00129    0.00078
S23   3    0.533669    0.121585    0.004692    11.00000    0.01479    0.01594 =
         0.01443   -0.00003   -0.00403   -0.00105
S24   3    0.530404    0.612575    0.095632    11.00000    0.01783    0.01787 =
         0.02689   -0.00266   -0.00150    0.00338
CL25  4    0.953552    0.000000    0.500000    10.50000    0.01996    0.03268 =
         0.03381    0.00172    0.00000    0.00000
S26   3    0.260497    0.058319    0.447277    11.00000    0.04990    0.05157 =
         0.06098    0.00334    0.00131   -0.01396

HKLF  4




REM   tsugaruite_0m8 in P 2 n n
REM R1 =  0.0427 for    3488 Fo > 4sig(Fo)  and  0.0539 for all    8315 data
REM    424 parameters refined using      1 restraints

END

WGHT      0.0000      0.0000

REM Highest difference peak  5.917,  deepest hole -5.512,  1-sigma level  0.591
Q1    1   0.9935  0.4574  0.7981  11.00000  0.05    5.92
Q2    1   0.4957  0.5598  0.7493  11.00000  0.05    5.81
Q3    1   0.4963  0.9408  0.2493  11.00000  0.05    5.75
Q4    1   0.4935  0.4564  0.7982  11.00000  0.05    5.57
Q5    1   0.9947  0.2997  1.0013  11.00000  0.05    5.25
Q6    1   0.9958  0.8002  0.4987  11.00000  0.05    5.23
Q7    1   0.4937  0.5858  0.8998  11.00000  0.05    5.22
Q8    1   0.9964  0.7963  0.5482  11.00000  0.05    5.14
Q9    1   0.9938  0.2966  0.9518  11.00000  0.05    5.06
Q10   1   0.4947  0.5603  0.7001  11.00000  0.05    5.04
Q11   1   0.4908  0.0846  0.5999  11.00000  0.05    4.98
Q12   1   0.4956  0.9398  0.2001  11.00000  0.05    4.82
Q13   1   0.9920  0.6868  0.6506  11.00000  0.05    4.79
Q14   1   0.9930  0.6875  0.6007  11.00000  0.05    4.72
Q15   1   0.9944  0.1857  0.8494  11.00000  0.05    4.60
Q16   1   0.9949  0.1872  0.8992  11.00000  0.05    4.51
Q17   1   0.9931  0.4606  0.8486  11.00000  0.05    4.49
Q18   1   0.4919  0.0915  0.5503  11.00000  0.05    4.37
Q19   1   0.4904  0.5918  0.9496  11.00000  0.05    4.31
Q20   1   0.4932  0.4603  0.8489  11.00000  0.05    4.31
Q21   1   0.2425  0.3087  0.7195  11.00000  0.05    4.05
Q22   1   0.4938  0.0735  0.6763  11.00000  0.05    4.04
Q23   1  -0.0052  0.0771  0.6756  11.00000  0.05    3.95
Q24   1   0.2432  0.3092  0.7693  11.00000  0.05    3.81
Q25   1  -0.0034  0.0706  0.8697  11.00000  0.05    3.31
Q26   1   0.4960  0.0706  0.8701  11.00000  0.05    3.30
Q27   1   0.9950  0.4190  0.9809  11.00000  0.05    3.15
Q28   1   0.9921  0.0811  0.4815  11.00000  0.05    3.08
Q29   1   0.7440  0.8665  0.9070  11.00000  0.05    3.05
Q30   1   0.4944 -0.0435  0.5805  11.00000  0.05    3.04
Q31   1   0.7439  0.0786  0.9461  11.00000  0.05    3.04
Q32   1  -0.0059  0.6981  0.9212  11.00000  0.05    3.03
Q33   1   0.4960  0.6967  0.9207  11.00000  0.05    3.02
Q34   1   0.4919  0.5391  0.0794  11.00000  0.05    2.97
Q35   1   0.4973  0.6917  0.7284  11.00000  0.05    2.95
Q36   1   0.4930  1.0420  0.2269  11.00000  0.05    2.90
Q37   1   0.4940  0.4563  0.7267  11.00000  0.05    2.89
Q38   1  -0.0065  0.6933  0.7365  11.00000  0.05    2.75
Q39   1   0.2410  0.7491  0.8566  11.00000  0.05    2.75
Q40   1   0.2415  0.8015  0.7224  11.00000  0.05    2.65
Q41   1   0.2419  0.7437  0.8068  11.00000  0.05    2.54
Q42   1   0.7436  0.8640  0.9580  11.00000  0.05    2.44
Q43   1   0.9839  0.2889  0.8826  11.00000  0.05    2.41
Q44   1   0.9975  0.7918  0.6202  11.00000  0.05    2.38
Q45   1   0.7437  0.0800  0.8570  11.00000  0.05    2.37
Q46   1   0.7445  0.1974  0.9574  11.00000  0.05    2.33
Q47   1   0.9973  0.1846 -0.0283  11.00000  0.05    2.29
Q48   1   0.4927  0.1842 -0.0293  11.00000  0.05    2.26
Q49   1   0.7453  0.8103  0.8493  11.00000  0.05    2.25
Q50   1   0.2418  0.7215  0.8323  11.00000  0.05    2.19
Q51   1   0.2438  0.8044  0.9557  11.00000  0.05    2.18
Q52   1   0.2401  0.1893  0.6893  11.00000  0.05    2.12
Q53   1   0.2438  0.1894  0.6394  11.00000  0.05    2.11
Q54   1   0.4914  0.0581 -0.0350  11.00000  0.05    2.03
Q55   1   0.7434  0.4536  0.7410  11.00000  0.05    2.00
Q56   1  -0.0029  0.1888  0.6734  11.00000  0.05    1.96
Q57   1   0.4840  0.3934  0.7876  11.00000  0.05    1.89
Q58   1   0.9957  0.0593 -0.0353  11.00000  0.05    1.88
Q59   1   0.7425  0.6940  0.5420  11.00000  0.05    1.86
Q60   1   0.4964  0.1900  0.6752  11.00000  0.05    1.85
Q61   1   0.2420  0.3010  0.6262  11.00000  0.05    1.82
Q62   1   0.2435  0.4555  0.7476  11.00000  0.05    1.80
Q63   1  -0.0095 -0.0477  0.8707  11.00000  0.05    1.73
Q64   1   0.9980  0.3939  0.7880  11.00000  0.05    1.72
Q65   1  -0.0057 -0.0619  0.9441  11.00000  0.05    1.69
Q66   1   1.2407  0.7984  0.6428  11.00000  0.05    1.65
Q67   1  -0.0167  0.8790  0.9030  11.00000  0.05    1.63
Q68   1   0.5034  0.8784  0.9038  11.00000  0.05    1.62
Q69   1   0.7450  0.9379  0.8689  11.00000  0.05    1.61
Q70   1   0.4914  0.9570  0.7974  11.00000  0.05    1.60
Q71   1   0.9964  0.0337  0.0326  11.00000  0.05    1.57
Q72   1   0.7443  0.8170  0.5634  11.00000  0.05    1.57
Q73   1   0.7404  0.6915  0.1272  11.00000  0.05    1.56
Q74   1   0.4949  0.0423  0.0356  11.00000  0.05    1.56
Q75   1   0.4999 -0.0471  0.8712  11.00000  0.05    1.56
Q76   1   0.2461  0.0766  0.8518  11.00000  0.05    1.55
Q77   1   0.7458  0.8056  0.9520  11.00000  0.05    1.55
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