data_matthiasweilite _audit_creation_method 'SHELXL-2016/6' _shelx_SHELXL_version_number '2016/6' _chemical_name_mineral 'matthiasweilite' _chemical_compound_source 'Delamar mine, Nevada' _chemical_formula_sum 'O30 Pb10 Te10' _chemical_formula_weight 3827.90 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'Pb' 'Pb' -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Te' 'Te' -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 7.0256(4) _cell_length_b 10.6345(6) _cell_length_c 11.9965(8) _cell_angle_alpha 78.513(6) _cell_angle_beta 83.104(6) _cell_angle_gamma 84.083(6) _cell_volume 869.10(9) _cell_formula_units_Z 1 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 10617 _cell_measurement_theta_min 3.3 _cell_measurement_theta_max 27.5 _exptl_crystal_description 'fragment' _exptl_crystal_colour 'yellow' _exptl_crystal_density_diffrn 7.314 _exptl_crystal_F_000 1580 _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.050 _exptl_absorpt_coefficient_mu 56.561 _shelx_estimated_absorpt_T_min 0.043 _shelx_estimated_absorpt_T_max 0.164 _exptl_absorpt_correction_type 'Multi-scan' _exptl_absorpt_correction_T_min 0.262 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details 'Higashi2001' _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71075 _diffrn_radiation_type MoK\a _diffrn_source 'Sealed Tube' _diffrn_radiation_monochromator 'Graphite Monochromator' _diffrn_measurement_device_type 'Rigaku R-axis RAPID II' _diffrn_measurement_method 'profile data from \w-scans' _diffrn_reflns_number 15542 _diffrn_reflns_av_unetI/netI 0.0966 _diffrn_reflns_av_R_equivalents 0.1481 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 3.253 _diffrn_reflns_theta_max 27.484 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_point_group_measured_fraction_full 0.997 _reflns_number_total 3973 _reflns_number_gt 3416 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0725P)^2^+0.1353P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3973 _refine_ls_number_parameters 226 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0592 _refine_ls_R_factor_gt 0.0523 _refine_ls_wR_factor_ref 0.1409 _refine_ls_wR_factor_gt 0.1346 _refine_ls_goodness_of_fit_ref 1.032 _refine_ls_restrained_S_all 1.032 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pb1 Pb 0.34113(8) 0.36442(6) 0.14602(5) 0.01894(18) Uani 1 1 d . . . . . Pb2 Pb 0.23507(7) 1.03265(6) 0.05025(5) 0.01875(18) Uani 1 1 d . . . . . Pb3 Pb 0.80224(8) 0.45192(6) 0.28559(5) 0.01866(18) Uani 1 1 d . . . . . Pb4 Pb 0.39741(8) 0.82380(6) 0.48598(5) 0.01746(17) Uani 1 1 d . . . . . Pb5 Pb -0.01803(8) 0.78032(5) 0.30192(5) 0.01810(18) Uani 1 1 d . . . . . Te1 Te 0.48553(14) 0.72684(9) 0.17970(9) 0.0142(2) Uani 1 1 d . . . . . Te2 Te 0.63423(14) 0.06057(10) 0.24161(9) 0.0166(2) Uani 1 1 d . . . . . Te3 Te -0.08701(13) 0.33204(9) -0.00757(8) 0.0166(2) Uani 1 1 d . . . . . Te4 Te 0.25453(12) 0.46880(9) 0.43240(8) 0.0138(2) Uani 1 1 d . . . . . Te5 Te 0.09862(13) 0.11968(9) 0.36733(8) 0.0145(2) Uani 1 1 d . . . . . O1 O 0.1387(13) 0.2951(10) 0.3068(10) 0.020(2) Uani 1 1 d . . . . . O2 O 0.5430(15) 0.8970(10) 0.1021(9) 0.023(2) Uani 1 1 d . . . . . O3 O 0.6983(14) 0.6827(10) 0.2635(9) 0.023(2) Uani 1 1 d . . . . . O4 O -0.0565(14) 0.1502(10) 0.4979(9) 0.023(2) Uani 1 1 d . . . . . O5 O 0.3265(14) 0.0612(10) 0.4365(9) 0.022(2) Uani 1 1 d . . . . . O6 O 0.3149(14) 0.7973(10) 0.2911(9) 0.023(2) Uani 1 1 d . . . . . O7 O 0.0514(14) 0.5165(10) 0.1107(9) 0.024(2) Uani 1 1 d . . . . . O8 O 0.3139(14) 0.5892(10) 0.5144(10) 0.026(3) Uani 1 1 d . . . . . O9 O 0.0277(14) 0.5597(11) 0.3764(9) 0.021(2) Uani 1 1 d . . . . . O10 O 0.6856(15) 0.1997(11) 0.3066(9) 0.025(3) Uani 1 1 d . . . . . O11 O -0.1050(15) 0.2278(11) -0.1132(9) 0.027(3) Uani 1 1 d . . . . . O12 O 0.4135(15) 0.1367(10) 0.1748(10) 0.024(3) Uani 1 1 d . . . . . O13 O 0.4115(14) 0.5072(11) 0.2954(9) 0.024(2) Uani 1 1 d . . . . . O14 O 0.1669(15) 0.2773(10) 0.0226(10) 0.025(3) Uani 1 1 d . . . . . O15 O 0.8188(16) 0.0840(12) 0.1160(10) 0.033(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pb1 0.0170(3) 0.0178(3) 0.0222(3) -0.0060(3) 0.0022(2) -0.0033(2) Pb2 0.0156(3) 0.0195(3) 0.0205(3) -0.0043(3) 0.0022(2) -0.0020(2) Pb3 0.0187(3) 0.0193(3) 0.0186(3) -0.0054(3) 0.0001(2) -0.0033(2) Pb4 0.0164(3) 0.0176(3) 0.0181(3) -0.0035(3) 0.0004(2) -0.0025(2) Pb5 0.0158(3) 0.0167(3) 0.0220(3) -0.0051(3) 0.0005(2) -0.0025(2) Te1 0.0153(5) 0.0122(5) 0.0163(5) -0.0054(4) -0.0019(4) -0.0013(4) Te2 0.0166(5) 0.0171(5) 0.0166(5) -0.0053(4) -0.0015(4) 0.0003(4) Te3 0.0198(5) 0.0155(5) 0.0144(5) -0.0043(4) -0.0006(4) 0.0001(4) Te4 0.0139(5) 0.0138(5) 0.0134(5) -0.0027(4) -0.0006(4) -0.0008(4) Te5 0.0145(5) 0.0131(5) 0.0167(5) -0.0048(4) -0.0009(4) -0.0022(4) O1 0.006(5) 0.019(6) 0.040(7) -0.016(5) -0.002(4) 0.002(4) O2 0.026(6) 0.014(5) 0.027(6) -0.006(5) 0.000(4) 0.005(4) O3 0.020(5) 0.026(6) 0.025(6) -0.004(5) -0.010(4) -0.004(4) O4 0.017(5) 0.030(6) 0.022(6) 0.001(5) -0.005(4) -0.001(4) O5 0.021(5) 0.022(6) 0.024(6) -0.007(5) -0.003(4) -0.008(4) O6 0.023(5) 0.034(7) 0.015(5) -0.006(5) -0.003(4) -0.007(5) O7 0.018(5) 0.031(6) 0.025(6) -0.011(5) 0.000(4) -0.002(5) O8 0.016(5) 0.017(6) 0.046(8) -0.014(5) 0.004(5) -0.008(4) O9 0.016(5) 0.037(7) 0.014(5) -0.013(5) -0.010(4) 0.000(5) O10 0.027(6) 0.041(7) 0.012(5) -0.005(5) -0.010(4) -0.012(5) O11 0.024(6) 0.041(7) 0.022(6) -0.009(5) -0.002(4) -0.016(5) O12 0.030(6) 0.022(6) 0.027(6) -0.017(5) -0.009(5) 0.001(5) O13 0.024(6) 0.034(7) 0.014(6) -0.004(5) -0.001(4) -0.007(5) O14 0.029(6) 0.012(5) 0.031(7) 0.001(5) -0.005(5) 0.000(4) O15 0.036(7) 0.045(8) 0.022(6) -0.019(6) 0.010(5) -0.012(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pb1 O1 2.297(11) . ? Pb1 O12 2.387(10) . ? Pb1 O14 2.401(11) . ? Pb1 O7 2.489(10) . ? Pb1 O13 2.685(11) . ? Pb1 O10 3.397(10) . ? Pb1 Te2 3.7035(11) . ? Pb1 Te3 3.7087(11) 2_565 ? Pb1 Te5 3.7150(11) . ? Pb1 Te3 3.7893(11) . ? Pb1 Te4 3.7792(11) . ? Pb1 Pb3 4.0466(8) 1_455 ? Pb1 Pb2 4.0848(9) 1_545 ? Pb1 O9 4.084(10) . ? Pb1 Pb3 4.0876(9) . ? Pb2 O2 2.311(11) 2_675 ? Pb2 O12 2.534(10) 1_565 ? Pb2 O2 2.543(10) . ? Pb2 O14 2.558(10) 1_565 ? Pb2 O15 2.632(11) 2_665 ? Pb2 O11 2.932(11) 2_565 ? Pb2 O15 2.960(11) 1_465 ? Pb2 O6 3.485(10) . ? Pb2 O11 3.513(11) 1_565 ? Pb2 Te1 3.6809(11) . ? Pb2 Te3 3.7081(11) 1_565 ? Pb2 Te2 3.8089(12) 2_665 ? Pb2 Pb2 3.8100(11) 2_675 ? Pb2 Pb2 3.8220(11) 2_575 ? Pb2 Te1 3.8638(12) 2_675 ? Pb3 O8 2.408(12) 2_666 ? Pb3 O3 2.459(10) . ? Pb3 O9 2.509(10) 1_655 ? Pb3 O7 2.594(11) 1_655 ? Pb3 O13 2.741(10) . ? Pb3 O1 2.756(9) 1_655 ? Pb3 O10 2.840(11) . ? Pb3 Te1 3.6015(11) . ? Pb3 Te4 3.6136(12) 2_666 ? Pb3 O4 3.803(10) 1_655 ? Pb3 Pb4 3.8469(9) 2_666 ? Pb3 Te4 3.8496(11) 1_655 ? Pb3 Pb5 3.8821(9) 1_655 ? Pb3 Te5 3.9210(11) 1_655 ? Pb3 Te3 3.9400(11) 1_655 ? Pb4 O4 2.371(10) 2_566 ? Pb4 O10 2.455(11) 2_666 ? Pb4 O5 2.487(10) 1_565 ? Pb4 O8 2.568(10) . ? Pb4 O6 2.550(10) . ? Pb4 O5 2.739(10) 2_666 ? Pb4 O3 3.665(11) . ? Pb4 Te2 3.6892(12) 2_666 ? Pb4 Te5 3.7290(10) 1_565 ? Pb4 Te5 3.7576(11) 2_566 ? Pb4 Te4 3.7964(11) 2_666 ? Pb4 Te2 3.8020(12) 1_565 ? Pb4 Te1 3.9721(12) . ? Pb4 Pb5 3.9801(8) . ? Pb5 O11 2.339(11) 2_565 ? Pb5 O9 2.342(11) . ? Pb5 O6 2.351(10) . ? Pb5 O3 2.470(10) 1_455 ? Pb5 O4 2.771(11) 2_566 ? Pb5 Te2 3.6659(11) 1_465 ? Pb5 O15 3.701(12) 1_465 ? Pb5 Te1 3.6960(11) . ? Pb5 O8 3.802(11) . ? Pb5 Te4 3.7999(11) . ? Pb5 O7 3.922(11) . ? Pb5 Te3 3.9133(11) 2_565 ? Pb5 O13 3.972(11) . ? Te1 O3 1.869(9) . ? Te1 O6 1.901(11) . ? Te1 O2 1.922(10) . ? Te1 O13 2.538(11) . ? Te1 O11 2.847(10) 2_565 ? Te1 O14 3.233(11) 2_665 ? Te1 Te3 3.8418(14) 2_565 ? Te1 Te4 3.9721(13) . ? Te1 Te2 4.0298(14) 1_565 ? Te1 O8 4.072(12) . ? Te2 O15 1.860(11) . ? Te2 O10 1.888(11) . ? Te2 O12 1.867(10) . ? Te2 O2 2.808(11) 1_545 ? Te2 O5 2.988(11) . ? Te2 O6 3.679(10) 1_545 ? Te2 O5 3.854(11) 2_656 ? Te2 Te5 3.9111(13) 1_655 ? Te2 Te5 3.9188(13) . ? Te3 O14 1.873(10) . ? Te3 O7 1.844(11) 2_565 ? Te3 O11 1.865(11) . ? Te3 O15 2.856(12) 1_455 ? Te3 O7 2.939(11) . ? Te3 O3 3.873(11) 2_665 ? Te3 Te3 3.937(2) 2_565 ? Te3 O10 3.955(11) 1_455 ? Te4 O13 1.864(10) . ? Te4 O8 1.869(10) . ? Te4 O9 1.899(9) . ? Te4 O9 2.836(11) 2_566 ? Te4 O1 2.838(10) . ? Te4 O8 3.146(10) 2_666 ? Te4 O6 3.610(11) . ? Te4 O3 3.722(10) 2_666 ? Te4 Te4 3.7959(18) 2_566 ? Te5 O5 1.883(10) . ? Te5 O4 1.862(11) . ? Te5 O1 1.899(10) . ? Te5 O12 2.992(12) . ? Te5 O4 3.025(10) 2_556 ? Te5 O10 3.070(10) 1_455 ? Te5 O6 3.839(11) 1_545 ? Te5 Te5 3.8695(19) 2_556 ? Te5 O15 3.889(11) 1_455 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Pb1 O12 78.2(4) . . ? O1 Pb1 O14 93.9(4) . . ? O12 Pb1 O14 70.9(3) . . ? O1 Pb1 O7 79.0(3) . . ? O12 Pb1 O7 136.4(4) . . ? O14 Pb1 O7 74.1(3) . . ? O1 Pb1 O13 75.9(3) . . ? O12 Pb1 O13 122.9(3) . . ? O14 Pb1 O13 159.4(3) . . ? O7 Pb1 O13 86.2(3) . . ? O1 Pb1 O10 83.3(3) . . ? O12 Pb1 O10 55.3(3) . . ? O14 Pb1 O10 125.7(3) . . ? O7 Pb1 O10 154.5(3) . . ? O13 Pb1 O10 71.6(3) . . ? O1 Pb1 Te2 84.2(2) . . ? O12 Pb1 Te2 25.7(2) . . ? O14 Pb1 Te2 95.2(2) . . ? O7 Pb1 Te2 159.4(2) . . ? O13 Pb1 Te2 101.4(2) . . ? O10 Pb1 Te2 30.45(19) . . ? O1 Pb1 Te3 103.8(2) . 2_565 ? O12 Pb1 Te3 152.3(2) . 2_565 ? O14 Pb1 Te3 81.4(2) . 2_565 ? O7 Pb1 Te3 26.3(2) . 2_565 ? O13 Pb1 Te3 83.7(2) . 2_565 ? O10 Pb1 Te3 152.02(19) . 2_565 ? Te2 Pb1 Te3 171.44(3) . 2_565 ? O1 Pb1 Te5 25.0(2) . . ? O12 Pb1 Te5 53.5(3) . . ? O14 Pb1 Te5 82.0(3) . . ? O7 Pb1 Te5 96.8(2) . . ? O13 Pb1 Te5 94.4(2) . . ? O10 Pb1 Te5 73.13(19) . . ? Te2 Pb1 Te5 63.77(2) . . ? Te3 Pb1 Te5 123.08(3) 2_565 . ? O1 Pb1 Te3 83.3(2) . . ? O12 Pb1 Te3 89.8(2) . . ? O14 Pb1 Te3 24.1(2) . . ? O7 Pb1 Te3 50.8(2) . . ? O13 Pb1 Te3 135.3(2) . . ? O10 Pb1 Te3 144.58(19) . . ? Te2 Pb1 Te3 115.44(3) . . ? Te3 Pb1 Te3 63.34(3) 2_565 . ? Te5 Pb1 Te3 81.06(2) . . ? O1 Pb1 Te4 48.5(3) . . ? O12 Pb1 Te4 109.4(3) . . ? O14 Pb1 Te4 138.6(3) . . ? O7 Pb1 Te4 81.2(2) . . ? O13 Pb1 Te4 27.4(2) . . ? O10 Pb1 Te4 73.37(19) . . ? Te2 Pb1 Te4 96.78(3) . . ? Te3 Pb1 Te4 90.89(2) 2_565 . ? Te5 Pb1 Te4 68.50(2) . . ? Te3 Pb1 Te4 119.05(3) . . ? O1 Pb1 Pb3 40.9(2) . 1_455 ? O12 Pb1 Pb3 110.6(3) . 1_455 ? O14 Pb1 Pb3 81.8(3) . 1_455 ? O7 Pb1 Pb3 38.2(2) . 1_455 ? O13 Pb1 Pb3 78.8(2) . 1_455 ? O10 Pb1 Pb3 121.92(19) . 1_455 ? Te2 Pb1 Pb3 124.08(3) . 1_455 ? Te3 Pb1 Pb3 63.42(2) 2_565 1_455 ? Te5 Pb1 Pb3 60.508(19) . 1_455 ? Te3 Pb1 Pb3 60.266(19) . 1_455 ? Te4 Pb1 Pb3 58.812(18) . 1_455 ? O1 Pb1 Pb2 84.8(3) . 1_545 ? O12 Pb1 Pb2 35.1(2) . 1_545 ? O14 Pb1 Pb2 35.8(2) . 1_545 ? O7 Pb1 Pb2 106.2(2) . 1_545 ? O13 Pb1 Pb2 154.7(2) . 1_545 ? O10 Pb1 Pb2 90.17(19) . 1_545 ? Te2 Pb1 Pb2 59.87(2) . 1_545 ? Te3 Pb1 Pb2 117.20(2) 2_565 1_545 ? Te5 Pb1 Pb2 62.75(2) . 1_545 ? Te3 Pb1 Pb2 56.038(19) . 1_545 ? Te4 Pb1 Pb2 131.19(2) . 1_545 ? Pb3 Pb1 Pb2 97.289(19) 1_455 1_545 ? O1 Pb1 O9 48.6(3) . . ? O12 Pb1 O9 125.4(3) . . ? O14 Pb1 O9 117.4(3) . . ? O7 Pb1 O9 53.7(3) . . ? O13 Pb1 O9 42.8(3) . . ? O10 Pb1 O9 100.8(2) . . ? Te2 Pb1 O9 121.16(14) . . ? Te3 Pb1 O9 67.21(14) 2_565 . ? Te5 Pb1 O9 73.50(16) . . ? Te3 Pb1 O9 94.49(13) . . ? Te4 Pb1 O9 27.61(13) . . ? Pb3 Pb1 O9 35.94(13) 1_455 . ? Pb2 Pb1 O9 129.36(15) 1_545 . ? O1 Pb1 Pb3 101.5(2) . . ? O12 Pb1 Pb3 97.6(2) . . ? O14 Pb1 Pb3 158.6(3) . . ? O7 Pb1 Pb3 123.2(2) . . ? O13 Pb1 Pb3 41.6(2) . . ? O10 Pb1 Pb3 43.38(19) . . ? Te2 Pb1 Pb3 71.92(2) . . ? Te3 Pb1 Pb3 108.82(2) 2_565 . ? Te5 Pb1 Pb3 106.11(2) . . ? Te3 Pb1 Pb3 171.81(3) . . ? Te4 Pb1 Pb3 61.602(18) . . ? Pb3 Pb1 Pb3 119.47(2) 1_455 . ? Pb2 Pb1 Pb3 130.556(19) 1_545 . ? O9 Pb1 Pb3 84.00(13) . . ? O2 Pb2 O12 88.5(4) 2_675 1_565 ? O2 Pb2 O2 76.7(4) 2_675 . ? O12 Pb2 O2 69.1(3) 1_565 . ? O2 Pb2 O14 78.0(4) 2_675 1_565 ? O12 Pb2 O14 66.1(4) 1_565 1_565 ? O2 Pb2 O14 128.5(3) . 1_565 ? O2 Pb2 O15 73.1(4) 2_675 2_665 ? O12 Pb2 O15 158.6(4) 1_565 2_665 ? O2 Pb2 O15 95.3(3) . 2_665 ? O14 Pb2 O15 118.8(4) 1_565 2_665 ? O2 Pb2 O11 125.4(3) 2_675 2_565 ? O12 Pb2 O11 124.9(3) 1_565 2_565 ? O2 Pb2 O11 77.8(3) . 2_565 ? O14 Pb2 O11 151.0(3) 1_565 2_565 ? O15 Pb2 O11 62.2(3) 2_665 2_565 ? O2 Pb2 O15 137.2(4) 2_675 1_465 ? O12 Pb2 O15 107.2(3) 1_565 1_465 ? O2 Pb2 O15 146.0(3) . 1_465 ? O14 Pb2 O15 73.2(3) 1_565 1_465 ? O15 Pb2 O15 94.0(3) 2_665 1_465 ? O11 Pb2 O15 77.8(3) 2_565 1_465 ? O2 Pb2 O6 127.3(3) 2_675 . ? O12 Pb2 O6 74.1(3) 1_565 . ? O2 Pb2 O6 50.6(3) . . ? O14 Pb2 O6 132.2(3) 1_565 . ? O15 Pb2 O6 108.0(3) 2_665 . ? O11 Pb2 O6 50.9(3) 2_565 . ? O15 Pb2 O6 95.5(3) 1_465 . ? O2 Pb2 O11 85.3(3) 2_675 1_565 ? O12 Pb2 O11 117.9(3) 1_565 1_565 ? O2 Pb2 O11 160.6(3) . 1_565 ? O14 Pb2 O11 52.2(3) 1_565 1_565 ? O15 Pb2 O11 72.5(3) 2_665 1_565 ? O11 Pb2 O11 107.9(2) 2_565 1_565 ? O15 Pb2 O11 52.1(3) 1_465 1_565 ? O6 Pb2 O11 146.9(2) . 1_565 ? O2 Pb2 Te1 100.8(2) 2_675 . ? O12 Pb2 Te1 86.1(2) 1_565 . ? O2 Pb2 Te1 29.3(2) . . ? O14 Pb2 Te1 152.1(2) 1_565 . ? O15 Pb2 Te1 86.5(3) 2_665 . ? O11 Pb2 Te1 49.4(2) 2_565 . ? O15 Pb2 Te1 119.3(2) 1_465 . ? O6 Pb2 Te1 30.61(17) . . ? O11 Pb2 Te1 155.52(18) 1_565 . ? O2 Pb2 Te3 92.9(2) 2_675 1_565 ? O12 Pb2 Te3 89.5(2) 1_565 1_565 ? O2 Pb2 Te3 156.2(2) . 1_565 ? O14 Pb2 Te3 27.8(2) 1_565 1_565 ? O15 Pb2 Te3 102.2(3) 2_665 1_565 ? O11 Pb2 Te3 124.7(2) 2_565 1_565 ? O15 Pb2 Te3 49.2(2) 1_465 1_565 ? O6 Pb2 Te3 134.93(17) . 1_565 ? O11 Pb2 Te3 29.78(18) 1_565 1_565 ? Te1 Pb2 Te3 165.45(3) . 1_565 ? O2 Pb2 Te2 47.2(3) 2_675 2_665 ? O12 Pb2 Te2 133.4(3) 1_565 2_665 ? O2 Pb2 Te2 84.5(2) . 2_665 ? O14 Pb2 Te2 108.8(3) 1_565 2_665 ? O15 Pb2 Te2 26.3(2) 2_665 2_665 ? O11 Pb2 Te2 83.1(2) 2_565 2_665 ? O15 Pb2 Te2 115.5(2) 1_465 2_665 ? O6 Pb2 Te2 117.64(18) . 2_665 ? O11 Pb2 Te2 78.00(19) 1_565 2_665 ? Te1 Pb2 Te2 88.74(3) . 2_665 ? Te3 Pb2 Te2 104.27(3) 1_565 2_665 ? O2 Pb2 Pb2 40.5(2) 2_675 2_675 ? O12 Pb2 Pb2 75.3(2) 1_565 2_675 ? O2 Pb2 Pb2 36.2(2) . 2_675 ? O14 Pb2 Pb2 106.8(2) 1_565 2_675 ? O15 Pb2 Pb2 83.4(2) 2_665 2_675 ? O11 Pb2 Pb2 102.2(2) 2_565 2_675 ? O15 Pb2 Pb2 177.0(2) 1_465 2_675 ? O6 Pb2 Pb2 86.75(16) . 2_675 ? O11 Pb2 Pb2 125.44(18) 1_565 2_675 ? Te1 Pb2 Pb2 62.07(2) . 2_675 ? Te3 Pb2 Pb2 129.92(3) 1_565 2_675 ? Te2 Pb2 Pb2 61.58(2) 2_665 2_675 ? O2 Pb2 Pb2 111.7(3) 2_675 2_575 ? O12 Pb2 Pb2 150.4(2) 1_565 2_575 ? O2 Pb2 Pb2 134.9(2) . 2_575 ? O14 Pb2 Pb2 96.2(2) 1_565 2_575 ? O15 Pb2 Pb2 50.6(2) 2_665 2_575 ? O11 Pb2 Pb2 61.0(2) 2_565 2_575 ? O15 Pb2 Pb2 43.4(2) 1_465 2_575 ? O6 Pb2 Pb2 106.63(16) . 2_575 ? O11 Pb2 Pb2 46.89(18) 1_565 2_575 ? Te1 Pb2 Pb2 109.73(3) . 2_575 ? Te3 Pb2 Pb2 68.86(2) 1_565 2_575 ? Te2 Pb2 Pb2 73.53(3) 2_665 2_575 ? Pb2 Pb2 Pb2 134.01(3) 2_675 2_575 ? O2 Pb2 Te1 21.9(2) 2_675 2_675 ? O12 Pb2 Te1 79.3(3) 1_565 2_675 ? O2 Pb2 Te1 92.0(2) . 2_675 ? O14 Pb2 Te1 56.1(3) 1_565 2_675 ? O15 Pb2 Te1 86.9(3) 2_665 2_675 ? O11 Pb2 Te1 145.8(2) 2_565 2_675 ? O15 Pb2 Te1 121.2(2) 1_465 2_675 ? O6 Pb2 Te1 139.81(16) . 2_675 ? O11 Pb2 Te1 72.83(18) 1_565 2_675 ? Te1 Pb2 Te1 119.40(2) . 2_675 ? Te3 Pb2 Te1 73.18(2) 1_565 2_675 ? Te2 Pb2 Te1 63.36(2) 2_665 2_675 ? Pb2 Pb2 Te1 57.32(2) 2_675 2_675 ? Pb2 Pb2 Te1 111.32(3) 2_575 2_675 ? O8 Pb3 O3 92.7(4) 2_666 . ? O8 Pb3 O9 76.1(3) 2_666 1_655 ? O3 Pb3 O9 71.0(3) . 1_655 ? O8 Pb3 O7 155.4(3) 2_666 1_655 ? O3 Pb3 O7 86.2(3) . 1_655 ? O9 Pb3 O7 80.3(3) 1_655 1_655 ? O8 Pb3 O13 74.1(3) 2_666 . ? O3 Pb3 O13 65.6(3) . . ? O9 Pb3 O13 125.1(3) 1_655 . ? O7 Pb3 O13 126.7(3) 1_655 . ? O8 Pb3 O1 96.2(3) 2_666 1_655 ? O3 Pb3 O1 138.1(3) . 1_655 ? O9 Pb3 O1 71.7(3) 1_655 1_655 ? O7 Pb3 O1 69.4(3) 1_655 1_655 ? O13 Pb3 O1 155.7(3) . 1_655 ? O8 Pb3 O10 80.3(3) 2_666 . ? O3 Pb3 O10 146.0(3) . . ? O9 Pb3 O10 137.1(3) 1_655 . ? O7 Pb3 O10 113.5(3) 1_655 . ? O13 Pb3 O10 80.5(3) . . ? O1 Pb3 O10 75.9(3) 1_655 . ? O8 Pb3 Te1 101.1(2) 2_666 . ? O3 Pb3 Te1 28.8(2) . . ? O9 Pb3 Te1 99.8(2) 1_655 . ? O7 Pb3 Te1 89.7(2) 1_655 . ? O13 Pb3 Te1 44.7(2) . . ? O1 Pb3 Te1 158.3(2) 1_655 . ? O10 Pb3 Te1 119.8(2) . . ? O8 Pb3 Te4 28.0(2) 2_666 2_666 ? O3 Pb3 Te4 72.8(3) . 2_666 ? O9 Pb3 Te4 51.4(2) 1_655 2_666 ? O7 Pb3 Te4 131.2(2) 1_655 2_666 ? O13 Pb3 Te4 84.1(2) . 2_666 ? O1 Pb3 Te4 97.8(2) 1_655 2_666 ? O10 Pb3 Te4 107.9(2) . 2_666 ? Te1 Pb3 Te4 91.52(3) . 2_666 ? O8 Pb3 O4 55.3(3) 2_666 1_655 ? O3 Pb3 O4 144.6(3) . 1_655 ? O9 Pb3 O4 85.4(3) 1_655 1_655 ? O7 Pb3 O4 116.1(3) 1_655 1_655 ? O13 Pb3 O4 112.2(3) . 1_655 ? O1 Pb3 O4 47.1(3) 1_655 1_655 ? O10 Pb3 O4 51.7(3) . 1_655 ? Te1 Pb3 O4 154.16(16) . 1_655 ? Te4 Pb3 O4 71.85(17) 2_666 1_655 ? O8 Pb3 Pb4 40.9(2) 2_666 2_666 ? O3 Pb3 Pb4 127.3(3) . 2_666 ? O9 Pb3 Pb4 107.6(2) 1_655 2_666 ? O7 Pb3 Pb4 146.5(2) 1_655 2_666 ? O13 Pb3 Pb4 76.2(2) . 2_666 ? O1 Pb3 Pb4 82.0(2) 1_655 2_666 ? O10 Pb3 Pb4 39.6(2) . 2_666 ? Te1 Pb3 Pb4 119.70(2) . 2_666 ? Te4 Pb3 Pb4 68.30(2) 2_666 2_666 ? O4 Pb3 Pb4 36.11(15) 1_655 2_666 ? O8 Pb3 Te4 77.1(2) 2_666 1_655 ? O3 Pb3 Te4 95.8(2) . 1_655 ? O9 Pb3 Te4 25.0(2) 1_655 1_655 ? O7 Pb3 Te4 78.6(2) 1_655 1_655 ? O13 Pb3 Te4 144.5(2) . 1_655 ? O1 Pb3 Te4 47.4(2) 1_655 1_655 ? O10 Pb3 Te4 114.6(2) . 1_655 ? Te1 Pb3 Te4 124.44(3) . 1_655 ? Te4 Pb3 Te4 61.05(3) 2_666 1_655 ? O4 Pb3 Te4 65.04(15) 1_655 1_655 ? Pb4 Pb3 Te4 95.13(2) 2_666 1_655 ? O8 Pb3 Pb5 92.7(2) 2_666 1_655 ? O3 Pb3 Pb5 38.1(2) . 1_655 ? O9 Pb3 Pb5 35.4(2) 1_655 1_655 ? O7 Pb3 Pb5 71.4(2) 1_655 1_655 ? O13 Pb3 Pb5 102.2(2) . 1_655 ? O1 Pb3 Pb5 100.5(2) 1_655 1_655 ? O10 Pb3 Pb5 171.7(2) . 1_655 ? Te1 Pb3 Pb5 65.86(2) . 1_655 ? Te4 Pb3 Pb5 64.86(2) 2_666 1_655 ? O4 Pb3 Pb5 120.34(16) 1_655 1_655 ? Pb4 Pb3 Pb5 133.01(2) 2_666 1_655 ? Te4 Pb3 Pb5 58.873(19) 1_655 1_655 ? O8 Pb3 Te5 83.1(2) 2_666 1_655 ? O3 Pb3 Te5 161.6(2) . 1_655 ? O9 Pb3 Te5 90.6(2) 1_655 1_655 ? O7 Pb3 Te5 90.2(2) 1_655 1_655 ? O13 Pb3 Te5 129.3(2) . 1_655 ? O1 Pb3 Te5 26.4(2) 1_655 1_655 ? O10 Pb3 Te5 51.0(2) . 1_655 ? Te1 Pb3 Te5 169.51(3) . 1_655 ? Te4 Pb3 Te5 96.41(3) 2_666 1_655 ? O4 Pb3 Te5 27.84(16) 1_655 1_655 ? Pb4 Pb3 Te5 57.848(19) 2_666 1_655 ? Te4 Pb3 Te5 65.74(2) 1_655 1_655 ? Pb5 Pb3 Te5 123.88(2) 1_655 1_655 ? O8 Pb3 Te3 149.5(2) 2_666 1_655 ? O3 Pb3 Te3 113.4(3) . 1_655 ? O9 Pb3 Te3 126.1(2) 1_655 1_655 ? O7 Pb3 Te3 48.2(2) 1_655 1_655 ? O13 Pb3 Te3 101.5(2) . 1_655 ? O1 Pb3 Te3 75.3(2) 1_655 1_655 ? O10 Pb3 Te3 69.2(2) . 1_655 ? Te1 Pb3 Te3 95.53(2) . 1_655 ? Te4 Pb3 Te3 172.90(3) 2_666 1_655 ? O4 Pb3 Te3 101.80(17) 1_655 1_655 ? Pb4 Pb3 Te3 108.60(2) 2_666 1_655 ? Te4 Pb3 Te3 113.73(2) 1_655 1_655 ? Pb5 Pb3 Te3 117.47(2) 1_655 1_655 ? Te5 Pb3 Te3 76.69(2) 1_655 1_655 ? O4 Pb4 O10 77.6(4) 2_566 2_666 ? O4 Pb4 O5 76.6(3) 2_566 1_565 ? O10 Pb4 O5 97.4(4) 2_666 1_565 ? O4 Pb4 O8 78.7(3) 2_566 . ? O10 Pb4 O8 85.2(4) 2_666 . ? O5 Pb4 O8 154.0(3) 1_565 . ? O4 Pb4 O6 76.3(4) 2_566 . ? O10 Pb4 O6 149.8(3) 2_666 . ? O5 Pb4 O6 91.2(3) 1_565 . ? O8 Pb4 O6 75.0(4) . . ? O4 Pb4 O5 133.8(4) 2_566 2_666 ? O10 Pb4 O5 74.2(3) 2_666 2_666 ? O5 Pb4 O5 71.7(4) 1_565 2_666 ? O8 Pb4 O5 133.1(3) . 2_666 ? O6 Pb4 O5 135.8(3) . 2_666 ? O4 Pb4 O3 124.7(3) 2_566 . ? O10 Pb4 O3 143.7(3) 2_666 . ? O5 Pb4 O3 114.5(3) 1_565 . ? O8 Pb4 O3 73.7(3) . . ? O6 Pb4 O3 50.8(3) . . ? O5 Pb4 O3 99.0(3) 2_666 . ? O4 Pb4 Te2 86.9(3) 2_566 2_666 ? O10 Pb4 Te2 27.5(3) 2_666 2_666 ? O5 Pb4 Te2 74.4(3) 1_565 2_666 ? O8 Pb4 Te2 112.4(3) . 2_666 ? O6 Pb4 Te2 160.1(2) . 2_666 ? O5 Pb4 Te2 52.9(2) 2_666 2_666 ? O3 Pb4 Te2 147.99(15) . 2_666 ? O4 Pb4 Te5 54.1(2) 2_566 1_565 ? O10 Pb4 Te5 103.5(3) 2_666 1_565 ? O5 Pb4 Te5 26.9(2) 1_565 1_565 ? O8 Pb4 Te5 127.4(2) . 1_565 ? O6 Pb4 Te5 72.7(2) . 1_565 ? O5 Pb4 Te5 98.5(2) 2_666 1_565 ? O3 Pb4 Te5 112.75(16) . 1_565 ? Te2 Pb4 Te5 88.92(3) 2_666 1_565 ? O4 Pb4 Te5 24.0(3) 2_566 2_566 ? O10 Pb4 Te5 54.5(2) 2_666 2_566 ? O5 Pb4 Te5 76.2(2) 1_565 2_566 ? O8 Pb4 Te5 84.6(2) . 2_566 ? O6 Pb4 Te5 100.3(2) . 2_566 ? O5 Pb4 Te5 113.8(2) 2_666 2_566 ? O3 Pb4 Te5 147.22(15) . 2_566 ? Te2 Pb4 Te5 63.36(2) 2_666 2_566 ? Te5 Pb4 Te5 62.24(3) 1_565 2_566 ? O4 Pb4 Te4 131.6(3) 2_566 2_666 ? O10 Pb4 Te4 83.9(3) 2_666 2_666 ? O5 Pb4 Te4 150.7(2) 1_565 2_666 ? O8 Pb4 Te4 55.3(2) . 2_666 ? O6 Pb4 Te4 102.4(2) . 2_666 ? O5 Pb4 Te4 80.6(2) 2_666 2_666 ? O3 Pb4 Te4 59.82(16) . 2_666 ? Te2 Pb4 Te4 96.73(3) 2_666 2_666 ? Te5 Pb4 Te4 172.03(3) 1_565 2_666 ? Te5 Pb4 Te4 125.41(3) 2_566 2_666 ? O4 Pb4 Te2 113.6(2) 2_566 1_565 ? O10 Pb4 Te2 138.5(3) 2_666 1_565 ? O5 Pb4 Te2 51.7(3) 1_565 1_565 ? O8 Pb4 Te2 135.3(3) . 1_565 ? O6 Pb4 Te2 67.5(2) . 1_565 ? O5 Pb4 Te2 70.1(2) 2_666 1_565 ? O3 Pb4 Te2 63.97(17) . 1_565 ? Te2 Pb4 Te2 111.10(3) 2_666 1_565 ? Te5 Pb4 Te2 62.70(2) 1_565 1_565 ? Te5 Pb4 Te2 124.71(3) 2_566 1_565 ? Te4 Pb4 Te2 109.82(2) 2_666 1_565 ? O4 Pb4 Pb3 70.9(2) 2_566 2_666 ? O10 Pb4 Pb3 47.5(3) 2_666 2_666 ? O5 Pb4 Pb3 136.0(3) 1_565 2_666 ? O8 Pb4 Pb3 37.9(3) . 2_666 ? O6 Pb4 Pb3 108.7(2) . 2_666 ? O5 Pb4 Pb3 111.8(2) 2_666 2_666 ? O3 Pb4 Pb3 108.26(17) . 2_666 ? Te2 Pb4 Pb3 74.93(3) 2_666 2_666 ? Te5 Pb4 Pb3 123.44(2) 1_565 2_666 ? Te5 Pb4 Pb3 62.064(19) 2_566 2_666 ? Te4 Pb4 Pb3 63.76(2) 2_666 2_666 ? Te2 Pb4 Pb3 172.19(2) 1_565 2_666 ? O4 Pb4 Te1 98.4(3) 2_566 . ? O10 Pb4 Te1 158.7(3) 2_666 . ? O5 Pb4 Te1 102.1(3) 1_565 . ? O8 Pb4 Te1 73.5(3) . . ? O6 Pb4 Te1 22.9(2) . . ? O5 Pb4 Te1 120.2(2) 2_666 . ? O3 Pb4 Te1 27.96(15) . . ? Te2 Pb4 Te1 172.86(3) 2_666 . ? Te5 Pb4 Te1 90.31(2) 1_565 . ? Te5 Pb4 Te1 122.26(2) 2_566 . ? Te4 Pb4 Te1 83.39(2) 2_666 . ? Te2 Pb4 Te1 62.40(2) 1_565 . ? Pb3 Pb4 Te1 111.28(2) 2_666 . ? O4 Pb4 Pb5 43.1(3) 2_566 . ? O10 Pb4 Pb5 116.8(2) 2_666 . ? O5 Pb4 Pb5 89.1(2) 1_565 . ? O8 Pb4 Pb5 67.0(2) . . ? O6 Pb4 Pb5 34.0(2) . . ? O5 Pb4 Pb5 159.4(2) 2_666 . ? O3 Pb4 Pb5 81.93(15) . . ? Te2 Pb4 Pb5 129.92(3) 2_666 . ? Te5 Pb4 Pb5 62.86(2) 1_565 . ? Te5 Pb4 Pb5 66.87(2) 2_566 . ? Te4 Pb4 Pb5 116.55(2) 2_666 . ? Te2 Pb4 Pb5 92.40(2) 1_565 . ? Pb3 Pb4 Pb5 87.019(19) 2_666 . ? Te1 Pb4 Pb5 55.392(19) . . ? O11 Pb5 O9 97.4(4) 2_565 . ? O11 Pb5 O6 73.4(4) 2_565 . ? O9 Pb5 O6 90.1(4) . . ? O11 Pb5 O3 87.0(4) 2_565 1_455 ? O9 Pb5 O3 73.6(3) . 1_455 ? O6 Pb5 O3 152.8(4) . 1_455 ? O11 Pb5 O4 144.2(3) 2_565 2_566 ? O9 Pb5 O4 93.2(3) . 2_566 ? O6 Pb5 O4 72.4(3) . 2_566 ? O3 Pb5 O4 128.9(3) 1_455 2_566 ? O11 Pb5 Te2 98.0(3) 2_565 1_465 ? O9 Pb5 Te2 146.5(2) . 1_465 ? O6 Pb5 Te2 122.9(3) . 1_465 ? O3 Pb5 Te2 77.6(2) 1_455 1_465 ? O4 Pb5 Te2 91.5(2) 2_566 1_465 ? O11 Pb5 O15 71.6(3) 2_565 1_465 ? O9 Pb5 O15 160.0(3) . 1_465 ? O6 Pb5 O15 102.1(3) . 1_465 ? O3 Pb5 O15 88.9(3) 1_455 1_465 ? O4 Pb5 O15 105.5(3) 2_566 1_465 ? Te2 Pb5 O15 29.25(17) 1_465 1_465 ? O11 Pb5 Te1 50.4(2) 2_565 . ? O9 Pb5 Te1 82.1(2) . . ? O6 Pb5 Te1 26.3(3) . . ? O3 Pb5 Te1 127.3(3) 1_455 . ? O4 Pb5 Te1 97.9(2) 2_566 . ? Te2 Pb5 Te1 130.02(3) 1_465 . ? O15 Pb5 Te1 101.87(17) 1_465 . ? O11 Pb5 O8 111.6(3) 2_565 . ? O9 Pb5 O8 48.0(3) . . ? O6 Pb5 O8 54.9(3) . . ? O3 Pb5 O8 119.5(3) 1_455 . ? O4 Pb5 O8 54.3(3) 2_566 . ? Te2 Pb5 O8 145.70(17) 1_465 . ? O15 Pb5 O8 151.2(2) 1_465 . ? Te1 Pb5 O8 65.77(16) . . ? O11 Pb5 Te4 95.2(3) 2_565 . ? O9 Pb5 Te4 23.5(2) . . ? O6 Pb5 Te4 67.2(3) . . ? O3 Pb5 Te4 96.9(2) 1_455 . ? O4 Pb5 Te4 81.4(2) 2_566 . ? Te2 Pb5 Te4 165.41(3) 1_465 . ? O15 Pb5 Te4 165.34(17) 1_465 . ? Te1 Pb5 Te4 63.98(2) . . ? O8 Pb5 Te4 28.47(16) . . ? O11 Pb5 Pb3 82.1(3) 2_565 1_455 ? O9 Pb5 Pb3 38.3(2) . 1_455 ? O6 Pb5 Pb3 118.7(3) . 1_455 ? O3 Pb5 Pb3 37.9(2) 1_455 1_455 ? O4 Pb5 Pb3 124.4(2) 2_566 1_455 ? Te2 Pb5 Pb3 115.54(2) 1_465 1_455 ? O15 Pb5 Pb3 122.00(18) 1_465 1_455 ? Te1 Pb5 Pb3 98.87(2) . 1_455 ? O8 Pb5 Pb3 86.34(15) . 1_455 ? Te4 Pb5 Pb3 60.136(19) . 1_455 ? O11 Pb5 O7 44.6(3) 2_565 . ? O9 Pb5 O7 56.9(3) . . ? O6 Pb5 O7 92.5(3) . . ? O3 Pb5 O7 60.5(3) 1_455 . ? O4 Pb5 O7 147.1(3) 2_566 . ? Te2 Pb5 O7 120.80(15) 1_465 . ? O15 Pb5 O7 106.2(2) 1_465 . ? Te1 Pb5 O7 67.06(14) . . ? O8 Pb5 O7 93.0(2) . . ? Te4 Pb5 O7 65.76(15) . . ? Pb3 Pb5 O7 38.83(16) 1_455 . ? O11 Pb5 Te3 19.0(3) 2_565 2_565 ? O9 Pb5 Te3 83.4(2) . 2_565 ? O6 Pb5 Te3 86.3(3) . 2_565 ? O3 Pb5 Te3 70.6(3) 1_455 2_565 ? O4 Pb5 Te3 158.5(2) 2_566 2_565 ? Te2 Pb5 Te3 103.03(3) 1_465 2_565 ? O15 Pb5 Te3 81.65(17) 1_465 2_565 ? Te1 Pb5 Te3 60.57(2) . 2_565 ? O8 Pb5 Te3 110.60(17) . 2_565 ? Te4 Pb5 Te3 87.53(2) . 2_565 ? Pb3 Pb5 Te3 63.23(2) 1_455 2_565 ? O7 Pb5 Te3 27.22(16) . 2_565 ? O11 Pb5 Pb4 110.8(2) 2_565 . ? O9 Pb5 Pb4 86.4(2) . . ? O6 Pb5 Pb4 37.4(2) . . ? O3 Pb5 Pb4 155.0(2) 1_455 . ? O4 Pb5 Pb4 35.8(2) 2_566 . ? Te2 Pb5 Pb4 115.26(2) 1_465 . ? O15 Pb5 Pb4 112.89(18) 1_465 . ? Te1 Pb5 Pb4 62.195(19) . . ? O8 Pb5 Pb4 38.45(15) . . ? Te4 Pb5 Pb4 65.165(19) . . ? Pb3 Pb5 Pb4 124.72(2) 1_455 . ? O7 Pb5 Pb4 120.32(14) . . ? Te3 Pb5 Pb4 122.69(2) 2_565 . ? O11 Pb5 O13 69.6(3) 2_565 . ? O9 Pb5 O13 43.7(3) . . ? O6 Pb5 O13 50.8(3) . . ? O3 Pb5 O13 105.1(3) 1_455 . ? O4 Pb5 O13 96.3(2) 2_566 . ? Te2 Pb5 O13 166.89(15) 1_465 . ? O15 Pb5 O13 137.7(2) 1_465 . ? Te1 Pb5 O13 38.44(15) . . ? O8 Pb5 O13 44.0(2) . . ? Te4 Pb5 O13 27.64(15) . . ? Pb3 Pb5 O13 68.10(15) 1_455 . ? O7 Pb5 O13 53.3(2) . . ? Te3 Pb5 O13 66.66(15) 2_565 . ? Pb4 Pb5 O13 67.51(15) . . ? O3 Te1 O6 98.2(5) . . ? O3 Te1 O2 99.5(5) . . ? O6 Te1 O2 90.4(4) . . ? O3 Te1 O13 78.2(4) . . ? O6 Te1 O13 86.7(4) . . ? O2 Te1 O13 176.0(4) . . ? O3 Te1 O11 164.0(4) . 2_565 ? O6 Te1 O11 69.1(4) . 2_565 ? O2 Te1 O11 90.6(4) . 2_565 ? O13 Te1 O11 90.9(3) . 2_565 ? O3 Te1 O14 78.7(4) . 2_665 ? O6 Te1 O14 156.6(4) . 2_665 ? O2 Te1 O14 67.7(4) . 2_665 ? O13 Te1 O14 114.8(3) . 2_665 ? O11 Te1 O14 116.9(3) 2_565 2_665 ? O3 Te1 Pb3 39.3(3) . . ? O6 Te1 Pb3 116.4(3) . . ? O2 Te1 Pb3 130.2(3) . . ? O13 Te1 Pb3 49.4(2) . . ? O11 Te1 Pb3 136.9(2) 2_565 . ? O14 Te1 Pb3 75.79(17) 2_665 . ? O3 Te1 Pb2 134.6(3) . . ? O6 Te1 Pb2 69.0(3) . . ? O2 Te1 Pb2 40.4(3) . . ? O13 Te1 Pb2 140.1(2) . . ? O11 Te1 Pb2 51.5(2) 2_565 . ? O14 Te1 Pb2 96.49(18) 2_665 . ? Pb3 Te1 Pb2 170.53(4) . . ? O3 Te1 Pb5 125.5(3) . . ? O6 Te1 Pb5 33.3(3) . . ? O2 Te1 Pb5 102.3(3) . . ? O13 Te1 Pb5 76.7(2) . . ? O11 Te1 Pb5 39.3(2) 2_565 . ? O14 Te1 Pb5 155.69(19) 2_665 . ? Pb3 Te1 Pb5 123.43(3) . . ? Pb2 Te1 Pb5 65.54(2) . . ? O3 Te1 Te3 156.2(3) . 2_565 ? O6 Te1 Te3 95.0(3) . 2_565 ? O2 Te1 Te3 100.2(3) . 2_565 ? O13 Te1 Te3 82.9(2) . 2_565 ? O11 Te1 Te3 27.6(2) 2_565 2_565 ? O14 Te1 Te3 96.53(19) 2_665 2_565 ? Pb3 Te1 Te3 116.88(3) . 2_565 ? Pb2 Te1 Te3 68.92(2) . 2_565 ? Pb5 Te1 Te3 62.52(2) . 2_565 ? O3 Te1 Pb2 91.8(3) . 2_675 ? O6 Te1 Pb2 116.7(3) . 2_675 ? O2 Te1 Pb2 26.6(3) . 2_675 ? O13 Te1 Pb2 155.8(2) . 2_675 ? O11 Te1 Pb2 102.6(2) 2_565 2_675 ? O14 Te1 Pb2 41.06(18) 2_665 2_675 ? Pb3 Te1 Pb2 110.19(3) . 2_675 ? Pb2 Te1 Pb2 60.60(2) . 2_675 ? Pb5 Te1 Pb2 126.03(3) . 2_675 ? Te3 Te1 Pb2 99.83(3) 2_565 2_675 ? O3 Te1 Pb4 66.8(3) . . ? O6 Te1 Pb4 31.4(3) . . ? O2 Te1 Pb4 93.7(3) . . ? O13 Te1 Pb4 82.3(2) . . ? O11 Te1 Pb4 100.3(2) 2_565 . ? O14 Te1 Pb4 137.6(2) 2_665 . ? Pb3 Te1 Pb4 91.17(3) . . ? Pb2 Te1 Pb4 91.01(2) . . ? Pb5 Te1 Pb4 62.41(2) . . ? Te3 Te1 Pb4 124.85(3) 2_565 . ? Pb2 Te1 Pb4 114.20(3) 2_675 . ? O3 Te1 Te4 81.6(3) . . ? O6 Te1 Te4 65.1(3) . . ? O2 Te1 Te4 155.2(3) . . ? O13 Te1 Te4 21.6(2) . . ? O11 Te1 Te4 84.0(2) 2_565 . ? O14 Te1 Te4 135.90(18) 2_665 . ? Pb3 Te1 Te4 64.20(2) . . ? Pb2 Te1 Te4 124.82(3) . . ? Pb5 Te1 Te4 59.28(2) . . ? Te3 Te1 Te4 86.12(3) 2_565 . ? Pb2 Te1 Te4 173.42(3) 2_675 . ? Pb4 Te1 Te4 63.70(2) . . ? O3 Te1 Te2 74.3(3) . 1_565 ? O6 Te1 Te2 65.6(3) . 1_565 ? O2 Te1 Te2 38.9(3) . 1_565 ? O13 Te1 Te2 137.0(2) . 1_565 ? O11 Te1 Te2 107.4(2) 2_565 1_565 ? O14 Te1 Te2 91.44(19) 2_665 1_565 ? Pb3 Te1 Te2 113.49(3) . 1_565 ? Pb2 Te1 Te2 60.57(2) . 1_565 ? Pb5 Te1 Te2 93.21(3) . 1_565 ? Te3 Te1 Te2 129.43(3) 2_565 1_565 ? Pb2 Te1 Te2 57.65(2) 2_675 1_565 ? Pb4 Te1 Te2 56.73(2) . 1_565 ? Te4 Te1 Te2 120.40(3) . 1_565 ? O3 Te1 O8 69.5(4) . . ? O6 Te1 O8 47.4(3) . . ? O2 Te1 O8 130.8(4) . . ? O13 Te1 O8 45.4(3) . . ? O11 Te1 O8 94.4(3) 2_565 . ? O14 Te1 O8 145.0(2) 2_665 . ? Pb3 Te1 O8 70.46(14) . . ? Pb2 Te1 O8 116.05(14) . . ? Pb5 Te1 O8 58.37(14) . . ? Te3 Te1 O8 106.53(14) 2_565 . ? Pb2 Te1 O8 149.85(14) 2_675 . ? Pb4 Te1 O8 37.21(14) . . ? Te4 Te1 O8 26.84(14) . . ? Te2 Te1 O8 93.67(14) 1_565 . ? O15 Te2 O10 97.8(5) . . ? O15 Te2 O12 101.0(5) . . ? O10 Te2 O12 97.9(4) . . ? O15 Te2 O2 75.6(4) . 1_545 ? O10 Te2 O2 167.1(4) . 1_545 ? O12 Te2 O2 73.0(4) . 1_545 ? O15 Te2 O5 172.3(4) . . ? O10 Te2 O5 76.6(4) . . ? O12 Te2 O5 74.9(4) . . ? O2 Te2 O5 108.8(3) 1_545 . ? O15 Te2 Pb5 76.4(4) . 1_645 ? O10 Te2 Pb5 112.9(3) . 1_645 ? O12 Te2 Pb5 149.2(3) . 1_645 ? O2 Te2 Pb5 76.7(2) 1_545 1_645 ? O5 Te2 Pb5 110.5(2) . 1_645 ? O15 Te2 O6 121.4(4) . 1_545 ? O10 Te2 O6 140.7(4) . 1_545 ? O12 Te2 O6 76.1(4) . 1_545 ? O2 Te2 O6 47.1(3) 1_545 1_545 ? O5 Te2 O6 64.4(3) . 1_545 ? Pb5 Te2 O6 79.32(16) 1_645 1_545 ? O15 Te2 Pb4 129.9(4) . 2_666 ? O10 Te2 Pb4 36.8(3) . 2_666 ? O12 Te2 Pb4 104.7(3) . 2_666 ? O2 Te2 Pb4 153.3(2) 1_545 2_666 ? O5 Te2 Pb4 47.0(2) . 2_666 ? Pb5 Te2 Pb4 99.74(3) 1_645 2_666 ? O6 Te2 Pb4 106.24(16) 1_545 2_666 ? O15 Te2 Pb1 94.9(4) . . ? O10 Te2 Pb1 65.8(3) . . ? O12 Te2 Pb1 33.7(3) . . ? O2 Te2 Pb1 103.4(2) 1_545 . ? O5 Te2 Pb1 78.0(2) . . ? Pb5 Te2 Pb1 171.10(4) 1_645 . ? O6 Te2 Pb1 107.41(16) 1_545 . ? Pb4 Te2 Pb1 84.15(3) 2_666 . ? O15 Te2 Pb4 146.9(4) . 1_545 ? O10 Te2 Pb4 105.7(3) . 1_545 ? O12 Te2 Pb4 98.6(4) . 1_545 ? O2 Te2 Pb4 85.0(2) 1_545 1_545 ? O5 Te2 Pb4 40.8(2) . 1_545 ? Pb5 Te2 Pb4 73.11(2) 1_645 1_545 ? O6 Te2 Pb4 39.81(16) 1_545 1_545 ? Pb4 Te2 Pb4 68.90(3) 2_666 1_545 ? Pb1 Te2 Pb4 115.79(3) . 1_545 ? O15 Te2 Pb2 38.8(4) . 2_665 ? O10 Te2 Pb2 134.2(3) . 2_665 ? O12 Te2 Pb2 82.1(3) . 2_665 ? O2 Te2 Pb2 37.1(2) 1_545 2_665 ? O5 Te2 Pb2 144.4(2) . 2_665 ? Pb5 Te2 Pb2 77.08(2) 1_645 2_665 ? O6 Te2 Pb2 84.09(16) 1_545 2_665 ? Pb4 Te2 Pb2 168.60(4) 2_666 2_665 ? Pb1 Te2 Pb2 97.54(3) . 2_665 ? Pb4 Te2 Pb2 119.65(3) 1_545 2_665 ? O15 Te2 O5 132.2(4) . 2_656 ? O10 Te2 O5 71.4(4) . 2_656 ? O12 Te2 O5 126.3(4) . 2_656 ? O2 Te2 O5 121.2(3) 1_545 2_656 ? O5 Te2 O5 51.4(3) . 2_656 ? Pb5 Te2 O5 66.68(16) 1_645 2_656 ? O6 Te2 O5 81.1(2) 1_545 2_656 ? Pb4 Te2 O5 38.43(16) 2_666 2_656 ? Pb1 Te2 O5 119.48(16) . 2_656 ? Pb4 Te2 O5 41.91(15) 1_545 2_656 ? Pb2 Te2 O5 142.74(16) 2_665 2_656 ? O15 Te2 Pb2 91.9(4) . 1_545 ? O10 Te2 Pb2 130.3(3) . 1_545 ? O12 Te2 Pb2 32.6(3) . 1_545 ? O2 Te2 Pb2 40.6(2) 1_545 1_545 ? O5 Te2 Pb2 87.90(19) . 1_545 ? Pb5 Te2 Pb2 116.76(3) 1_645 1_545 ? O6 Te2 Pb2 54.66(15) 1_545 1_545 ? Pb4 Te2 Pb2 130.72(3) 2_666 1_545 ? Pb1 Te2 Pb2 64.93(2) . 1_545 ? Pb4 Te2 Pb2 90.34(3) 1_545 1_545 ? Pb2 Te2 Pb2 59.22(2) 2_665 1_545 ? O5 Te2 Pb2 131.20(15) 2_656 1_545 ? O15 Te2 Te5 75.6(4) . 1_655 ? O10 Te2 Te5 50.3(3) . 1_655 ? O12 Te2 Te5 145.8(3) . 1_655 ? O2 Te2 Te5 135.6(2) 1_545 1_655 ? O5 Te2 Te5 104.1(2) . 1_655 ? Pb5 Te2 Te5 64.09(2) 1_645 1_655 ? O6 Te2 Te5 135.21(15) 1_545 1_655 ? Pb4 Te2 Te5 59.17(2) 2_666 1_655 ? Pb1 Te2 Te5 112.14(3) . 1_655 ? Pb4 Te2 Te5 101.98(3) 1_545 1_655 ? Pb2 Te2 Te5 110.12(3) 2_665 1_655 ? O5 Te2 Te5 61.68(15) 2_656 1_655 ? Pb2 Te2 Te5 167.01(4) 1_545 1_655 ? O15 Te2 Te5 148.3(4) . . ? O10 Te2 Te5 86.5(3) . . ? O12 Te2 Te5 47.5(4) . . ? O2 Te2 Te5 93.5(2) 1_545 . ? O5 Te2 Te5 27.68(19) . . ? Pb5 Te2 Te5 130.61(4) 1_645 . ? O6 Te2 Te5 60.60(16) 1_545 . ? Pb4 Te2 Te5 68.46(3) 2_666 . ? Pb1 Te2 Te5 58.26(2) . . ? Pb4 Te2 Te5 57.74(2) 1_545 . ? Pb2 Te2 Te5 121.97(3) 2_665 . ? O5 Te2 Te5 78.96(15) 2_656 . ? Pb2 Te2 Te5 62.78(2) 1_545 . ? Te5 Te2 Te5 127.61(4) 1_655 . ? O14 Te3 O7 100.9(4) . 2_565 ? O14 Te3 O11 97.3(5) . . ? O7 Te3 O11 97.6(5) 2_565 . ? O14 Te3 O15 86.0(4) . 1_455 ? O7 Te3 O15 168.2(4) 2_565 1_455 ? O11 Te3 O15 71.9(4) . 1_455 ? O14 Te3 O7 71.7(4) . . ? O7 Te3 O7 71.4(4) 2_565 . ? O11 Te3 O7 161.9(4) . . ? O15 Te3 O7 120.2(3) 1_455 . ? O14 Te3 Pb2 39.5(3) . 1_545 ? O7 Te3 Pb2 130.4(3) 2_565 1_545 ? O11 Te3 Pb2 69.3(3) . 1_545 ? O15 Te3 Pb2 51.6(2) 1_455 1_545 ? O7 Te3 Pb2 106.4(2) . 1_545 ? O14 Te3 Pb1 135.7(3) . 2_565 ? O7 Te3 Pb1 36.8(3) 2_565 2_565 ? O11 Te3 Pb1 100.3(3) . 2_565 ? O15 Te3 Pb1 138.1(2) 1_455 2_565 ? O7 Te3 Pb1 79.6(2) . 2_565 ? Pb2 Te3 Pb1 164.18(3) 1_545 2_565 ? O14 Te3 Pb1 31.5(3) . . ? O7 Te3 Pb1 92.9(3) 2_565 . ? O11 Te3 Pb1 128.8(3) . . ? O15 Te3 Pb1 97.9(2) 1_455 . ? O7 Te3 Pb1 41.04(19) . . ? Pb2 Te3 Pb1 66.02(2) 1_545 . ? Pb1 Te3 Pb1 116.66(3) 2_565 . ? O14 Te3 O3 61.5(4) . 2_665 ? O7 Te3 O3 63.1(4) 2_565 2_665 ? O11 Te3 O3 58.7(4) . 2_665 ? O15 Te3 O3 113.3(3) 1_455 2_665 ? O7 Te3 O3 103.2(3) . 2_665 ? Pb2 Te3 O3 69.90(15) 1_545 2_665 ? Pb1 Te3 O3 94.60(15) 2_565 2_665 ? Pb1 Te3 O3 83.04(14) . 2_665 ? O14 Te3 Te1 142.3(3) . 2_565 ? O7 Te3 Te1 88.3(3) 2_565 2_565 ? O11 Te3 Te1 45.0(3) . 2_565 ? O15 Te3 Te1 80.5(2) 1_455 2_565 ? O7 Te3 Te1 144.65(19) . 2_565 ? Pb2 Te3 Te1 108.72(3) 1_545 2_565 ? Pb1 Te3 Te1 67.42(2) 2_565 2_565 ? Pb1 Te3 Te1 173.78(4) . 2_565 ? O3 Te3 Te1 92.07(15) 2_665 2_565 ? O14 Te3 Pb5 89.5(4) . 2_565 ? O7 Te3 Pb5 76.7(3) 2_565 2_565 ? O11 Te3 Pb5 24.1(3) . 2_565 ? O15 Te3 Pb5 94.0(2) 1_455 2_565 ? O7 Te3 Pb5 138.5(2) . 2_565 ? Pb2 Te3 Pb5 75.31(2) 1_545 2_565 ? Pb1 Te3 Pb5 90.43(2) 2_565 2_565 ? Pb1 Te3 Pb5 117.45(3) . 2_565 ? O3 Te3 Pb5 36.98(15) 2_665 2_565 ? Te1 Te3 Pb5 56.92(2) 2_565 2_565 ? O14 Te3 Te3 81.6(3) . 2_565 ? O7 Te3 Te3 45.0(3) 2_565 2_565 ? O11 Te3 Te3 140.5(3) . 2_565 ? O15 Te3 Te3 146.5(2) 1_455 2_565 ? O7 Te3 Te3 26.3(2) . 2_565 ? Pb2 Te3 Te3 121.00(4) 1_545 2_565 ? Pb1 Te3 Te3 59.33(2) 2_565 2_565 ? Pb1 Te3 Te3 57.33(3) . 2_565 ? O3 Te3 Te3 87.65(16) 2_665 2_565 ? Te1 Te3 Te3 126.52(4) 2_565 2_565 ? Pb5 Te3 Te3 116.79(4) 2_565 2_565 ? O14 Te3 Pb3 91.3(4) . 1_455 ? O7 Te3 Pb3 102.3(3) 2_565 1_455 ? O11 Te3 Pb3 156.4(3) . 1_455 ? O15 Te3 Pb3 86.9(2) 1_455 1_455 ? O7 Te3 Pb3 41.2(2) . 1_455 ? Pb2 Te3 Pb3 105.85(3) 1_545 1_455 ? Pb1 Te3 Pb3 88.39(2) 2_565 1_455 ? Pb1 Te3 Pb3 63.10(2) . 1_455 ? O3 Te3 Pb3 143.09(15) 2_665 1_455 ? Te1 Te3 Pb3 122.58(3) 2_565 1_455 ? Pb5 Te3 Pb3 178.82(3) 2_565 1_455 ? Te3 Te3 Pb3 62.50(3) 2_565 1_455 ? O14 Te3 O10 94.9(4) . 1_455 ? O7 Te3 O10 141.7(4) 2_565 1_455 ? O11 Te3 O10 114.9(4) . 1_455 ? O15 Te3 O10 45.6(3) 1_455 1_455 ? O7 Te3 O10 81.0(3) . 1_455 ? Pb2 Te3 O10 82.23(17) 1_545 1_455 ? Pb1 Te3 O10 113.39(17) 2_565 1_455 ? Pb1 Te3 O10 82.67(14) . 1_455 ? O3 Te3 O10 151.9(2) 2_665 1_455 ? Te1 Te3 O10 100.16(14) 2_565 1_455 ? Pb5 Te3 O10 138.62(16) 2_565 1_455 ? Te3 Te3 O10 104.55(16) 2_565 1_455 ? Pb3 Te3 O10 42.16(16) 1_455 1_455 ? O14 Te3 Pb3 80.6(3) . 2_665 ? O7 Te3 Pb3 27.5(3) 2_565 2_665 ? O11 Te3 Pb3 81.9(3) . 2_665 ? O15 Te3 Pb3 148.7(2) 1_455 2_665 ? O7 Te3 Pb3 82.1(2) . 2_665 ? Pb2 Te3 Pb3 103.47(3) 1_545 2_665 ? Pb1 Te3 Pb3 62.325(19) 2_565 2_665 ? Pb1 Te3 Pb3 85.19(2) . 2_665 ? O3 Te3 Pb3 35.86(16) 2_665 2_665 ? Te1 Te3 Pb3 93.10(3) 2_565 2_665 ? Pb5 Te3 Pb3 58.01(2) 2_565 2_665 ? Te3 Te3 Pb3 58.78(3) 2_565 2_665 ? Pb3 Te3 Pb3 121.28(3) 1_455 2_665 ? O10 Te3 Pb3 163.10(16) 1_455 2_665 ? O13 Te4 O8 102.7(5) . . ? O13 Te4 O9 95.8(4) . . ? O8 Te4 O9 97.5(4) . . ? O13 Te4 O9 170.8(4) . 2_566 ? O8 Te4 O9 77.2(4) . 2_566 ? O9 Te4 O9 75.1(4) . 2_566 ? O13 Te4 O1 78.8(4) . . ? O8 Te4 O1 176.0(3) . . ? O9 Te4 O1 78.7(4) . . ? O9 Te4 O1 100.7(3) 2_566 . ? O13 Te4 O8 71.7(4) . 2_666 ? O8 Te4 O8 71.1(4) . 2_666 ? O9 Te4 O8 160.0(4) . 2_666 ? O9 Te4 O8 116.4(3) 2_566 2_666 ? O1 Te4 O8 112.9(3) . 2_666 ? O13 Te4 O6 58.6(4) . . ? O8 Te4 O6 59.7(4) . . ? O9 Te4 O6 65.9(4) . . ? O9 Te4 O6 114.8(3) 2_566 . ? O1 Te4 O6 118.9(3) . . ? O8 Te4 O6 94.1(2) 2_666 . ? O13 Te4 Pb3 138.6(3) . 2_666 ? O8 Te4 Pb3 37.2(3) . 2_666 ? O9 Te4 Pb3 99.0(3) . 2_666 ? O9 Te4 Pb3 43.7(2) 2_566 2_666 ? O1 Te4 Pb3 142.0(2) . 2_666 ? O8 Te4 Pb3 81.9(2) 2_666 2_666 ? O6 Te4 Pb3 93.26(17) . 2_666 ? O13 Te4 O3 138.7(3) . 2_666 ? O8 Te4 O3 69.2(4) . 2_666 ? O9 Te4 O3 124.9(4) . 2_666 ? O9 Te4 O3 50.0(2) 2_566 2_666 ? O1 Te4 O3 112.2(3) . 2_666 ? O8 Te4 O3 67.4(3) 2_666 2_666 ? O6 Te4 O3 128.8(2) . 2_666 ? Pb3 Te4 O3 39.13(17) 2_666 2_666 ? O13 Te4 Pb1 41.5(3) . . ? O8 Te4 Pb1 143.9(3) . . ? O9 Te4 Pb1 85.2(3) . . ? O9 Te4 Pb1 137.2(2) 2_566 . ? O1 Te4 Pb1 37.3(2) . . ? O8 Te4 Pb1 94.7(2) 2_666 . ? O6 Te4 Pb1 89.75(17) . . ? Pb3 Te4 Pb1 175.56(3) 2_666 . ? O3 Te4 Pb1 136.81(17) 2_666 . ? O13 Te4 Pb4 87.5(3) . 2_666 ? O8 Te4 Pb4 105.0(3) . 2_666 ? O9 Te4 Pb4 156.0(3) . 2_666 ? O9 Te4 Pb4 101.5(2) 2_566 2_666 ? O1 Te4 Pb4 78.69(19) . 2_666 ? O8 Te4 Pb4 42.13(18) 2_666 2_666 ? O6 Te4 Pb4 133.68(16) . 2_666 ? Pb3 Te4 Pb4 93.89(3) 2_666 2_666 ? O3 Te4 Pb4 58.33(16) 2_666 2_666 ? Pb1 Te4 Pb4 81.67(2) . 2_666 ? O13 Te4 Pb5 81.3(3) . . ? O8 Te4 Pb5 75.8(3) . . ? O9 Te4 Pb5 29.5(3) . . ? O9 Te4 Pb5 89.8(2) 2_566 . ? O1 Te4 Pb5 100.9(2) . . ? O8 Te4 Pb5 130.69(19) 2_666 . ? O6 Te4 Pb5 36.88(15) . . ? Pb3 Te4 Pb5 93.24(3) 2_666 . ? O3 Te4 Pb5 130.81(17) 2_666 . ? Pb1 Te4 Pb5 91.13(2) . . ? Pb4 Te4 Pb5 168.63(3) 2_666 . ? O13 Te4 Te4 142.0(3) . 2_566 ? O8 Te4 Te4 84.2(3) . 2_566 ? O9 Te4 Te4 46.2(3) . 2_566 ? O9 Te4 Te4 28.92(19) 2_566 2_566 ? O1 Te4 Te4 92.35(19) . 2_566 ? O8 Te4 Te4 143.3(2) 2_666 2_566 ? O6 Te4 Te4 96.25(16) . 2_566 ? Pb3 Te4 Te4 62.55(3) 2_666 2_566 ? O3 Te4 Te4 78.82(16) 2_666 2_566 ? Pb1 Te4 Te4 120.37(4) . 2_566 ? Pb4 Te4 Te4 127.28(4) 2_666 2_566 ? Pb5 Te4 Te4 64.02(3) . 2_566 ? O13 Te4 Pb3 94.2(3) . 1_455 ? O8 Te4 Pb3 130.4(3) . 1_455 ? O9 Te4 Pb3 33.9(3) . 1_455 ? O9 Te4 Pb3 79.35(18) 2_566 1_455 ? O1 Te4 Pb3 45.64(18) . 1_455 ? O8 Te4 Pb3 157.5(2) 2_666 1_455 ? O6 Te4 Pb3 93.09(15) . 1_455 ? Pb3 Te4 Pb3 118.95(3) 2_666 1_455 ? O3 Te4 Pb3 122.48(16) 2_666 1_455 ? Pb1 Te4 Pb3 64.063(19) . 1_455 ? Pb4 Te4 Pb3 122.24(3) 2_666 1_455 ? Pb5 Te4 Pb3 60.991(18) . 1_455 ? Te4 Te4 Pb3 56.41(2) 2_566 1_455 ? O13 Te4 Te1 30.1(3) . . ? O8 Te4 Te1 79.6(3) . . ? O9 Te4 Te1 80.0(3) . . ? O9 Te4 Te1 143.1(2) 2_566 . ? O1 Te4 Te1 100.6(2) . . ? O8 Te4 Te1 81.8(2) 2_666 . ? O6 Te4 Te1 28.53(17) . . ? Pb3 Te4 Te1 116.56(3) 2_666 . ? O3 Te4 Te1 141.45(16) 2_666 . ? Pb1 Te4 Te1 65.42(2) . . ? Pb4 Te4 Te1 112.02(3) 2_666 . ? Pb5 Te4 Te1 56.74(2) . . ? Te4 Te4 Te1 120.70(4) 2_566 . ? Pb3 Te4 Te1 94.80(3) 1_455 . ? O5 Te5 O4 97.7(4) . . ? O5 Te5 O1 101.9(4) . . ? O4 Te5 O1 95.8(5) . . ? O5 Te5 O12 74.6(4) . . ? O4 Te5 O12 161.8(4) . . ? O1 Te5 O12 70.3(4) . . ? O5 Te5 O4 71.5(4) . 2_556 ? O4 Te5 O4 77.9(4) . 2_556 ? O1 Te5 O4 169.9(4) . 2_556 ? O12 Te5 O4 114.0(3) . 2_556 ? O5 Te5 O10 167.8(4) . 1_455 ? O4 Te5 O10 70.9(4) . 1_455 ? O1 Te5 O10 84.1(3) . 1_455 ? O12 Te5 O10 117.6(3) . 1_455 ? O4 Te5 O10 101.0(3) 2_556 1_455 ? O5 Te5 Pb1 92.9(3) . . ? O4 Te5 Pb1 126.3(3) . . ? O1 Te5 Pb1 30.7(3) . . ? O12 Te5 Pb1 39.9(2) . . ? O4 Te5 Pb1 153.6(2) 2_556 . ? O10 Te5 Pb1 97.4(2) 1_455 . ? O5 Te5 Pb4 36.7(3) . 1_545 ? O4 Te5 Pb4 101.1(3) . 1_545 ? O1 Te5 Pb4 136.7(3) . 1_545 ? O12 Te5 Pb4 82.8(2) . 1_545 ? O4 Te5 Pb4 39.40(18) 2_556 1_545 ? O10 Te5 Pb4 139.2(2) 1_455 1_545 ? Pb1 Te5 Pb4 117.32(3) . 1_545 ? O5 Te5 Pb4 127.4(3) . 2_566 ? O4 Te5 Pb4 31.2(3) . 2_566 ? O1 Te5 Pb4 96.9(3) . 2_566 ? O12 Te5 Pb4 157.3(2) . 2_566 ? O4 Te5 Pb4 81.85(19) 2_556 2_566 ? O10 Te5 Pb4 40.6(2) 1_455 2_566 ? Pb1 Te5 Pb4 124.02(3) . 2_566 ? Pb4 Te5 Pb4 117.76(3) 1_545 2_566 ? O5 Te5 O6 68.4(4) . 1_545 ? O4 Te5 O6 128.9(4) . 1_545 ? O1 Te5 O6 134.6(3) . 1_545 ? O12 Te5 O6 64.3(3) . 1_545 ? O4 Te5 O6 51.0(3) 2_556 1_545 ? O10 Te5 O6 115.0(3) 1_455 1_545 ? Pb1 Te5 O6 103.93(16) . 1_545 ? Pb4 Te5 O6 39.35(15) 1_545 1_545 ? Pb4 Te5 O6 124.87(15) 2_566 1_545 ? O5 Te5 Te5 79.4(3) . 2_556 ? O4 Te5 Te5 49.9(3) . 2_556 ? O1 Te5 Te5 144.9(3) . 2_556 ? O12 Te5 Te5 140.8(2) . 2_556 ? O4 Te5 Te5 28.1(2) 2_556 2_556 ? O10 Te5 Te5 89.5(2) 1_455 2_556 ? Pb1 Te5 Te5 170.25(5) . 2_556 ? Pb4 Te5 Te5 59.24(3) 1_545 2_556 ? Pb4 Te5 Te5 58.52(2) 2_566 2_556 ? O6 Te5 Te5 79.04(16) 1_545 2_556 ? O5 Te5 O15 142.5(4) . 1_455 ? O4 Te5 O15 114.6(3) . 1_455 ? O1 Te5 O15 93.6(4) . 1_455 ? O12 Te5 O15 78.9(3) . 1_455 ? O4 Te5 O15 96.3(3) 2_556 1_455 ? O10 Te5 O15 46.1(3) 1_455 1_455 ? Pb1 Te5 O15 83.16(17) . 1_455 ? Pb4 Te5 O15 114.37(18) 1_545 1_455 ? Pb4 Te5 O15 83.38(16) 2_566 1_455 ? O6 Te5 O15 76.5(2) 1_545 1_455 ? Te5 Te5 O15 106.60(18) 2_556 1_455 ? O5 Te5 Te2 152.1(3) . 1_455 ? O4 Te5 Te2 88.1(3) . 1_455 ? O1 Te5 Te2 104.7(3) . 1_455 ? O12 Te5 Te2 106.4(2) . 1_455 ? O4 Te5 Te2 83.23(18) 2_556 1_455 ? O10 Te5 Te2 28.2(2) 1_455 1_455 ? Pb1 Te5 Te2 105.55(3) . 1_455 ? Pb4 Te5 Te2 115.45(3) 1_545 1_455 ? Pb4 Te5 Te2 57.47(2) 2_566 1_455 ? O6 Te5 Te2 86.72(14) 1_545 1_455 ? Te5 Te5 Te2 83.79(3) 2_556 1_455 ? O15 Te5 Te2 27.59(16) 1_455 1_455 ? O5 Te5 Te2 47.5(3) . . ? O4 Te5 Te2 143.4(3) . . ? O1 Te5 Te2 83.5(3) . . ? O12 Te5 Te2 27.4(2) . . ? O4 Te5 Te2 96.77(19) 2_556 . ? O10 Te5 Te2 144.6(2) 1_455 . ? Pb1 Te5 Te2 57.97(2) . . ? Pb4 Te5 Te2 59.56(2) 1_545 . ? Pb4 Te5 Te2 174.66(3) 2_566 . ? O6 Te5 Te2 56.61(15) 1_545 . ? Te5 Te5 Te2 118.60(4) 2_556 . ? O15 Te5 Te2 101.92(16) 1_455 . ? Te2 Te5 Te2 127.61(4) 1_455 . ? O5 Te5 Pb3 136.1(3) . 1_455 ? O4 Te5 Pb3 72.5(3) . 1_455 ? O1 Te5 Pb3 40.1(3) . 1_455 ? O12 Te5 Pb3 101.2(2) . 1_455 ? O4 Te5 Pb3 141.42(19) 2_556 1_455 ? O10 Te5 Pb3 46.0(2) 1_455 1_455 ? Pb1 Te5 Pb3 63.94(2) . 1_455 ? Pb4 Te5 Pb3 170.75(3) 1_545 1_455 ? Pb4 Te5 Pb3 60.086(19) 2_566 1_455 ? O6 Te5 Pb3 149.83(15) 1_545 1_455 ? Te5 Te5 Pb3 117.83(4) 2_556 1_455 ? O15 Te5 Pb3 74.74(18) 1_455 1_455 ? Te2 Te5 Pb3 71.68(2) 1_455 1_455 ? Te2 Te5 Pb3 121.71(3) . 1_455 ? Te5 O1 Pb1 124.3(5) . . ? Te5 O1 Pb3 113.5(4) . 1_455 ? Pb1 O1 Pb3 106.1(4) . 1_455 ? Te5 O1 Te4 124.6(5) . . ? Pb1 O1 Te4 94.2(3) . . ? Pb3 O1 Te4 87.0(3) 1_455 . ? Te1 O2 Pb2 131.5(5) . 2_675 ? Te1 O2 Pb2 110.3(5) . . ? Pb2 O2 Pb2 103.3(4) 2_675 . ? Te1 O2 Te2 115.6(5) . 1_565 ? Pb2 O2 Te2 95.7(4) 2_675 1_565 ? Pb2 O2 Te2 93.4(3) . 1_565 ? Te1 O2 Pb5 76.4(3) . 1_655 ? Pb2 O2 Pb5 89.3(3) 2_675 1_655 ? Pb2 O2 Pb5 152.9(4) . 1_655 ? Te2 O2 Pb5 61.14(19) 1_565 1_655 ? Te1 O3 Pb5 139.4(5) . 1_655 ? Te1 O3 Pb3 111.9(5) . . ? Pb5 O3 Pb3 103.9(3) 1_655 . ? Te1 O3 Pb4 85.2(4) . . ? Pb5 O3 Pb4 90.8(3) 1_655 . ? Pb3 O3 Pb4 123.2(4) . . ? Te1 O3 Te4 132.3(5) . 2_666 ? Pb5 O3 Te4 78.3(3) 1_655 2_666 ? Pb3 O3 Te4 68.1(2) . 2_666 ? Pb4 O3 Te4 61.85(18) . 2_666 ? Te1 O3 Te3 97.5(4) . 2_665 ? Pb5 O3 Te3 72.4(3) 1_655 2_665 ? Pb3 O3 Te3 76.8(3) . 2_665 ? Pb4 O3 Te3 157.3(3) . 2_665 ? Te4 O3 Te3 126.4(3) 2_666 2_665 ? Te1 O3 Te2 78.7(3) . 1_565 ? Pb5 O3 Te2 64.8(2) 1_655 1_565 ? Pb3 O3 Te2 168.8(4) . 1_565 ? Pb4 O3 Te2 59.70(16) . 1_565 ? Te4 O3 Te2 108.1(3) 2_666 1_565 ? Te3 O3 Te2 98.6(2) 2_665 1_565 ? Te5 O4 Pb4 124.7(5) . 2_566 ? Te5 O4 Pb5 133.3(5) . 2_566 ? Pb4 O4 Pb5 101.2(4) 2_566 2_566 ? Te5 O4 Te5 102.1(4) . 2_556 ? Pb4 O4 Te5 86.5(3) 2_566 2_556 ? Pb5 O4 Te5 87.9(3) 2_566 2_556 ? Te5 O4 Pb3 79.6(3) . 1_455 ? Pb4 O4 Pb3 73.0(2) 2_566 1_455 ? Pb5 O4 Pb3 109.1(3) 2_566 1_455 ? Te5 O4 Pb3 155.3(3) 2_556 1_455 ? Te5 O4 Te4 80.2(3) . . ? Pb4 O4 Te4 119.9(3) 2_566 . ? Pb5 O4 Te4 68.4(2) 2_566 . ? Te5 O4 Te4 146.7(3) 2_556 . ? Pb3 O4 Te4 58.03(15) 1_455 . ? Te5 O5 Pb4 116.5(5) . 1_545 ? Te5 O5 Pb4 135.1(5) . 2_666 ? Pb4 O5 Pb4 108.3(4) 1_545 2_666 ? Te5 O5 Te2 104.8(4) . . ? Pb4 O5 Te2 87.5(3) 1_545 . ? Pb4 O5 Te2 80.1(3) 2_666 . ? Te5 O5 Te2 126.3(4) . 2_656 ? Pb4 O5 Te2 67.2(2) 1_545 2_656 ? Pb4 O5 Te2 68.0(2) 2_666 2_656 ? Te2 O5 Te2 128.6(3) . 2_656 ? Te5 O5 Te5 72.8(3) . 2_556 ? Pb4 O5 Te5 66.4(2) 1_545 2_556 ? Pb4 O5 Te5 125.2(3) 2_666 2_556 ? Te2 O5 Te5 147.5(3) . 2_556 ? Te2 O5 Te5 59.86(16) 2_656 2_556 ? Te5 O5 Pb5 81.0(3) . 2_566 ? Pb4 O5 Pb5 113.9(3) 1_545 2_566 ? Pb4 O5 Pb5 77.7(2) 2_666 2_566 ? Te2 O5 Pb5 153.1(3) . 2_566 ? Te2 O5 Pb5 54.48(15) 2_656 2_566 ? Te5 O5 Pb5 59.42(15) 2_556 2_566 ? Te1 O6 Pb5 120.4(5) . . ? Te1 O6 Pb4 125.7(4) . . ? Pb5 O6 Pb4 108.6(4) . . ? Te1 O6 Pb2 80.4(3) . . ? Pb5 O6 Pb2 84.0(3) . . ? Pb4 O6 Pb2 129.0(4) . . ? Te1 O6 Te4 86.4(4) . . ? Pb5 O6 Te4 76.0(3) . . ? Pb4 O6 Te4 83.9(3) . . ? Pb2 O6 Te4 145.9(3) . . ? Te1 O6 Te2 86.3(3) . 1_565 ? Pb5 O6 Te2 136.3(4) . 1_565 ? Pb4 O6 Te2 72.7(2) . 1_565 ? Pb2 O6 Te2 65.90(18) . 1_565 ? Te4 O6 Te2 144.6(3) . 1_565 ? Te1 O6 Te5 141.9(5) . 1_565 ? Pb5 O6 Te5 77.0(3) . 1_565 ? Pb4 O6 Te5 68.0(2) . 1_565 ? Pb2 O6 Te5 67.37(19) . 1_565 ? Te4 O6 Te5 131.7(3) . 1_565 ? Te2 O6 Te5 62.79(17) 1_565 1_565 ? Te3 O7 Pb1 116.9(5) 2_565 . ? Te3 O7 Pb3 133.3(5) 2_565 1_455 ? Pb1 O7 Pb3 105.5(4) . 1_455 ? Te3 O7 Te3 108.6(4) 2_565 . ? Pb1 O7 Te3 88.1(3) . . ? Pb3 O7 Te3 90.6(3) 1_455 . ? Te3 O7 Pb5 76.1(3) 2_565 . ? Pb1 O7 Pb5 113.2(3) . . ? Pb3 O7 Pb5 69.7(2) 1_455 . ? Te3 O7 Pb5 153.8(3) . . ? Te3 O7 Te4 118.9(4) 2_565 . ? Pb1 O7 Te4 62.9(2) . . ? Pb3 O7 Te4 64.1(2) 1_455 . ? Te3 O7 Te4 131.5(3) . . ? Pb5 O7 Te4 55.72(14) . . ? Te4 O8 Pb3 114.7(5) . 2_666 ? Te4 O8 Pb4 141.2(6) . . ? Pb3 O8 Pb4 101.2(4) 2_666 . ? Te4 O8 Te4 108.9(4) . 2_666 ? Pb3 O8 Te4 92.3(3) 2_666 2_666 ? Pb4 O8 Te4 82.6(3) . 2_666 ? Te4 O8 Pb5 75.7(3) . . ? Pb3 O8 Pb5 118.7(3) 2_666 . ? Pb4 O8 Pb5 74.5(2) . . ? Te4 O8 Pb5 144.2(3) 2_666 . ? Te4 O8 Te4 68.5(3) . 2_566 ? Pb3 O8 Te4 67.6(2) 2_666 2_566 ? Pb4 O8 Te4 116.2(3) . 2_566 ? Te4 O8 Te4 154.1(4) 2_666 2_566 ? Pb5 O8 Te4 61.51(14) . 2_566 ? Te4 O8 Te1 73.6(4) . . ? Pb3 O8 Te1 169.7(4) 2_666 . ? Pb4 O8 Te1 69.3(2) . . ? Te4 O8 Te1 90.5(2) 2_666 . ? Pb5 O8 Te1 55.86(16) . . ? Te4 O8 Te1 112.3(3) 2_566 . ? Te4 O9 Pb5 126.9(5) . . ? Te4 O9 Pb3 121.1(5) . 1_455 ? Pb5 O9 Pb3 106.3(3) . 1_455 ? Te4 O9 Te4 104.9(4) . 2_566 ? Pb5 O9 Te4 101.7(4) . 2_566 ? Pb3 O9 Te4 84.9(3) 1_455 2_566 ? Te4 O9 Pb1 67.2(3) . . ? Pb5 O9 Pb1 111.9(3) . . ? Pb3 O9 Pb1 71.2(2) 1_455 . ? Te4 O9 Pb1 142.9(4) 2_566 . ? Te4 O9 Te1 72.8(3) . . ? Pb5 O9 Te1 63.4(2) . . ? Pb3 O9 Te1 119.5(3) 1_455 . ? Te4 O9 Te1 153.5(3) 2_566 . ? Pb1 O9 Te1 61.68(15) . . ? Te2 O10 Pb4 115.7(5) . 2_666 ? Te2 O10 Pb3 151.3(5) . . ? Pb4 O10 Pb3 92.9(3) 2_666 . ? Te2 O10 Te5 101.5(4) . 1_655 ? Pb4 O10 Te5 84.9(3) 2_666 1_655 ? Pb3 O10 Te5 83.0(3) . 1_655 ? Te2 O10 Pb1 83.8(3) . . ? Pb4 O10 Pb1 114.7(4) 2_666 . ? Pb3 O10 Pb1 81.4(3) . . ? Te5 O10 Pb1 155.4(4) 1_655 . ? Te2 O10 Te3 83.2(3) . 1_655 ? Pb4 O10 Te3 160.6(4) 2_666 1_655 ? Pb3 O10 Te3 68.6(2) . 1_655 ? Te5 O10 Te3 87.0(3) 1_655 1_655 ? Pb1 O10 Te3 69.67(19) . 1_655 ? Te3 O11 Pb5 136.8(6) . 2_565 ? Te3 O11 Te1 107.4(5) . 2_565 ? Pb5 O11 Te1 90.3(3) 2_565 2_565 ? Te3 O11 Pb2 123.6(5) . 2_565 ? Pb5 O11 Pb2 97.9(4) 2_565 2_565 ? Te1 O11 Pb2 79.1(3) 2_565 2_565 ? Te3 O11 Pb2 80.9(3) . 1_545 ? Pb5 O11 Pb2 103.7(4) 2_565 1_545 ? Te1 O11 Pb2 149.3(4) 2_565 1_545 ? Pb2 O11 Pb2 72.1(2) 2_565 1_545 ? Te2 O12 Pb1 120.6(5) . . ? Te2 O12 Pb2 124.1(5) . 1_545 ? Pb1 O12 Pb2 112.2(4) . 1_545 ? Te2 O12 Te5 105.2(5) . . ? Pb1 O12 Te5 86.6(3) . . ? Pb2 O12 Te5 94.6(3) 1_545 . ? Te2 O12 Pb2 70.4(3) . 2_665 ? Pb1 O12 Pb2 122.2(4) . 2_665 ? Pb2 O12 Pb2 66.9(2) 1_545 2_665 ? Te5 O12 Pb2 149.6(4) . 2_665 ? Te4 O13 Te1 128.3(5) . . ? Te4 O13 Pb1 111.1(5) . . ? Te1 O13 Pb1 106.7(4) . . ? Te4 O13 Pb3 121.3(4) . . ? Te1 O13 Pb3 86.0(3) . . ? Pb1 O13 Pb3 97.8(3) . . ? Te4 O13 Pb5 71.0(3) . . ? Te1 O13 Pb5 64.9(2) . . ? Pb1 O13 Pb5 107.2(3) . . ? Pb3 O13 Pb5 145.8(4) . . ? Te4 O13 Pb4 65.9(3) . 2_666 ? Te1 O13 Pb4 147.5(3) . 2_666 ? Pb1 O13 Pb4 90.2(3) . 2_666 ? Pb3 O13 Pb4 64.0(2) . 2_666 ? Pb5 O13 Pb4 136.9(3) . 2_666 ? Te3 O14 Pb1 124.4(5) . . ? Te3 O14 Pb2 112.7(5) . 1_545 ? Pb1 O14 Pb2 110.9(4) . 1_545 ? Te3 O14 Te1 122.0(5) . 2_665 ? Pb1 O14 Te1 95.9(3) . 2_665 ? Pb2 O14 Te1 82.8(3) 1_545 2_665 ? Te3 O14 Te3 71.6(3) . 2_565 ? Pb1 O14 Te3 63.3(2) . 2_565 ? Pb2 O14 Te3 174.1(4) 1_545 2_565 ? Te1 O14 Te3 98.5(3) 2_665 2_565 ? Te3 O14 Te5 101.9(4) . . ? Pb1 O14 Te5 62.9(2) . . ? Pb2 O14 Te5 70.6(2) 1_545 . ? Te1 O14 Te5 134.9(3) 2_665 . ? Te3 O14 Te5 104.8(3) 2_565 . ? Te2 O15 Pb2 114.9(5) . 2_665 ? Te2 O15 Te3 123.1(5) . 1_655 ? Pb2 O15 Te3 101.7(4) 2_665 1_655 ? Te2 O15 Pb2 141.7(6) . 1_645 ? Pb2 O15 Pb2 86.0(3) 2_665 1_645 ? Te3 O15 Pb2 79.2(3) 1_655 1_645 ? Te2 O15 Pb5 74.3(4) . 1_645 ? Pb2 O15 Pb5 93.2(3) 2_665 1_645 ? Te3 O15 Pb5 147.1(4) 1_655 1_645 ? Pb2 O15 Pb5 72.7(3) 1_645 1_645 ? Te2 O15 Te5 76.8(4) . 1_655 ? Pb2 O15 Te5 151.5(4) 2_665 1_655 ? Te3 O15 Te5 91.3(3) 1_655 1_655 ? Pb2 O15 Te5 71.5(2) 1_645 1_655 ? Pb5 O15 Te5 63.99(19) 1_645 1_655 ? _refine_diff_density_max 6.772 _refine_diff_density_min -3.220 _refine_diff_density_rms 0.811 _shelx_res_file ; TITL DLMR-203 dlmr-203.res created by SHELXL-2016/6 at 19:53:41 on 23-Jun-2021 CELL 0.71075 7.02558 10.63450 11.99646 78.51320 83.10420 84.08340 ZERR 1 0.00038 0.00060 0.00084 0.00550 0.00590 0.00590 LATT 1 SFAC O Te Pb UNIT 30 10 10 L.S. 10 omit 1 1 14 omit 1 1 0 CONN 15 3.0 PB1 CONN 15 3.0 PB2 CONN 15 3.0 PB3 CONN 15 3.0 PB4 CONN 15 3.0 PB5 CONN 15 3.0 TE1 CONN 15 3.0 TE2 CONN 15 3.0 TE3 CONN 15 3.0 TE4 CONN 15 3.0 TE5 FMAP 2 PLAN 8 ACTA SIZE 0.150 0.100 0.050 WGHT 0.072500 0.135300 FVAR 0.08105 PB1 3 0.341126 0.364419 0.146023 11.00000 0.01704 0.01781 = 0.02225 -0.00599 0.00220 -0.00334 PB2 3 0.235066 1.032651 0.050246 11.00000 0.01559 0.01948 = 0.02052 -0.00432 0.00217 -0.00200 PB3 3 0.802240 0.451921 0.285587 11.00000 0.01865 0.01934 = 0.01862 -0.00543 0.00015 -0.00333 PB4 3 0.397413 0.823796 0.485984 11.00000 0.01644 0.01755 = 0.01811 -0.00346 0.00045 -0.00248 PB5 3 -0.018029 0.780321 0.301915 11.00000 0.01582 0.01671 = 0.02204 -0.00512 0.00046 -0.00251 TE1 2 0.485526 0.726843 0.179703 11.00000 0.01529 0.01224 = 0.01627 -0.00539 -0.00191 -0.00126 TE2 2 0.634231 0.060572 0.241612 11.00000 0.01655 0.01708 = 0.01658 -0.00525 -0.00147 0.00033 TE3 2 -0.087014 0.332039 -0.007574 11.00000 0.01982 0.01549 = 0.01438 -0.00431 -0.00061 0.00005 TE4 2 0.254533 0.468798 0.432399 11.00000 0.01391 0.01380 = 0.01336 -0.00268 -0.00058 -0.00076 TE5 2 0.098621 0.119680 0.367334 11.00000 0.01453 0.01313 = 0.01666 -0.00475 -0.00090 -0.00220 O1 1 0.138735 0.295138 0.306816 11.00000 0.00587 0.01878 = 0.04023 -0.01600 -0.00163 0.00167 O2 1 0.542982 0.897044 0.102088 11.00000 0.02560 0.01401 = 0.02655 -0.00551 0.00048 0.00456 O3 1 0.698300 0.682701 0.263501 11.00000 0.02003 0.02574 = 0.02547 -0.00379 -0.00956 -0.00377 O4 1 -0.056506 0.150235 0.497880 11.00000 0.01677 0.02951 = 0.02241 0.00062 -0.00467 -0.00145 O5 1 0.326472 0.061151 0.436480 11.00000 0.02097 0.02249 = 0.02433 -0.00681 -0.00262 -0.00781 O6 1 0.314881 0.797334 0.291111 11.00000 0.02270 0.03400 = 0.01470 -0.00569 -0.00283 -0.00717 O7 1 0.051381 0.516542 0.110661 11.00000 0.01752 0.03089 = 0.02469 -0.01083 0.00021 -0.00162 O8 1 0.313950 0.589246 0.514441 11.00000 0.01605 0.01732 = 0.04610 -0.01366 0.00422 -0.00821 O9 1 0.027696 0.559665 0.376357 11.00000 0.01604 0.03696 = 0.01430 -0.01263 -0.00980 0.00041 O10 1 0.685578 0.199719 0.306611 11.00000 0.02675 0.04116 = 0.01197 -0.00531 -0.00981 -0.01233 O11 1 -0.105046 0.227789 -0.113207 11.00000 0.02355 0.04079 = 0.02186 -0.00938 -0.00198 -0.01553 O12 1 0.413501 0.136704 0.174805 11.00000 0.02979 0.02247 = 0.02669 -0.01736 -0.00949 0.00142 O13 1 0.411505 0.507153 0.295361 11.00000 0.02410 0.03441 = 0.01360 -0.00368 -0.00144 -0.00698 O14 1 0.166905 0.277275 0.022591 11.00000 0.02934 0.01155 = 0.03085 0.00126 -0.00543 -0.00027 O15 1 0.818797 0.084043 0.116041 11.00000 0.03561 0.04536 = 0.02202 -0.01896 0.00988 -0.01197 HKLF 4 REM DLMR-203 REM R1 = 0.0523 for 3416 Fo > 4sig(Fo) and 0.0592 for all 3973 data REM 226 parameters refined using 0 restraints END WGHT 0.0725 0.1353 REM Highest difference peak 6.772, deepest hole -3.220, 1-sigma level 0.811 Q1 1 0.1837 0.9573 0.0748 11.00000 0.05 6.77 Q2 1 -0.0486 0.7050 0.3234 11.00000 0.05 6.05 Q3 1 0.3161 0.2886 0.1631 11.00000 0.05 5.87 Q4 1 0.7938 0.3681 0.2835 11.00000 0.05 5.74 Q5 1 0.4324 0.8976 0.4784 11.00000 0.05 5.68 Q6 1 0.7566 0.3782 0.3067 11.00000 0.05 5.43 Q7 1 0.8524 0.5179 0.2633 11.00000 0.05 5.42 Q8 1 0.4236 0.4378 0.1016 11.00000 0.05 5.39 ; _shelx_res_checksum 34861 _shelx_hkl_file ; 0 0 2 6.01 0.64 0 0 -2 8.12 0.97 0 0 3 18.24 0.39 0 0 3 14.22 1.88 0 0 -3 12.59 1.24 0 0 4 354.03 7.80 0 0 4 260.36 12.42 0 0 -4 360.77 7.75 0 0 5 298.42 6.92 0 0 5 238.80 16.18 0 0 -5 304.66 6.80 0 0 6 201.96 14.49 0 0 6 226.42 5.44 0 0 7 208.71 5.79 0 0 7 220.56 17.00 0 0 8 1.96 2.22 0 0 8 0.48 0.34 0 0 9 312.99 22.27 0 0 10 4.02 3.36 0 0 11 1.48 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56.90 5.38 0 -6 9 118.23 12.34 0 -6 9 124.09 21.87 0 -6 9 10.84 11.15 0 6 -8 36.10 4.29 0 -6 8 73.01 8.60 0 -6 8 63.09 15.90 0 -6 8 1.13 7.55 0 6 -7 0.27 1.22 0 6 -7 1.10 1.63 0 -6 7 1.81 2.65 0 -6 7 12.24 3.52 0 -6 7 3.17 1.83 0 6 -6 461.59 30.83 0 6 -6 502.35 36.22 0 -6 6 610.19 44.58 0 -6 6 710.42 74.78 0 6 -5 4.87 1.73 0 6 -5 7.59 2.17 0 -6 5 8.42 2.84 0 -6 5 8.83 1.98 0 -6 5 8.67 3.65 0 6 -4 4.01 1.27 0 6 -4 6.67 1.69 0 -6 4 4.77 2.40 0 -6 4 6.01 1.65 0 6 -3 2.48 1.89 0 -6 3 6.09 1.57 0 -6 3 4.03 3.19 0 6 -2 1982.12 186.48 0 -6 2 2351.55 232.66 0 -6 2 2482.10 222.07 0 6 -1 21.46 2.61 0 -6 1 27.76 4.54 0 -6 1 29.07 4.21 0 6 0 46.86 3.71 0 -6 0 50.09 4.14 0 -6 0 54.50 4.98 0 6 1 27.84 4.51 0 -6 -1 35.91 4.61 0 -6 -1 29.86 3.22 0 6 2 81.70 7.64 0 -6 -2 69.86 4.50 0 -6 -2 65.46 6.88 0 6 3 227.79 9.51 0 6 3 167.82 9.43 0 -6 -3 135.44 7.59 0 -6 -3 137.74 6.73 0 6 4 387.21 14.63 0 6 4 350.96 22.46 0 -6 -4 274.48 14.22 0 -6 -4 278.45 17.83 0 6 5 3.01 0.85 0 6 5 2.64 2.30 0 -6 -5 1.82 1.09 0 -6 -5 2.46 0.94 0 6 6 71.43 7.37 0 6 6 69.53 2.86 0 -6 -6 50.77 4.86 0 -6 -6 49.34 3.79 0 6 7 3.13 1.55 0 6 7 2.61 1.04 0 6 7 2.29 0.90 0 -6 -7 1.71 1.51 0 6 8 42.86 4.53 0 6 8 64.72 7.61 0 6 8 64.99 3.08 0 -6 -8 42.67 4.29 0 6 9 142.04 9.87 0 6 9 219.84 13.21 0 6 9 225.23 10.29 0 -6 -9 186.17 13.00 0 6 10 39.04 6.86 0 6 10 23.03 3.07 0 6 10 35.48 3.93 0 -6 -10 28.55 5.22 0 6 11 122.33 7.37 0 6 11 71.85 6.21 0 6 11 119.50 13.28 0 6 12 108.05 6.64 0 6 12 191.61 11.75 0 6 12 189.94 17.87 0 6 13 80.07 10.95 0 6 13 75.57 6.74 0 6 13 33.74 4.47 0 6 14 222.60 26.70 0 -7 11 1.15 7.27 0 -7 11 -3.13 8.63 0 -7 11 5.03 3.17 0 -7 10 25.35 12.85 0 -7 10 37.87 10.08 0 -7 10 24.35 8.81 0 7 -9 195.49 18.56 0 -7 9 349.61 35.76 0 -7 9 320.26 35.31 0 -7 9 425.71 59.79 0 7 -8 32.77 6.46 0 -7 8 67.30 10.79 0 -7 8 93.83 19.48 0 -7 8 70.96 10.85 0 7 -7 60.29 7.58 0 7 -7 55.14 5.02 0 -7 7 54.52 11.29 0 -7 7 69.51 7.18 0 -7 7 101.84 14.19 0 7 -6 1.87 1.24 0 7 -6 2.25 2.37 0 -7 6 4.54 2.80 0 -7 6 9.46 5.85 0 -7 6 2.04 2.99 0 7 -5 335.82 21.71 0 7 -5 278.52 16.64 0 -7 5 429.61 35.76 0 -7 5 352.51 29.29 0 -7 5 340.08 38.89 0 7 -4 46.85 6.33 0 7 -4 70.41 6.22 0 -7 4 61.81 9.98 0 -7 4 62.61 6.04 0 7 -3 7.39 3.06 0 -7 3 15.32 2.75 0 -7 3 13.25 2.92 0 7 -2 39.47 5.53 0 -7 2 50.91 4.99 0 -7 2 41.07 7.37 0 7 -1 24.80 3.16 0 -7 1 35.03 5.63 0 -7 1 30.41 5.16 0 7 0 82.15 8.26 0 -7 0 85.25 9.58 0 -7 0 85.17 8.08 0 7 1 212.63 12.62 0 -7 -1 213.83 13.66 0 -7 -1 198.30 13.74 0 7 2 13.46 3.56 0 -7 -2 11.50 3.35 0 -7 -2 10.69 2.12 0 7 3 12.26 2.21 0 -7 -3 9.12 2.88 0 -7 -3 7.82 1.75 0 7 4 102.75 5.78 0 7 4 89.12 6.48 0 -7 -4 64.95 4.52 0 -7 -4 60.69 5.02 0 7 5 89.61 9.97 0 7 5 95.28 4.61 0 -7 -5 63.61 7.14 0 -7 -5 59.38 5.52 0 7 6 12.97 2.84 0 -7 -6 6.86 2.86 0 -7 -6 9.70 1.73 0 7 7 370.59 21.43 0 7 7 394.18 16.44 0 -7 -7 257.80 14.63 0 -7 -7 242.99 18.86 0 7 8 188.26 14.29 0 7 8 292.71 11.28 0 7 8 317.16 25.16 0 -7 -8 215.84 13.17 0 7 9 34.82 3.19 0 7 9 48.41 2.88 0 7 9 54.74 5.74 0 -7 -9 48.71 4.87 0 7 10 4.60 3.38 0 7 10 1.24 1.08 0 7 10 2.60 1.12 0 -7 -10 2.74 2.16 0 7 11 212.82 13.26 0 7 11 380.22 30.41 0 7 11 372.81 16.70 0 7 12 36.03 7.89 0 7 12 15.43 2.44 0 7 12 33.53 3.11 0 7 13 1.71 1.64 0 7 13 0.87 2.52 0 7 14 8.06 3.45 0 7 14 2.00 2.02 0 -8 10 -0.14 4.26 0 -8 10 -1.55 3.67 0 -8 10 3.56 3.21 0 8 -9 1.10 2.20 0 -8 9 1.51 4.03 0 -8 9 7.06 5.59 0 -8 9 1.97 7.28 0 8 -8 2.15 2.60 0 -8 8 5.44 4.85 0 -8 8 0.85 5.44 0 -8 8 4.91 2.72 0 8 -7 15.26 2.76 0 8 -7 14.87 4.94 0 -8 7 23.06 11.62 0 -8 7 11.41 6.28 0 -8 7 17.27 8.24 0 8 -6 77.06 6.89 0 8 -6 107.02 9.61 0 -8 6 158.43 29.76 0 -8 6 102.54 13.00 0 -8 6 121.11 15.70 0 8 -5 193.62 14.34 0 8 -5 137.66 14.24 0 -8 5 152.56 17.46 0 -8 5 191.68 21.10 0 -8 5 246.58 24.12 0 8 -4 8.54 2.67 0 8 -4 4.04 2.94 0 -8 4 6.86 2.58 0 -8 4 6.62 4.39 0 8 -3 7.30 2.32 0 -8 3 13.73 4.92 0 -8 3 15.84 3.19 0 8 -2 0.93 2.06 0 -8 2 1.92 1.65 0 -8 2 3.29 2.74 0 8 -1 8.29 3.69 0 -8 1 13.23 3.82 0 -8 1 12.13 2.85 0 8 0 40.44 4.20 0 -8 0 36.97 5.94 0 -8 0 40.97 4.95 0 8 1 103.62 10.82 0 -8 -1 95.12 8.26 0 -8 -1 84.22 8.42 0 8 2 14.70 4.19 0 -8 -2 10.62 2.58 0 -8 -2 12.56 4.01 0 8 3 16.08 3.02 0 -8 -3 9.41 2.40 0 -8 -3 14.47 3.78 0 8 4 2171.59 185.20 0 -8 -4 1705.49 137.06 0 -8 -4 1715.07 147.04 0 8 5 4.60 1.19 0 8 5 8.05 2.48 0 -8 -5 6.04 1.73 0 -8 -5 8.83 2.15 0 8 6 11.17 3.14 0 8 6 12.67 2.12 0 -8 -6 9.76 2.13 0 -8 -6 10.17 1.98 0 8 7 16.26 5.13 0 8 7 13.51 1.70 0 8 7 0.84 1.82 0 -8 -7 15.29 3.00 0 -8 -7 7.49 2.23 0 8 8 26.97 2.13 0 8 8 21.24 7.06 0 8 8 11.52 2.35 0 -8 -8 15.32 3.61 0 -8 -8 12.63 2.77 0 8 9 3.43 2.60 0 8 9 8.68 1.42 0 8 9 9.94 3.10 0 -8 -9 5.95 2.07 0 8 10 290.26 27.87 0 8 10 156.81 15.32 0 8 10 287.95 11.84 0 -8 -10 241.81 20.02 0 8 11 15.57 5.46 0 8 11 10.70 2.76 0 8 11 8.57 2.01 0 8 12 3.36 2.40 0 8 12 10.01 3.65 0 8 13 10.03 4.03 0 8 13 4.14 2.71 0 8 14 7.19 3.88 0 8 14 2.26 2.36 0 9 -9 12.39 5.58 0 -9 9 47.87 13.19 0 -9 9 13.83 9.98 0 -9 9 67.80 17.06 0 9 -8 0.21 2.72 0 9 -8 10.22 4.74 0 -9 8 36.30 7.85 0 -9 8 25.26 9.18 0 -9 8 19.41 4.71 0 9 -7 284.78 33.68 0 9 -7 217.75 24.46 0 -9 7 330.28 39.69 0 -9 7 439.01 67.13 0 -9 7 308.22 46.15 0 9 -6 13.29 3.73 0 9 -6 7.92 4.00 0 -9 6 16.80 6.75 0 -9 6 25.79 7.30 0 -9 6 13.03 8.02 0 9 -5 -2.02 2.17 0 9 -5 3.88 1.93 0 -9 5 0.62 3.68 0 -9 5 4.60 5.16 0 -9 5 -1.63 3.32 0 9 -4 2.73 2.50 0 9 -4 5.33 3.52 0 -9 4 0.13 2.32 0 -9 4 1.94 2.34 0 -9 4 1.63 3.48 0 9 -3 765.14 75.46 0 -9 3 1086.93 103.33 0 -9 3 946.24 99.44 0 9 -2 12.47 3.18 0 -9 2 24.96 5.95 0 9 -1 87.82 11.96 0 -9 1 109.49 14.98 0 -9 1 96.24 12.75 0 9 0 11.31 4.42 0 -9 0 10.85 4.07 0 -9 0 18.06 5.14 0 9 1 161.57 11.77 0 -9 -1 123.90 13.03 0 -9 -1 137.71 18.45 0 9 2 92.14 8.19 0 -9 -2 76.32 10.98 0 -9 -2 67.77 7.95 0 9 3 211.82 21.42 0 -9 -3 150.73 17.01 0 -9 -3 157.37 12.79 0 9 4 18.11 6.20 0 -9 -4 14.61 2.84 0 -9 -4 15.21 4.61 0 9 5 83.76 8.21 0 -9 -5 57.01 5.88 0 -9 -5 59.76 8.57 0 9 6 18.93 3.75 0 -9 -6 7.79 3.20 0 -9 -6 8.94 2.55 0 9 7 99.19 14.77 0 -9 -7 66.46 6.64 0 -9 -7 61.41 9.74 0 9 8 195.98 10.14 0 9 8 186.42 22.93 0 9 8 96.97 8.91 0 -9 -8 138.27 11.05 0 -9 -8 111.93 14.14 0 9 9 11.79 1.72 0 9 9 9.38 3.47 0 9 9 18.86 4.09 0 -9 -9 5.14 2.54 0 9 10 84.41 10.19 0 9 10 100.13 6.50 0 9 10 158.25 19.10 0 9 11 78.62 7.41 0 9 11 156.54 19.35 0 9 12 46.27 6.95 0 9 12 19.08 3.25 0 9 13 271.38 21.64 0 9 13 99.87 10.60 0 10 -8 18.97 9.74 0 -10 8 72.55 14.87 0 -10 8 52.23 10.80 0 -10 8 43.83 9.17 0 10 -7 4.74 4.64 0 10 -7 4.15 3.44 0 -10 7 9.45 9.40 0 -10 7 4.93 5.83 0 -10 7 5.34 4.39 0 10 -6 131.99 18.46 0 10 -6 215.60 29.76 0 -10 6 249.11 34.04 0 -10 6 198.40 25.31 0 -10 6 296.80 36.89 0 10 -5 6.43 5.09 0 10 -5 5.37 3.33 0 -10 5 1.26 8.68 0 -10 5 6.71 3.69 0 -10 5 12.51 6.01 0 10 -4 32.37 8.51 0 10 -4 19.04 5.88 0 -10 4 5.55 7.90 0 -10 4 22.84 7.96 0 -10 4 26.77 7.53 0 10 -3 35.22 7.82 0 -10 3 34.11 6.81 0 -10 3 43.41 10.42 0 10 -2 21.53 6.03 0 -10 2 19.55 7.46 0 -10 2 23.00 5.13 0 10 -1 106.36 9.96 0 -10 1 96.58 10.57 0 -10 1 113.85 12.13 0 10 0 174.38 14.37 0 -10 0 131.00 17.50 0 -10 0 164.18 15.79 0 10 1 1.98 2.82 0 -10 -1 2.38 3.00 0 -10 -1 0.44 2.16 0 10 2 -0.23 2.92 0 -10 -2 2.43 1.94 0 -10 -2 0.49 2.84 0 10 3 38.52 8.93 0 -10 -3 34.19 5.17 0 -10 -3 25.76 7.50 0 10 4 15.40 5.83 0 -10 -4 11.45 4.73 0 -10 -4 10.22 1.95 0 10 5 7.02 4.51 0 -10 -5 3.96 3.23 0 -10 -5 2.78 2.21 0 10 6 186.00 16.79 0 -10 -6 133.46 17.09 0 -10 -6 138.35 12.45 0 10 7 198.41 17.87 0 -10 -7 151.89 15.64 0 -10 -7 140.64 18.29 0 10 8 74.52 12.89 0 10 8 37.09 5.29 0 -10 -8 42.35 5.95 0 -10 -8 32.23 9.37 0 10 9 2.98 2.99 0 10 9 2.50 2.77 0 10 10 240.59 21.29 0 10 10 449.89 46.61 0 10 11 3.06 6.47 0 10 11 5.20 2.12 0 10 12 1.78 3.72 0 10 12 2.39 2.50 0 11 -6 78.79 15.04 0 11 -6 131.48 25.08 0 -11 6 194.89 42.65 0 -11 6 122.00 28.63 0 -11 6 153.51 26.63 0 11 -5 0.82 2.78 0 11 -5 1.76 4.13 0 -11 5 0.22 2.98 0 -11 5 4.21 4.66 0 -11 5 2.75 3.15 0 11 -4 8.32 6.23 0 11 -4 5.12 4.29 0 -11 4 9.23 4.27 0 -11 4 9.68 9.94 0 -11 4 10.43 6.51 0 11 -3 13.13 5.30 0 11 -3 20.56 5.42 0 -11 3 19.05 7.15 0 -11 3 0.87 7.36 0 -11 3 17.99 5.10 0 11 -2 4.71 3.78 0 -11 2 3.45 2.98 0 -11 2 5.00 3.17 0 11 -1 38.18 8.07 0 -11 1 13.83 7.62 0 -11 1 31.98 9.67 0 11 0 60.40 11.02 0 -11 0 40.98 12.71 0 -11 0 40.64 9.57 0 11 1 20.98 6.43 0 -11 -1 17.68 5.10 0 -11 -1 11.98 4.44 0 11 2 2.42 3.75 0 -11 -2 0.64 2.48 0 -11 -2 3.25 2.28 0 11 3 1064.73 101.63 0 -11 -3 724.08 67.41 0 -11 -3 711.51 64.60 0 11 4 3.65 4.40 0 -11 -4 2.46 2.44 0 -11 -4 3.61 2.35 0 11 5 26.23 8.07 0 -11 -5 12.65 4.59 0 -11 -5 24.74 6.27 0 11 6 1.68 3.73 0 -11 -6 -0.07 1.89 0 -11 -6 1.58 2.64 0 11 7 1.99 1.64 0 11 7 -0.08 2.50 0 -11 -7 -0.38 1.75 0 -11 -7 2.41 2.89 0 11 8 2.16 2.30 0 11 8 6.71 5.53 0 -11 -8 6.02 3.91 0 11 9 159.91 17.86 0 11 9 96.25 16.00 0 -11 -9 106.63 11.53 0 11 10 2.32 2.16 0 11 10 3.83 5.63 0 11 11 3.47 4.09 0 11 11 12.72 4.96 0 12 -4 359.13 38.32 0 12 -4 207.87 32.80 0 -12 4 369.36 53.13 0 -12 4 280.91 50.33 0 -12 4 521.78 59.18 0 12 -3 20.37 11.17 0 12 -3 17.29 7.14 0 -12 3 18.98 6.59 0 -12 3 12.75 15.49 0 -12 3 31.18 6.79 0 12 -2 143.71 19.03 0 12 -2 89.20 11.87 0 -12 2 173.18 22.41 0 -12 2 91.63 20.61 0 -12 2 142.98 23.95 0 12 -1 7.60 5.77 0 -12 1 16.25 4.94 0 -12 1 8.70 3.85 0 12 0 192.37 26.01 0 -12 0 136.14 22.88 0 -12 0 187.75 19.17 0 12 1 31.09 5.80 0 -12 -1 17.09 7.13 0 -12 -1 25.05 9.09 0 12 2 124.21 12.66 0 -12 -2 103.98 18.99 0 -12 -2 69.43 14.69 0 12 3 57.39 8.91 0 -12 -3 50.48 8.28 0 -12 -3 48.19 9.56 0 12 4 51.70 7.62 0 -12 -4 16.54 6.84 0 -12 -4 36.88 6.42 0 12 5 82.59 15.64 0 -12 -5 49.16 12.12 0 -12 -5 54.73 6.58 0 12 6 69.78 16.29 0 -12 -6 54.24 9.25 0 -12 -6 57.89 12.44 0 12 7 78.18 12.08 0 12 7 46.84 7.91 0 -12 -7 60.87 13.06 0 12 8 1.71 5.21 0 12 8 2.03 2.16 0 -12 -8 1.43 2.49 0 12 9 73.58 11.99 0 12 9 39.71 11.55 0 -12 -9 49.77 8.20 0 13 -2 86.41 12.77 0 13 -2 134.01 29.36 0 -13 2 177.63 36.57 0 -13 2 116.53 17.76 0 13 -1 126.25 21.72 0 13 -1 168.42 21.39 0 -13 1 120.61 25.49 0 -13 1 100.73 22.31 0 -13 1 190.77 35.76 0 13 0 13.30 7.19 0 -13 0 19.59 6.58 0 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5 1 252.55 10.90 -2 5 1 215.09 8.85 2 -5 0 21.42 2.09 2 -5 0 24.04 2.29 -2 5 0 24.30 2.63 -2 5 0 19.06 2.65 -2 5 0 29.90 3.79 2 -5 1 23.71 3.58 2 -5 1 24.08 2.36 -2 5 -1 31.24 4.05 -2 5 -1 24.10 2.53 -2 5 -1 13.56 2.27 2 -5 2 25.07 2.72 2 -5 2 27.59 4.29 -2 5 -2 26.17 2.53 -2 5 -2 16.00 2.19 -2 5 -2 39.24 5.19 2 -5 3 9.10 1.88 2 -5 3 10.01 3.01 -2 5 -3 9.87 1.65 -2 5 -3 9.04 1.46 2 -5 4 43.50 4.58 2 -5 4 40.85 4.06 -2 5 -4 46.56 2.94 -2 5 -4 43.24 2.25 2 -5 5 111.29 12.83 2 -5 5 101.36 7.58 -2 5 -5 109.95 5.77 -2 5 -5 107.83 5.84 2 -5 6 1.61 1.83 2 -5 6 3.40 2.06 -2 5 -6 4.66 1.04 2 -5 7 40.31 5.36 2 -5 7 41.41 8.41 -2 5 -7 38.96 2.62 2 -5 8 94.52 14.90 2 -5 8 110.38 10.06 -2 5 -8 81.78 7.29 -2 5 -8 87.83 5.38 2 -5 9 584.39 41.88 2 -5 9 498.88 50.69 -2 5 -9 400.15 18.49 -2 5 -9 360.18 21.47 2 -5 10 -5.42 3.56 2 -5 10 0.78 1.47 2 -5 10 5.43 3.25 2 -5 11 15.25 7.66 2 -5 11 20.32 7.84 2 -5 11 17.99 3.42 2 -5 12 4.06 3.88 2 -5 12 6.63 8.12 2 -5 12 3.03 5.44 -2 4 14 239.14 26.08 -2 4 14 226.34 27.57 2 -4 -13 85.58 24.49 -2 4 13 133.91 10.50 -2 4 13 132.76 14.79 -2 4 13 67.56 7.95 2 -4 -12 107.36 22.44 -2 4 12 92.55 7.77 -2 4 12 144.50 14.41 -2 4 12 140.11 10.95 2 -4 -11 68.17 15.79 -2 4 11 90.16 9.94 -2 4 11 63.55 5.70 -2 4 11 103.81 10.66 2 -4 -10 10.84 6.83 -2 4 10 22.82 2.80 -2 4 10 29.15 5.14 -2 4 10 22.45 5.15 2 -4 -9 103.96 11.69 -2 4 9 124.69 7.56 -2 4 9 152.36 12.09 -2 4 9 166.39 12.49 2 -4 -8 20.30 5.72 -2 4 8 32.72 4.71 -2 4 8 26.41 4.39 -2 4 8 27.78 2.89 2 -4 -7 102.53 11.77 -2 4 7 133.02 8.90 -2 4 7 135.25 9.17 -2 4 7 104.39 4.68 2 -4 -6 40.77 6.11 -2 4 6 50.69 3.07 -2 4 6 57.39 5.02 -2 4 6 42.99 3.62 2 -4 -5 21.36 2.66 -2 4 5 33.05 3.32 -2 4 5 25.45 2.55 -2 4 5 28.95 2.97 2 -4 -4 316.38 15.99 -2 4 4 398.29 15.86 -2 4 4 401.30 17.66 -2 4 4 357.31 13.73 2 -4 -3 160.95 7.79 -2 4 3 189.97 9.43 -2 4 3 183.00 8.36 -2 4 3 161.57 7.85 2 -4 -2 1.66 0.79 2 -4 -2 2.48 0.98 -2 4 2 2.68 1.29 -2 4 2 3.34 0.71 -2 4 2 2.13 0.70 2 -4 -1 15.24 1.53 2 -4 -1 11.15 1.29 -2 4 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13 5.70 7.29 2 -4 13 3.86 4.88 -2 3 14 92.28 9.72 -2 3 14 97.82 10.84 2 -3 -13 4.15 5.35 -2 3 13 3.08 3.11 -2 3 13 1.09 1.48 -2 3 13 1.04 3.54 2 -3 -12 41.78 9.97 -2 3 12 39.81 4.43 -2 3 12 55.88 9.21 -2 3 12 50.00 7.47 2 -3 -11 196.20 23.78 -2 3 11 281.92 23.51 -2 3 11 283.05 15.29 -2 3 11 198.97 12.85 2 -3 -10 3.82 2.40 -2 3 10 1.40 0.77 -2 3 10 1.35 2.56 2 -3 -9 248.37 22.48 -2 3 9 376.98 17.80 -2 3 9 375.15 20.95 -2 3 9 316.56 15.73 2 -3 -8 31.78 8.85 -2 3 8 49.40 3.51 -2 3 8 63.26 6.50 -2 3 8 57.38 3.55 2 -3 -7 0.53 2.70 2 -3 -7 4.47 0.89 -2 3 7 4.76 1.11 -2 3 7 3.12 1.39 -2 3 7 3.16 1.27 2 -3 -6 237.26 15.23 2 -3 -6 286.64 10.86 -2 3 6 299.97 11.38 -2 3 6 325.13 18.04 -2 3 6 273.96 12.06 2 -3 -5 2584.50 227.32 2 -3 -5 2797.28 208.12 -2 3 5 3117.89 227.66 -2 3 5 3030.69 236.39 -2 3 5 2579.14 183.89 2 -3 -4 173.10 7.52 2 -3 -4 131.37 9.75 -2 3 4 147.93 6.50 -2 3 4 159.05 8.89 -2 3 4 168.27 5.54 2 -3 -3 29.34 2.28 2 -3 -3 27.08 3.05 -2 3 3 26.42 1.81 -2 3 3 24.57 2.06 -2 3 3 27.57 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28.40 4.39 2 4 11 20.70 2.35 2 4 11 12.79 1.41 2 4 11 7.79 1.86 2 4 11 20.74 3.71 2 4 12 243.58 13.09 2 4 12 181.71 11.35 2 4 12 107.78 6.17 2 4 12 124.38 4.93 2 4 12 231.63 14.22 2 4 13 93.56 9.84 2 4 13 104.20 8.15 2 4 13 73.00 7.62 2 4 14 -0.93 1.73 2 4 14 0.81 1.58 2 4 14 0.74 2.22 2 4 15 26.67 5.04 -2 -5 12 28.10 9.80 -2 -5 12 24.79 13.64 -2 -5 11 2.02 4.37 -2 -5 11 4.84 6.12 2 5 -10 189.85 14.52 -2 -5 10 384.08 35.93 -2 -5 10 389.27 34.41 2 5 -9 2.02 1.35 -2 -5 9 3.47 4.97 -2 -5 9 1.88 3.71 2 5 -8 79.63 6.92 -2 -5 8 156.19 22.88 -2 -5 8 138.34 10.38 2 5 -7 66.51 4.36 -2 -5 7 119.22 12.59 -2 -5 7 104.40 8.16 2 5 -6 4.30 1.44 2 5 -6 3.00 1.73 -2 -5 6 5.00 3.20 -2 -5 6 7.27 3.33 2 5 -5 581.87 37.79 2 5 -5 590.33 40.35 -2 -5 5 832.50 72.68 -2 -5 5 834.05 49.10 2 5 -4 7.57 2.31 2 5 -4 7.58 1.66 -2 -5 4 11.30 4.57 -2 -5 4 17.46 3.64 2 5 -3 9.79 1.57 2 5 -3 8.39 1.62 -2 -5 3 10.14 4.02 -2 -5 3 13.79 3.41 2 5 -2 62.38 4.46 2 5 -2 58.85 6.25 -2 -5 2 73.55 6.01 -2 -5 2 72.67 7.60 2 5 -1 2638.19 256.03 2 5 -1 2864.26 294.34 -2 -5 1 3284.72 342.89 -2 -5 1 3309.46 330.83 2 5 0 36.99 5.06 2 5 0 35.03 4.84 -2 -5 0 43.60 5.06 -2 -5 0 38.10 3.70 2 5 1 24.78 3.00 2 5 1 24.25 3.84 -2 -5 -1 25.53 2.83 -2 -5 -1 28.59 3.34 2 5 2 84.88 5.30 2 5 2 82.67 8.19 -2 -5 -2 78.97 4.56 -2 -5 -2 70.93 7.69 2 5 3 65.94 4.72 2 5 3 67.81 6.67 -2 -5 -3 54.23 6.50 -2 -5 -3 56.75 3.08 2 5 4 170.63 10.14 2 5 4 214.54 14.28 -2 -5 -4 168.90 12.45 2 5 5 129.38 10.04 2 5 5 102.28 6.51 -2 -5 -5 99.67 5.59 2 5 6 88.18 5.45 2 5 6 53.35 4.44 -2 -5 -6 56.66 5.63 2 5 7 68.19 7.41 2 5 7 50.36 4.16 -2 -5 -7 56.35 3.74 2 5 8 9.84 2.78 2 5 8 14.99 3.70 2 5 9 8.42 2.12 2 5 9 4.73 2.28 2 5 10 39.18 5.40 2 5 10 89.78 8.85 2 5 10 64.23 2.12 2 5 10 75.12 2.47 2 5 11 33.45 4.83 2 5 11 52.17 2.67 2 5 11 73.21 8.20 2 5 11 40.57 3.45 2 5 11 69.76 3.07 2 5 12 67.72 5.39 2 5 12 32.06 2.87 2 5 12 53.40 4.17 2 5 12 14.03 3.85 2 5 12 36.40 3.67 2 5 13 129.46 9.22 2 5 13 116.27 6.58 2 5 13 49.62 5.92 2 5 14 66.16 7.75 2 5 15 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8.28 4.46 -4 -6 4 8.13 3.17 4 6 -3 602.84 60.86 4 6 -3 390.33 26.06 4 6 -3 377.95 25.11 -4 -6 3 524.83 51.35 -4 -6 3 517.89 44.97 -4 -6 3 608.19 52.26 4 6 -2 2.52 1.51 4 6 -2 4.16 4.54 4 6 -2 2.92 2.41 -4 -6 2 4.04 3.98 -4 -6 2 3.06 2.06 -4 -6 2 3.31 3.25 4 6 -1 35.61 5.37 4 6 -1 18.51 2.95 4 6 -1 16.87 3.20 -4 -6 1 33.44 7.45 -4 -6 1 21.32 5.92 -4 -6 1 28.36 4.12 4 6 0 19.09 5.48 4 6 0 7.58 3.40 4 6 0 9.67 3.63 -4 -6 0 15.82 2.97 -4 -6 0 9.95 2.86 -4 -6 0 19.75 3.75 4 6 1 69.08 8.30 4 6 1 30.42 5.66 4 6 1 38.21 4.32 -4 -6 -1 49.97 7.68 -4 -6 -1 55.81 6.70 -4 -6 -1 21.59 5.63 4 6 2 384.46 25.64 4 6 2 219.56 15.20 4 6 2 250.24 20.72 -4 -6 -2 227.81 22.67 -4 -6 -2 206.61 17.03 4 6 3 76.43 6.55 4 6 3 40.39 6.86 4 6 3 49.51 4.48 -4 -6 -3 44.15 5.09 -4 -6 -3 36.59 4.02 4 6 4 0.08 1.76 4 6 4 1.13 1.75 4 6 4 1.20 1.14 -4 -6 -4 -0.57 1.82 -4 -6 -4 0.15 1.00 4 6 5 118.02 10.03 4 6 5 71.74 9.50 -4 -6 -5 69.07 6.18 -4 -6 -5 61.31 2.97 4 6 6 1759.01 151.08 4 6 6 1326.43 123.23 -4 -6 -6 1210.48 111.03 4 6 7 106.19 11.88 4 6 7 72.59 9.03 -4 -6 -7 70.25 5.90 4 6 8 6.76 3.43 4 6 8 4.44 2.55 -4 -6 -8 4.09 2.51 4 6 9 17.43 3.93 4 6 9 20.95 3.77 -4 -6 -9 15.30 3.78 4 6 10 18.26 5.09 4 6 10 5.59 2.84 4 6 11 33.35 5.40 4 6 11 21.50 4.31 4 6 12 145.72 18.93 4 6 12 72.69 8.85 4 6 13 113.28 18.06 4 6 14 5.75 3.59 4 7 -9 0.05 1.27 -4 -7 9 0.41 3.81 -4 -7 9 2.08 3.15 4 7 -8 30.36 4.62 -4 -7 8 66.65 11.82 -4 -7 8 62.85 10.57 4 7 -7 37.79 7.80 -4 -7 7 66.34 11.81 4 7 -6 4.82 2.36 4 7 -6 4.52 3.40 -4 -7 6 10.41 4.52 4 7 -5 454.62 43.49 4 7 -5 503.74 46.25 -4 -7 5 850.45 87.72 -4 -7 5 735.53 56.00 4 7 -4 6.01 3.43 4 7 -4 7.26 2.25 -4 -7 4 9.76 4.11 -4 -7 4 6.31 5.44 4 7 -3 -0.12 2.25 4 7 -3 0.84 2.36 -4 -7 3 3.26 2.35 -4 -7 3 0.59 3.33 4 7 -2 76.04 10.99 4 7 -2 85.03 7.71 -4 -7 2 105.46 16.57 -4 -7 2 112.57 10.65 4 7 -1 769.82 71.27 4 7 -1 697.41 63.97 -4 -7 1 988.93 74.30 -4 -7 1 928.19 89.64 4 7 0 20.35 3.77 4 7 0 19.25 5.23 -4 -7 0 33.08 7.36 -4 -7 0 24.99 3.99 4 7 1 53.17 9.07 4 7 1 59.18 8.95 -4 -7 -1 57.48 7.34 -4 -7 -1 60.71 5.98 4 7 2 168.56 19.39 4 7 2 213.36 19.72 -4 -7 -2 200.73 15.74 -4 -7 -2 150.34 14.97 4 7 3 100.07 9.46 4 7 3 133.59 13.25 -4 -7 -3 107.67 14.69 -4 -7 -3 92.40 7.94 4 7 4 235.36 17.60 4 7 4 291.50 18.47 -4 -7 -4 213.49 23.29 -4 -7 -4 189.48 11.52 4 7 5 70.08 6.14 4 7 5 63.25 8.49 -4 -7 -5 45.03 5.62 -4 -7 -5 37.12 2.43 4 7 6 15.25 3.19 4 7 6 10.04 4.15 -4 -7 -6 7.46 4.02 4 7 7 121.30 14.94 4 7 7 87.36 8.20 -4 -7 -7 69.85 10.82 4 7 8 13.59 4.60 4 7 8 4.51 2.30 -4 -7 -8 7.10 2.13 4 7 9 56.40 10.29 4 7 9 35.58 7.45 -4 -7 -9 40.93 4.93 4 7 10 36.53 8.32 4 7 10 16.99 5.24 4 7 11 42.96 11.30 4 7 11 33.11 4.70 4 7 12 31.98 8.92 4 7 12 13.73 4.63 4 7 13 122.06 12.08 4 7 13 23.83 8.56 4 8 -8 10.15 5.11 -4 -8 8 20.27 8.17 -4 -8 8 23.06 6.93 4 8 -7 8.64 4.23 -4 -8 7 13.86 10.44 -4 -8 7 20.40 8.77 4 8 -6 1.34 2.09 4 8 -6 2.53 1.88 -4 -8 6 0.81 6.02 -4 -8 6 7.28 5.54 4 8 -5 74.87 8.68 4 8 -5 83.41 9.34 -4 -8 5 148.07 22.72 -4 -8 5 122.77 14.35 4 8 -4 257.09 29.37 4 8 -4 223.12 27.72 -4 -8 4 442.34 51.64 -4 -8 4 348.97 43.02 4 8 -3 42.88 8.13 4 8 -3 34.80 5.36 -4 -8 3 68.38 12.57 -4 -8 3 37.07 7.90 4 8 -2 1.72 3.15 4 8 -2 5.33 3.04 -4 -8 2 0.93 4.37 -4 -8 2 1.34 4.19 4 8 -1 1.78 2.78 4 8 -1 0.32 1.84 -4 -8 1 3.35 2.13 -4 -8 1 -0.41 3.85 4 8 0 77.12 12.64 4 8 0 79.21 13.71 -4 -8 0 113.45 16.84 -4 -8 0 94.68 13.25 4 8 1 57.09 7.46 4 8 1 67.85 10.46 -4 -8 -1 59.26 12.77 -4 -8 -1 56.88 9.41 4 8 2 62.22 7.31 4 8 2 72.35 11.04 -4 -8 -2 56.46 12.81 -4 -8 -2 61.66 9.07 4 8 3 64.80 11.25 4 8 3 82.12 10.99 -4 -8 -3 55.33 12.90 -4 -8 -3 59.48 6.72 4 8 4 9.63 4.23 4 8 4 9.50 4.03 -4 -8 -4 11.03 4.29 -4 -8 -4 3.67 2.03 4 8 5 22.60 6.40 4 8 5 27.54 6.28 -4 -8 -5 13.13 4.09 4 8 6 17.80 5.78 4 8 6 17.71 5.56 -4 -8 -6 9.23 3.36 4 8 7 12.92 5.28 4 8 7 10.71 4.69 -4 -8 -7 5.22 4.14 4 8 8 -0.66 1.81 4 8 8 0.64 2.25 -4 -8 -8 0.34 2.04 4 8 9 287.38 32.82 4 8 9 215.03 24.83 -4 -8 -9 196.66 23.08 4 8 10 7.50 3.72 4 8 10 9.48 2.65 -4 -8 -10 7.46 3.88 4 8 11 58.19 12.58 4 8 11 29.68 8.28 4 8 12 425.91 36.10 4 8 12 200.37 29.38 4 8 13 5.96 5.28 4 8 13 0.08 2.90 4 9 -7 -2.47 2.39 4 9 -7 3.07 2.93 -4 -9 7 9.43 6.40 -4 -9 7 2.40 3.59 4 9 -6 -0.55 3.11 4 9 -6 3.26 2.12 -4 -9 6 5.36 5.95 -4 -9 6 -2.42 5.60 4 9 -5 2.17 3.26 4 9 -5 4.18 2.11 -4 -9 5 1.21 6.22 -4 -9 5 1.34 3.90 4 9 -4 241.31 23.23 4 9 -4 285.35 25.05 -4 -9 4 465.21 56.76 -4 -9 4 402.11 52.04 4 9 -3 5.38 3.82 4 9 -3 2.17 3.64 -4 -9 3 6.73 3.97 -4 -9 3 7.02 5.95 4 9 -2 10.84 3.34 4 9 -2 12.59 5.04 -4 -9 2 14.13 7.48 -4 -9 2 8.13 7.05 4 9 -1 9.24 5.15 4 9 -1 15.25 5.70 -4 -9 1 14.14 6.65 -4 -9 1 13.49 5.00 4 9 0 6.76 4.25 4 9 0 5.89 3.10 -4 -9 0 7.78 3.08 -4 -9 0 6.95 3.71 4 9 1 267.32 29.99 4 9 1 261.46 23.14 -4 -9 -1 282.94 27.43 -4 -9 -1 307.35 30.44 4 9 2 39.19 11.32 4 9 2 58.34 10.41 -4 -9 -2 38.90 12.63 -4 -9 -2 54.79 8.47 4 9 3 9.04 4.16 4 9 3 10.83 4.06 -4 -9 -3 -1.39 4.66 -4 -9 -3 1.37 2.23 4 9 4 47.44 6.59 4 9 4 57.11 9.78 -4 -9 -4 22.69 9.61 -4 -9 -4 21.62 4.84 -4 -9 -4 45.74 4.65 4 9 5 963.95 81.51 4 9 5 1051.80 83.95 -4 -9 -5 702.38 68.82 4 9 6 83.45 10.04 4 9 6 80.03 9.31 -4 -9 -6 50.74 8.19 4 9 7 45.73 10.93 4 9 7 39.09 6.36 -4 -9 -7 26.59 5.76 4 9 8 36.02 9.45 4 9 8 26.30 5.61 -4 -9 -8 23.27 4.79 4 9 9 1.92 3.79 4 9 9 5.01 3.04 -4 -9 -9 2.14 2.26 4 9 10 36.24 11.70 4 9 10 40.80 9.46 -4 -9 -10 33.99 8.88 4 9 11 163.26 17.73 4 9 11 122.93 18.31 4 9 12 29.50 10.87 4 9 12 18.37 7.39 4 10 -6 318.56 43.04 4 10 -6 279.45 41.20 -4 -10 6 639.70 84.00 -4 -10 6 495.90 73.54 4 10 -5 -4.90 2.34 4 10 -5 -0.69 3.76 -4 -10 5 -0.86 6.82 -4 -10 5 0.77 6.90 4 10 -4 0.27 2.09 4 10 -4 2.34 2.01 -4 -10 4 3.59 3.60 -4 -10 4 -1.12 3.47 4 10 -3 29.19 8.02 4 10 -3 16.69 5.12 -4 -10 3 29.13 13.00 -4 -10 3 32.59 11.39 4 10 -2 275.30 38.50 4 10 -2 317.91 29.54 -4 -10 2 426.94 43.39 -4 -10 2 485.84 55.53 4 10 -1 -0.16 2.93 4 10 -1 -0.85 3.32 -4 -10 1 0.88 4.35 -4 -10 1 -1.41 3.56 4 10 0 56.77 12.18 4 10 0 58.40 9.07 -4 -10 0 77.03 14.45 -4 -10 0 84.85 17.41 4 10 1 157.63 23.50 4 10 1 163.77 24.22 -4 -10 -1 209.18 26.12 -4 -10 -1 204.07 31.80 4 10 2 253.83 32.23 4 10 2 256.70 22.09 -4 -10 -2 247.76 26.57 -4 -10 -2 254.13 27.81 4 10 3 199.90 18.22 4 10 3 228.23 18.68 -4 -10 -3 182.03 21.27 -4 -10 -3 164.41 18.36 -4 -10 -3 167.81 18.76 4 10 4 63.50 7.63 4 10 4 73.54 7.75 -4 -10 -4 53.27 8.12 -4 -10 -4 22.77 6.75 -4 -10 -4 38.84 4.96 4 10 5 2.73 3.34 4 10 5 -0.11 3.39 -4 -10 -5 0.81 0.59 -4 -10 -5 2.33 2.25 -4 -10 -5 0.49 0.82 4 10 6 147.46 21.17 4 10 6 126.61 19.90 -4 -10 -6 93.08 13.32 4 10 7 57.64 8.54 4 10 7 44.99 11.58 -4 -10 -7 33.47 7.21 4 10 8 81.11 17.48 4 10 8 86.89 15.95 -4 -10 -8 58.10 9.06 4 10 9 24.66 8.13 4 10 9 13.21 4.65 -4 -10 -9 10.51 4.09 4 10 10 26.95 6.44 4 10 10 16.40 5.10 -4 -10 -10 16.29 4.60 4 10 11 39.25 12.56 4 10 11 22.21 9.37 -4 -10 -11 22.96 5.47 4 11 -4 6.82 3.04 4 11 -4 4.36 4.93 -4 -11 4 3.04 5.49 -4 -11 4 5.21 4.94 4 11 -3 9.70 4.25 4 11 -3 4.68 5.88 -4 -11 3 7.52 10.38 -4 -11 3 16.38 5.70 4 11 -2 0.45 4.26 4 11 -2 7.09 4.21 -4 -11 2 4.27 4.04 -4 -11 2 -2.18 5.37 4 11 -1 61.12 15.77 4 11 -1 76.46 17.05 -4 -11 1 98.02 23.10 -4 -11 1 107.34 19.60 4 11 0 33.96 11.12 4 11 0 41.78 7.92 -4 -11 0 53.91 13.20 -4 -11 0 44.99 10.53 4 11 1 61.87 9.13 4 11 1 61.07 14.94 -4 -11 -1 65.37 14.65 -4 -11 -1 86.11 18.07 -4 -11 -1 68.75 8.84 4 11 2 94.27 11.75 4 11 2 88.88 11.29 -4 -11 -2 84.35 13.59 -4 -11 -2 80.93 21.50 -4 -11 -2 78.65 14.33 4 11 3 5.87 2.76 4 11 3 1.49 4.13 -4 -11 -3 -1.05 4.95 -4 -11 -3 0.78 2.78 -4 -11 -3 0.20 2.15 4 11 4 20.09 8.76 4 11 4 30.47 8.59 -4 -11 -4 13.18 6.05 4 11 5 1.29 4.63 4 11 5 4.98 4.38 -4 -11 -5 1.36 2.96 4 11 6 4.44 5.96 4 11 6 9.76 3.96 -4 -11 -6 5.55 3.71 4 11 7 2.69 4.59 4 11 7 4.48 4.22 -4 -11 -7 -0.39 2.55 4 11 8 239.47 35.02 4 11 8 211.96 31.82 -4 -11 -8 136.16 18.42 4 11 9 18.03 9.09 4 11 9 11.07 7.81 -4 -11 -9 13.48 6.72 4 11 10 30.83 11.11 4 11 10 16.90 6.13 -4 -11 -10 21.50 8.28 4 12 -2 19.86 8.56 4 12 -2 11.14 7.93 -4 -12 2 23.26 10.57 4 12 -1 0.57 4.97 4 12 -1 4.80 3.55 -4 -12 1 1.03 6.32 -4 -12 1 4.58 5.08 -4 -12 1 6.71 3.83 4 12 0 189.33 21.81 4 12 0 219.60 23.79 -4 -12 0 258.98 38.91 -4 -12 0 241.52 45.19 -4 -12 0 217.89 35.07 4 12 1 19.09 9.79 4 12 1 29.08 5.99 -4 -12 -1 19.24 6.15 -4 -12 -1 35.20 12.20 -4 -12 -1 20.19 4.92 4 12 2 20.81 7.06 4 12 2 11.83 5.02 -4 -12 -2 15.44 6.14 -4 -12 -2 4.29 4.63 -4 -12 -2 10.01 5.87 4 12 3 53.73 15.14 4 12 3 55.72 10.70 -4 -12 -3 44.94 16.68 4 12 4 445.87 60.92 4 12 4 495.18 46.43 -4 -12 -4 372.16 62.66 4 12 5 43.44 13.85 4 12 5 47.60 9.01 -4 -12 -5 38.70 14.81 4 12 6 65.38 19.28 4 12 6 102.58 19.26 -4 -12 -6 57.36 11.89 4 12 7 27.03 11.77 4 12 7 37.11 8.03 -4 -12 -7 20.32 7.01 4 12 8 36.71 12.91 4 12 8 21.82 11.38 -4 -12 -8 21.14 6.66 5 -10 -5 176.69 23.45 -5 10 5 179.92 24.80 -5 10 5 223.85 28.66 -5 10 5 125.38 22.22 5 -10 -4 29.97 7.91 -5 10 4 21.83 8.67 -5 10 4 25.97 5.32 -5 10 4 34.18 6.85 5 -10 -3 45.36 9.80 -5 10 3 33.69 9.18 -5 10 3 30.43 6.13 -5 10 3 53.75 12.88 5 -10 -2 2.53 4.74 -5 10 2 -0.78 1.99 -5 10 2 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13.94 4.45 -5 9 -3 3.40 5.57 -5 9 -3 7.25 4.00 5 -9 4 34.04 11.73 -5 9 -4 20.67 6.13 5 -9 5 7.28 5.04 -5 9 -5 5.65 2.34 -5 8 9 3.64 3.11 -5 8 9 5.73 3.72 5 -8 -8 15.29 11.48 -5 8 8 22.37 6.88 -5 8 8 18.64 4.67 -5 8 8 16.72 3.71 5 -8 -7 9.24 7.18 -5 8 7 5.09 4.62 -5 8 7 9.06 4.98 -5 8 7 7.01 4.07 5 -8 -6 10.11 6.61 -5 8 6 4.97 4.15 -5 8 6 6.60 3.09 -5 8 6 6.55 3.97 5 -8 -5 103.22 20.36 -5 8 5 115.67 15.36 -5 8 5 115.75 16.12 -5 8 5 87.35 9.10 5 -8 -4 8.79 4.56 -5 8 4 2.43 2.25 -5 8 4 2.77 3.01 -5 8 4 -2.19 3.04 5 -8 -3 12.31 7.97 -5 8 3 14.62 6.31 -5 8 3 13.82 4.79 -5 8 3 18.16 5.09 5 -8 -2 3.50 4.43 -5 8 2 1.81 2.50 -5 8 2 0.95 2.82 -5 8 2 3.44 3.74 5 -8 -1 34.79 11.32 -5 8 1 46.65 6.45 -5 8 1 24.75 6.77 -5 8 1 21.01 5.40 5 -8 0 130.53 15.93 -5 8 0 108.23 13.61 -5 8 0 62.07 8.92 -5 8 0 162.73 20.89 5 -8 1 674.07 56.87 -5 8 -1 538.64 49.22 -5 8 -1 332.03 30.37 -5 8 -1 752.84 72.45 5 -8 2 145.02 24.10 -5 8 -2 181.04 17.87 -5 8 -2 138.37 15.83 5 -8 3 11.86 5.32 -5 8 -3 35.19 6.45 -5 8 -3 12.61 4.87 5 -8 4 4.64 3.91 -5 8 -4 -2.60 3.01 -5 8 -4 0.70 1.30 5 -8 5 5.30 4.08 -5 8 -5 4.57 3.02 5 -8 6 1.71 5.02 -5 8 -6 1.65 2.25 5 -8 7 -2.48 3.43 -5 8 -7 -1.27 2.22 5 -7 -9 10.98 10.48 -5 7 9 13.61 6.07 -5 7 9 14.16 3.38 -5 7 9 15.33 6.71 5 -7 -8 6.54 7.37 -5 7 8 3.92 2.75 -5 7 8 9.32 3.77 -5 7 8 10.39 3.17 5 -7 -7 98.13 25.68 -5 7 7 115.31 14.09 -5 7 7 94.06 8.86 -5 7 7 130.01 16.07 5 -7 -6 156.02 25.66 -5 7 6 154.66 11.80 -5 7 6 156.53 17.72 -5 7 6 119.52 14.88 5 -7 -5 47.80 13.23 -5 7 5 46.43 7.84 -5 7 5 51.51 9.14 -5 7 5 40.89 7.90 5 -7 -4 55.49 14.71 -5 7 4 73.80 9.61 -5 7 4 73.85 7.31 -5 7 4 61.92 6.18 5 -7 -3 4.81 4.40 -5 7 3 3.14 3.53 -5 7 3 3.47 2.62 -5 7 3 1.50 1.87 5 -7 -2 276.30 34.32 -5 7 2 293.41 29.17 -5 7 2 231.42 20.13 -5 7 2 232.96 17.24 5 -7 -1 4.38 3.36 -5 7 1 4.00 2.34 -5 7 1 7.95 3.07 -5 7 1 4.13 3.15 5 -7 0 38.63 7.21 -5 7 0 56.14 9.36 -5 7 0 34.04 6.43 -5 7 0 18.27 3.86 5 -7 1 42.59 10.58 -5 7 -1 39.87 4.31 -5 7 -1 17.12 3.05 -5 7 -1 47.97 9.84 5 -7 2 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58.41 6.23 5 7 11 9.75 5.31 5 7 11 5.50 3.36 5 7 12 0.66 3.46 5 7 12 0.54 1.91 5 7 13 244.12 32.61 5 8 -7 102.31 12.47 -5 -8 7 299.48 37.96 -5 -8 7 212.09 26.70 5 8 -6 -1.19 2.04 5 8 -6 1.42 1.85 -5 -8 6 0.64 3.33 -5 -8 6 7.67 3.57 5 8 -5 9.57 2.55 5 8 -5 3.58 3.85 -5 -8 5 2.65 4.42 -5 -8 5 7.49 6.99 5 8 -4 1.92 1.76 5 8 -4 -0.08 1.84 -5 -8 4 3.58 4.93 -5 -8 4 6.67 4.87 5 8 -3 20.92 4.04 5 8 -3 20.54 6.22 -5 -8 3 17.25 10.36 -5 -8 3 29.09 6.78 5 8 -2 23.29 7.10 5 8 -2 24.33 4.77 -5 -8 2 44.20 7.20 -5 -8 2 29.26 10.76 5 8 -1 15.98 5.37 5 8 -1 12.48 5.10 -5 -8 1 14.68 7.99 -5 -8 1 15.05 7.31 5 8 0 163.76 20.99 5 8 0 172.70 15.91 -5 -8 0 235.36 29.44 -5 -8 0 188.93 23.81 5 8 1 8.29 2.87 5 8 1 6.75 4.08 -5 -8 -1 4.49 5.52 -5 -8 -1 7.05 3.82 5 8 2 -0.31 2.56 5 8 2 0.73 2.55 -5 -8 -2 -0.77 3.27 -5 -8 -2 1.86 1.92 5 8 3 1.45 3.24 5 8 3 4.26 3.00 -5 -8 -3 1.64 3.60 -5 -8 -3 0.93 1.84 5 8 4 18.38 6.13 5 8 4 22.14 3.95 -5 -8 -4 12.37 7.14 -5 -8 -4 11.72 2.89 5 8 5 50.39 6.27 5 8 5 63.37 6.25 -5 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1.30 6 7 6 4.52 2.59 6 7 6 0.57 3.10 6 7 6 5.84 3.22 -6 -7 -6 2.06 1.94 -6 -7 -6 2.24 1.31 6 7 7 4.15 2.63 6 7 7 4.44 3.20 6 7 7 13.83 3.55 -6 -7 -7 5.16 3.30 6 7 8 27.94 7.46 6 7 8 50.73 5.95 -6 -7 -8 30.27 7.06 6 7 9 15.20 5.59 6 7 9 8.50 2.88 -6 -7 -9 9.74 2.69 6 7 10 174.54 20.69 6 7 10 97.04 15.65 -6 -7 -10 104.79 10.22 6 7 11 3.05 2.65 6 7 11 1.73 2.59 6 8 -5 -1.11 1.85 6 8 -5 2.30 2.72 -6 -8 5 2.05 3.13 6 8 -4 1.34 2.44 6 8 -4 3.98 3.83 -6 -8 4 9.15 4.19 -6 -8 4 5.83 4.12 6 8 -3 199.19 18.39 6 8 -3 200.15 26.96 -6 -8 3 300.64 41.71 -6 -8 3 317.33 43.71 6 8 -2 18.87 7.42 6 8 -2 11.77 5.38 6 8 -2 14.67 5.98 -6 -8 2 25.53 5.98 -6 -8 2 12.69 7.89 6 8 -1 9.48 3.04 6 8 -1 12.90 5.38 6 8 -1 6.30 4.07 -6 -8 1 10.39 7.26 -6 -8 1 8.36 3.95 6 8 0 6.65 6.05 6 8 0 5.37 3.42 6 8 0 0.65 3.80 -6 -8 0 7.83 5.60 -6 -8 0 5.21 4.10 6 8 1 16.31 5.64 6 8 1 16.97 7.75 6 8 1 15.55 3.30 -6 -8 -1 7.04 7.36 -6 -8 -1 6.90 5.09 6 8 2 379.19 39.13 6 8 2 265.04 20.79 6 8 2 206.63 19.84 -6 -8 -2 286.15 36.46 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-6 19.28 10.16 9 0 0 35.83 13.81 9 0 0 18.01 4.24 -9 0 0 12.17 5.43 -9 0 0 27.60 6.44 9 0 1 19.05 4.19 9 0 1 28.91 9.46 -9 0 -1 14.34 8.30 -9 0 -1 25.58 9.71 9 0 2 46.84 6.29 9 0 2 65.36 18.92 -9 0 -2 28.46 12.24 -9 0 -2 65.86 14.15 9 0 3 8.60 2.94 -9 0 -3 5.37 6.25 -9 0 -3 17.25 8.05 9 1 0 63.37 18.36 9 1 0 32.16 5.65 -9 -1 0 56.41 9.22 -9 -1 0 20.25 11.49 9 1 1 76.23 19.73 9 1 1 42.20 6.19 -9 -1 -1 26.40 8.02 -9 -1 -1 67.24 10.61 9 1 2 56.19 7.25 9 1 2 96.61 24.20 -9 -1 -2 55.63 9.15 -9 -1 -2 89.12 12.18 9 1 3 17.97 6.03 9 1 3 39.25 13.62 -9 -1 -3 10.52 8.10 -9 -1 -3 31.59 11.14 9 1 4 11.18 4.79 -9 -1 -4 15.10 8.19 9 2 0 84.39 21.78 9 2 0 46.64 10.66 -9 -2 0 84.72 18.79 -9 -2 0 26.61 8.72 9 2 1 -1.57 5.87 9 2 1 -2.68 2.86 -9 -2 -1 5.32 3.44 -9 -2 -1 2.72 3.18 9 2 2 237.45 24.95 9 2 2 122.98 18.71 -9 -2 -2 105.75 22.17 -9 -2 -2 193.93 21.58 9 2 3 63.97 15.52 9 2 3 29.49 7.90 -9 -2 -3 24.06 9.57 -9 -2 -3 41.71 13.53 9 2 4 30.62 7.99 -9 -2 -4 20.56 6.34 -9 -2 -4 52.45 14.24 9 3 1 63.86 17.32 9 3 1 32.24 8.22 -9 -3 -1 18.77 6.88 -9 -3 -1 55.17 15.87 9 3 2 8.63 5.49 9 3 2 2.76 4.11 -9 -3 -2 9.21 5.07 -9 -3 -2 10.20 4.91 9 3 3 87.94 19.13 9 3 3 43.93 9.12 -9 -3 -3 29.85 10.76 -9 -3 -3 61.26 11.59 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 63344