data_exp_283_mo_a _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'Hf0.17 K Na0.17 O12 P3 Zr2' _chemical_formula_weight 540.03 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'K' 'K' 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Zr' 'Zr' -2.9673 0.5597 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Hf' 'Hf' -0.5830 6.1852 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Na' 'Na' 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system trigonal _space_group_IT_number 167 _space_group_name_H-M_alt 'R -3 c :H' _space_group_name_Hall '-R 3 2"c' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, -z+1/2' 'x-y, -y, -z+1/2' '-x, -x+y, -z+1/2' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'y+2/3, x+1/3, -z+5/6' 'x-y+2/3, -y+1/3, -z+5/6' '-x+2/3, -x+y+1/3, -z+5/6' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' 'y+1/3, x+2/3, -z+7/6' 'x-y+1/3, -y+2/3, -z+7/6' '-x+1/3, -x+y+2/3, -z+7/6' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-y, -x, z-1/2' '-x+y, y, z-1/2' 'x, x-y, z-1/2' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-y+2/3, -x+1/3, z-1/6' '-x+y+2/3, y+1/3, z-1/6' 'x+2/3, x-y+1/3, z-1/6' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' '-y+1/3, -x+2/3, z+1/6' '-x+y+1/3, y+2/3, z+1/6' 'x+1/3, x-y+2/3, z+1/6' _cell_length_a 8.72050(10) _cell_length_b 8.72050(10) _cell_length_c 23.9436(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_volume 1576.89(4) _cell_formula_units_Z 6 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 3.412 _exptl_crystal_F_000 1523 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_absorpt_coefficient_mu 4.539 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 11872 _diffrn_reflns_av_unetI/netI 0.0069 _diffrn_reflns_av_R_equivalents 0.0180 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -37 _diffrn_reflns_limit_l_max 35 _diffrn_reflns_theta_min 3.189 _diffrn_reflns_theta_max 35.727 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.960 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.960 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.960 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 791 _reflns_number_gt 775 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0177P)^2^+1.3936P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 791 _refine_ls_number_parameters 31 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0115 _refine_ls_R_factor_gt 0.0110 _refine_ls_wR_factor_ref 0.0349 _refine_ls_wR_factor_gt 0.0347 _refine_ls_goodness_of_fit_ref 1.238 _refine_ls_restrained_S_all 1.238 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zr Zr 0.6667 0.3333 0.68366(2) 0.00486(5) Uani 0.9656(16) 3 d S T P . . Hf Hf 0.6667 0.3333 0.68366(2) 0.00486(5) Uani 0.0344(16) 3 d S T P . . P P 0.6667 0.62076(3) 0.5833 0.00620(8) Uani 1 2 d S T P . . K K 1.0000 1.0000 0.5000 0.0382(3) Uani 0.967(11) 6 d S T P . . Na Na 1.0000 1.0000 0.5000 0.0382(3) Uani 0.033(11) 6 d S T P . . O1 O 0.82702(9) 0.80170(9) 0.59612(3) 0.01317(13) Uani 1 1 d . . . . . O2 O 0.62291(10) 0.50061(10) 0.63435(3) 0.01553(14) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zr 0.00515(6) 0.00515(6) 0.00428(7) 0.000 0.000 0.00258(3) Hf 0.00515(6) 0.00515(6) 0.00428(7) 0.000 0.000 0.00258(3) P 0.00681(12) 0.00582(10) 0.00631(12) -0.00073(4) -0.00146(8) 0.00340(6) K 0.0528(4) 0.0528(4) 0.0088(3) 0.000 0.000 0.0264(2) Na 0.0528(4) 0.0528(4) 0.0088(3) 0.000 0.000 0.0264(2) O1 0.0111(3) 0.0095(3) 0.0133(3) -0.0046(2) -0.0025(2) 0.0010(2) O2 0.0193(3) 0.0161(3) 0.0136(3) 0.0074(2) 0.0006(2) 0.0107(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zr O2 2.0553(7) 2_655 ? Zr O2 2.0553(7) 3_665 ? Zr O2 2.0554(7) . ? Zr O1 2.0740(6) 27_546 ? Zr O1 2.0740(7) 25_666 ? Zr O1 2.0740(6) 26_456 ? Zr K 3.58376(13) 7_445 ? Zr Na 3.58376(13) 7_445 ? P O1 1.5272(7) 18_655 ? P O1 1.5272(7) . ? P O2 1.5282(7) . ? P O2 1.5283(7) 18_655 ? P K 3.70868(14) 16_445 ? P K 3.70874(15) . ? K O1 2.8203(7) . ? K O1 2.8203(7) 20_566 ? K O1 2.8203(7) 2_765 ? K O1 2.8203(7) 21_656 ? K O1 2.8203(7) 3_675 ? K O1 2.8203(7) 19_776 ? K Zr 3.58373(12) 25_666 ? K Hf 3.58373(12) 13_554 ? K Zr 3.58373(12) 13_554 ? K Hf 3.58373(12) 25_666 ? K P 3.70876(14) 2_765 ? O1 Hf 2.0740(6) 25_666 ? O1 Zr 2.0740(6) 25_666 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 Zr O2 90.28(3) 2_655 3_665 ? O2 Zr O2 90.28(3) 2_655 . ? O2 Zr O2 90.28(3) 3_665 . ? O2 Zr O1 89.42(3) 2_655 27_546 ? O2 Zr O1 94.54(3) 3_665 27_546 ? O2 Zr O1 175.17(3) . 27_546 ? O2 Zr O1 175.17(3) 2_655 25_666 ? O2 Zr O1 89.42(3) 3_665 25_666 ? O2 Zr O1 94.54(3) . 25_666 ? O1 Zr O1 85.79(3) 27_546 25_666 ? O2 Zr O1 94.54(3) 2_655 26_456 ? O2 Zr O1 175.17(3) 3_665 26_456 ? O2 Zr O1 89.42(3) . 26_456 ? O1 Zr O1 85.79(3) 27_546 26_456 ? O1 Zr O1 85.79(3) 25_666 26_456 ? O2 Zr K 125.06(2) 2_655 7_445 ? O2 Zr K 125.06(2) 3_665 7_445 ? O2 Zr K 125.06(2) . 7_445 ? O1 Zr K 51.811(19) 27_546 7_445 ? O1 Zr K 51.81(2) 25_666 7_445 ? O1 Zr K 51.811(19) 26_456 7_445 ? O2 Zr Na 125.06(2) 2_655 7_445 ? O2 Zr Na 125.06(2) 3_665 7_445 ? O2 Zr Na 125.06(2) . 7_445 ? O1 Zr Na 51.811(19) 27_546 7_445 ? O1 Zr Na 51.81(2) 25_666 7_445 ? O1 Zr Na 51.811(19) 26_456 7_445 ? K Zr Na 0.0 7_445 7_445 ? O1 P O1 109.76(6) 18_655 . ? O1 P O2 108.14(4) 18_655 . ? O1 P O2 109.51(4) . . ? O1 P O2 109.50(4) 18_655 18_655 ? O1 P O2 108.14(4) . 18_655 ? O2 P O2 111.78(6) . 18_655 ? O1 P K 44.12(3) 18_655 16_445 ? O1 P K 98.21(3) . 16_445 ? O2 P K 72.75(3) . 16_445 ? O2 P K 148.99(3) 18_655 16_445 ? O1 P K 98.21(3) 18_655 . ? O1 P K 44.11(3) . . ? O2 P K 148.99(3) . . ? O2 P K 72.75(3) 18_655 . ? K P K 120.023(7) 16_445 . ? O1 K O1 119.93(2) . 20_566 ? O1 K O1 60.07(2) . 2_765 ? O1 K O1 180.0 20_566 2_765 ? O1 K O1 119.93(2) . 21_656 ? O1 K O1 60.07(2) 20_566 21_656 ? O1 K O1 119.93(2) 2_765 21_656 ? O1 K O1 60.07(2) . 3_675 ? O1 K O1 119.93(2) 20_566 3_675 ? O1 K O1 60.07(2) 2_765 3_675 ? O1 K O1 180.000(15) 21_656 3_675 ? O1 K O1 180.00(3) . 19_776 ? O1 K O1 60.07(2) 20_566 19_776 ? O1 K O1 119.93(2) 2_765 19_776 ? O1 K O1 60.07(2) 21_656 19_776 ? O1 K O1 119.93(2) 3_675 19_776 ? O1 K Zr 35.310(13) . 25_666 ? O1 K Zr 144.690(13) 20_566 25_666 ? O1 K Zr 35.310(13) 2_765 25_666 ? O1 K Zr 144.690(13) 21_656 25_666 ? O1 K Zr 35.310(13) 3_675 25_666 ? O1 K Zr 144.690(13) 19_776 25_666 ? O1 K Hf 144.690(13) . 13_554 ? O1 K Hf 35.310(13) 20_566 13_554 ? O1 K Hf 144.690(13) 2_765 13_554 ? O1 K Hf 35.310(13) 21_656 13_554 ? O1 K Hf 144.690(13) 3_675 13_554 ? O1 K Hf 35.310(13) 19_776 13_554 ? Zr K Hf 180.0 25_666 13_554 ? O1 K Zr 144.690(13) . 13_554 ? O1 K Zr 35.310(13) 20_566 13_554 ? O1 K Zr 144.690(13) 2_765 13_554 ? O1 K Zr 35.310(13) 21_656 13_554 ? O1 K Zr 144.690(13) 3_675 13_554 ? O1 K Zr 35.310(13) 19_776 13_554 ? Zr K Zr 180.0 25_666 13_554 ? Hf K Zr 0.0 13_554 13_554 ? O1 K Hf 35.310(13) . 25_666 ? O1 K Hf 144.690(13) 20_566 25_666 ? O1 K Hf 35.310(13) 2_765 25_666 ? O1 K Hf 144.690(13) 21_656 25_666 ? O1 K Hf 35.310(13) 3_675 25_666 ? O1 K Hf 144.690(13) 19_776 25_666 ? Zr K Hf 0.0 25_666 25_666 ? Hf K Hf 180.0 13_554 25_666 ? Zr K Hf 180.0 13_554 25_666 ? O1 K P 22.144(13) . . ? O1 K P 101.110(15) 20_566 . ? O1 K P 78.890(15) 2_765 . ? O1 K P 101.429(15) 21_656 . ? O1 K P 78.571(15) 3_675 . ? O1 K P 157.856(13) 19_776 . ? Zr K P 57.452(2) 25_666 . ? Hf K P 122.548(2) 13_554 . ? Zr K P 122.548(2) 13_554 . ? Hf K P 57.452(2) 25_666 . ? O1 K P 78.570(15) . 2_765 ? O1 K P 157.857(13) 20_566 2_765 ? O1 K P 22.143(13) 2_765 2_765 ? O1 K P 101.111(14) 21_656 2_765 ? O1 K P 78.889(14) 3_675 2_765 ? O1 K P 101.430(15) 19_776 2_765 ? Zr K P 57.451(1) 25_666 2_765 ? Hf K P 122.549(2) 13_554 2_765 ? Zr K P 122.549(2) 13_554 2_765 ? Hf K P 57.451(1) 25_666 2_765 ? P K P 93.774(2) . 2_765 ? P O1 Hf 153.36(4) . 25_666 ? P O1 Zr 153.36(4) . 25_666 ? Hf O1 Zr 0.0 25_666 25_666 ? P O1 K 113.74(3) . . ? Hf O1 K 92.88(2) 25_666 . ? Zr O1 K 92.88(2) 25_666 . ? P O2 Zr 150.98(5) . . ? _refine_diff_density_max 0.374 _refine_diff_density_min -0.486 _refine_diff_density_rms 0.090 _shelx_res_file ; exp_283_mo_a.res created by SHELXL-2014/7 TITL exp_283_mo_a.res in R-3c REM Old TITL exp_283_Mo in R-3c kosnarite CELL 0.71073 8.7205 8.7205 23.9436 90.000 90.000 120.000 ZERR 6.000 0.0001 0.0001 0.0003 0.000 0.000 0.000 LATT 3 SYMM -Y, X-Y, Z SYMM -X+Y, -X, Z SYMM Y, X, 1/2-Z SYMM X-Y, -Y, 1/2-Z SYMM -X, -X+Y, 1/2-Z SFAC O P K ZR HF NA UNIT 72.00 18.00 6.00 12.00 1.00 1.00 L.S. 20 BOND $H ACTA EXYZ ZR HF EXYZ K NA EADP ZR HF EADP K NA LIST 6 FMAP 2 PLAN 20 WGHT 0.017700 1.393600 FVAR 0.22290 0.96561 0.96671 ZR 4 0.666667 0.333333 0.683661 20.33333 0.00515 0.00515 = 0.00428 0.00000 0.00000 0.00258 HF 5 0.666667 0.333333 0.683661 -20.33333 0.00515 0.00515 = 0.00428 0.00000 0.00000 0.00258 P 2 0.666667 0.620763 0.583333 10.50000 0.00681 0.00582 = 0.00631 -0.00073 -0.00146 0.00340 K 3 1.000000 1.000000 0.500000 30.16667 0.05283 0.05283 = 0.00881 0.00000 0.00000 0.02642 NA 6 1.000000 1.000000 0.500000 -30.16667 0.05283 0.05283 = 0.00881 0.00000 0.00000 0.02642 O1 1 0.827023 0.801700 0.596119 11.00000 0.01110 0.00947 = 0.01334 -0.00459 -0.00247 0.00095 O2 1 0.622906 0.500611 0.634346 11.00000 0.01926 0.01615 = 0.01365 0.00744 0.00059 0.01069 HKLF 4 REM exp_283_mo_a.res in R-3c REM R1 = 0.0110 for 775 Fo > 4sig(Fo) and 0.0115 for all 791 data REM 31 parameters refined using 0 restraints END WGHT 0.0174 1.4674 REM Highest difference peak 0.374, deepest hole -0.486, 1-sigma level 0.090 Q1 1 0.6239 0.5501 0.6108 11.00000 0.05 0.37 Q2 1 0.8522 0.8067 0.6203 11.00000 0.05 0.28 Q3 1 0.7784 0.7209 0.5842 11.00000 0.05 0.25 Q4 1 0.6930 0.4853 0.6473 11.00000 0.05 0.23 Q5 1 0.6756 0.4634 0.6234 11.00000 0.05 0.23 Q6 1 0.6667 0.3333 0.5833 10.16667 0.05 0.23 Q7 1 0.7069 0.5638 0.6580 11.00000 0.05 0.21 Q8 1 0.6126 0.4283 0.6495 11.00000 0.05 0.21 Q9 1 0.8530 0.8857 0.6147 11.00000 0.05 0.21 Q10 1 0.8868 0.8642 0.5675 11.00000 0.05 0.17 Q11 1 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-3 -5 -10 1915.75 34.37 -3 -5 -10 1848.85 23.58 3 -8 -10 1910.45 26.54 8 -5 10 1912.05 34.45 8 -3 -10 1983.62 34.40 -8 3 7 98.51 6.53 -5 -3 7 82.95 4.55 -3 8 7 79.48 2.30 8 -3 -7 94.23 5.85 5 -8 7 104.13 4.00 3 5 7 97.93 6.21 8 -5 7 85.30 5.23 5 -8 7 93.52 5.30 -3 8 7 87.78 6.22 -5 8 -7 110.27 6.91 -8 5 -7 88.44 6.27 -8 3 7 103.74 6.77 -5 -3 7 85.30 6.09 3 -8 -7 88.92 6.61 -3 -5 -7 101.47 6.57 -3 -5 -7 99.79 3.42 -5 -3 7 85.06 4.62 -3 -5 -7 97.40 6.26 5 3 -7 82.35 4.21 5 -8 7 96.76 6.80 3 -8 -7 80.00 4.20 8 -5 7 78.69 5.97 8 -3 -7 96.10 6.45 -3 8 4 649.72 17.68 5 -8 4 633.29 14.03 8 -3 -4 615.02 15.69 5 -8 4 613.14 9.21 3 5 4 642.29 16.66 8 -5 4 614.29 14.36 3 -8 -4 655.64 13.78 -8 3 4 622.41 17.43 5 3 -4 636.10 10.26 -5 -3 4 627.36 17.28 3 -8 -4 646.53 18.00 -3 -5 -4 636.90 11.00 -5 -3 4 650.73 14.89 5 -8 4 643.08 15.63 -3 -5 -4 636.97 16.23 8 -5 4 646.47 17.92 3 -8 -4 674.47 13.83 3 5 4 594.07 11.53 -8 3 1 67.45 5.48 5 -8 1 68.05 4.13 3 5 1 73.34 5.37 8 -3 -1 75.20 5.17 8 -5 1 87.95 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305.14 13.05 -10 6 14 290.31 13.54 -4 -6 14 328.19 9.11 6 4 14 326.31 14.03 10 -4 14 353.25 14.39 -4 -6 14 313.37 12.15 -4 10 -14 320.46 13.18 -6 10 14 285.37 12.67 4 6 -14 305.59 9.77 -10 4 -14 309.04 13.20 -6 -4 -14 347.74 13.54 -4 -6 14 303.28 13.08 -6 -4 -14 308.79 10.75 6 -10 -14 299.57 14.40 -6 -4 -14 309.55 13.87 10 -6 -14 320.42 15.07 10 -6 -14 306.92 13.15 4 6 -14 326.73 13.57 10 -4 17 173.07 9.61 -6 10 17 172.92 8.54 -10 6 17 168.04 10.56 -4 -6 17 178.97 9.69 -4 -6 17 163.09 7.06 6 4 17 161.57 10.03 10 -4 17 165.14 10.03 -4 10 -17 161.51 9.16 -6 10 17 164.85 9.43 -10 4 -17 168.50 9.63 4 6 -17 171.25 7.75 -6 -4 -17 156.61 8.97 -4 -6 17 159.65 9.27 -10 4 -17 170.53 10.71 -6 -4 -17 150.17 8.07 6 -10 -17 172.68 11.04 -6 -4 -17 155.97 10.19 4 6 -17 167.43 10.03 10 -6 -17 150.71 9.01 10 -4 20 1982.13 36.54 -6 10 20 1921.61 34.76 -10 6 20 1986.27 41.41 -4 -6 20 1988.98 32.61 6 4 20 1973.44 40.23 10 -4 20 1973.14 40.04 -4 -6 20 2022.37 38.98 -4 10 -20 2017.08 36.50 -6 10 20 1966.37 36.86 -10 4 -20 1997.61 36.92 4 6 -20 1933.66 33.78 -6 -4 -20 1973.31 36.24 -4 -6 20 1944.61 36.59 10 -6 -20 1921.71 42.07 -10 4 -20 2027.65 41.34 -6 -4 -20 1982.29 36.18 -6 -4 -20 2087.90 42.00 4 6 -20 1991.08 40.29 10 -6 -20 1976.17 36.46 4 6 -23 18.66 4.00 4 -10 23 21.63 4.50 10 -6 -23 16.97 3.11 -10 6 23 20.36 4.16 6 4 23 22.71 4.13 10 -4 23 16.45 3.72 -4 10 -23 17.06 3.13 10 -6 -23 17.14 4.08 4 6 -23 17.07 3.07 -6 -4 -23 22.16 3.49 -6 -4 -23 20.35 3.66 -10 4 -23 16.75 3.78 6 -10 -23 17.17 4.09 -6 -4 -23 24.90 4.50 -4 -6 23 14.37 3.52 4 6 -26 307.62 12.84 -6 -4 -26 308.61 13.84 -7 -3 26 134.57 8.99 3 7 26 147.28 9.36 7 3 -26 131.64 8.60 -3 -7 -26 130.51 9.20 10 -3 -23 41.17 5.79 -10 3 23 50.86 6.18 -7 -3 23 38.89 4.73 3 7 23 42.38 5.06 10 -7 23 35.01 4.71 3 -10 -23 31.11 5.10 7 3 -23 33.64 4.17 7 -10 23 40.87 5.63 -3 -7 -23 40.19 4.34 -3 -7 -23 49.12 5.53 -3 -7 -23 42.66 5.68 -10 3 20 2247.03 44.35 -7 -3 20 2237.67 39.28 3 7 20 2230.97 40.61 10 -7 20 2347.72 41.24 -3 10 20 2304.36 40.64 -7 10 -20 2270.81 39.83 3 -10 -20 2326.19 46.45 -10 3 20 2251.47 40.75 -7 -3 20 2309.40 40.95 10 -7 20 2284.79 39.34 7 3 -20 2238.17 37.50 -3 -7 -20 2273.04 39.70 7 -10 20 2268.35 45.08 -3 -7 -20 2294.13 40.52 -3 -7 -20 2300.54 44.87 10 -7 20 2294.65 40.39 10 -7 17 3.07 1.88 10 -3 -17 5.93 2.34 10 -7 17 4.94 1.91 7 -10 17 5.59 2.53 -10 3 17 6.90 2.58 -7 -3 17 5.27 1.73 3 7 17 4.90 1.96 10 -7 17 4.95 2.00 -3 10 17 6.85 2.29 -7 10 -17 9.00 2.56 -10 3 17 5.97 2.35 -7 -3 17 5.55 2.32 7 3 -17 4.42 1.65 -3 -7 -17 3.60 1.71 -3 -7 -17 6.14 2.51 10 -3 -14 387.04 14.71 -10 3 14 384.97 15.43 10 -3 -14 395.95 14.93 -7 -3 14 387.00 12.73 7 3 -14 396.03 16.64 3 7 14 416.51 14.63 10 -7 14 418.25 13.86 -7 10 -14 398.14 14.91 -3 10 14 429.43 15.72 3 -10 -14 409.43 16.93 -10 3 14 403.93 15.38 -7 -3 14 385.07 14.86 7 3 -14 368.60 11.22 -3 -7 -14 404.00 14.89 10 -7 14 408.75 13.81 7 -10 14 372.50 15.76 -3 -7 -14 401.98 15.70 10 -7 14 383.32 14.86 10 -3 -11 28.37 4.16 10 -3 -11 28.97 3.99 7 3 -11 38.34 5.13 3 7 11 35.66 4.27 10 -7 11 35.11 3.79 -3 10 11 45.18 5.09 -7 10 -11 33.69 4.41 3 -10 -11 31.95 4.75 -10 3 11 35.11 4.63 7 -10 11 35.33 3.33 -7 -3 11 38.25 4.72 7 3 -11 38.60 3.16 -3 -7 -11 38.53 4.67 10 -7 11 42.66 3.97 10 -7 11 42.19 4.35 7 -10 11 34.89 4.78 -3 -7 -11 31.84 4.37 10 -7 11 42.55 4.93 10 -3 -8 621.22 19.26 10 -3 -8 609.95 18.05 7 3 -8 596.15 19.67 3 7 8 608.26 17.60 10 -7 8 606.39 15.43 -3 10 8 623.63 19.45 -7 10 -8 607.94 18.97 3 -10 -8 603.49 20.09 -10 3 8 575.90 18.79 -7 -3 8 613.75 19.12 7 3 -8 588.94 11.80 -3 -7 -8 590.84 18.64 7 -10 8 600.54 15.66 -3 -7 -8 589.00 10.88 -7 -3 8 613.32 15.34 -3 -7 -8 617.93 18.39 7 -10 8 610.39 20.01 10 -7 8 630.52 16.95 10 -7 8 590.48 16.95 10 -7 8 618.84 19.59 10 -7 5 2.03 1.56 10 -7 5 2.25 1.56 -3 -7 -5 0.69 0.79 10 -3 -5 -0.72 1.43 7 3 -5 -0.38 1.36 10 -3 -5 1.56 1.45 3 7 5 -0.30 1.29 10 -7 5 0.78 0.97 -3 10 5 7.62 2.43 -7 10 -5 0.36 1.35 3 -10 -5 0.77 1.45 -10 3 5 1.47 1.53 7 3 -5 0.61 0.57 -7 -3 5 -0.36 1.29 -3 -7 -5 -0.36 1.48 -7 -3 5 0.99 1.36 -3 -7 -5 0.89 1.33 7 -10 5 1.06 1.38 3 7 2 727.41 19.62 7 3 -2 693.79 21.26 10 -3 -2 755.79 20.22 10 -7 2 756.68 15.85 -3 10 2 730.78 21.27 3 -10 -2 745.29 21.40 -10 3 2 736.89 21.55 -3 -7 -2 761.98 14.65 -7 -3 2 729.76 21.11 -7 -3 2 769.05 19.38 7 -10 2 748.32 19.63 -3 -7 -2 766.39 19.02 10 -7 2 762.71 22.22 10 -7 2 723.14 20.19 10 -3 1 46.56 5.31 3 7 -1 39.02 4.49 10 -7 -1 36.22 3.03 10 -3 1 41.97 4.71 -3 10 -1 42.48 4.99 3 -10 1 40.15 4.70 -7 10 1 44.19 5.08 -10 3 -1 40.16 4.96 -3 -7 1 44.93 3.47 -7 -3 -1 39.42 4.75 -3 -7 1 45.83 5.18 -7 -3 -1 37.28 4.26 -3 -7 1 40.53 3.95 7 -10 -1 43.82 4.74 3 7 -1 41.84 3.69 3 -10 1 42.56 4.75 10 -7 -1 41.13 5.00 10 -7 -1 34.07 4.41 10 -3 4 291.62 13.00 10 -7 -4 265.64 8.05 3 7 -4 262.58 11.59 10 -3 4 270.97 11.92 3 -10 4 295.02 12.07 -7 10 4 282.60 12.71 -3 -7 4 277.59 9.61 -3 -7 4 275.38 12.67 -10 3 -4 292.81 13.52 -7 -3 -4 291.98 12.24 -3 -7 4 281.48 9.78 3 -10 4 301.82 12.91 7 -10 -4 280.57 12.58 3 7 -4 295.12 10.55 10 -7 -4 266.84 12.55 10 -3 7 114.97 8.08 3 7 -7 116.08 7.88 3 -10 7 139.33 7.86 10 -3 7 123.21 8.17 -3 10 -7 121.10 8.23 -7 10 7 120.60 8.27 -3 -7 7 117.86 6.58 -10 3 -7 118.82 8.21 -7 -3 -7 115.09 7.97 -3 -7 7 119.44 8.25 -10 3 -7 115.51 8.50 -7 -3 -7 132.77 8.51 -3 -7 7 111.16 5.38 3 -10 7 138.55 8.85 10 -7 -7 132.18 9.06 7 -10 -7 113.45 8.20 10 -7 -7 125.09 8.65 3 7 -7 114.75 7.00 10 -3 10 1923.07 37.13 3 7 -10 1815.02 36.43 10 -3 10 1914.37 37.07 -3 10 -10 1836.03 36.31 -7 10 10 1840.28 36.72 -3 -7 10 1823.35 32.57 -10 3 -10 1803.63 36.37 -7 -3 -10 1827.98 35.97 -3 -7 10 1844.58 36.52 -10 3 -10 1851.81 38.43 3 -10 10 1875.73 37.60 -7 -3 -10 1901.88 37.29 10 -7 -10 1772.86 38.05 7 -10 -10 1819.95 37.85 10 -7 -10 1898.89 37.26 3 7 -10 1835.35 34.16 3 7 -13 4.72 2.14 10 -7 -13 2.51 1.92 10 -3 13 3.18 1.75 3 -10 13 2.44 1.62 7 -10 -13 3.43 2.13 10 -7 -13 1.31 1.74 7 3 13 3.18 1.91 10 -3 13 3.88 1.98 -3 10 -13 1.75 1.83 -7 10 13 3.93 1.87 3 7 -13 3.33 1.31 -10 3 -13 5.67 2.17 -7 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349.52 16.01 -7 -3 -22 374.83 16.71 7 -10 -22 360.26 16.80 3 7 -22 357.84 15.88 10 -7 -22 385.40 14.01 -7 10 25 7.42 2.65 3 7 -25 7.74 2.48 -7 -3 -25 7.07 2.53 -3 -7 25 7.25 2.83 -8 -2 24 560.80 18.69 2 8 24 530.48 17.12 8 2 -24 523.47 17.13 8 -10 21 29.58 4.73 2 8 21 31.96 4.14 -10 2 21 28.84 4.75 -8 -2 21 26.26 4.12 10 -8 21 27.97 3.83 2 -10 -21 29.69 4.85 -10 2 21 35.82 4.55 -8 -2 21 28.19 4.04 10 -8 21 33.13 4.40 -2 -8 -21 34.85 4.31 -2 -8 -21 29.93 4.78 10 -8 21 35.39 4.49 -10 2 18 89.59 7.58 -8 -2 18 91.36 6.80 2 8 18 93.46 6.74 10 -8 18 96.32 6.74 -2 10 18 90.51 7.15 -10 2 18 84.19 7.00 -8 -2 18 83.40 6.90 -2 -8 -18 100.34 7.30 10 -8 18 96.13 7.15 8 -10 18 87.03 7.80 -2 -8 -18 91.92 7.83 10 -8 18 87.85 7.00 -10 2 15 63.13 6.29 -8 -2 15 56.86 5.24 10 -2 -15 51.50 5.82 8 2 -15 59.28 6.62 2 8 15 50.68 4.86 10 -8 15 66.68 5.26 -2 10 15 74.37 6.56 2 -10 -15 53.60 6.34 -8 10 -15 62.12 5.99 -10 2 15 56.60 5.75 -8 -2 15 65.77 6.19 -2 -8 -15 61.81 5.85 10 -8 15 61.70 5.68 8 -10 15 64.17 6.61 -2 -8 -15 64.22 6.38 10 -8 15 65.36 6.13 10 -2 -12 35.35 4.68 8 2 -12 34.50 5.03 2 8 12 41.41 4.43 10 -8 12 37.99 3.72 -2 10 12 45.63 5.21 2 -10 -12 44.70 5.63 -8 10 -12 44.06 5.04 -10 2 12 46.25 5.31 -8 -2 12 48.33 5.37 -2 -8 -12 38.69 4.82 10 -8 12 40.37 4.60 8 -10 12 40.13 5.23 -2 -8 -12 32.13 4.41 -2 -8 -12 41.32 3.18 10 -8 12 44.58 5.21 10 -2 -9 115.17 8.12 -2 10 9 120.61 4.69 10 -2 -9 112.41 7.97 8 2 -9 119.42 8.81 2 8 9 113.98 7.06 10 -8 9 120.89 6.15 -2 10 9 116.24 8.26 2 -10 -9 110.77 8.55 -8 10 -9 107.32 7.86 10 -8 9 123.41 6.95 -10 2 9 107.58 8.03 -8 -2 9 112.06 8.13 8 -10 9 108.59 6.22 -2 -8 -9 117.18 5.46 -2 -8 -9 113.11 7.80 8 -10 9 119.29 8.60 10 -8 9 121.14 7.86 10 -8 9 113.90 8.33 10 -2 -6 1258.55 29.35 -2 10 6 1254.06 19.50 8 2 -6 1273.82 30.34 10 -2 -6 1241.91 28.40 2 8 6 1349.76 26.88 10 -8 6 1317.77 22.03 2 -10 -6 1265.33 30.33 -2 10 6 1337.73 30.21 -8 10 -6 1314.17 29.97 -10 2 6 1266.98 29.59 -8 -2 6 1221.91 29.66 10 -8 6 1275.88 26.44 -8 -2 6 1256.27 25.88 -2 -8 -6 1278.67 21.97 -2 -8 -6 1271.58 27.49 8 -10 6 1301.16 25.81 10 -8 6 1294.81 30.31 2 8 3 122.41 7.33 8 2 -3 123.44 8.69 10 -2 -3 118.44 8.09 2 -10 -3 120.74 8.51 -2 10 3 107.15 7.96 -10 2 3 135.05 8.86 -8 -2 3 119.57 8.40 10 -8 3 112.06 7.43 -2 -8 -3 132.34 6.21 -8 -2 3 107.61 7.15 -2 -8 -3 122.41 7.35 10 -8 3 112.69 8.37 8 -10 3 126.91 7.66 10 -2 0 1623.30 34.18 2 8 0 1623.99 30.84 8 2 0 1534.04 33.86 10 -2 0 1572.45 32.76 2 -10 0 1590.01 33.42 -2 10 0 1620.70 34.08 -8 10 0 1601.94 33.89 -10 2 0 1568.49 33.81 -8 -2 0 1626.56 34.22 -2 -8 0 1604.91 27.30 10 -8 0 1578.23 32.39 -8 -2 0 1620.09 31.89 -2 -8 0 1630.19 29.40 2 -10 0 1635.54 32.35 10 -8 0 1619.08 34.77 8 -10 0 1600.50 32.00 8 -10 -3 111.24 7.87 10 -2 3 114.07 8.21 2 8 -3 125.75 7.75 8 2 3 132.25 8.94 10 -2 3 103.69 7.65 2 -10 3 136.20 8.53 -8 10 3 125.96 8.60 -2 -8 3 118.74 6.64 10 -8 -3 129.21 8.64 -10 2 -3 114.18 8.36 -8 -2 -3 132.87 8.43 2 -10 3 129.79 8.32 -2 -8 3 126.07 6.62 10 -2 6 1351.02 30.50 8 -10 -6 1275.46 29.93 2 8 -6 1307.65 28.30 8 2 6 1308.30 30.56 10 -2 6 1325.54 30.02 -2 10 -6 1331.66 30.34 -8 10 6 1335.03 30.37 -10 2 -6 1332.61 30.45 -2 -8 6 1324.02 26.14 -8 -2 -6 1354.07 30.41 10 -8 -6 1290.78 30.58 -10 2 -6 1347.22 31.60 -8 -2 -6 1324.25 29.68 2 -10 6 1359.91 29.88 -2 -8 6 1338.28 23.05 2 8 -6 1319.83 26.53 10 -8 -6 1327.83 31.03 8 -10 -9 100.36 8.05 10 -2 9 104.86 7.88 8 2 9 94.30 7.70 10 -2 9 108.88 8.10 -2 10 -9 92.25 7.37 -8 10 9 99.82 7.67 -10 2 -9 110.42 8.13 -2 -8 9 111.83 7.18 -8 -2 -9 93.09 7.35 10 -8 -9 97.09 8.03 2 -10 9 103.31 7.76 -10 2 -9 104.82 8.30 -8 -2 -9 87.94 7.28 2 8 -9 107.25 7.15 10 -8 -9 89.48 7.52 8 -10 -12 31.34 4.79 8 2 12 38.78 5.14 10 -2 12 43.57 5.36 -2 10 -12 33.37 4.53 -8 10 12 35.62 4.64 -2 -8 12 39.99 4.63 -10 2 -12 37.47 4.74 10 -8 -12 33.33 4.98 -8 -2 -12 40.61 4.96 2 -10 12 42.32 5.20 -10 2 -12 38.32 5.17 -8 -2 -12 38.36 5.05 2 8 -12 30.70 4.14 10 -8 -12 42.42 5.20 10 -2 15 79.49 7.27 -2 10 -15 67.36 6.16 -8 10 15 64.98 6.16 -2 -8 15 67.61 6.29 10 -8 -15 64.94 6.90 -10 2 -15 71.59 6.41 -8 -2 -15 60.88 5.85 2 -10 15 79.54 7.27 -2 -8 15 68.82 6.44 -10 2 -15 70.04 7.02 -8 -2 -15 63.99 6.59 2 8 -15 73.66 6.59 10 -8 -15 67.25 6.36 8 -10 -15 63.14 6.93 -8 10 18 59.04 5.77 -10 8 18 54.46 6.24 10 -2 18 56.09 6.40 -2 10 -18 63.00 5.95 2 8 -18 69.64 5.20 -2 -8 18 72.57 6.85 -10 2 -18 63.91 6.02 -8 -2 -18 56.27 5.63 2 -10 18 71.09 7.18 -2 -8 18 59.57 5.92 -8 -2 -18 53.78 6.21 2 8 -18 75.20 6.96 10 -8 -18 65.15 6.13 8 -10 -18 50.80 6.41 -8 10 21 49.04 5.43 -10 8 21 56.61 6.37 10 -2 21 44.74 5.78 10 -8 -21 50.90 6.45 2 8 -21 59.55 5.70 -2 10 -21 53.43 5.33 -2 -8 21 58.79 6.44 2 8 -21 55.86 5.07 -10 2 -21 47.48 5.15 2 -10 21 59.98 6.87 -8 -2 -21 52.13 5.31 -2 -8 21 46.62 5.08 -10 2 -21 43.48 5.94 -8 -2 -21 59.30 6.63 2 8 -21 57.46 6.34 10 -8 -21 46.39 5.07 -8 10 24 592.67 19.49 -2 -8 24 591.25 21.38 2 8 -24 591.10 17.92 9 -10 22 26.69 4.59 -10 1 22 30.14 4.74 -9 -1 22 27.44 4.42 10 -9 22 31.65 4.62 -1 -9 -22 31.04 4.21 10 -9 19 21.90 3.80 10 -9 19 23.37 3.98 9 -10 19 20.12 3.92 -1 -9 -19 16.13 3.78 -10 1 19 21.30 3.98 -9 -1 19 20.29 3.66 1 -10 -19 28.05 4.76 1 9 19 18.50 3.02 1 9 19 19.42 3.63 -1 10 19 28.24 4.14 -10 1 19 21.73 3.77 -9 -1 19 21.99 3.80 -1 -9 -19 18.34 3.54 -10 1 16 655.80 20.48 -9 -1 16 674.63 19.53 9 1 -16 653.64 22.44 -1 -9 -16 678.47 22.90 1 9 16 650.39 17.36 1 9 16 669.18 20.61 -1 10 16 696.27 20.88 -10 1 16 635.48 20.24 -9 -1 16 639.08 20.21 10 -9 16 659.91 20.32 9 -10 16 655.62 21.41 10 -9 16 672.30 20.78 10 -1 -13 83.35 7.43 9 1 -13 68.42 6.93 1 9 13 83.66 5.89 1 -10 -13 64.63 7.04 1 9 13 76.81 6.86 -1 10 13 73.04 6.75 -10 1 13 78.57 6.96 -9 -1 13 67.14 6.43 10 -9 13 71.01 6.50 9 -10 13 76.83 6.99 10 -9 13 71.93 6.71 10 -1 -10 760.96 22.69 9 1 -10 752.03 23.21 -1 10 10 760.91 15.64 1 9 10 749.34 18.49 10 -9 10 759.87 17.89 1 -10 -10 739.72 23.48 -1 10 10 756.19 22.32 -9 10 -10 751.70 22.09 -10 1 10 749.09 22.27 -9 -1 10 752.14 22.32 9 -10 10 753.88 22.53 10 -9 10 758.22 21.51 -1 -9 -10 764.52 17.30 10 -9 10 745.20 22.64 -1 10 7 21.22 2.47 1 9 7 22.67 3.06 9 -10 7 21.63 3.72 9 -10 7 18.37 2.91 1 -10 -7 26.37 4.34 10 -9 7 22.75 3.27 9 1 -7 21.75 3.95 10 -1 -7 16.62 3.38 -1 10 7 23.87 4.05 -9 10 -7 24.31 4.04 -10 1 7 17.57 3.51 -9 -1 7 23.53 4.08 -1 -9 -7 20.68 2.79 9 -10 4 921.31 22.09 -1 10 4 912.02 17.99 1 9 4 937.88 20.92 9 1 -4 933.93 25.59 10 -1 -4 881.71 24.31 1 -10 -4 878.92 25.04 -1 10 4 934.79 25.20 10 -9 4 917.41 22.43 -10 1 4 883.89 24.63 -9 -1 4 901.41 24.86 -9 -1 4 923.11 23.10 -1 -9 -4 926.05 19.99 1 -10 -4 945.62 22.39 -1 -9 -1 4.68 1.67 10 -9 1 3.34 1.70 1 -10 -1 3.05 1.76 1 -10 -1 3.17 1.84 -1 10 1 5.83 1.55 1 9 1 8.54 2.18 9 1 -1 0.80 1.74 10 -1 -1 5.34 2.15 -1 10 1 4.72 2.16 9 -10 1 5.18 2.02 -9 10 -1 7.40 2.43 -10 1 1 8.23 2.62 -9 -1 1 2.74 1.82 -9 -1 1 6.11 2.16 1 9 -2 28.05 3.64 9 -10 -2 31.18 4.31 9 1 2 27.78 4.31 10 -1 2 33.31 4.61 -9 10 2 30.10 4.46 10 -9 -2 30.05 4.22 -1 -9 2 31.26 3.70 -9 -1 -2 25.36 3.87 1 -10 2 26.27 3.76 -1 -9 2 24.37 3.16 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14 877.40 24.99 -10 1 -14 887.51 25.77 -9 -1 -14 891.68 25.84 1 9 -14 898.53 23.97 10 -9 -14 853.11 24.36 -1 -9 17 9.07 2.93 1 -10 17 7.98 2.82 10 -9 -17 4.21 2.25 9 1 17 8.29 2.87 10 -1 17 12.87 3.49 9 -10 -17 10.61 3.22 1 9 -17 11.80 2.90 -1 10 -17 5.11 2.36 -10 1 -17 10.59 2.77 -9 -1 -17 7.22 2.49 -1 -9 17 11.80 3.03 10 -9 -17 5.86 2.81 -10 1 -17 15.49 3.59 -9 -1 -17 2.26 1.96 1 9 -17 10.07 3.02 -9 10 20 755.73 22.39 -10 9 20 738.75 23.23 9 1 20 756.90 24.64 10 -1 20 765.92 24.68 1 9 -20 763.23 21.59 -1 10 -20 783.54 21.63 -1 -9 20 712.09 23.21 -10 1 -20 735.55 21.24 1 -10 20 775.08 24.84 -9 -1 -20 750.49 21.24 -1 -9 20 744.58 21.67 -9 -1 -20 764.67 24.70 1 9 -20 762.25 23.56 9 -10 -20 777.59 22.12 10 -9 -20 751.58 21.50 1 9 -23 53.51 5.42 -1 10 -23 48.79 5.01 -10 1 -23 46.81 5.18 -9 -1 -23 58.41 5.56 -10 0 20 1769.99 36.83 -10 0 20 1737.27 35.84 10 -10 20 1748.19 37.43 0 -10 -20 1711.86 34.69 10 -10 20 1753.76 35.69 10 -10 17 -0.38 1.53 10 -10 17 -1.22 1.62 0 -10 -17 -0.49 1.86 -10 0 17 2.97 2.36 0 10 17 -0.38 1.52 -10 0 17 -0.39 1.92 10 0 -14 234.61 13.02 0 10 14 235.04 12.15 -10 0 14 246.01 12.58 10 -10 14 239.67 12.39 10 -10 14 259.68 12.82 10 -10 11 0.40 1.51 0 -10 -11 0.94 1.78 10 0 -11 0.43 1.65 0 10 11 0.87 1.35 0 10 11 -0.81 1.88 -10 0 11 -0.41 1.55 10 -10 8 768.10 19.02 10 0 -8 760.94 23.32 0 10 8 786.59 17.73 0 -10 -8 789.25 24.61 0 10 8 780.85 23.26 -10 0 8 771.76 23.17 0 -10 -8 812.39 19.57 10 -10 8 797.34 23.24 0 -10 -5 0.54 1.33 0 10 5 0.22 1.01 10 0 -5 -0.41 1.65 0 10 5 4.14 2.05 10 -10 5 2.09 1.72 -10 0 5 -0.82 1.78 0 10 2 527.17 14.46 10 0 -2 487.16 18.27 10 -10 2 514.11 16.86 0 10 2 540.05 19.16 -10 0 2 507.01 18.55 -10 0 2 499.25 17.49 0 -10 -2 524.55 15.82 0 -10 1 2.41 1.62 0 10 -1 3.88 1.54 10 0 1 -0.41 1.65 0 10 -1 1.25 1.66 -10 0 -1 -1.23 1.48 10 -10 -1 -0.73 1.69 -10 0 -1 0.39 1.54 10 0 4 332.00 14.91 10 -10 -4 302.37 13.83 0 -10 4 313.89 12.83 -10 0 -4 342.46 14.87 0 -10 7 0.35 1.61 10 0 7 0.43 1.55 0 10 -7 0.41 1.64 -10 0 -7 -0.41 2.01 10 -10 -7 -1.26 2.02 -10 0 -7 3.76 2.13 10 -10 -10 1815.28 39.47 10 0 10 1894.04 40.02 0 10 -10 1902.77 38.94 -10 0 -10 1872.72 38.50 0 -10 10 1915.09 37.78 -10 0 -10 1835.72 39.22 0 -10 13 -0.80 1.87 10 0 13 0.91 1.65 0 10 -13 -0.40 1.59 -10 0 -13 1.97 2.17 10 -10 -13 1.88 2.03 -10 0 -13 1.35 1.79 10 -10 -16 90.86 8.52 10 0 16 92.68 8.32 0 10 -16 100.47 7.84 0 -10 16 94.99 8.10 -10 0 -16 90.09 7.46 -10 0 -16 92.29 8.31 10 -10 -16 88.15 7.71 0 -10 19 0.92 1.84 10 -10 -19 0.39 1.76 0 10 -19 0.37 1.61 -10 0 -19 -0.37 2.03 0 10 -22 144.72 8.95 -10 0 -22 151.69 9.20 5 6 23 43.61 5.48 11 -6 23 38.69 5.21 -5 -6 -23 38.26 4.51 11 -6 20 932.92 24.02 11 -5 -20 908.56 23.49 5 6 20 943.71 25.79 11 -6 20 916.40 24.83 -5 11 20 896.75 23.66 -6 11 -20 952.37 23.87 -6 -5 20 955.06 24.58 -5 -6 -20 914.28 23.50 6 -11 20 931.22 27.69 -5 -6 -20 942.18 27.33 11 -5 -20 945.60 28.38 11 -5 -17 176.77 10.10 11 -5 -17 185.28 12.08 5 6 17 188.50 10.92 11 -6 17 168.81 9.83 -5 11 17 163.54 9.88 -6 11 -17 182.16 10.08 -6 -5 17 160.18 9.73 5 -11 -17 172.18 11.48 -5 -6 -17 186.59 10.25 6 -11 17 184.62 11.62 -5 -6 -17 184.87 11.23 11 -6 17 172.08 10.15 6 5 -14 834.42 25.54 5 6 14 845.05 23.52 11 -6 14 870.13 22.71 -5 11 14 800.10 22.93 -6 11 -14 843.83 23.11 -11 5 14 818.18 23.55 -6 -5 14 830.71 23.29 5 -11 -14 864.11 25.99 -5 -6 -14 855.55 23.20 6 -11 14 867.62 25.46 -5 -6 -14 822.73 24.00 11 -6 14 829.37 23.46 11 -5 -14 812.08 23.02 11 -5 -11 115.76 7.26 6 5 -11 122.11 9.20 5 6 11 107.78 7.95 11 -6 11 120.13 7.72 -5 11 11 116.96 8.48 -6 11 -11 114.38 8.30 -11 5 11 110.68 8.36 5 -11 -11 126.87 9.37 -6 -5 11 129.88 8.86 -5 -6 -11 117.08 8.33 6 -11 11 132.19 9.41 -5 -6 -11 121.20 8.55 11 -6 11 114.30 8.43 11 -5 -11 114.64 8.41 11 -5 -8 110.87 7.00 6 5 -8 109.24 8.54 5 6 8 121.15 8.30 11 -6 8 126.50 7.59 -5 11 8 135.60 9.09 -6 11 -8 117.66 8.43 6 -11 8 110.61 6.67 -11 6 -8 99.55 8.03 -11 5 8 98.29 7.98 5 -11 -8 108.56 8.54 -6 -5 8 108.14 8.15 -5 -6 -8 106.08 7.97 -5 -6 -8 123.24 8.34 11 -6 8 110.49 6.37 11 -6 8 111.67 8.37 11 -5 -8 128.82 8.88 6 5 -5 97.51 7.86 11 -5 -5 100.19 6.61 5 6 5 95.94 7.37 11 -6 5 89.41 6.20 -5 11 5 95.91 7.66 -6 11 -5 100.56 7.83 -11 6 -5 107.13 8.19 -11 5 5 92.23 7.76 6 -11 5 94.74 6.60 5 -11 -5 96.23 7.65 -6 -5 5 93.01 7.56 -5 -6 -5 88.60 7.36 -6 -5 5 86.46 5.69 -5 -6 -5 90.44 6.83 5 6 5 93.49 4.14 11 -6 5 86.89 7.44 11 -5 -5 98.66 7.87 11 -6 2 19.34 3.75 6 5 -2 14.01 3.21 11 -5 -2 18.13 2.98 5 6 2 19.40 3.60 11 -6 2 14.59 2.51 -5 11 2 21.46 3.81 5 -11 -2 18.34 3.44 -11 5 2 16.87 3.61 -6 -5 2 10.93 2.82 6 -11 2 15.77 3.00 -6 -5 2 17.67 2.93 -5 -6 -2 16.47 3.01 5 6 2 17.51 2.29 5 6 -1 212.17 11.10 11 -6 -1 176.19 8.28 6 5 1 190.52 10.77 11 -5 1 204.74 9.62 -5 11 -1 207.05 11.26 -6 11 1 198.92 11.12 5 -11 1 205.15 10.49 -11 6 1 196.18 11.20 -11 5 -1 186.10 10.90 -6 -5 -1 193.06 10.87 6 -11 -1 196.64 10.56 -5 -6 1 206.92 11.29 -6 -5 -1 184.89 9.39 -5 -6 1 201.51 9.33 11 -6 -1 194.92 11.25 5 6 -1 198.19 8.21 11 -5 1 187.68 10.99 5 6 -4 1158.15 28.23 11 -6 -4 1139.04 23.04 6 5 4 1161.06 28.27 11 -5 4 1141.28 25.39 -5 -6 4 1137.19 19.03 -6 11 4 1164.99 28.69 5 -11 4 1170.81 26.10 -11 6 4 1134.73 28.83 -5 -6 4 1185.45 28.84 6 -11 -4 1201.00 28.65 -5 -6 4 1172.54 23.21 -6 -5 -4 1166.45 26.45 5 -11 4 1172.82 28.94 5 6 -4 1180.46 23.95 11 -5 4 1135.23 28.70 11 -6 -7 101.42 6.07 5 6 -7 87.40 7.45 6 5 7 95.97 7.61 11 -5 7 83.44 6.58 -5 -6 7 83.97 5.00 5 -11 7 84.54 6.13 -5 11 -7 90.44 7.43 -6 11 7 87.70 7.34 -11 6 7 99.53 7.97 -11 5 -7 91.76 7.58 -6 -5 -7 89.73 7.43 -5 -6 7 75.87 6.89 6 -11 -7 79.08 7.18 -6 -5 -7 97.06 7.38 5 -11 7 103.38 8.18 11 -6 -7 102.29 7.99 11 -5 7 83.97 7.26 5 6 -7 79.32 5.99 5 6 -10 601.95 20.37 11 -6 -10 563.46 20.63 6 5 10 574.57 19.19 5 -11 10 563.51 15.44 11 -5 10 606.49 18.60 -5 -6 10 590.83 15.29 -5 11 -10 586.69 19.19 -6 11 10 594.72 19.52 -11 6 10 581.87 19.65 -11 5 -10 599.41 19.85 -6 -5 -10 590.75 19.25 -5 -6 10 586.40 19.45 6 -11 -10 587.61 20.47 5 -11 10 557.64 19.72 -6 -5 -10 601.91 19.49 11 -6 -10 596.74 19.57 5 6 -10 613.37 18.15 11 -5 10 615.89 19.99 5 6 -13 32.45 4.91 6 5 13 25.57 4.17 11 -5 13 37.36 4.74 -5 -6 13 28.22 3.61 -6 11 13 30.97 4.48 11 -6 -13 27.08 4.67 -5 11 -13 25.06 3.90 -11 5 -13 34.23 4.84 -6 -5 -13 33.62 4.62 -5 -6 13 40.10 5.08 6 -11 -13 41.23 5.62 -6 -5 -13 28.99 4.45 11 -6 -13 29.44 4.39 5 6 -13 29.72 4.30 11 -5 13 32.66 4.62 11 -5 16 920.50 24.55 -11 6 16 896.20 26.19 6 5 16 938.60 25.80 11 -5 16 939.46 25.16 -5 -6 16 913.17 22.53 -5 11 -16 969.49 24.73 -6 11 16 918.29 24.62 -11 5 -16 944.89 25.01 -6 -5 -16 935.93 24.22 -5 -6 16 929.58 24.72 6 -11 -16 860.63 26.65 -6 -5 -16 948.56 26.55 5 6 -16 905.67 24.96 11 -6 -16 909.15 24.38 11 -5 19 48.98 5.34 -11 6 19 48.93 6.09 6 5 19 53.06 6.11 11 -5 19 51.73 5.88 -5 11 -19 53.31 5.50 -6 11 19 46.99 5.40 -6 -5 -19 55.00 5.51 -5 -6 19 46.87 5.33 -11 5 -19 49.24 6.09 11 -6 -19 45.48 6.26 -6 -5 -19 54.24 6.33 5 6 -19 39.73 5.31 11 -6 -19 54.50 5.73 11 -6 -22 0.65 1.73 6 5 22 1.75 1.82 11 -5 22 2.11 2.21 -5 11 -22 1.29 1.77 -6 -5 -22 3.23 1.82 -11 5 -22 2.30 1.83 4 7 21 25.88 4.12 11 -7 21 15.02 3.33 -7 11 -21 17.70 3.39 -4 -7 -21 24.74 3.93 11 -4 -21 24.92 4.81 11 -4 -18 468.67 16.48 -11 4 18 480.78 18.54 -7 -4 18 431.77 13.86 4 7 18 461.37 16.73 11 -7 18 424.42 15.40 -4 11 18 422.10 16.07 -7 11 -18 462.21 16.35 -11 4 18 447.02 16.74 -7 -4 18 443.18 16.49 -4 -7 -18 444.02 16.08 7 -11 18 427.64 18.08 -4 -7 -18 438.07 17.71 11 -7 18 453.33 16.47 11 -7 15 1.90 1.94 11 -4 -15 0.74 1.77 7 -11 15 1.81 1.96 -7 -4 15 0.69 1.33 7 4 -15 1.40 1.86 4 7 15 0.36 1.55 11 -7 15 1.56 1.55 -4 11 15 1.13 1.75 -7 11 -15 2.21 2.17 4 -11 -15 0.48 2.14 -11 4 15 1.17 1.87 -7 -4 15 2.30 1.72 -4 -7 -15 0.36 1.51 -4 -7 -15 1.24 1.72 11 -4 -12 521.52 18.15 11 -4 -12 515.85 16.97 4 7 12 543.55 17.79 11 -7 12 516.72 15.92 -4 11 12 544.61 18.66 -7 11 -12 546.58 18.35 4 -11 -12 526.08 19.79 -11 4 12 524.90 18.67 -7 -4 12 531.49 18.47 -4 -7 -12 544.87 18.30 11 -7 12 528.84 15.51 7 -11 12 507.02 19.00 -4 -7 -12 529.71 18.27 11 -7 12 528.16 18.41 11 -4 -9 22.54 3.94 11 -7 9 20.83 3.23 7 -11 9 25.16 4.29 11 -4 -9 20.81 3.45 4 7 9 22.14 3.65 11 -7 9 20.17 2.99 -4 11 9 22.66 3.96 -7 11 -9 16.05 3.56 7 -11 9 21.14 2.95 4 -11 -9 24.46 4.23 -11 4 9 20.85 3.80 -7 -4 9 24.59 4.09 -4 -7 -9 21.44 3.88 -4 -7 -9 24.89 3.93 11 -7 9 27.92 4.29 11 -7 9 22.25 3.35 11 -4 -6 217.10 11.72 11 -7 6 222.27 10.66 11 -4 -6 217.11 10.49 4 7 6 220.10 10.93 11 -7 6 218.67 9.12 -4 11 6 222.00 11.81 -7 11 -6 233.65 11.96 4 -11 -6 220.53 12.06 -11 4 6 206.68 11.56 7 -11 6 227.24 9.99 -7 -4 6 222.49 11.79 -4 -7 -6 230.11 11.84 -7 -4 6 219.33 9.23 -4 -7 -6 226.75 10.95 7 -11 6 219.90 12.09 11 -7 6 236.45 12.24 11 -7 3 8.56 2.68 11 -7 3 8.28 2.49 11 -4 -3 14.95 2.93 4 7 3 17.67 3.28 11 -7 3 8.81 1.98 -4 11 3 7.90 2.64 4 -11 -3 10.90 2.96 -11 4 3 10.05 2.86 -7 -4 3 5.90 2.36 7 -11 3 12.20 2.74 -7 -4 3 8.55 2.22 -4 -7 -3 10.64 2.53 11 -7 0 3076.62 51.84 4 7 0 3096.52 50.73 11 -7 0 3206.22 43.60 11 -4 0 3068.97 49.38 -4 11 0 3186.26 53.20 4 -11 0 3090.69 51.36 -7 11 0 3065.61 52.91 -4 -7 0 3145.21 39.06 -11 4 0 3046.62 53.05 -7 -4 0 3091.96 52.69 -4 -7 0 3115.44 52.93 7 -11 0 3131.92 50.65 -7 -4 0 3123.77 48.85 -4 -7 0 3201.73 47.65 4 7 0 3126.55 42.98 11 -7 0 3268.29 54.29 11 -4 0 3181.62 53.90 11 -4 3 24.11 4.13 4 -11 3 15.50 3.30 4 7 -3 22.14 3.62 4 -11 3 14.29 2.99 7 4 3 19.03 3.63 11 -4 3 21.24 3.55 -7 11 3 24.77 4.07 -4 -7 3 23.48 2.54 11 -7 -3 12.58 3.17 -4 -7 3 21.06 3.79 -4 -7 3 23.91 3.09 -7 -4 -3 16.86 3.11 7 -11 -3 26.24 4.05 4 7 -3 21.19 2.92 11 -4 6 220.80 11.84 4 7 -6 197.87 10.87 7 4 6 218.41 11.78 11 -4 6 225.89 11.18 4 -11 6 210.90 10.20 -4 11 -6 224.12 11.75 -7 11 6 207.28 11.39 -4 -7 6 220.89 8.47 -11 4 -6 219.71 11.82 -7 -4 -6 212.90 11.46 -4 -7 6 208.41 11.45 -7 -4 -6 239.64 11.62 7 -11 -6 206.53 11.41 4 -11 6 229.85 12.03 4 7 -6 229.50 9.96 11 -7 -6 231.92 12.25 11 -7 -6 224.17 12.22 4 7 -9 11.82 2.68 11 -7 -9 12.84 3.16 11 -4 9 10.29 2.81 4 -11 9 14.02 3.29 4 -11 9 14.96 2.72 4 7 -9 4.32 2.06 7 4 9 11.32 3.00 11 -4 9 11.77 2.79 -4 11 -9 12.38 3.08 -7 11 9 9.78 2.78 -11 4 -9 11.91 3.05 -7 -4 -9 16.01 3.27 -4 -7 9 11.12 2.90 -7 -4 -9 9.55 2.60 11 -7 -9 23.24 4.21 -4 -7 9 12.39 2.46 7 -11 -9 10.58 3.01 11 -4 12 479.07 17.44 7 4 12 454.41 17.62 11 -4 12 484.30 17.52 -4 -7 12 452.42 14.61 -7 11 12 459.84 17.16 -11 4 -12 485.74 17.71 -7 -4 -12 492.88 17.33 -4 -7 12 424.15 16.62 -4 11 -12 459.21 16.87 4 -11 12 469.22 17.99 -7 -4 -12 473.74 17.68 7 -11 -12 475.62 18.53 11 -7 -12 453.46 18.48 4 7 -12 446.54 15.86 11 -7 -12 449.91 17.02 4 7 -15 2.24 1.74 11 -7 -15 3.42 2.14 11 -4 15 4.52 2.26 4 -11 15 1.82 2.04 11 -7 -15 1.44 2.09 7 4 15 4.29 2.06 11 -4 15 0.41 1.70 -4 11 -15 4.07 1.99 -7 11 15 1.15 1.79 -11 4 -15 1.92 1.78 -7 -4 -15 1.47 1.60 -4 -7 15 3.09 2.07 -7 -4 -15 3.45 2.14 -4 -7 15 0.63 1.78 7 -11 -15 0.47 1.96 11 -4 18 467.90 16.77 -11 7 18 470.94 18.65 7 4 18 463.13 18.24 11 -4 18 459.05 17.91 -4 -7 18 491.09 16.98 -4 11 -18 480.70 16.80 -7 11 18 484.14 17.32 -11 4 -18 489.09 17.44 -7 -4 -18 477.91 16.80 -4 -7 18 475.00 17.13 4 -11 18 502.65 19.55 -11 4 -18 498.76 19.54 7 -11 -18 492.34 19.76 -7 -4 -18 480.21 18.87 4 7 -18 482.50 17.99 11 -7 -18 472.21 16.92 4 7 -21 14.07 3.62 11 -7 -21 17.66 3.44 7 4 21 5.92 3.00 11 -4 21 18.55 3.86 -4 11 -21 12.11 2.86 -11 4 -21 16.74 3.35 -7 -4 -21 10.47 2.78 -11 4 -21 16.00 3.79 -4 -7 21 13.72 3.30 -8 -3 22 112.60 7.85 3 8 22 125.87 8.44 -3 -8 -22 118.06 7.98 11 -8 19 11.97 2.96 8 -11 19 10.29 3.13 -11 3 19 10.13 3.31 -8 -3 19 8.14 2.40 3 8 19 13.74 3.14 -3 11 19 16.62 3.33 -8 11 -19 9.24 2.60 -11 3 19 13.21 3.24 -8 -3 19 10.89 2.96 -3 -8 -19 12.62 2.92 -3 -8 -19 9.89 3.06 -8 -3 16 329.48 12.29 3 8 16 328.45 13.35 -3 11 16 336.75 14.42 3 -11 -16 350.06 16.39 -8 11 -16 366.08 14.71 -11 3 16 343.40 14.82 -8 -3 16 358.61 15.08 -3 -8 -16 321.12 13.94 11 -8 16 330.69 12.96 8 -11 16 341.13 15.71 -3 -8 -16 351.24 15.50 11 -8 16 320.48 14.20 11 -8 13 2.76 1.77 11 -3 -13 1.15 1.65 11 -8 13 2.16 1.61 8 -11 13 0.88 1.59 11 -3 -13 0.75 1.79 8 3 -13 0.46 1.76 3 8 13 1.96 1.62 -3 11 13 6.64 2.39 3 -11 -13 3.29 2.18 -8 11 -13 0.77 1.52 -11 3 13 1.60 2.15 -8 -3 13 1.99 1.97 -3 -8 -13 1.90 1.71 -3 -8 -13 2.00 1.59 11 -3 -10 899.15 24.69 11 -3 -10 908.21 24.10 8 3 -10 841.22 25.53 3 8 10 889.08 22.52 -3 11 10 870.08 24.65 3 -11 -10 901.91 26.37 -8 11 -10 915.59 24.87 -11 3 10 855.60 24.69 -8 -3 10 880.70 24.71 11 -8 10 876.87 20.70 -3 -8 -10 887.69 24.50 11 -8 10 879.84 22.20 8 -11 10 894.12 25.65 -3 -8 -10 910.04 24.34 11 -8 10 945.95 25.64 11 -8 7 2.39 1.69 11 -8 7 1.24 1.79 11 -3 -7 5.94 2.47 8 -11 7 6.86 2.47 11 -8 7 4.07 1.76 11 -3 -7 3.57 1.91 8 3 -7 1.30 1.80 3 8 7 5.14 2.04 3 -11 -7 4.72 2.42 -3 11 7 4.41 1.99 -8 11 -7 8.74 2.61 -11 3 7 2.04 2.02 -8 -3 7 2.02 1.68 -3 -8 -7 6.73 2.60 8 -11 7 4.78 1.86 -8 -3 7 4.06 1.75 -3 -8 -7 8.87 2.49 11 -3 -4 387.69 15.91 8 3 -4 434.55 17.11 11 -3 -4 415.37 15.42 3 8 4 406.09 14.64 3 -11 -4 405.65 16.46 -3 11 4 409.35 16.29 -11 3 4 393.98 16.20 -8 -3 4 375.46 15.63 11 -8 4 390.99 14.64 -8 -3 4 410.93 14.16 8 -11 4 388.82 13.89 -3 -8 -4 401.85 14.34 11 -8 4 410.34 16.59 8 -11 1 9.31 2.50 -3 -8 -1 9.53 1.84 11 -8 1 12.25 3.05 11 -3 -1 11.28 3.02 3 -11 -1 11.90 2.94 11 -8 1 11.07 2.91 3 -11 -1 13.09 3.03 3 8 1 6.50 2.31 8 3 -1 9.68 2.90 11 -3 -1 5.74 2.28 -3 11 1 8.87 2.74 -8 11 -1 10.07 2.82 -11 3 1 9.02 2.70 -8 -3 1 12.49 3.02 -3 -8 -1 9.70 3.22 -8 -3 1 11.10 2.56 -3 -8 -1 10.40 2.46 11 -3 2 360.03 15.32 3 8 -2 348.92 13.79 11 -3 2 339.28 14.24 3 -11 2 331.61 13.89 -8 11 2 349.03 15.04 -3 -8 2 339.78 10.55 -3 -8 2 349.77 15.06 11 -8 -2 321.21 14.10 -8 -3 -2 335.42 13.66 -3 -8 2 340.21 11.84 8 -11 -2 318.49 13.72 3 -11 2 363.31 14.63 3 8 -2 338.39 11.15 3 8 -5 7.02 2.12 -3 -8 5 6.31 1.82 11 -8 -5 10.96 3.24 11 -3 5 6.86 2.47 8 -11 -5 5.48 2.26 3 -11 5 7.30 2.57 11 -8 -5 6.97 2.61 3 -11 5 5.65 2.11 3 8 -5 7.36 2.45 11 -3 5 7.46 2.41 -3 11 -5 9.63 2.81 -8 11 5 10.92 2.87 -11 3 -5 7.32 2.72 -8 -3 -5 10.79 2.92 -3 -8 5 4.49 2.35 -8 -3 -5 5.86 2.16 11 -3 8 233.56 12.16 3 8 -8 212.72 11.20 11 -3 8 208.58 11.44 -3 11 -8 216.01 11.69 -8 11 8 199.35 11.29 -3 -8 8 208.29 9.38 -11 3 -8 219.23 11.92 -8 -3 -8 221.68 11.73 -3 -8 8 215.18 11.71 11 -8 -8 209.52 12.07 -11 3 -8 221.07 12.50 3 -11 8 223.99 11.92 -8 -3 -8 232.32 11.92 8 -11 -8 210.82 11.81 3 8 -8 216.66 10.20 11 -8 -8 206.12 11.74 3 8 -11 17.22 3.31 11 -8 -11 18.43 3.69 11 -3 11 22.20 3.87 3 -11 11 14.72 3.54 8 -11 -11 20.99 4.16 11 -3 11 15.71 3.44 -3 11 -11 12.98 3.14 -8 11 11 18.79 3.69 -11 3 -11 23.52 4.07 -8 -3 -11 16.03 3.39 -3 -8 11 18.39 3.84 -11 3 -11 13.97 3.47 -8 -3 -11 25.51 4.25 11 -8 -11 15.11 3.52 -3 -8 11 19.05 3.21 11 -3 14 470.91 17.28 8 3 14 465.10 18.33 11 -3 14 485.45 18.49 -3 11 -14 495.72 17.58 -3 -8 14 478.48 16.19 -8 11 14 453.49 17.18 -11 3 -14 474.76 17.51 -8 -3 -14 474.72 17.25 11 -8 -14 470.85 19.27 -3 -8 14 463.25 17.42 3 -11 14 463.84 18.18 -11 3 -14 459.24 18.96 -8 -3 -14 470.95 18.38 8 -11 -14 464.91 18.87 3 8 -14 461.64 16.78 11 -8 -14 466.18 17.40 3 8 -17 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-5 0.45 1.71 6 -13 -5 1.33 1.77 -13 6 5 0.48 1.80 -7 -6 5 -0.46 1.85 -6 -7 -5 -0.46 1.81 -6 -7 -5 -0.37 1.78 7 6 -2 141.07 10.10 13 -7 2 145.74 9.94 6 7 2 140.78 9.80 -6 13 2 153.31 10.60 6 -13 -2 136.23 9.59 7 -13 2 142.52 9.10 -13 6 2 139.11 10.34 -7 -6 2 146.81 10.37 -6 -7 -2 147.52 8.90 7 -13 2 152.19 10.64 13 -7 2 150.93 10.70 13 -6 1 1.90 2.35 6 -13 1 3.66 2.20 13 -7 -1 6.64 2.86 6 7 -1 4.35 2.34 7 6 1 5.39 2.53 6 -13 1 5.74 2.39 -6 13 -1 4.11 2.52 -7 13 1 8.22 2.95 7 -13 -1 5.99 2.54 -13 6 -1 8.12 2.87 -7 -6 -1 5.09 2.49 -6 -7 1 6.98 2.79 -7 -6 -1 6.74 2.25 13 -7 -4 224.64 13.01 6 7 -4 204.16 12.21 7 6 4 234.37 12.89 6 -13 4 199.52 10.61 -7 13 4 195.70 11.93 -13 6 -4 231.73 13.16 7 -13 -4 210.41 12.07 -7 -6 -4 235.30 13.14 -6 -7 4 231.77 13.01 -7 -6 -4 210.73 11.24 6 -13 4 214.55 12.50 13 -7 -4 221.98 12.89 13 -6 4 228.23 13.09 6 7 -7 11.96 2.64 13 -7 -7 9.41 3.20 13 -6 7 12.53 3.48 6 -13 7 8.01 3.05 6 7 -7 12.37 3.39 7 6 7 14.74 3.56 -6 13 -7 10.75 3.23 -7 13 7 17.97 3.85 13 -7 -7 11.23 3.32 -13 6 -7 15.48 3.82 7 -13 -7 5.48 2.63 -7 -6 -7 8.57 3.02 -6 -7 7 9.72 3.34 -7 -6 -7 12.48 3.13 13 -6 10 1233.76 31.65 6 7 -10 1267.90 32.97 7 6 10 1249.30 31.52 -6 13 -10 1257.15 31.42 -7 13 10 1237.69 31.44 -13 6 -10 1230.60 32.00 7 -13 -10 1268.45 32.96 -7 -6 -10 1205.88 30.82 -6 -7 10 1259.88 32.06 -7 -6 -10 1287.13 31.43 6 7 -10 1232.92 28.09 13 -7 -10 1249.73 31.94 6 7 -13 14.46 3.45 5 8 12 1.59 2.03 13 -5 -9 92.42 8.27 5 8 9 97.66 7.92 -5 13 9 94.96 8.30 5 -13 -9 110.70 9.17 -8 13 -9 87.81 7.95 -13 5 9 94.42 8.52 -8 -5 9 87.23 8.05 -5 -8 -9 91.96 8.17 -5 -8 -9 97.06 7.89 13 -8 9 84.21 7.95 13 -5 -6 1313.42 32.79 8 5 -6 1274.57 33.13 5 8 6 1235.25 30.44 -5 13 6 1299.80 32.44 5 -13 -6 1301.72 32.50 -8 13 -6 1243.15 31.79 -13 5 6 1260.72 32.61 -8 -5 6 1265.69 32.35 -5 -8 -6 1264.07 31.94 -5 -8 -6 1251.18 29.62 13 -8 6 1240.69 29.15 8 -13 6 1362.08 33.98 13 -8 6 1257.02 32.49 8 5 -3 89.19 8.20 13 -5 -3 95.48 7.32 5 8 3 87.52 7.47 5 -13 -3 83.26 7.52 -5 13 3 90.65 8.16 -13 5 3 89.67 8.36 8 -13 3 86.25 7.03 -8 -5 3 72.40 7.36 -5 -8 -3 92.24 7.06 13 -8 3 87.39 7.39 13 -8 3 86.22 8.11 13 -5 0 318.14 15.51 5 8 0 328.26 14.81 8 5 0 323.20 15.57 13 -5 0 320.29 13.64 5 -13 0 328.00 14.55 -5 13 0 300.20 14.77 -8 13 0 307.55 15.07 -13 5 0 301.66 15.32 8 -13 0 317.37 13.98 -8 -5 0 309.41 15.23 -5 -8 0 334.60 15.69 13 -8 0 322.85 14.95 5 -13 0 333.23 15.25 13 -8 0 312.81 15.42 13 -5 3 84.16 7.98 5 8 -3 87.02 7.73 8 5 3 98.48 8.61 13 -5 3 94.39 7.52 5 -13 3 98.06 7.63 -8 13 3 96.93 8.42 8 -13 -3 99.09 8.09 -5 -8 3 98.02 8.48 -8 -5 -3 106.62 8.10 5 -13 3 104.03 8.58 13 -8 -3 98.96 8.47 13 -5 6 738.69 24.04 5 8 -6 700.01 22.93 8 5 6 713.96 23.63 13 -5 6 697.96 21.40 -5 13 -6 704.92 23.16 -8 13 6 739.05 23.81 -13 5 -6 717.16 23.84 -8 -5 -6 720.53 23.42 -5 -8 6 700.64 23.36 8 -13 -6 716.49 23.19 -8 -5 -6 696.87 21.89 5 -13 6 717.84 23.28 13 -8 -6 688.84 23.45 5 8 -6 710.34 18.83 13 -8 -6 665.48 23.07 13 -5 9 76.38 7.53 5 8 -9 80.06 7.77 8 5 9 63.59 7.70 13 -5 9 76.98 7.04 -5 13 -9 73.43 7.31 -8 13 9 78.70 7.54 -13 5 -9 80.00 7.86 -8 -5 -9 69.34 7.15 -5 -8 9 83.80 7.91 8 -13 -9 89.47 8.30 5 -13 9 84.17 8.00 -8 -5 -9 82.34 7.58 5 8 -9 79.22 6.54 13 -8 -9 72.02 7.47 5 8 -12 21.39 3.86 13 -5 12 23.10 4.24 4 9 13 49.44 5.68 4 9 10 764.26 22.24 -4 -9 -10 756.10 23.04 4 -13 -7 11.95 3.40 13 -4 -7 8.46 2.92 4 9 7 9.72 2.81 -4 -9 -7 15.17 3.44 13 -4 -4 646.74 22.31 13 -4 -4 632.52 20.40 4 9 4 595.85 19.56 4 -13 -4 618.91 21.48 -4 13 4 603.93 21.52 -9 13 -4 619.84 21.78 -13 4 4 636.87 22.61 -9 -4 4 631.55 22.20 13 -9 4 610.19 19.83 -4 -9 -4 638.16 22.20 -4 -9 -4 611.74 19.10 4 -13 -4 645.52 20.97 9 -13 4 609.24 22.04 13 -9 4 625.00 22.25 4 9 1 75.09 6.88 13 -4 -1 71.49 6.78 4 -13 -1 54.46 6.17 -4 13 1 62.07 6.82 -9 13 -1 73.25 7.35 -13 4 1 69.26 7.31 -9 -4 1 59.90 6.79 13 -9 1 66.20 6.73 -4 -9 -1 80.89 7.84 9 -13 1 84.02 7.10 4 -13 -1 77.32 7.13 13 -9 1 75.05 7.61 13 -4 2 25.92 4.88 4 -13 2 26.89 4.62 13 -4 2 32.43 4.85 4 -13 2 26.50 4.28 4 9 -2 23.67 4.08 -9 13 2 28.81 4.77 -4 -9 2 29.01 4.98 9 -13 -2 26.18 4.40 13 -9 -2 27.58 4.50 -9 -4 -2 24.22 4.10 4 9 -5 46.32 5.65 9 4 5 51.35 6.34 13 -4 5 43.20 5.44 -4 13 -5 64.85 6.98 -9 13 5 44.95 5.99 -13 4 -5 47.34 6.26 -9 -4 -5 48.20 6.12 13 -9 -5 40.35 5.70 -4 -9 5 55.24 6.66 9 -13 -5 38.75 5.52 -9 -4 -5 61.29 6.38 4 -13 5 44.95 5.78 13 -9 -5 50.37 6.44 4 9 -8 62.73 6.68 13 -4 8 57.81 6.44 4 -13 8 58.29 6.58 9 -13 -8 57.14 6.68 -9 -4 -8 62.11 6.75 4 9 -8 67.35 5.82 13 -4 11 4.44 2.67 4 9 -11 6.88 2.55 13 -3 -8 164.45 10.70 3 10 8 164.55 9.40 -3 -10 -8 159.92 10.05 3 -13 -8 165.77 10.00 3 -13 -5 1.15 2.21 13 -10 5 1.85 1.72 3 10 5 1.37 1.65 13 -3 -5 -1.69 2.16 3 10 2 124.81 8.45 13 -3 -2 127.81 9.30 3 -13 -2 137.36 9.92 13 -10 2 129.20 9.06 10 -13 2 132.45 8.83 3 -13 -2 126.23 8.87 3 -13 1 6.83 2.73 13 -10 -1 7.64 2.93 3 10 -1 8.77 2.67 13 -3 1 5.25 2.52 -10 -3 -1 10.23 2.91 10 -13 -1 5.60 2.45 3 10 -4 237.19 12.14 13 -3 4 241.86 13.01 13 -10 -4 251.59 13.57 -10 -3 -4 230.18 12.54 3 -13 4 242.94 12.66 10 -13 -4 247.58 13.09 3 -13 7 1.72 2.31 -10 -3 -7 2.20 2.05 2 -13 -6 524.59 17.61 2 -13 -3 17.63 3.57 13 -11 0 568.46 19.87 2 -13 0 557.02 18.75 11 -13 0 581.96 19.52 2 -13 3 16.72 3.71 7 -14 0 1317.11 31.19 14 -7 6 125.46 9.02 8 -14 1 1.16 2.03 6 -14 2 62.80 6.31 0 0 0 0.00 0.00 TITL exp_283_Mo in R-3c REM R-3c (#167 in standard setting) CELL 0.71073 8.720539 8.720539 23.943640 90.0000 90.0000 120.0000 ZERR 6.00 0.000099 0.000099 0.000308 0.0000 0.0000 0.0000 LATT 3 SYMM -y, x-y, z SYMM -x+y,-x, z SYMM y, x,-z+1/2 SYMM x-y,-y,-z+1/2 SYMM -x,-x+y,-z+1/2 SFAC O P K Zr UNIT 72.00 18.00 6.00 12.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 95840